CN105695080A - Preparation method of tea oil - Google Patents
Preparation method of tea oil Download PDFInfo
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- CN105695080A CN105695080A CN201610175405.8A CN201610175405A CN105695080A CN 105695080 A CN105695080 A CN 105695080A CN 201610175405 A CN201610175405 A CN 201610175405A CN 105695080 A CN105695080 A CN 105695080A
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- camelliae
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
- C11B1/08—Production of fats or fatty oils from raw materials by pressing by hot pressing
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Microbiology (AREA)
- Edible Oils And Fats (AREA)
Abstract
The invention discloses a preparation method of tea oil, and belongs to the technical field of tea oil preparation. The preparation method comprises the following steps of harvesting tea fruits in October after ripening; putting the harvested tea fruits into a room, wherein the indoor temperature is 23-25 DEG C, and the indoor humidity is 40-50 percent; after stacking for one week, putting the tea fruits under sunlight outdoors, and airing for 3-4 days; airing oil tea seeds, or drying at the temperature of 35-40 DEG C until the water content of the oil tea seeds is 10-15 percent; cooling the aired or dried oil tea seeds to room temperature, and storing in a shade and dry place; putting the oil tea seeds into an extraction machine, extracting, and preparing the tea oil and an oil cake, wherein the extraction temperature is 50-80 DEG C, and the oil residual amount of the oil cake is less than or equal to 6 percent; using the oil cake to process crude oil; refining the crude oil, including (1) dewatering and decolorizing, and (2) vacuum breaking; settling, and filtering. The tea oil prepared by the preparation method has the advantages that the yield rate is high, and the purity is high.
Description
Technical field
The present invention relates to Oleum Camelliae preparing technical field, be specifically related to a kind of Oleum Camelliae preparation method。
Background technology
Oleum Camelliae, also known as Camellia oil, camellia seed oil, is the distinctive Camellia woody edible oil of south China, is one of big xylophyta oil in the world four。Oleum Camelliae is to extract from oil tea mature seed and obtain, and golden yellow color or pale yellow, clear, abnormal smells from the patient delicate fragrance have the laudatory title of " east olive oil "。
Oleum Camelliae is rich in omega-3 fatty acid and Ω-6 fatty acid, a small amount of poor Saponin and tea polyphenols, without cholesterol, erucic acid and the acid of mountain cornel。Its physicochemical properties are similar to olive oil, have good stability and non-oxidizability, are easily absorbed by the body。The preparation of current Oleum Camelliae mainly adopts hot moulding method and extraction, and wherein hot moulding method is generally squeezed for visitor, and the oil yield of shell is low, and band shell squeezing can adsorb to walk oil content, affects oil yield, and the Oleum Camelliae prepared is with obvious astringent taste;Seed chitin is slightly hard, causes component wear, consumes bigger power。Extraction adopts solvent to extract, operation is: peel off seed coat, with ether after pulverizing, petroleum ether lixiviate 24 hours, after filtration, recycling design obtains seed oil, the height of the relative hot moulding method of pick-up rate of the method Oleum Camelliae, pick-up rate is up to 87%, but owing to extraction uses organic solvent to carry out lixiviate, it is thus achieved that Oleum Camelliae finished product in unavoidable residual organic solvent, causing that Oleum Camelliae is impure, the highest being only capable of of purity reaches 85%。
Summary of the invention
The present invention is directed to the technical problem that above-mentioned Oleum Camelliae pick-up rate machine Oleum Camelliae purity is low, it is provided that a kind of pick-up rate and the high Oleum Camelliae preparation method of purity。
In order to solve above-mentioned technical problem, the present invention provides following technical scheme: a kind of Oleum Camelliae preparation method, comprises the following steps:
Step one, tea fruit are gathered: gather after tea fruit maturation during October, gather complete with a collection of tea fruit in one week;
Step 2, tea fruit process: the tea fruit gathered is disposed within, and indoor temperature is 23~25 DEG C, and indoor humidity is 40~50%, after stacking one week, then are placed under outdoor solar light by tea fruit dry in the sun 3~4 days;
Step 3, the preparation of Semen Camelliae and storage: tea fruit, after dry in the sun, takes out Semen Camelliae from tea fruit, filtered out by the impurity in Semen Camelliae, then Semen Camelliae is dried or in 35~40 DEG C dry to Semen Camelliae moisture content be 10~15%;Semen Camelliae after drying or drying is positioned over lucifuge after being cooled to room temperature, dry place preserves;
Step 4, Semen Camelliae squeezing processing: being put into by Semen Camelliae and carry out squeezing in squeezer and produce Oleum Camelliae and oil cake, pressing temperature is 50~80 DEG C, and oil cake is used for processing crude oil by oil cake resid amount≤6%;
Step 5, refine: crude oil is carried out refining treatment: (1) dehydration, decolouring: crude oil is placed in de-airing mixer and is sequentially carried out dehydration, desolventing technology;(2) vacuum breaker: carry out vacuum breaker process then through vapor distillation, cooling after crude oil decolouring;
Step 6, precipitation, filtration: be placed in the sedimentation tank of 9~10 DEG C to precipitate the crude oil after refine, filter after mix with the Oleum Camelliae in step 4 and both to obtain finished product Oleum Camelliae。
The invention have the benefit that the tea fruit gathered is positioned over temperature by this programme is 23~25 DEG C, humidity is during the indoor stacking one week of 40~50%, guarantee that the tea fruit of outer ripe interior life is thoroughly well-done within the time period, and under the specified conditions of scheme, ensure tea fruit stack during not moldy metamorphism, keep fresh, the Oleum Camelliae prepared is made to keep pure, it is placed under outdoor solar light dry in the sun 3~4 days again, tea fruit is preliminarily dried in the sun, sunlight irradiates in the lower tea fruit promoting after ripening thorough, synthesize the composition interphase interaction of Oleum Camelliae and synthesize Oleum Camelliae, and then improve the content of Oleum Camelliae, basic condition is provided for improving Oleum Camelliae pick-up rate;Semen Camelliae is dried to water content 10~15% and ensures that in the longer resting period, Semen Camelliae does not go bad, and preserves the oil content in Semen Camelliae and purity;It addition, crude oil prepared by oil cake, then the process that crude oil carries out refine adopts physical refining method, it is not necessary to mixes with organic solvent, is absent from organic solvent residual problem;Last filtration and deposition condition, efficiently separate the impurity in Oleum Camelliae and Oleum Camelliae。The present invention program prepares the pick-up rate height of Oleum Camelliae in sum, and purity is high, and pick-up rate is up to more than 96%, high purity more than 95%。
Further, Semen Camelliae is carried out by step 4 Oleum Camelliae squeezing pre-treatment in advance, namely before Semen Camelliae squeezing processing, Semen Camelliae is taken out dry in the sun again 1~2 day。Being dried before squeezing, the oil yield of Semen Camelliae improves again, then in oil cake, resid amount reduces, and crude oil amount reduces accordingly。
Further, in (1) of step 5, during dehydration, setting the vacuum of de-airing mixer as 96KPa, be warming up to Oleum Camelliae temperature for 92~96 DEG C with the speed of 1~1.5 DEG C/min, the rotating speed then regulating de-airing mixer is that 55~65r/min carries out dehydration 40min。Under this condition, the efficiency of refine improves。
Further, in (1) of step 5, after completing dehydration, adding percetage by weight in Oleum Camelliae is the decolorising agent of 2%, and the rotating speed regulating de-airing mixer is 55~65r/min, and decolour 30min。Under this condition, the efficiency of decolouring improves。
Further, in (2) of step 5, vapo(u)rizing temperature is 110 DEG C, distillation time is 300min。While ensureing good purification effect, improve purification efficiency。
Detailed description of the invention
Below in conjunction with embodiment, technical solution of the present invention is further illustrated:
Embodiment 1: a kind of Oleum Camelliae preparation method, comprises the following steps:
Step one, tea fruit are gathered: gather after tea fruit maturation during October, gather complete with a collection of tea fruit in one week;
Step 2, tea fruit process: the tea fruit gathered is disposed within, and indoor temperature is 23~25 DEG C, and indoor humidity is 40%, after stacking one week, then are placed under outdoor solar light by tea fruit dry in the sun 4 days;
Step 3, the preparation of Semen Camelliae and storage: tea fruit, after dry in the sun, takes out Semen Camelliae from tea fruit, filtered out by the impurity in Semen Camelliae, then Semen Camelliae is dried to Semen Camelliae moisture content be 10~15%;Semen Camelliae after drying is positioned over lucifuge after being cooled to room temperature, dry place preserves;
Step 4, Semen Camelliae squeezing processing: being put into by Semen Camelliae and carry out squeezing in squeezer and produce Oleum Camelliae and oil cake, pressing temperature is 50~80 DEG C, and oil cake is used for processing crude oil by oil cake resid amount≤6%;
Step 5, refine: crude oil is carried out refining treatment: (1) dehydration, decolouring: crude oil is placed in de-airing mixer and is sequentially carried out dehydration, desolventing technology;(2) vacuum breaker: carry out vacuum breaker process then through vapor distillation, cooling after crude oil decolouring;
Step 6, precipitation, filtration: be placed in the sedimentation tank of 9~10 DEG C to precipitate the crude oil after refine, filter after mix with the Oleum Camelliae in step 4 and both to obtain finished product Oleum Camelliae。
This programme Oleum Camelliae pick-up rate >=96%, purity >=95%。
Embodiment 2: a kind of Oleum Camelliae preparation method, comprises the following steps:
Step one, tea fruit are gathered: gather after tea fruit maturation during October, gather complete with a collection of tea fruit in one week;
Step 2, tea fruit process: the tea fruit gathered is disposed within, and indoor temperature is 23~25 DEG C, and indoor humidity is 40%, after stacking one week, then are placed under outdoor solar light by tea fruit dry in the sun 3 days;
Step 3, the preparation of Semen Camelliae and storage: tea fruit, after dry in the sun, takes out Semen Camelliae from tea fruit, filtered out by the impurity in Semen Camelliae, then Semen Camelliae is placed in 35~40 DEG C dry to Semen Camelliae moisture content be 10~15%;Semen Camelliae after drying is positioned over lucifuge after being cooled to room temperature, dry place preserves;
Step 4, Semen Camelliae squeezing processing: putting into after Semen Camelliae taking out dry in the sun again 1~2 day and carry out squeezing in squeezer and produce Oleum Camelliae and oil cake, pressing temperature is 50~80 DEG C, and oil cake is used for processing crude oil by oil cake resid amount≤4%;
Step 5, refine: crude oil is carried out refining treatment: (1) dehydration, decolouring: crude oil is placed in de-airing mixer and is sequentially carried out dehydration, desolventing technology;During dehydration, setting the vacuum of de-airing mixer as 96KPa, be warming up to Oleum Camelliae temperature for 92~96 DEG C with the speed of 1~1.5 DEG C/min, the rotating speed then regulating de-airing mixer is that 55~65r/min carries out dehydration 40min;After dehydration, adding percetage by weight in Oleum Camelliae is the decolorising agent of 2%, and the rotating speed regulating de-airing mixer is 55~65r/min, and decolour 30min;(2) vacuum breaker: carry out vacuum breaker process then through vapor distillation, cooling after crude oil decolouring;Vapo(u)rizing temperature is 110 DEG C, distillation time is 300min;
Step 6, precipitation, filtration: be placed in the sedimentation tank of 9~10 DEG C to precipitate the crude oil after refine, filter after mix with the Oleum Camelliae in step 4 and both to obtain finished product Oleum Camelliae。
This programme Oleum Camelliae pick-up rate >=96%, purity >=98%。
For a person skilled in the art, under the premise without departing from present configuration, it is also possible to make some deformation and improvement, these also should be considered as protection scope of the present invention, and these are all without affecting effect of the invention process and practical applicability。
Claims (5)
1. an Oleum Camelliae preparation method, it is characterised in that: comprise the following steps:
Step one, tea fruit are gathered: gather after tea fruit maturation during October, gather complete with a collection of tea fruit in one week;
Step 2, tea fruit process: the tea fruit gathered is disposed within, and indoor temperature is 23~25 DEG C, and indoor humidity is 40~50%, after stacking one week, then are placed under outdoor solar light by tea fruit dry in the sun 3~4 days;
Step 3, the preparation of Semen Camelliae and storage: tea fruit, after dry in the sun, takes out Semen Camelliae from tea fruit, filtered out by the impurity in Semen Camelliae, then Semen Camelliae is dried or in 35~40 DEG C dry to Semen Camelliae moisture content be 10~15%;Semen Camelliae after drying or drying is positioned over lucifuge after being cooled to room temperature, dry place preserves;
Step 4, Semen Camelliae squeezing processing: being put into by Semen Camelliae and carry out squeezing in squeezer and produce Oleum Camelliae and oil cake, pressing temperature is 50~80 DEG C, and oil cake is used for processing crude oil by oil cake resid amount≤6%;
Step 5, refine: crude oil is carried out refining treatment: (1) dehydration, decolouring: crude oil is placed in de-airing mixer and is sequentially carried out dehydration, desolventing technology;(2) vacuum breaker: carry out vacuum breaker process then through vapor distillation, cooling after crude oil decolouring;
Step 6, precipitation, filtration: be placed in the sedimentation tank of 9~10 DEG C to precipitate the crude oil after refine, filter after mix with the Oleum Camelliae in step 4 and both to obtain finished product Oleum Camelliae。
2. Oleum Camelliae preparation method as claimed in claim 1, it is characterised in that: Semen Camelliae is carried out Oleum Camelliae squeezing pre-treatment by step 4 in advance, namely before Semen Camelliae squeezing processing, Semen Camelliae is taken out dry in the sun again 1~2 day。
3. Oleum Camelliae preparation method as claimed in claim 2, it is characterized in that: in (1) of step 5, during dehydration, set the vacuum of de-airing mixer as 96KPa, being warming up to Oleum Camelliae temperature for 92~96 DEG C with the speed of 1~1.5 DEG C/min, the rotating speed then regulating de-airing mixer is that 55~65r/min carries out dehydration 40min。
4. the Oleum Camelliae preparation method as according to any one of claims 1 to 3, it is characterized in that: in (1) of step 5, after completing dehydration, adding percetage by weight in Oleum Camelliae is the decolorising agent of 2%, the rotating speed regulating de-airing mixer is 55~65r/min, and decolour 30min。
5. Oleum Camelliae preparation method as claimed in claim 4, it is characterised in that: in (2) of step 5, vapo(u)rizing temperature is 110 DEG C, distillation time is 300min。
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106147993A (en) * | 2016-08-25 | 2016-11-23 | 钟石娣 | The manufacture method of natural Camellia oil oral liquid |
CN106190532A (en) * | 2016-08-14 | 2016-12-07 | 林亚东 | A kind of Oleum Camelliae preparation method |
CN106318602A (en) * | 2016-08-19 | 2017-01-11 | 贵州石阡佛顶山野生油茶油业有限公司 | Processing method of high-quality camellia oil |
CN110283654A (en) * | 2019-06-26 | 2019-09-27 | 贵州大学 | A kind of anti-oxidant and relax bowel and defecation dual-purpose of drug and food tea oil preparation method |
CN112029568A (en) * | 2020-07-31 | 2020-12-04 | 赣州哈克生物科技有限公司 | Special equipment for high-quality original-fragrance initial-pressing tea oil |
CN113817543A (en) * | 2021-09-29 | 2021-12-21 | 广西壮族自治区林业科学研究院 | Method for preparing high-quality tea oil by directly granulating tea seeds at low temperature |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1827754A (en) * | 2006-03-27 | 2006-09-06 | 郴州邦尔泰苏仙油脂有限公司 | Physical low-temperature cold-squeezing process for tea-seed oil |
CN102807918A (en) * | 2012-09-01 | 2012-12-05 | 湖南大三湘油茶科技有限公司 | Original-fragrant camellia oil rich in active components and producing method thereof |
CN103421612A (en) * | 2013-08-30 | 2013-12-04 | 湖南大三湘油茶科技有限公司 | Method for manufacturing oil by using tea oil residues |
CN103725408A (en) * | 2013-12-31 | 2014-04-16 | 贵州省黎平县侗乡米业有限公司 | Processing technology of camellia oil |
CN104031737A (en) * | 2014-07-06 | 2014-09-10 | 福建乘龙农业综合开发有限公司 | Pressing process for preparing camellia oil purely physically |
CN104388182A (en) * | 2014-11-16 | 2015-03-04 | 湖南中富植物油脂有限公司 | Physically pressed tea seed oil and extracting preparation method thereof |
CN105219517A (en) * | 2015-09-25 | 2016-01-06 | 潜山县经汇农业综合发展有限公司 | A kind of organic tea oil production technique |
CN105219520A (en) * | 2015-09-25 | 2016-01-06 | 潜山县经汇农业综合发展有限公司 | A kind of camellia seed oil low-temperature cold pressing preparation technology |
-
2016
- 2016-03-25 CN CN201610175405.8A patent/CN105695080A/en active Pending
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1827754A (en) * | 2006-03-27 | 2006-09-06 | 郴州邦尔泰苏仙油脂有限公司 | Physical low-temperature cold-squeezing process for tea-seed oil |
CN102807918A (en) * | 2012-09-01 | 2012-12-05 | 湖南大三湘油茶科技有限公司 | Original-fragrant camellia oil rich in active components and producing method thereof |
CN103421612A (en) * | 2013-08-30 | 2013-12-04 | 湖南大三湘油茶科技有限公司 | Method for manufacturing oil by using tea oil residues |
CN103725408A (en) * | 2013-12-31 | 2014-04-16 | 贵州省黎平县侗乡米业有限公司 | Processing technology of camellia oil |
CN104031737A (en) * | 2014-07-06 | 2014-09-10 | 福建乘龙农业综合开发有限公司 | Pressing process for preparing camellia oil purely physically |
CN104388182A (en) * | 2014-11-16 | 2015-03-04 | 湖南中富植物油脂有限公司 | Physically pressed tea seed oil and extracting preparation method thereof |
CN105219517A (en) * | 2015-09-25 | 2016-01-06 | 潜山县经汇农业综合发展有限公司 | A kind of organic tea oil production technique |
CN105219520A (en) * | 2015-09-25 | 2016-01-06 | 潜山县经汇农业综合发展有限公司 | A kind of camellia seed oil low-temperature cold pressing preparation technology |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106190532A (en) * | 2016-08-14 | 2016-12-07 | 林亚东 | A kind of Oleum Camelliae preparation method |
CN106318602A (en) * | 2016-08-19 | 2017-01-11 | 贵州石阡佛顶山野生油茶油业有限公司 | Processing method of high-quality camellia oil |
CN106147993A (en) * | 2016-08-25 | 2016-11-23 | 钟石娣 | The manufacture method of natural Camellia oil oral liquid |
CN110283654A (en) * | 2019-06-26 | 2019-09-27 | 贵州大学 | A kind of anti-oxidant and relax bowel and defecation dual-purpose of drug and food tea oil preparation method |
CN112029568A (en) * | 2020-07-31 | 2020-12-04 | 赣州哈克生物科技有限公司 | Special equipment for high-quality original-fragrance initial-pressing tea oil |
CN113817543A (en) * | 2021-09-29 | 2021-12-21 | 广西壮族自治区林业科学研究院 | Method for preparing high-quality tea oil by directly granulating tea seeds at low temperature |
CN113817543B (en) * | 2021-09-29 | 2024-04-19 | 广西壮族自治区林业科学研究院 | Method for preparing high-quality tea oil by directly low-temperature grain finishing of tea seeds |
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