CN105602725A - Base with ripe fruit sweetness and aroma - Google Patents
Base with ripe fruit sweetness and aroma Download PDFInfo
- Publication number
- CN105602725A CN105602725A CN201610189655.7A CN201610189655A CN105602725A CN 105602725 A CN105602725 A CN 105602725A CN 201610189655 A CN201610189655 A CN 201610189655A CN 105602725 A CN105602725 A CN 105602725A
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- China
- Prior art keywords
- essence
- isoamyl
- acetate
- ethyl
- iso
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
- Seasonings (AREA)
Abstract
The invention provides a base which can be combined with multiple fruit essences and enable the fruit essences to generate sweetness and aroma. The base contains 2-10% of isoamyl isovalerate, 10-20% of isoamyl acetate, 15-20% of ethyl acetate, 10-20% of butyl acetate, 1-2% of sweet orange oil, 0.8-1.5% of lemon oil, 10-20% of isoamyl butyrate and 20-30% of ethyl butyrate. The base can be used in food, tobaccos and daily necessities, such as toothpaste, shampoo, toilet soap and the like.
Description
Technical field
The present invention relates to food flavor, specifically a kind of essence with the fragrant and sweet taste of mature fruit.
Background technology
The fragrant and sweet taste of mature fruit can give happy sensation and receive an acclaim, but the fragrant and sweet taste of existing essence is not obvious.
CN102304429A discloses a kind of tobacco feeding essence formula with the fresh and sweet fragrance of fruit, ethyl maltol 2 ~ 4%, ethyl sauce fruit ketone 2 ~ 3%, leaf-alcohol 0.1 ~ 0.3%, damascone 0.05 ~ 0.1%, ethyl phenylacetate 0.1 ~ 0.5%, nerolidol 0.01 ~ 0.1%, jujube tincture 8 ~ 10%, linalool 0.01 ~ 0.05%, ethyl isovalerate 0.02 ~ 0.08%, benzoic acid 0.1 ~ 0.3%, B position violet ketone 0.05 ~ 0.16%, geranyl acetone 0.02 ~ 0.08%, glycerine 20 ~ 30%, propane diols 40 ~ 55% and edible ethanol 10 ~ 18%.
The preparation method of the open fruit essence of CN102465055A, the composition of essence and proportioning are: 12～43 parts of fruit perfume bases, 10～30 parts of fruit inspissated juices, 28～45 parts of propane diols, 18～32 parts of HFCSs, 3～20 parts of fruit extracts.
CN103451018A the invention discloses a kind of compound chewing gum essence special, it consists of ethyl butyrate 9.0～12.0%, ethyl acetate 2.0～4.0%, isoamyl acetate 8.0～11.0%, allyl hexanoate 3.0～5.0%, Natural menthol 3.0～5.0%, vanillic aldehyde 4.0～7.0%, the orange oil 8.0～10.0% of colding pressing, glyceryl triacetate 22.4～52.8%, ethyl isovalerate 1.5～3.0%, gaultherolin 0.5～1.5%, has the fruit characteristic perfume features such as sweet orange, lemon, pineapple, banana.
CN102634412A discloses the compound method of a kind of toothpaste fruit type essence, taking menthol, lemon oil as major ingredient, prepares essence taking bergamot mint oil, borneol, sassafras oil, tea oil, ethyl butyrate, phenylmethyl acetate as auxiliary material.
Summary of the invention
The object of the present invention is to provide one to be combined with various fruits essence, make fruit essence produce the perfume base of sweet ripe fragrance.
Perfume base of the present invention contains iso-amyl iso-valeriate 2-10%, isoamyl acetate 10-20%, ethyl acetate 15-20%, butyl acetate 10-20%, orange oil 1-2%, lemon oil 0.8-1.5%, isoamyl butyrate 10-20%, ethyl butyrate 20-30% by weight percentage.
Preferably, contain by weight percentage iso-amyl iso-valeriate 6-8%, isoamyl acetate 13-18%, ethyl acetate 15-20%, butyl acetate 12-18%, orange oil 1-2%, lemon oil 0.8-1.2%, isoamyl butyrate 12-16%, ethyl butyrate 24-28%.
Be more preferably, by weight by iso-amyl iso-valeriate 7.5%, isoamyl acetate 15.5%, ethyl acetate 18.3%, butyl acetate 15.5%, orange oil 1.6%, lemon oil 0.95%, isoamyl butyrate 14.5%, ethyl butyrate 26.15% forms.
Percentage by weight of the present invention can also also contain 0.3-1.0% cinnamic acid methyl esters, at least one in 0.3-1.0% citral. Preferably, by iso-amyl iso-valeriate 7.5%, isoamyl acetate 15.5%, ethyl acetate 17.3%, butyl acetate 15.5%, orange oil 1.6%, lemon oil 0.95%, isoamyl butyrate 14.3%, ethyl butyrate 26.15%, cinnamic acid methyl esters 0.6%, citral 0.6% forms.
The present invention can coordinate with various fruits essence, makes fruit essence produce sweet ripe fragrance, has natural, the distinctive sweet sense of mature fruit, fruital. Be added in fruit essence as fruit perfume base, give fruit essence new, the fragrant sense of ripe hesperidium natural, full, that feature is outstanding, screening is subject to popular ripe hesperidium perfume (or spice) deeply, improves the fragrance odor type of fruit essence entirety.
The present invention can be used for food, tobacco, commodity as toothpaste, shampoo, perfumed soap etc.
Detailed description of the invention
Embodiment 1
Get 7.5 grams of iso-amyl iso-valeriates, 15.5 grams of isoamyl acetates, 18.3 grams, ethyl acetate, 15.5 grams of butyl acetates, 1.6 grams of orange oils, 0.95 gram of lemon oil, 14.5 grams of isoamyl butyrates, 26.15 grams of ethyl butyrates, adopt automatic charging equipment, successively monomer is dropped into agitator, under normal temperature sealing, use screw mixing 3 hours, rotating speed is 30 turn/min, cold chamber is placed slaking in 5-10 days, obtains having the essence of the fragrant and sweet taste of mature fruit.
Sensory evaluation
1. choose fresh, high-quality, ripe 5 kinds of fruit of apple, honey peach, banana, pineapple, grape, normal temperature is deposited further slaking in 5 days, cleaning, peeling and core, respectively pulp is squeezed the juice, filter to obtain clarified solution fruit juice, be used for contrasting and judging with essence of the present invention.
2. (Guangdong is along food seasoning Co., Ltd production greatly to choose commercially available flavoring apple essence, model: 25011025, specification 10kg/ bucket, formula: hexanal 0.65%, isoamyl acetate 0.95%, isoamyl alcohol 0.95%, hexyl acetate 1.14%, hexyl formate 0.41%, vanillic aldehyde 0.47%, natural cognac 0.97%, n-hexyl alcohol 0.57%, caproic acid 0.76%, 2,5-dimethyl-3 (2H)-furanone 0.36%, γ-hexalactone 0.61%, hexyl hexanoate 1.48%, propane diols 0.45%, apple essential oil 7.95%, water 82.28%), (Guangdong is along food seasoning Co., Ltd production greatly for commercially available peach flavor, model: DJ012C specification: 25kg/ bucket, formula: gamma-valerolactone 0.27%, γ-hexalactone 0.15%, γ-octalactone 0.05%, γ-decalactone (98%in ethanol) 1.85%, delta-undeca lactone 0.64%, δ-decalactone 0.14%, ethyl maltol 0.06%, ethyl myristate 0.15%, ethyl laurate 0.11%, hexyl acetate 0.06%, 2-hexen-1-ol 0.18%, caproic acid 0.12%, glacial acetic acid 0.05%, linalool 0.13%, ethyl acetate 1.22%, 8-sulfydryl menthones (1%in ethanol) 0.06%, hexyl-benzoate 0.03%, acetaldehyde (40%in ethanol) 0.29%, ethyl isovalerate 0.12%, benzaldehyde 0.10%, ethanol 70%. water 24.22%), (Guangdong is along food seasoning Co., Ltd production greatly for commercially available flavoring banana essence, model: W1205316, specification 5kg*4/ case, formula: isobutyric acid Fructus Hordei Germinatus phenolic ester 0.03%, isoamyl alcohol 0.03%, glacial acetic acid 0.09%, butyric acid 0.07%, isoamyl acetate 4.61%, ethyl acetate 0.45%, isobutyl acetate 0.02%, iso-amyl iso-valeriate 3.30%, methyl octine carbonate 0.02%, acetaldehyde (40%in ethanol) 0.15%, 2-hexen-1-ol 0.02%, geranium oil (10%in ethanol) 0.06%, clove bud oil 0.24%, ethanol 60.91%, water 30%), (Guangdong is along food seasoning Co., Ltd production greatly for commercially available flavoring pineapple essence, model: OC229G, specification: 20kg/ bucket, formula: ethyl maltol 0.05%, ethyl butyrate 0.004%, ethyl acetoacetate 0.62%, diethyl malonate 19.074%, allyl hexanoate 0.15%, ethanol 0.045%, orange oil 0.022%, leaf-alcohol 0.002%, water 0.033%, propane diols 80%), (Guangdong is along food seasoning Co., Ltd production greatly for commercially available grape essence, model: HEN050, specification 20kg/ bucket, formula: glacial acetic acid 1%, 3-hydroxy-2-butanone 0.15%, hexadecanoyl 0.01%, iso-amyl iso-valeriate 0.05%, phenmethylol 0.5%, cinnamyl propionate 0.2%, ethyl o-aminobenzoate 0.25%, methyl anthranilate 1.65%, ethyl propionate 0.17%, furfural 0.03%, methyl β-naphthalenone 0.1%, β-damascone 0.05%, ethyl acetate 0.86%, ethyl maltol 0.71%, ethyl butyrate 1.15%, ethyl isovalerate 0.47%, geraniol 0.1%, 2 mercaptopropionic acid 0.1%, raspberry ketone 0.7%, methyl benzoate 0.1%, propane diols 0.84%, benzyl isovalerate 0.2%, cinnamyl alcohol 0.6%, indoles (1%in phenmethylol) 0.01%, propane diols 90%), add embodiment 1 essence, after dilute with water, carry out smell and mouthfeel is judged with the fruit juice of corresponding fruit, application products configuration proportion is as follows:
First group: blank sample A: flavoring apple essence 15mL+ water 985mL;
Sample B: flavoring apple essence 10mL+ embodiment 1 essence 5mL+ water 985mL;
Sample C: flavoring apple essence 5mL+ embodiment 1 essence 10mL+ water 985mL;
Second group: blank sample D: peach flavor 15mL+ water 985mL;
Sample E: peach flavor 10mL+ embodiment 1 essence 5mL+ water 985mL;
Sample F: peach flavor 5mL+ embodiment 1 essence 10mL+ water 985mL;
The 3rd group: blank sample G: flavoring banana essence 15mL+ water 985mL;
Sample H: flavoring banana essence 10mL+ embodiment 1 essence 5mL+ water 985mL;
Sample I: flavoring banana essence 5mL+ embodiment 1 essence 10mL+ water 985mL;
The 4th group: blank sample J: flavoring pineapple essence 15mL+ water 985mL;
Sample K: flavoring pineapple essence 10mL+ embodiment 1 essence 5mL+ water 985mL;
Sample L: flavoring pineapple essence 5mL+ embodiment 1 essence 10mL+ water 985mL;
The 5th group: blank sample N: grape essence 15mL+ water 985mL;
Sample M: grape essence 10mL+ embodiment 1 essence 5mL+ water 985mL;
Sample O: grape essence 5mL+ embodiment 1 essence 10mL+ water 985mL.
Totally 7 people of sensory evaluation group is judged above sample. Judge principle: sample is contrasted with corresponding fruit juice respectively, the sweet ripe fruital feature degree of approximation is by 0-5 points of 6 ranks, score is higher, the sweet ripe fruital that more approaches natural fruit is described, 0 point of explanation has obvious difference compared with fruit juice, reaches 5 points of explanations and fruit juice contrast indistinguishable.
It is as follows that smell is judged result:
It is as follows that mouthfeel is judged result:
Can find out and in commercially available fruit essence, add essence of the present invention, can obviously promote the fragrance odor type of original fruit essence, harmonious, nature, has given ripe fragrant and sweet gas fruit high-quality, deeply ace-high, full, fruital breath.
Embodiment 2
Get 7.5 grams of iso-amyl iso-valeriates, 15.5 grams of isoamyl acetates, 17.3 grams, ethyl acetate, 15.5 grams of butyl acetates, 1.6 grams of orange oils, 0.95 gram of lemon oil, 14.3 grams of isoamyl butyrates, 26.15 grams of ethyl butyrates, 0.6 gram of cinnamic acid methyl esters, 0.6 gram of citral, adopts automatic charging equipment, successively monomer is dropped into agitator, under normal temperature sealing, use screw mixing 3 hours, rotating speed is 30 turn/min, cold chamber is placed slaking in 5-10 days, obtains having the essence of the fragrant and sweet taste of mature fruit.
Adopt the method for embodiment 1 to judge, judge result close with embodiment 2, can obviously promote the fragrance odor type of original fruit essence, given ripe fragrant and sweet gas fruit high-quality, full.
Claims (5)
1. one kind has the perfume base of the fragrant and sweet taste of mature fruit, it is characterized in that, contain by weight percentage iso-amyl iso-valeriate 2-10%, isoamyl acetate 10-20%, ethyl acetate 15-20%, butyl acetate 10-20%, orange oil 1-2%, lemon oil 0.8-1.5%, isoamyl butyrate 10-20%, ethyl butyrate 20-30%.
2. there is according to claim 1 the perfume base of the fragrant and sweet taste of mature fruit, it is characterized in that, contain by weight iso-amyl iso-valeriate 6-8%, isoamyl acetate 13-18%, ethyl acetate 15-20%, butyl acetate 12-18%, orange oil 1-2%, lemon oil 0.8-1.2%, isoamyl butyrate 12-16%, ethyl butyrate 24-28%.
3. according to the perfume base described in claim 1 or 2 with the fragrant and sweet taste of mature fruit, it is characterized in that, also contain by weight percentage 0.3-1.0% cinnamic acid methyl esters, at least one in 0.3-1.0% citral.
4. there is according to claim 2 the perfume base of the fragrant and sweet taste of mature fruit, it is characterized in that, by weight by iso-amyl iso-valeriate 7.5%, isoamyl acetate 15.5%, ethyl acetate 18.3%, butyl acetate 15.5%, orange oil 1.6%, lemon oil 0.95%, isoamyl butyrate 14.5%, ethyl butyrate 26.15% forms.
5. there is according to claim 3 the perfume base of the fragrant and sweet taste of mature fruit, it is characterized in that, by weight by iso-amyl iso-valeriate 7.5%, isoamyl acetate 15.5%, ethyl acetate 17.3%, butyl acetate 15.5%, orange oil 1.6%, lemon oil 0.95%, isoamyl butyrate 14.3%, ethyl butyrate 26.15%, cinnamic acid methyl esters 0.6%, citral 0.6% forms.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610189655.7A CN105602725A (en) | 2016-03-30 | 2016-03-30 | Base with ripe fruit sweetness and aroma |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610189655.7A CN105602725A (en) | 2016-03-30 | 2016-03-30 | Base with ripe fruit sweetness and aroma |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105602725A true CN105602725A (en) | 2016-05-25 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610189655.7A Pending CN105602725A (en) | 2016-03-30 | 2016-03-30 | Base with ripe fruit sweetness and aroma |
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| Country | Link |
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| CN (1) | CN105602725A (en) |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106367204A (en) * | 2016-08-31 | 2017-02-01 | 恒枫食品科技有限公司 | Osmanthus flower essence containing natural osmanthus flower fragrance and preparation method thereof |
| CN106497677A (en) * | 2016-10-17 | 2017-03-15 | 上海应用技术大学 | A kind of edible children's toothpaste essence and preparation method thereof |
| CN107460039A (en) * | 2016-06-04 | 2017-12-12 | 沈秀珍 | A kind of orange flavor preparation method |
| CN107603739A (en) * | 2017-10-24 | 2018-01-19 | 湖北中烟工业有限责任公司 | It is a kind of to be used for cigarette blue or green lemon essence of mouth rod and its preparation method and application |
| CN108576752A (en) * | 2018-05-10 | 2018-09-28 | 上海应用技术大学 | A kind of allotment type almond benevolence essence and preparation method thereof |
| CN108634282A (en) * | 2018-02-28 | 2018-10-12 | 浙江安赛生物科技股份有限公司 | Loquat essence and preparation method thereof |
| CN109181868A (en) * | 2018-09-20 | 2019-01-11 | 双凯食品配料（昆山）有限公司 | A kind of "Hami" melon taste composition |
| CN109430807A (en) * | 2018-12-15 | 2019-03-08 | 陆智 | A kind of blackcurrant essence and its preparation method and application |
| CN109452684A (en) * | 2019-01-03 | 2019-03-12 | 四川中烟工业有限责任公司 | A kind of electronic cigarette liquid and preparation method thereof with pineapple flavor fragrance |
| CN109588685A (en) * | 2018-12-26 | 2019-04-09 | 沈昌亮 | A kind of sweetness perfume base group and preparation method thereof |
| CN109674017A (en) * | 2018-12-07 | 2019-04-26 | 沈昌亮 | A kind of flavoring apple essence group and preparation method thereof |
| CN111184256A (en) * | 2020-03-20 | 2020-05-22 | 云南中烟工业有限责任公司 | Sugar candy orange essence bead for cigarettes and preparation method thereof |
| CN111449283A (en) * | 2020-03-27 | 2020-07-28 | 河南中烟工业有限责任公司 | Replaceable filter stick with fruit sweet fragrance and application |
| CN113355157A (en) * | 2021-04-30 | 2021-09-07 | 深圳烟草工业有限责任公司 | Tobacco essence capable of increasing fragrance of cigarette jam |
| CN113424945A (en) * | 2021-07-05 | 2021-09-24 | 上海应用技术大学 | Banana essence applied to sugar reduction and sweetening and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103451018A (en) * | 2013-08-22 | 2013-12-18 | 广州市凯虹香精香料有限公司 | Special mix-fruit essence for composite chewing gum |
-
2016
- 2016-03-30 CN CN201610189655.7A patent/CN105602725A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103451018A (en) * | 2013-08-22 | 2013-12-18 | 广州市凯虹香精香料有限公司 | Special mix-fruit essence for composite chewing gum |
Non-Patent Citations (1)
| Title |
|---|
| 刘钟栋等: "《食品添加剂》", 31 August 2006, 东南大学出版社 * |
Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107460039A (en) * | 2016-06-04 | 2017-12-12 | 沈秀珍 | A kind of orange flavor preparation method |
| CN106367204A (en) * | 2016-08-31 | 2017-02-01 | 恒枫食品科技有限公司 | Osmanthus flower essence containing natural osmanthus flower fragrance and preparation method thereof |
| CN106497677A (en) * | 2016-10-17 | 2017-03-15 | 上海应用技术大学 | A kind of edible children's toothpaste essence and preparation method thereof |
| CN107603739A (en) * | 2017-10-24 | 2018-01-19 | 湖北中烟工业有限责任公司 | It is a kind of to be used for cigarette blue or green lemon essence of mouth rod and its preparation method and application |
| CN108634282B (en) * | 2018-02-28 | 2021-09-21 | 杭州安赛生物科技有限公司 | Loquat essence and preparation method thereof |
| CN108634282A (en) * | 2018-02-28 | 2018-10-12 | 浙江安赛生物科技股份有限公司 | Loquat essence and preparation method thereof |
| CN108576752A (en) * | 2018-05-10 | 2018-09-28 | 上海应用技术大学 | A kind of allotment type almond benevolence essence and preparation method thereof |
| CN109181868A (en) * | 2018-09-20 | 2019-01-11 | 双凯食品配料（昆山）有限公司 | A kind of "Hami" melon taste composition |
| CN109674017A (en) * | 2018-12-07 | 2019-04-26 | 沈昌亮 | A kind of flavoring apple essence group and preparation method thereof |
| CN109430807A (en) * | 2018-12-15 | 2019-03-08 | 陆智 | A kind of blackcurrant essence and its preparation method and application |
| CN109588685A (en) * | 2018-12-26 | 2019-04-09 | 沈昌亮 | A kind of sweetness perfume base group and preparation method thereof |
| CN109452684A (en) * | 2019-01-03 | 2019-03-12 | 四川中烟工业有限责任公司 | A kind of electronic cigarette liquid and preparation method thereof with pineapple flavor fragrance |
| CN111184256A (en) * | 2020-03-20 | 2020-05-22 | 云南中烟工业有限责任公司 | Sugar candy orange essence bead for cigarettes and preparation method thereof |
| CN111449283A (en) * | 2020-03-27 | 2020-07-28 | 河南中烟工业有限责任公司 | Replaceable filter stick with fruit sweet fragrance and application |
| CN113355157A (en) * | 2021-04-30 | 2021-09-07 | 深圳烟草工业有限责任公司 | Tobacco essence capable of increasing fragrance of cigarette jam |
| CN113424945A (en) * | 2021-07-05 | 2021-09-24 | 上海应用技术大学 | Banana essence applied to sugar reduction and sweetening and preparation method thereof |
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Effective date of registration: 20170116 Address after: Kwun Tong Zhen an industrial zone, Guangdong province Chaozhou city Xiangqiao District 515633 Applicant after: GUANGDONG SHUNDA FOOD FLAVORING CO., LTD. Applicant after: CHAOZHOU SHUNGUAN BIOLOGICAL TECHNOLOGY CO., LTD. Address before: Kwun Tong Zhen an industrial zone, Guangdong province Chaozhou city Xiangqiao District 515633 Applicant before: GUANGDONG SHUNDA FOOD FLAVORING CO., LTD. |
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Application publication date: 20160525 |