CN105623676A - Preparation method of halogen-free flame retardation composition - Google Patents
Preparation method of halogen-free flame retardation composition Download PDFInfo
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- CN105623676A CN105623676A CN201410586142.0A CN201410586142A CN105623676A CN 105623676 A CN105623676 A CN 105623676A CN 201410586142 A CN201410586142 A CN 201410586142A CN 105623676 A CN105623676 A CN 105623676A
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Abstract
The invention discloses a preparation method of a halogen-free flame retardation composition. The composition comprises, by weight, 1-3 parts of antimony dioxide, 1-2 parts of citric acid, 3-7 parts of aluminum hydroxide, 1-3 parts of hydrotalcite, 7-12 parts of melamine phosphate and 8-15 parts of water. The preparation method comprises the following steps: taking above raw materials according to above proportions, mixing the raw materials except water according to an arbitrary sequence, stirring the mixed raw materials until uniformity, and adding water to precipitate.
Description
Technical field
The present invention relates to fire retardant manufacturing technology. Particularly a kind of halogen-free, flame-retardant composition.
Background technology
Fire retardant and compositions thereof have vital effect for current modern industry and scientific and technological industry, and there is a large amount of use in a lot of fields. And the fire-resistant characteristic that traditional fire retardant utilizes halogen mostly carries out fire-retardant. But the problem of environmental pollution that this raw material causes is increasingly severe in modern society. So, for this phenomenon, much research and propose fire retardant and the compositions thereof of halogen-free environmental. Chinese patent (publication number 103911866A) proposes a kind of anti-flaming dope and flame-retardant textile, wherein utilizes isocyanate group to eliminate halogen. Further, Chinese patent (publication number 103709437A) also discloses that a kind of halogen-free flame retardants. But both the above scheme all exists the defect of complex manufacturing technology, it is both needed to substantial amounts of operating procedure, utilizes that mixing kettle etc. is large-scale adds working equipment.
Summary of the invention
For the defect existed in above technology, the preparation method that the present invention provides a kind of halogen-free, flame-retardant composition.
It is characterized in that comprising the following steps:
The first step, antimony trichloride 1��3 part, citric acid 1��2 part, aluminium hydroxide 3��7 parts, brucite 1��3 part, melamine phosphate 7-12 part, 8��15 parts of water.
Second step, mixes in addition to water by thing mixed above.
3rd step, blends.
Detailed description of the invention
Embodiment 1
Antimony trichloride 3 parts, citric acid 2 parts, aluminium hydroxide 5 parts, brucite 3 parts, melamine phosphate 11 parts, 12 parts of water.
The above compositions in addition to water of mixing in any order, after stirring, aqueous precipitation.
Embodiment 2
Antimony trichloride 2 parts, citric acid 1 part, aluminium hydroxide 4 parts, brucite 1 part, melamine phosphate 7 parts, 10 parts of water.
The above compositions in addition to water of mixing in any order, after stirring, aqueous precipitation.
Embodiment 3
Antimony trichloride 1 part, citric acid 2 parts, 5 parts of magnesium hydroxide, brucite 1.5 parts, melamine phosphate 10 parts, 12.5 parts of water.
The above compositions in addition to water of mixing in any order, after stirring, aqueous precipitation.
Claims (3)
1. the preparation method of a halogen-free, flame-retardant composition, it is characterised in that comprise the following steps:
The first step, antimony trichloride 1��3 part, citric acid 1��2 part, aluminium hydroxide 3��7 parts, brucite 1��3 part, melamine phosphate 7-12 part, 8��15 parts of water.
Second step, mixes in addition to water by thing mixed above.
3rd step, blends.
2. the preparation method of halogen-free, flame-retardant composition according to claim 1, it is characterised in that: include following proportioning composition (by weight): antimony trichloride 3 parts, citric acid 2 parts, aluminium hydroxide 5 parts, brucite 3 parts, melamine phosphate 11 parts, 12 parts of water.
3. halogen-free, flame-retardant composition according to claim 1, it is characterised in that described aluminium hydroxide available hydrogen magnesium oxide substitutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410586142.0A CN105623676A (en) | 2014-10-27 | 2014-10-27 | Preparation method of halogen-free flame retardation composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410586142.0A CN105623676A (en) | 2014-10-27 | 2014-10-27 | Preparation method of halogen-free flame retardation composition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105623676A true CN105623676A (en) | 2016-06-01 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410586142.0A Pending CN105623676A (en) | 2014-10-27 | 2014-10-27 | Preparation method of halogen-free flame retardation composition |
Country Status (1)
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| CN (1) | CN105623676A (en) |
Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20080089717A (en) * | 2007-04-02 | 2008-10-08 | 주식회사 케이씨씨 | Fire retardant composition and decorative sheet using the same |
| KR20090124030A (en) * | 2008-05-29 | 2009-12-03 | 정주영 | Fireproofing and retardedfire agent |
| CN101693835A (en) * | 2009-08-25 | 2010-04-14 | 太仓市华鼎塑料有限公司 | Environment-friendly polypropylene composite material with high efficiency flame retardance |
| JP2010534757A (en) * | 2007-07-28 | 2010-11-11 | ケミスケ ファブリック ブデンヘイム ケージー | Halogen-free flame retardant |
| CN102869724A (en) * | 2010-09-28 | 2013-01-09 | 东丽株式会社 | Thermoplastic resin composition and molded item formed from same |
| CN102977899A (en) * | 2012-12-24 | 2013-03-20 | 胶州市富田化工有限公司 | Environment-friendly flame retardant |
| CN103074087A (en) * | 2012-12-30 | 2013-05-01 | 胶州市富田化工有限公司 | Composite fire retardant |
| CN103074080A (en) * | 2012-12-30 | 2013-05-01 | 胶州市富田化工有限公司 | Flame retardant |
| CN103074079A (en) * | 2012-12-30 | 2013-05-01 | 胶州市富田化工有限公司 | Halogen-free flame retardant |
| CN103201355A (en) * | 2010-08-23 | 2013-07-10 | 卡特纳添加剂有限公司 | Flame protection agent compositions containing triazine intercalated metal phosphates |
| CN103588994A (en) * | 2013-10-30 | 2014-02-19 | 山东吉青化工有限公司 | Efficient composite flame retardant |
-
2014
- 2014-10-27 CN CN201410586142.0A patent/CN105623676A/en active Pending
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20080089717A (en) * | 2007-04-02 | 2008-10-08 | 주식회사 케이씨씨 | Fire retardant composition and decorative sheet using the same |
| JP2010534757A (en) * | 2007-07-28 | 2010-11-11 | ケミスケ ファブリック ブデンヘイム ケージー | Halogen-free flame retardant |
| KR20090124030A (en) * | 2008-05-29 | 2009-12-03 | 정주영 | Fireproofing and retardedfire agent |
| CN101693835A (en) * | 2009-08-25 | 2010-04-14 | 太仓市华鼎塑料有限公司 | Environment-friendly polypropylene composite material with high efficiency flame retardance |
| CN103201355A (en) * | 2010-08-23 | 2013-07-10 | 卡特纳添加剂有限公司 | Flame protection agent compositions containing triazine intercalated metal phosphates |
| CN102869724A (en) * | 2010-09-28 | 2013-01-09 | 东丽株式会社 | Thermoplastic resin composition and molded item formed from same |
| CN102977899A (en) * | 2012-12-24 | 2013-03-20 | 胶州市富田化工有限公司 | Environment-friendly flame retardant |
| CN103074087A (en) * | 2012-12-30 | 2013-05-01 | 胶州市富田化工有限公司 | Composite fire retardant |
| CN103074080A (en) * | 2012-12-30 | 2013-05-01 | 胶州市富田化工有限公司 | Flame retardant |
| CN103074079A (en) * | 2012-12-30 | 2013-05-01 | 胶州市富田化工有限公司 | Halogen-free flame retardant |
| CN103588994A (en) * | 2013-10-30 | 2014-02-19 | 山东吉青化工有限公司 | Efficient composite flame retardant |
Non-Patent Citations (1)
| Title |
|---|
| 王媛原等: "阻燃剂及材料的阻燃处理", 《化学教育》 * |
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| C06 | Publication | ||
| PB01 | Publication | ||
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| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20160601 |