CN105696112B - A kind of copper ion antibacterial socks - Google Patents
A kind of copper ion antibacterial socks Download PDFInfo
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- CN105696112B CN105696112B CN201610130487.4A CN201610130487A CN105696112B CN 105696112 B CN105696112 B CN 105696112B CN 201610130487 A CN201610130487 A CN 201610130487A CN 105696112 B CN105696112 B CN 105696112B
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- copper ion
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- ion antibacterial
- copper
- nitrate
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/14—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/12—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyamide as constituent
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04B—KNITTING
- D04B1/00—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
- D04B1/14—Other fabrics or articles characterised primarily by the use of particular thread materials
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04B—KNITTING
- D04B1/00—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
- D04B1/22—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes specially adapted for knitting goods of particular configuration
- D04B1/24—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes specially adapted for knitting goods of particular configuration wearing apparel
- D04B1/26—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes specially adapted for knitting goods of particular configuration wearing apparel stockings
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Artificial Filaments (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a kind of copper ion antibacterial socks, preparation is followed the steps below：Silver nitrate, copper nitrate and cerous nitrate are configured to solution A and add chitosan, constant temperature stirs to obtain copper ion antiseptic；Copper ion antiseptic, sorbic acid, polyester, nano titanium oxide, nano zine oxide, Tea Polyphenols, beta cyclodextrin extruding pelletization are obtained into copper ion antibacterial matrices；Copper ion antibacterial matrices and slices of caprone spinning are obtained into copper ion antibacterial nylon fiber；Copper ion antibacterial nylon fiber and combed cotton mixed weaving are obtained into the copper ion antibacterial socks.Copper ion antimicrobial socks proposed by the present invention, it uses the fiber of antibiotic property to be made, and health-care effect is good, has the effect of antibacterial, deodorization, and the validity of antibacterial and long-term effect are excellent.
Description
Technical field
The present invention relates to socks technical field, more particularly to a kind of copper ion antibacterial socks.
Background technology
As the prosperity of economy, the continuous raising of people's living standard, the development of production technology are become better and better, people
It is more and more harsher to the requirement in terms of oneself dress, in life, we are for socks requirement also more and more higher, it is often desired to energy
Enough by improving the service efficiency of socks to the innovation of socks, it is allowed to give play to the value of maximum.But currently on the market
Socks still suffer from a series of problem, such as material improper use, the generation for situations such as also having foot odour, making soaked with sweat, some uses
Person's toe is injured, bacterium infection easily occurs, is unfavorable for health care of foot etc., result in production requirement cannot improve, nothing
Method meets the needs of using.
The content of the invention
Based on technical problem existing for background technology, the present invention proposes a kind of copper ion antimicrobial socks, and it uses antibacterial
Property fiber be made, health-care effect is good, has the effect of antibacterial, deodorization, and the validity of antibacterial and long-term effect are excellent.
A kind of copper ion antibacterial socks proposed by the present invention, follow the steps below preparation：
S1, solution A will be configured in silver nitrate, copper nitrate and cerous nitrate 100 parts by weight water of addition, wherein, in solution A,
The concentration of silver nitrate is 1.5-2.5mmol/L, and the concentration of copper nitrate is 0.2-0.4mmol/L, and the concentration of cerous nitrate is 0.1-
0.5mmol/L, 0.8-1.5 parts by weight chitosans then adding, constant temperature stirs 3-4.5h at 40-55 DEG C, through filtering, drying,
Grinding obtains copper ion antiseptic；
S2, by weight by 5-20 part copper ions antiseptic, 0.5-3 parts sorbic acid, 30-50 parts polyester, 2-10 part nanometers
Titanium dioxide, 3-10 parts nano zine oxide, 2-8 parts Tea Polyphenols, 3-10 parts beta-schardinger dextrin are added in double screw extruder to extrude and made
Grain obtains copper ion antibacterial matrices；
S3, copper ion antibacterial matrices and slices of caprone spinning are obtained into copper ion antibacterial nylon fiber；
S4, copper ion antibacterial nylon fiber and combed cotton mixed weaving obtained into the copper ion antibacterial socks.
Preferably, in S1, in solution A, the concentration of silver nitrate is 2-2.5mmol/L, and the concentration of copper nitrate is 0.3-
0.4mmol/L, the concentration of cerous nitrate is 0.2-0.3mmol/L.
Preferably, in S1, silver nitrate, copper nitrate and cerous nitrate is added in 100 parts by weight water and are configured to solution A, its
In, in solution A, the concentration of silver nitrate is 2.2mmol/L, and the concentration of copper nitrate is 0.36mmol/L, and the concentration of cerous nitrate is
0.27mmol/L, 1 parts by weight chitosan is then added, constant temperature stirs 3.8h at 50 DEG C, through filtering, drying, grinding and obtain copper
Ion antibacterial agent.
Preferably, in S2, copper ion antiseptic, sorbic acid, polyester, nano titanium oxide, nano zine oxide, tea are more
Phenol, the weight ratio of beta-schardinger dextrin are 10-16：1.3-2.1：37-43：5.5-7：6-7：4.8-6：5-8.
Preferably, in S2, by weight by 12 parts of copper ion antiseptics, 2 parts of sorbic acids, 40 parts of polyester, 6.2 parts of nanometers
Titanium dioxide, 6.5 parts of nano zine oxides, 5.3 parts of Tea Polyphenols and 7 parts of beta-schardinger dextrins add extruding pelletization in double screw extruder and obtained
To copper ion antibacterial matrices.
Preferably, in the copper ion antibacterial socks, the content of copper ion antibacterial nylon fiber is 12-20%, combed cotton
Content is 80-88%.
Preferably, in the copper ion antibacterial socks, the content of copper ion antibacterial nylon fiber is 15%, the content of combed cotton
For 85%.
Preferably, the copper ion antibacterial socks are five-toe socks.
In the present invention, after silver nitrate, copper nitrate, cerous nitrate are mixed with chitosan, by controlling technological parameter, it is allowed to send out
Reaction is given birth to, and during being reacted according to the technological parameter in the present invention, silver nitrate, copper nitrate and cerous nitrate gather in shell
The lamellar structure surface of sugar forms substantial amounts of little particle, and little particle has reached most optimal sorting in the lamellar structure of chitosan
Dissipate, while add the consistency of chitosan, obtained copper ion antimicrobial agent stability is good, in system, on the one hand, can with it is thin
Bacterium reacts, and some enzymes destroyed in bacterium cell structure and built-in system, causes bacterial death, plays a part of sterilization,
On the other hand, the lamellar structure of chitosan, as silver, the carrier of copper and cerium, serve the effect of sustained release, substantially prolongs copper from
The long-term effect of sub- antiseptic；In sorbic acid, Tea Polyphenols, beta-schardinger dextrin addition system, on the one hand, promote nano titanium oxide and
The dispersiveness of nano zine oxide, on the other hand, have with copper ion antiseptic, nano titanium oxide and nano zine oxide and cooperate with
Property, significantly improve the anti-microbial property of copper ion antibacterial matrices；By copper ion antibacterial matrices and slices of caprone spinning be made copper from
Sub- antibacterial nylon fiber, not dissolution, stability are good in the fibre for antimicrobial component, can textile it is good, with combed cotton in specific proportions
The socks being woven into can preferably suppress various fungies and grow, and have excellent antibiotic property, wear for a long time except deodorization can be with
Prevent and treat tinea pedis, pin moss and onychomycosis.
The copper ion antibacterial socks prepared in the present invention are entered according to the examination criteria of FZ/T73023-2006 antibiosis knitting product
Row detection, testing result are as shown in the table：
As seen from the above table, the copper ion antibacterial socks obtained in the present invention are to staphylococcus aureus, Candida albicans, large intestine
Bacillus bacteriostasis rate is all higher than 99%, reaches national textile industry highest AAA levels standard and international SGS standards.
Embodiment
Below, technical scheme is described in detail by specific embodiment.
Embodiment 1
A kind of copper ion antibacterial socks proposed by the present invention, follow the steps below preparation：
S1, solution A will be configured in silver nitrate, copper nitrate and cerous nitrate 100 parts by weight water of addition, wherein, in solution A,
The concentration of silver nitrate is 1.5mmol/L, and the concentration of copper nitrate is 0.4mmol/L, and the concentration of cerous nitrate is 0.1mmol/L, then
1.5 parts by weight chitosans are added, constant temperature stirs 4.5h at 40 DEG C, through filtering, drying, grinding and obtain copper ion antiseptic；
S2, by weight by 5 parts of copper ion antiseptics, 3 parts of sorbic acids, 30 parts of polyester, 10 parts of nano titanium oxides, 3 parts
Nano zine oxide, 8 parts of Tea Polyphenols, 3 parts of beta-schardinger dextrins add extruding pelletization in double screw extruder and obtain copper ion antibacterial matrices；
S3, copper ion antibacterial matrices and slices of caprone spinning are obtained into copper ion antibacterial nylon fiber；
S4, copper ion antibacterial nylon fiber and combed cotton mixed weaving obtained into the copper ion antibacterial socks.
Embodiment 2
A kind of copper ion antibacterial socks proposed by the present invention, follow the steps below preparation：
S1, solution A will be configured in silver nitrate, copper nitrate and cerous nitrate 100 parts by weight water of addition, wherein, in solution A,
The concentration of silver nitrate is 2.5mmol/L, and the concentration of copper nitrate is 0.2mmol/L, and the concentration of cerous nitrate is 0.5mmol/L, then
0.8 parts by weight chitosan is added, constant temperature stirs 3h at 55 DEG C, through filtering, drying, grinding and obtain copper ion antiseptic；
S2, by weight by 20 parts of copper ion antiseptics, 0.5 part of sorbic acid, 50 parts of polyester, 2 parts of nano titanium oxides, 10
Part nano zine oxide, 2 parts of Tea Polyphenols, 10 parts of beta-schardinger dextrins add extruding pelletization in double screw extruders and obtain copper ion antibacterial mother
Grain；
S3, copper ion antibacterial matrices and slices of caprone spinning are obtained into copper ion antibacterial nylon fiber；
S4, copper ion antibacterial nylon fiber and combed cotton mixed weaving obtained into the copper ion antibacterial socks.
Embodiment 3
A kind of copper ion antibacterial socks proposed by the present invention, follow the steps below preparation：
S1, solution A will be configured in silver nitrate, copper nitrate and cerous nitrate 100 parts by weight water of addition, wherein, in solution A,
The concentration of silver nitrate is 2mmol/L in solution A, and the concentration of copper nitrate is 0.4mmol/L, and the concentration of cerous nitrate is 0.2mmol/L,
Then 1 parts by weight chitosan is added, constant temperature stirs 3.6h at 52 DEG C, through filtering, drying, grinding and obtain copper ion antiseptic；
S2, by weight by 16 parts of copper ion antiseptics, 1.3 parts of sorbic acids, 43 parts of polyester, 5.5 parts of nano titanium oxides,
7 parts of nano zine oxides, 4.8 parts of Tea Polyphenols, 8 parts of beta-schardinger dextrins add extruding pelletization in double screw extruder and obtain copper ion antibacterial
Master batch；
S3, copper ion antibacterial matrices and slices of caprone spinning are obtained into copper ion antibacterial nylon fiber；
S4, copper ion antibacterial nylon fiber and combed cotton mixed weaving obtained into the copper ion antibacterial socks；
Wherein, in the copper ion antibacterial socks, the content of copper ion antibacterial nylon fiber is 12%, and the content of combed cotton is
88%.
Embodiment 4
A kind of copper ion antibacterial socks proposed by the present invention, follow the steps below preparation：
S1, solution A will be configured in silver nitrate, copper nitrate and cerous nitrate 100 parts by weight water of addition, wherein, in solution A,
The concentration of silver nitrate is 2.5mmol/L in solution A, and the concentration of copper nitrate is 0.3mmol/L, and the concentration of cerous nitrate is 0.3mmol/
L, 1.2 parts by weight chitosans are then added, constant temperature stirs 4.3h at 47 DEG C, through filtering, drying, grinding and obtain copper ion antibacterial
Agent；
S2, by weight by 10 parts of copper ion antiseptics, 2.1 parts of sorbic acids, 37 parts of polyester, 7 parts of nano titanium oxides, 6
Part nano zine oxide, 6 parts of Tea Polyphenols, 5 parts of beta-schardinger dextrins add extruding pelletization in double screw extruders and obtain copper ion antibacterial mother
Grain；
S3, copper ion antibacterial matrices and slices of caprone spinning are obtained into copper ion antibacterial nylon fiber；
S4, copper ion antibacterial nylon fiber and combed cotton mixed weaving obtained into the copper ion antibacterial socks；
Wherein, in the copper ion antibacterial socks, the content of copper ion antibacterial nylon fiber is 20%, and the content of combed cotton is
80%.
Embodiment 5
A kind of copper ion antibacterial socks proposed by the present invention, follow the steps below preparation：
S1, solution A will be configured in silver nitrate, copper nitrate and cerous nitrate 100 parts by weight water of addition, wherein, nitre in solution A
The concentration of sour silver is 2.2mmol/L, and the concentration of copper nitrate is 0.36mmol/L, and the concentration of cerous nitrate is 0.27mmol/L, then
1 parts by weight chitosan is added, constant temperature stirs 3.8h at 50 DEG C, through filtering, drying, grinding and obtain copper ion antiseptic；
S2, by weight by 12 parts of copper ion antiseptics, 2 parts of sorbic acids, 40 parts of polyester, 6.2 parts of nano titanium oxides,
6.5 parts of nano zine oxides, 5.3 parts of Tea Polyphenols and 7 parts of beta-schardinger dextrins add extruding pelletization in double screw extruder and obtain copper ion
Antibacterial matrices；
S3, copper ion antibacterial matrices and slices of caprone spinning are obtained into copper ion antibacterial nylon fiber；
S4, copper ion antibacterial nylon fiber and combed cotton mixed weaving obtained into the copper ion antibacterial socks；
Wherein, in the copper ion antibacterial socks, the content of copper ion antibacterial nylon fiber is 15%, and the content of combed cotton is
85%；The copper ion antibacterial socks are five-toe socks.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (7)
1. a kind of copper ion antibacterial socks, it is characterised in that follow the steps below preparation：
S1, solution A will be configured in silver nitrate, copper nitrate and cerous nitrate 100 parts by weight water of addition, wherein, in solution A, nitric acid
The concentration of silver is 1.5-2.5mmol/L, and the concentration of copper nitrate is 0.2-0.4mmol/L, and the concentration of cerous nitrate is 0.1-
0.5mmol/L, 0.8-1.5 parts by weight chitosans then adding, constant temperature stirs 3-4.5h at 40-55 DEG C, through filtering, drying,
Grinding obtains copper ion antiseptic；
S2, by weight by 5-20 part copper ions antiseptic, 0.5-3 parts sorbic acid, 30-50 parts polyester, 2-10 part nano-silicas
Change extruding pelletization in titanium, 3-10 parts nano zine oxide, 2-8 parts Tea Polyphenols, 3-10 parts beta-schardinger dextrin addition double screw extruder to obtain
To copper ion antibacterial matrices；
S3, copper ion antibacterial matrices and slices of caprone spinning are obtained into copper ion antibacterial nylon fiber；
S4, copper ion antibacterial nylon fiber and combed cotton mixed weaving obtained into the copper ion antibacterial socks；
In S2, copper ion antiseptic, sorbic acid, polyester, nano titanium oxide, nano zine oxide, Tea Polyphenols, beta-schardinger dextrin
Weight ratio is 10-16：1.3-2.1：37-43：5.5-7：6-7：4.8-6：5-8.
2. copper ion antibacterial socks according to claim 1, it is characterised in that in S1, in solution A, the concentration of silver nitrate is
2-2.5mmol/L, the concentration of copper nitrate is 0.3-0.4mmol/L, and the concentration of cerous nitrate is 0.2-0.3mmol/L.
3. copper ion antibacterial socks according to claim 1 or claim 2, it is characterised in that in S1, by silver nitrate, copper nitrate and nitre
Sour cerium adds in 100 parts by weight water and is configured to solution A, wherein, in solution A, the concentration of silver nitrate is 2.2mmol/L, copper nitrate
Concentration be 0.36mmol/L, the concentration of cerous nitrate is 0.27mmol/L, then adds 1 parts by weight chitosan, permanent at 50 DEG C
Temperature stirring 3.8h, through filtering, drying, grinding and obtain copper ion antiseptic.
4. copper ion antibacterial socks according to claim 1 or claim 2, it is characterised in that in S2, by weight by 12 parts of copper ions
Antiseptic, 2 parts of sorbic acids, 40 parts of polyester, 6.2 parts of nano titanium oxides, 6.5 parts of nano zine oxides, 5.3 parts of Tea Polyphenols and 7 parts
Beta-schardinger dextrin adds extruding pelletization in double screw extruder and obtains copper ion antibacterial matrices.
5. copper ion antibacterial socks according to claim 1 or claim 2, it is characterised in that in the copper ion antibacterial socks, copper ion resists
The content of bacterium nylon fibre is 12-20%, and the content of combed cotton is 80-88%.
6. copper ion antibacterial socks according to claim 1 or claim 2, it is characterised in that in the copper ion antibacterial socks, copper ion resists
The content of bacterium nylon fibre is 15%, and the content of combed cotton is 85%.
7. copper ion antibacterial socks according to claim 1 or claim 2, it is characterised in that the copper ion antibacterial socks are five-toe socks.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610130487.4A CN105696112B (en) | 2016-03-08 | 2016-03-08 | A kind of copper ion antibacterial socks |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610130487.4A CN105696112B (en) | 2016-03-08 | 2016-03-08 | A kind of copper ion antibacterial socks |
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| CN105696112A CN105696112A (en) | 2016-06-22 |
| CN105696112B true CN105696112B (en) | 2017-12-26 |
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| CN107916463A (en) * | 2016-10-11 | 2018-04-17 | 杭州鱼非鱼纺织品有限公司 | A kind of novel antibacterial socks |
| CN107385597B (en) * | 2017-07-17 | 2019-05-31 | 福建省晋江市华宇织造有限公司 | Copper ion antibacterial nylon yarn for mesh fabric production |
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| CN113403726B (en) * | 2021-07-07 | 2022-11-15 | 杭州宽明纺织有限公司 | Antibacterial functional fabric and production process thereof |
| CN114318614A (en) * | 2021-12-24 | 2022-04-12 | 江苏微笑新材料科技有限公司 | Preparation method of copper-containing antibacterial polyester yarn, fabric and garment |
| CN114345492A (en) * | 2021-12-27 | 2022-04-15 | 深圳市金阳盛城市服务集团有限公司 | Intelligent garbage treatment equipment and garbage treatment method |
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