CN105647702A - Preparation method of aloe soap achieving skin beautifying - Google Patents
Preparation method of aloe soap achieving skin beautifying Download PDFInfo
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- CN105647702A CN105647702A CN201610027599.7A CN201610027599A CN105647702A CN 105647702 A CN105647702 A CN 105647702A CN 201610027599 A CN201610027599 A CN 201610027599A CN 105647702 A CN105647702 A CN 105647702A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a preparation method of aloe soap achieving skin beautifying. The method comprises the steps that shea butter and coconut oil are mixed in proportion, water-bath heating is conducted, the mixture is melted, continuous stirring is conducted, and the mixture is mixed to be uniform, wherein the temperature ranges from 55 DEG C to 70 DEG C; 10-30 parts of aloe extracting solution is weighed and put in a water bath, wherein the temperature ranges from 55 DEG C to 70 DEG C; after an oil phase and an extracting solution phase both reach the same temperature, the extracting solution is poured into the oil phase, stirring is conducted for 1-2 min, 0.2-1.5 parts of sodium hydroxide is added in the stirring state, continuous stirring is conducted, under the action of saponification reaction, the two phases which are insoluble originally start to change and gradually change into milk white emulsion, the reaction is completed after 8-15 min, stirring is stopped, obtained liquid soap is poured into a mold, standing is conducted at room temperature, and the aloe soap achieving skin beautifying is obtained.
Description
Technical field
The invention belongs to household chemicals production technical field, the preparation method being specifically related to a kind of Aloe care skin soap.
Background technology
Fancy soap is requisite washing and nursing article in daily life, with sodium soap and other surfactants for primary raw material, adds quality improver and appearance modifying agents, the product made after machine-shaping. The function of fancy soap is cleaning washing, it is used in above skin that yes removes earth dirt, skin secretion, Excreta, chemical substance or antibacterial etc., in the today stressing cosmetic result, removing the cosmetics of skin surface, skin care products or medicine is also one of its main purposes. In the prior art, the more insights of fancy soap are fatty acid sodium salts is the Cake-shape soap of soap base, although having good cleaning force, foaming characteristic and easy washability, but weak to hard water, producing incrustation scale during washing, form calcium and magnesium soap, degreasing power is strong, the soap of human body life-time service meta-alkalescence can make skin feel dry and astringent, has excitement.
Aloe (formal name used at school: Aloe) is generally called Aloe, originates in Mediterranean, Africa, for Eremurus chinensis section herbaceos perennial, according to wild aloe kind kind more than 300 of textual criticism, is distributed mainly on the ground such as Africa. this kind of plant is quite liked by masses, mainly because it is prone to plantation, for the ornamental plant that floral leaf has both. owing to Aloe has bactericidal action, antiinflammatory action, moistening beautification function, effect is let out under stomach invigorating, the heart tonifying effect of invigorating blood circulation, immunity and regeneration, immunity and antitumor action, Detoxication, anti-aging effects, analgesia, sedation, anti-sunlight function, insect protected, antisepsis, effect that deodorant effect etc. is peculiar, cause scientific circles, the particularly extensive attention of medical circle, especially the western developed country being representative with the U.S., put into substantial amounts of manpower, material resources, financial resources research and development application Aloe, thus define one " Aloe heat ", Aloe development is very fast, development utilizes notable, economic benefit is huge, its achievement in research is applied not only to medical treatment, beauty treatment, health care of food, but also it is applied to dyestuff, metallurgical, weaving, pesticide, in the fields such as herding, from then on Aloe finds oneself greatly elevated in fame and status.
But existing commercially available aloe vera soap, its health-care effect is not notable, the Chinese patent that such as publication number is CN104312799A discloses a kind of aloe moisture-keeping type fancy soap, and described fancy soap is formulated by glycol distearate 3-9 part, silicone oil 3-7 part, titanium dioxide 2-6 part, Oleum Terebinthinae 0.4-0.7 part, Aloe powder 2-3 part, natural oil 4-6 part, kefir milk element 0.7-0.9 part and water 30-60 part.Although this invention has the effects such as strong, the sterilization of dirt-removing power, but it is to add with the form of Aloe powder so that its active component utilization rate is not high, it is difficult to well play effect of Aloe.
Summary of the invention
Goal of the invention: for the deficiencies in the prior art, the preparation method that the invention provides a kind of Aloe care skin soap, described method adopts special extracting mode to obtain Aloe extraction solution, it is possible to effect of more effective performance Aloe.
Technical scheme: the preparation method that the invention provides a kind of Aloe care skin soap, step is: making it melt with heating in water bath after shea butter, cocos nucifera oil being mixed in proportion and do not stop stirring so that it is mix homogeneously, temperature range is 55��70 DEG C; Weighing the Aloe extraction solution of 10-30 part, be placed in water-bath, temperature range is 55��70 DEG C; After oil phase, extraction liquid phase have all reached same temperature, first extracting solution is poured in oil phase, stir 1-2 minute, 0.2-1.5 part sodium hydroxide solution is added under stirring, continuing stirring, under the effect of saponification, originally insoluble biphase beginning changes, gradually become milky emulsion, react completely after 8-15 minute, stop stirring, pour gained soap lye into mould, room temperature is placed, and obtains Aloe care skin soap.
Concrete, the method that obtains of above-mentioned Aloe extract is: take fresh aloe clean, micronizing, add 5-20 times of water, mix homogeneously; Frost-melt repetition 2��3 times; Then carry out supersound extraction, be centrifuged, filter, take supernatant, obtain Aloe extraction solution. The ground product that described micronizing obtains is jelly.
Frost-thawing described in said process is to be freezed 10��24 hours at the temperature of-40��-20 DEG C by mixed liquor, and ambient temperatare is put until it melts.
Described microwave extraction condition is: microwave power is 400��800W; The microwave time is 20s��300s.
Beneficial effect: microwave extraction can make aloe cell internal temperature rise rapidly owing to absorbing microwave energy so that it is cell interior pressure exceedes cell wall expansion ability to bear, cell rupture. In cell, effective ingredient freely flows out, and under relatively low temperature conditions, spe medium is caught and dissolves, and both quickly, effectively, can keep again activity.
The present invention contains a large amount of Aloe extraction solution, human body skin is all had good nutrition, moistens by multivitamin therein and polysaccharide component, moisturizing, anti-acne effect, make skin more smooth flexible.
Detailed description of the invention:
Embodiment 1
Step 1) take fresh aloe clean, micronizing, add 5-20 times of water, mix homogeneously.
Step 2) by step 1) mixed liquor that obtains freezes 10��24 hours at the temperature of-40��-20 DEG C, ambient temperatare is put until it melts; Repeat frost-thawing step 2��3 times; So, cell can, while forming ice pellets and increasing residue cytosol salinity, occur swelling, broken. Make active component fully be discharged, and also keep activity.
Step 3) by step 2) gained mixed liquor carries out microwave extraction, microwave power is 400W; The microwave time is 300s.
Step 4) by step 3) mixed liquor of gained is centrifuged, filters, takes supernatant, obtains Aloe extraction solution.
Step 5) by shea butter 2.5 parts, 5 parts of Hybrid Heating of cocos nucifera oil, maintain temperature 55 DEG C, take Aloe extraction solution 10 parts, heating adds in above-mentioned oil phase after 55 DEG C, after stirring 1-2 minute, adds sodium hydroxide solution 0.2 part under stirring, it is stirred continuously, originally insoluble biphase beginning changes, and gradually becomes milky emulsion, reacts completely after 15 minutes, stop stirring, pouring gained soap lye into mould, room temperature is placed, and obtains Aloe care skin soap.
Embodiment 2
Step 1) take fresh aloe clean, micronizing, add 5-20 times of water, mix homogeneously.
Step 2) by step 1) mixed liquor that obtains freezes 10��24 hours at the temperature of-40��-20 DEG C, ambient temperatare is put until it melts; Repeat frost-thawing step 2��3 times; So, cell can, while forming ice pellets and increasing residue cytosol salinity, occur swelling, broken. Make active component fully be discharged, and also keep activity.
Step 3) by step 2) gained mixed liquor carries out microwave extraction, microwave power is 400W; The microwave time is 300s.
Step 4) by step 3) mixed liquor of gained is centrifuged, filters, takes supernatant, obtains Aloe extraction solution.
Step 5) by shea butter 5 parts, 10 parts of Hybrid Heating of cocos nucifera oil, maintain temperature 55 DEG C, take Aloe extraction solution 20 parts, heating adds in above-mentioned oil phase after 55 DEG C, after stirring 1-2 minute, adds sodium hydroxide solution 1.5 parts under stirring, it is stirred continuously, originally insoluble biphase beginning changes, and gradually becomes milky emulsion, reacts completely after 15 minutes, stop stirring, pouring gained soap lye into mould, room temperature is placed, and obtains Aloe care skin soap.
Embodiment 3
Step 1) take fresh aloe clean, micronizing, add 5-20 times of water, mix homogeneously.
Step 2) by step 1) mixed liquor that obtains freezes 10��24 hours at the temperature of-40��-20 DEG C, ambient temperatare is put until it melts; Repeat frost-thawing step 2��3 times; So, cell can, while forming ice pellets and increasing residue cytosol salinity, occur swelling, broken. Make active component fully be discharged, and also keep activity.
Step 3) by step 2) gained mixed liquor carries out microwave extraction, microwave power is 400W; The microwave time is 300s.
Step 4) by step 3) mixed liquor of gained is centrifuged, filters, takes supernatant, obtains Aloe extraction solution.
Step 5) by shea butter 5 parts, 10 parts of Hybrid Heating of cocos nucifera oil, maintain temperature 55 DEG C, take Aloe extraction solution 30 parts, heating adds in above-mentioned oil phase after 55 DEG C, after stirring 1-2 minute, adds sodium hydroxide solution 1.2 parts under stirring, it is stirred continuously, originally insoluble biphase beginning changes, and gradually becomes milky emulsion, reacts completely after 15 minutes, stop stirring, pouring gained soap lye into mould, room temperature is placed, and obtains Aloe care skin soap.
Embodiment 4
Step 1) take fresh aloe clean, micronizing, add 5-20 times of water, mix homogeneously.
Step 2) by step 1) mixed liquor that obtains freezes 10��24 hours at the temperature of-40��-20 DEG C, ambient temperatare is put until it melts; Repeat frost-thawing step 2��3 times; So, cell can, while forming ice pellets and increasing residue cytosol salinity, occur swelling, broken. Make active component fully be discharged, and also keep activity.
Step 3) by step 2) gained mixed liquor carries out microwave extraction, microwave power is 640W; The microwave time is 100s.
Step 4) by step 3) mixed liquor of gained is centrifuged, filters, takes supernatant, obtains Aloe extraction solution.
Step 5) by shea butter 2.5 parts, 5 parts of Hybrid Heating of cocos nucifera oil, maintain temperature 70 C, take Aloe extraction solution 10 parts, heating adds in above-mentioned oil phase after 70 DEG C, after stirring 1-2 minute, adds sodium hydroxide solution 0.2 part under stirring, it is stirred continuously, originally insoluble biphase beginning changes, and gradually becomes milky emulsion, reacts completely after 8 minutes, stop stirring, pouring gained soap lye into mould, room temperature is placed, and obtains Aloe care skin soap.
Embodiment 5
Step 1) take fresh aloe clean, micronizing, add 5-20 times of water, mix homogeneously.
Step 2) by step 1) mixed liquor that obtains freezes 10��24 hours at the temperature of-40��-20 DEG C, ambient temperatare is put until it melts; Repeat frost-thawing step 2��3 times; So, cell can, while forming ice pellets and increasing residue cytosol salinity, occur swelling, broken. Make active component fully be discharged, and also keep activity.
Step 3) by step 2) gained mixed liquor carries out microwave extraction, microwave power is 640W; The microwave time is 100s.
Step 4) by step 3) mixed liquor of gained is centrifuged, filters, takes supernatant, obtains Aloe extraction solution.
Step 5) by shea butter 5 parts, 10 parts of Hybrid Heating of cocos nucifera oil, maintain temperature 70 C, take Aloe extraction solution 20 parts, heating adds in above-mentioned oil phase after 70 DEG C, after stirring 1-2 minute, adds sodium hydroxide solution 1.5 parts under stirring, it is stirred continuously, originally insoluble biphase beginning changes, and gradually becomes milky emulsion, reacts completely after 8 minutes, stop stirring, pouring gained soap lye into mould, room temperature is placed, and obtains Aloe care skin soap.
Embodiment 6
Step 1) take fresh aloe clean, micronizing, add 5-20 times of water, mix homogeneously.
Step 2) by step 1) mixed liquor that obtains freezes 10��24 hours at the temperature of-40��-20 DEG C, ambient temperatare is put until it melts; Repeat frost-thawing step 2��3 times; So, cell can, while forming ice pellets and increasing residue cytosol salinity, occur swelling, broken. Make active component fully be discharged, and also keep activity.
Step 3) by step 2) gained mixed liquor carries out microwave extraction, microwave power is 640W; The microwave time is 100s.
Step 4) by step 3) mixed liquor of gained is centrifuged, filters, takes supernatant, obtains Aloe extraction solution.
Step 5) by shea butter 5 parts, 10 parts of Hybrid Heating of cocos nucifera oil, maintain temperature 60 C, take Aloe extraction solution 30 parts, heating adds in above-mentioned oil phase after 60 DEG C, after stirring 1-2 minute, adds sodium hydroxide solution 1.2 parts under stirring, it is stirred continuously, originally insoluble biphase beginning changes, and gradually becomes milky emulsion, reacts completely after 8 minutes, stop stirring, pouring gained soap lye into mould, room temperature is placed, and obtains Aloe care skin soap.
Embodiment 7
Step 1) take fresh aloe clean, micronizing, add 5-20 times of water, mix homogeneously.
Step 2) by step 1) mixed liquor that obtains freezes 10��24 hours at the temperature of-40��-20 DEG C, ambient temperatare is put until it melts; Repeat frost-thawing step 2��3 times; So, cell can, while forming ice pellets and increasing residue cytosol salinity, occur swelling, broken. Make active component fully be discharged, and also keep activity.
Step 3) by step 2) gained mixed liquor carries out microwave extraction, microwave power is 800W; The microwave time is 20s.
Step 4) by step 3) mixed liquor of gained is centrifuged, filters, takes supernatant, obtains Aloe extraction solution.
Step 5) by shea butter 2.5 parts, 5 parts of Hybrid Heating of cocos nucifera oil, maintain temperature 60 C, take Aloe extraction solution 10 parts, heating adds in above-mentioned oil phase after 60 DEG C, after stirring 1-2 minute, adds sodium hydroxide solution 0.2 part under stirring, it is stirred continuously, originally insoluble biphase beginning changes, and gradually becomes milky emulsion, reacts completely after 12 minutes, stop stirring, pouring gained soap lye into mould, room temperature is placed, and obtains Aloe care skin soap.
Embodiment 8
Step 1) take fresh aloe clean, micronizing, add 5-20 times of water, mix homogeneously.
Step 2) by step 1) mixed liquor that obtains freezes 10��24 hours at the temperature of-40��-20 DEG C, ambient temperatare is put until it melts; Repeat frost-thawing step 2��3 times; So, cell can, while forming ice pellets and increasing residue cytosol salinity, occur swelling, broken. Make active component fully be discharged, and also keep activity.
Step 3) by step 2) gained mixed liquor carries out microwave extraction, microwave power is 800W; The microwave time is 20s.
Step 4) by step 3) mixed liquor of gained is centrifuged, filters, takes supernatant, obtains Aloe extraction solution.
Step 5) by shea butter 5 parts, 10 parts of Hybrid Heating of cocos nucifera oil, maintain temperature 60 C, take Aloe extraction solution 20 parts, heating adds in above-mentioned oil phase after 60 DEG C, after stirring 1-2 minute, adds sodium hydroxide solution 1.5 parts under stirring, it is stirred continuously, originally insoluble biphase beginning changes, and gradually becomes milky emulsion, reacts completely after 12 minutes, stop stirring, pouring gained soap lye into mould, room temperature is placed, and obtains Aloe care skin soap.
Embodiment 9
Step 1) take fresh aloe clean, micronizing, add 5-20 times of water, mix homogeneously.
Step 2) by step 1) mixed liquor that obtains freezes 10��24 hours at the temperature of-40��-20 DEG C, ambient temperatare is put until it melts; Repeat frost-thawing step 2��3 times; So, cell can, while forming ice pellets and increasing residue cytosol salinity, occur swelling, broken. Make active component fully be discharged, and also keep activity.
Step 3) by step 2) gained mixed liquor carries out microwave extraction, microwave power is 800W; The microwave time is 20s.
Step 4) by step 3) mixed liquor of gained is centrifuged, filters, takes supernatant, obtains Aloe extraction solution.
Step 5) by shea butter 5 parts, 10 parts of Hybrid Heating of cocos nucifera oil, maintain temperature 60 C, take Aloe extraction solution 30 parts, heating adds in above-mentioned oil phase after 60 DEG C, after stirring 1-2 minute, adds sodium hydroxide solution 1.2 parts under stirring, it is stirred continuously, originally insoluble biphase beginning changes, and gradually becomes milky emulsion, reacts completely after 12 minutes, stop stirring, pouring gained soap lye into mould, room temperature is placed, and obtains Aloe care skin soap.
Claims (5)
1. the preparation method of an Aloe care skin soap, it is characterised in that: making it melt with heating in water bath after shea butter, cocos nucifera oil being mixed in proportion and do not stop stirring so that it is mix homogeneously, temperature range is 55��70 DEG C; Weighing the Aloe extraction solution of 10-30 part, be placed in water-bath, temperature range is 55��70 DEG C; After oil phase, extraction liquid phase have all reached same temperature, first extracting solution is poured in oil phase, stir 1-2 minute, 0.2-1.5 part sodium hydroxide is added under stirring, continuing stirring, under the effect of saponification, originally insoluble biphase beginning changes, gradually become milky emulsion, react completely after 8-15 minute, stop stirring, pour gained soap lye into mould, room temperature is placed, and obtains Aloe care skin soap.
2. preparation method as claimed in claim 1, it is characterised in that the method that obtains of described Aloe extract is: take fresh aloe clean, micronizing, add 5-20 times of water, mix homogeneously; Frost-melt repetition 2��3 times;Then carry out supersound extraction, be centrifuged, filter, take supernatant, obtain Aloe extraction solution.
3. preparation method as claimed in claim 1, it is characterised in that the ground product that described micronizing obtains is jelly.
4. preparation method as claimed in claim 1, it is characterised in that described frost-thawing is to be freezed 10��24 hours at the temperature of-40��-20 DEG C by mixed liquor, ambient temperatare is put until it melts.
5. preparation method as claimed in claim 1, it is characterised in that described microwave extraction condition is: microwave power is 400��800W; The microwave time is 20s��300s.
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| CN201610027599.7A CN105647702A (en) | 2016-01-15 | 2016-01-15 | Preparation method of aloe soap achieving skin beautifying |
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| CN201610027599.7A CN105647702A (en) | 2016-01-15 | 2016-01-15 | Preparation method of aloe soap achieving skin beautifying |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105950322A (en) * | 2016-06-24 | 2016-09-21 | 山东省十里香芝麻制品有限公司 | Fresh ground sesame seed oil soap |
| CN107868737A (en) * | 2016-09-23 | 2018-04-03 | 金凯 | A kind of preparation method of new amino acid Aloe care skin soap |
| CN108659999A (en) * | 2018-05-08 | 2018-10-16 | 贵州大学 | A kind of aloe handmade soap preparation method |
| CN115670982A (en) * | 2022-11-25 | 2023-02-03 | 南京科技职业学院 | Essential oil-containing liquid crystal hand cream and preparation method thereof |
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| CN102329702A (en) * | 2011-08-25 | 2012-01-25 | 杭州师范大学 | Pure natural plant perfumed soap and preparation method thereof |
| CN104130888A (en) * | 2014-08-07 | 2014-11-05 | 张萍 | Special formula of cold-process handmade soap as well as preparation method and application thereof |
| CN104419567A (en) * | 2013-08-29 | 2015-03-18 | 青岛蓝色科技信息管理有限公司 | Inflammation diminishing handmade soap |
| CN105154265A (en) * | 2015-10-30 | 2015-12-16 | 南京科技职业学院 | Preparation method and product of natural shampoo soap |
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2016
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| CN1582713A (en) * | 2003-08-19 | 2005-02-23 | 徐敏 | Method for preparing aloe gel, aloe leaf gel and aloe skin gel and technology of preparing polysaccharide products of aloe |
| CN102329702A (en) * | 2011-08-25 | 2012-01-25 | 杭州师范大学 | Pure natural plant perfumed soap and preparation method thereof |
| CN104419567A (en) * | 2013-08-29 | 2015-03-18 | 青岛蓝色科技信息管理有限公司 | Inflammation diminishing handmade soap |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105950322A (en) * | 2016-06-24 | 2016-09-21 | 山东省十里香芝麻制品有限公司 | Fresh ground sesame seed oil soap |
| CN107868737A (en) * | 2016-09-23 | 2018-04-03 | 金凯 | A kind of preparation method of new amino acid Aloe care skin soap |
| CN108659999A (en) * | 2018-05-08 | 2018-10-16 | 贵州大学 | A kind of aloe handmade soap preparation method |
| CN115670982A (en) * | 2022-11-25 | 2023-02-03 | 南京科技职业学院 | Essential oil-containing liquid crystal hand cream and preparation method thereof |
| CN115670982B (en) * | 2022-11-25 | 2024-03-12 | 南京科技职业学院 | Liquid crystal hand cream containing essential oil and preparation method thereof |
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Application publication date: 20160608 |