CN105596276A - Natural extract based whitening skincare facial mask and preparation method thereof - Google Patents
Natural extract based whitening skincare facial mask and preparation method thereof Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61Q19/00—Preparations for care of the skin
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Abstract
The invention provides a natural extract based whitening skincare facial mask which comprises, by weight, 0.4-0.6 part of superoxide dismutase, 1-3 parts of anthocyanin, 0.2-0.25 part of Fructus Schisandrae Chinensis, 0.30-0.35 part of lumbricus peptide, 0.3-0.4 part of catalase, 1-3 parts of astaxanthin, 3-5 parts of resveratrol oligomers, 6-7 parts of formononetin, 15-18 parts of emulsifier, 10-15 parts of Xanthan gum and 5-10 parts of powder of Tremella fuciformis Berk. The invention further provides a preparation method of the natural extract based whitening skincare facial mask.
Description
Technical field
The present invention relates to cosmetic skincare product preparing technical field, especially a kind of based on natural extractWhitening and skin-protecting facial mask and preparation method thereof.
Background technology
Along with social development and the raising of living standards of the people, consumer to the requirement of daily nursing product alsoMore and more higher, effect of product is required to also more and more refinement. Since yellow's colour of skin problem, ChineseThe problems such as obscure, the dim Huang of the ubiquity colour of skin, shortage gloss, easy allergy, pigment deposition. Expert dataShow, pigmentation phenomenon accounts for about 80% ratio in women, and another data shows Chinese Human-FemaleProperty 80% is all Combination skin, and the colour of skin is irregular is the greatest problem that this class skin faces, how whitening,Also be one of topic of being concerned about most of Chinese Consumer's.
But existing whitening product or most of formulated by chemicals, to user's facial skinStimulate larger. In whitening product, adopt various natural plants (being mainly the plant that is similar to fruits and vegetables)Proportioning forms.
Such as the Chinese patent literature that publication number is CN104825655A, a kind of nti-freckle, U.S. are disclosedIn vain, moulding composition, include following component: rosebud powder 100-150 part, donkey-hide gelatin powder 105-155Part, matrimony vine 200-300 part, dried rhizome of rehmannia 70-130 part, linseed 100-150 part, soybean 20-41 part,Icing Sugar 80-120, oligomeric maltose 3-75 part, natrium citricum 8-12 part, dolomol 8-12 part,Dextrin 100-124 part. People are very difficult knows that by said ratio which composition produces effect to whitening, whichComposition is inoperative to whitening.
The Chinese patent literature that publication number is CN104825379A for another example, discloses a kind of minimizing blackThe shining skin late frost of whitening of pigment deposition, the weight proportion of each bulk drug is as follows, is weight portion: tomato redElement 20-30, cow-bezoar 5-15, aloe 5-15, sea-tangle 6-16, cucumber 10-20, chamomile 15-25Green-tea extract 6-10, Caulis et Folium Lactucae sativae extract 8-20, vitamin e1 0-15, glycerine 2-6, astaxanthin 5-9.This patent also exists above-mentioned same defect. The cow-bezoar even mentioned in this patent documentation description,Effect of sea-tangle does not just at all contact with whitening effect at all.
Although the cleawhite pack that therefore in prior art, employing natural plants proportioning forms is with respect to chemicalsFormulated cleawhite pack safety, but due to the composition in various fruits and vegetables, whitening being played a role notBright, and interaction mechanism between various composition unclear, therefore utilize various fruits and vegetables proportionings andThe whitening effect of the cleawhite pack becoming is with respect to poor by the formulated cleawhite pack of chemicals.
Summary of the invention
In view of this, the invention provides one both harmless, and cosmetic result good based on naturalWhitening and skin-protecting facial mask of extract and preparation method thereof.
A whitening and skin-protecting facial mask based on natural extract, it comprises following component, below component beWeight ratio:
Superoxide dismutase 0.4-0.6 part, anthocyanidin 1-3 part, fruit of Chinese magnoliavine 0.2-0.25 part, earthwormPeptide 0.30-0.35 part, catalase 0.3-0.4 part, astaxanthin 1-3 part, resveratrol oligomer class3-5 part, formoononetin 6-7 part, emulsifying agent 15-18 part, xanthans 10-15 part, white fungus powder 5-10Part.
In the whitening and skin-protecting facial mask based on natural extract of the present invention, it also comprises following groupPoint, below component be weight ratio:
Trans dioxy morin 2.5-2.6 part, motherwort powder 4-8 part, linoleic acid 1.3-1.7 part.
In the whitening and skin-protecting facial mask based on natural extract of the present invention,
Described emulsifying agent is the mixture of the hard ester alcohol of spermaceti, stearic acid, inulin lauryl carbamate;The ratio of the hard ester alcohol of described spermaceti, stearic acid, inulin lauryl carbamate is 2:2:3.
The present invention also provides a kind of preparation method of the whitening and skin-protecting facial mask based on based on natural extract, itsComprise the steps: that the umber that following steps occur is weight ratio,
The blueberry of S1, the purple grape of getting 50-80 part, 50-100 part, the mulberries of 40-60 part, be placed inIn container, and the water that adds 100-160 part, undertaken forming for stirring to pulp 30-60 minute by mixerPulp mixed liquor, is controlled at 4-6 DEG C by temperature, and rotating speed is 400-450 rev/min;
S2, the pulp mixed liquor of purple grape, blueberry and mulberries is carried out to traditional vacuum processing obtain slurries;In slurries, add 3-4 part cellulase to carry out enzymolysis, the temperature of enzymolysis is at 22-25 DEG C, slurries enzymolysis5-10 days, extremely residual monose is less than 3%, separates tank switching and obtains zymotic fluid;
S3, by zymotic fluid leave standstill 4-7 hour, temperature is controlled at 4-6 DEG C; Get the zymotic fluid after leaving standstillSupernatant liquor; Supernatant liquor is transferred to container for evaporation and carry out heating evaporation, by the air pressure in container for evaporationBe controlled at 1800 to 2600 handkerchiefs, until water content drops in the supernatant liquor in container for evaporation10-15% forms the first paste;
S4, the first paste is taken out to put into storage vessel for subsequent use, the temperature control by storage in vesselAt 12-18 DEG C, the airborne oxygen content amount of storage vessel is controlled at 2% to 3%;
S5, get the patter of rain haematococcus of 30-60 part, and by the patter of rain haematococcus shady and cool ventilation at 28-26 DEG C3-5 days is placed at place, gets the reticulate millettia of 40-50 part, and haematococcus pluvialis and reticulate millettia mixed grinding are formedParticle diameter is the mixed-powder of 0.05-0.1mm; To in mixed-powder, add the water-soluble solution of 80-100 part,And filter and obtain the red ball of the patter of rain with the filter membrane that aperture is 0.30-0.35um after traditional vacuum is processedThe hybrid filtering liquid of algae and reticulate millettia;
S6, the pH value of the hybrid filtering liquid of patter of rain haematococcus and reticulate millettia is adjusted to 7.15-7.25After again filter and obtained cleaner liquid with the filter membrane that aperture is 0.30-0.35um, pass through container for evaporationCarry out heating evaporation to crossing cleaner liquid, the air pressure in container for evaporation be controlled to 1000 to 1400 handkerchiefs,Until the water content of crossing in cleaner liquid in container for evaporation drops to 20-35% and forms the second paste;
S7, get 30-35 part LUMBRICUS and 2-3 part fruit of Chinese magnoliavine is ground, form particle diameter and beThe mixed powder powder of 0.05-0.1mm; To in mixed powder powder, add the ether dissolution of 30-50 part,Remove undissolved impurity and obtain, and ether evaporation is obtained to the solid matter after evaporation;
The first paste of S8, mixed merga pass agitator whipping step S3, the second cream of step S6Solid matter in xanthans, 5-10 part white fungus powder and the step S7 of shape thing, 10-15 part, and addEnter emulsifying agent 15-18 part, stir and within 2-4 hour, form whitening and skin-protecting facial mask composition finished product, the speed of stirringFor 700-800 rev/min, the temperature in agitator is controlled to 12-18 DEG C; And stir after by U.S.The whitening and skin-protecting facial mask finished product that it is 0.3-1.2mm that white facial treatment mask composition finished product flattens as thickness.
In the preparation method of the whitening and skin-protecting facial mask based on based on natural extract of the present invention,After step S8, also comprise:
S9, whitening and skin-protecting facial mask finished product is positioned in airtight container, the condition in airtight container is as follows:Airborne oxygen content amount is controlled at 2% to 3%, and passes into helium and remain on a standard atmospheric pressure,Atmospheric pressure error is in positive and negative 5 percent, and relative air humidity is at 40%-45%, and temperature scope is12-18℃；
S10, by ultraviolet ray to airtight container sterilizing 60-120 minute, the intensity of ultraviolet disinfection isEvery square centimeter of 100-110 microwatt.
In the preparation method of the whitening and skin-protecting facial mask based on based on natural extract of the present invention,
While stirring, also add trans dioxy morin 2.5-2.6 part, motherwort powder in described step S84-8 part, linoleic acid 1.3-1.7 part.
The present invention is directed to cleawhite pack that available technology adopting natural plants proportioning forms with respect to chemistryThe cleawhite pack safety that product are formulated, but due to the composition in various fruits and vegetables, whitening being played a role notBright, and interaction mechanism between various composition unclear, therefore utilize various fruits and vegetables proportionings andThe whitening effect of the cleawhite pack becoming is with respect to passing through poor the lacking of the formulated cleawhite pack of chemicalsFall into, extract composition useful to whitening in various natural materials, and measure by experiment each group of whitening and haveThe ratio of the composition of benefit.
Brief description of the drawings
Fig. 1 is the preparation method's of the whitening and skin-protecting facial mask based on based on natural extract flow chart.
Detailed description of the invention
By various embodiments of the invention, principle of the present invention is made an explanation below.
Embodiment 1, a kind of whitening and skin-protecting facial mask based on natural extract, it comprises following component, withLower component is weight ratio:
0.4 part of superoxide dismutase, 1 part of anthocyanidin, 0.2 part, the fruit of Chinese magnoliavine, 0.30 part of earthworm peptide,0.3 part of catalase, 1 part of astaxanthin, 3 parts of resveratrol oligomer classes, 6 parts of formoononetins,15 parts of emulsifying agents, 10 parts of xanthans, 5 parts, white fungus powder. Wherein superoxide dismutase, anthocyanidin,The fruit of Chinese magnoliavine, earthworm peptide, catalase, astaxanthin, resveratrol oligomer class all can play eliminationThe effect of free radical, these compositions all can be taken from natural plants or algae etc. Such as superoxides discriminationChange enzyme, catalase can be taken from purple grape, and anthocyanidin can be taken from blueberry, and earthworm peptide can be taken fromEarthworm is dry, and astaxanthin can be taken from patter of rain haematococcus, and resveratrol oligomer class can be taken from mulberries, awnsBright florigen can be taken from reticulate millettia. Emulsifying agent is preferably the emulsifying agent of hydrophilic portion. Because mentioned component is all gotFrom in natural animals and plants or algae etc., therefore few to the stimulation of human body face.
It should be noted that in embodiments of the present invention, earthworm peptide has obvious resisting age of skin effect,Can be applied to cosmetics for resisting age of skin and health products. But earthworm peptide itself has necessarily human body skinExcitant effect, therefore earthworm peptide shared ratio in the whitening and skin-protecting facial mask based on natural extractCan not be too high, in all embodiment of the present invention, it is old that the accounting of earthworm peptide all can meet anti-skin simultaneouslyThe effect of changing, the unlikely stimulation that causes human body skin again.
The embodiment of the present invention is used for reference the theory of monarch drug in a prescription, ministerial drug, adjutant in tcm theory. In above-mentioned formula,Superoxide dismutase, catalase and calycosin are monarch drug in a prescription, whitening effect are played to main workWith composition. Wherein anthocyanidin, the fruit of Chinese magnoliavine, earthworm peptide, astaxanthin, resveratrol oligomer class are ministerMedicine, can strengthen the whitening effect of superoxide dismutase, catalase and calycosin. EmulsificationAgent, as adjutant, can guide monarch drug in a prescription and ministerial drug to be absorbed by human body face.
Xanthans, white fungus powder are as the carrier of whitening composition. Xanthans is soluble in hot water or cold water, solutionNeutrality, resistance and freeze and thawing, is insoluble to ethanol, meets aqueous dispersion, emulsification becomes stable hydrophily thicknessColloid; White fungus is rich in natural plant colloid, and has the effect of enriching yin, can long-term takingGood moisturizing food. Carrier using xanthans, white fungus powder as whitening composition, not only can be to human bodySkin has stimulation, can make whitening cost slowly-releasing be absorbed by the body, and is extraordinary whitening carrier.
Embodiment 2, a kind of whitening and skin-protecting facial mask based on natural extract, it comprises following component, withLower component is weight ratio:
0.6 part of superoxide dismutase, 3 parts of anthocyanidin, 0.25 part, the fruit of Chinese magnoliavine, 0.35 part of earthworm peptide,0.4 part of catalase, 3 parts of astaxanthins, 5 parts of resveratrol oligomer classes, 7 parts of formoononetins,18 parts of emulsifying agents, 15 parts of xanthans, 10 parts, white fungus powder.
Embodiment 3, a kind of whitening and skin-protecting facial mask based on natural extract, it comprises following component, withLower component is weight ratio:
0.5 part of superoxide dismutase, 2 parts of anthocyanidin, 0.23 part, the fruit of Chinese magnoliavine, 0.32 part of earthworm peptide,0.37 part of catalase, 2 parts of astaxanthins, 35 parts of resveratrol oligomer classes, formoononetin6.4 parts, 16 parts of emulsifying agents, 13 parts of xanthans, 7 parts, white fungus powder.
Embodiment 4, a kind of whitening and skin-protecting facial mask based on natural extract, it comprises following component, withLower component is weight ratio:
0.44 part of superoxide dismutase, 1.8 parts of anthocyanidin, 0.25 part, the fruit of Chinese magnoliavine, earthworm peptide 0.31Part, 0.3 part of catalase, 1 part of astaxanthin, 3 parts of resveratrol oligomer classes, formoononetin6.7 parts, 16.8 parts of emulsifying agents, 12 parts of xanthans, 6 parts, white fungus powder.
Embodiment 5, a kind of whitening and skin-protecting facial mask based on natural extract, it comprises following component, withLower component is weight ratio:
0.44 part of superoxide dismutase, 1.8 parts of anthocyanidin, 0.25 part, the fruit of Chinese magnoliavine, earthworm peptide 0.31Part, 0.3 part of catalase, 1 part of astaxanthin, 3 parts of resveratrol oligomer classes, formoononetin6.7 parts, 16.8 parts of emulsifying agents, 14 parts of xanthans, 8 parts, white fungus powder, trans dioxy morin 2.5Part, 4 parts of motherwort powders, 1.3 parts of linoleic acid. Wherein trans dioxy morin can take from fustic,Osage apple. Wherein motherwort powder can play effect promoting blood circulation and removing blood stasis, and linoleic acid can play softening blood vesselEffect, trans dioxy morin can check melanin generative process in the activity of tyrosinase, simultaneouslyCan not damage the eubolism process of melanocyte. And by adding motherwort powder and sub-oilAcid, can expand human body face capillary, promotes the absorption of each active ingredient in the embodiment of the present invention.Trans dioxy morin, motherwort powder, linoleic acid be simultaneously as adjutant, can promote monarch drug in a prescription and ministerial drugAbsorb.
Embodiment 6, a kind of whitening and skin-protecting facial mask based on natural extract, it comprises following component, withLower component is weight ratio:
0.44 part of superoxide dismutase, 1.8 parts of anthocyanidin, 0.25 part, the fruit of Chinese magnoliavine, earthworm peptide 0.31Part, 0.3 part of catalase, 1 part of astaxanthin, 3 parts of resveratrol oligomer classes, formoononetin6.7 parts, 16.8 parts of emulsifying agents, 11 parts of xanthans, 6 parts, white fungus powder, trans dioxy morin 2.5Part, 4 parts of motherwort powders, 1.3 parts of linoleic acid.
Embodiment 7, a kind of whitening and skin-protecting facial mask based on natural extract, it comprises following component, withLower component is weight ratio:
0.44 part of superoxide dismutase, 1.8 parts of anthocyanidin, 0.25 part, the fruit of Chinese magnoliavine, earthworm peptide 0.31Part, 0.3 part of catalase, 1 part of astaxanthin, 3 parts of resveratrol oligomer classes, formoononetin6.7 parts, 16.8 parts of emulsifying agents, 15 parts of xanthans, 9 parts, white fungus powder, trans dioxy morin 2.6Part, 8 parts of motherwort powders, 1.7 parts of linoleic acid.
Alternatively, in the above each embodiment,
Described emulsifying agent is the mixture of the hard ester alcohol of spermaceti, stearic acid, inulin lauryl carbamate;The ratio of the hard ester alcohol of described spermaceti, stearic acid, inulin lauryl carbamate is 2:2:3.
Experimentation and result are as follows: by tested object same arm in upper divide 7 tested districtsTerritory, what region area was 1.5*1.5cm is square, and between each region, interval is at least 2cm. Successively will be realThe whitening and skin-protecting facial mask based on natural extract of executing example 1 to 7 record is applied to the first to the 7th region.Smear continuously 30 days, the applying amount of each various whitening and skin-protecting facial masks is identical. The hand at place, tested regionArm is not subject to direct sunlight. After smearing for the first time, add up the skin brightness in each tested region 45 days timeValue and do not smear the skin brightness value in the region of whitening and skin-protecting facial mask. The statistical method of skin brightness value asUnder, the skin brightness value before smearing is made as to 1, will smear the latter 45 days skins value in bright region the most in vainBe set to 10. Then according to the principle of gradual change, skin brightness is divided into 10 grades.
Through statistics, using the skin brightness grade of whitening facial treatment mask in embodiment 1 is 4, uses realThe skin brightness of executing whitening facial treatment mask in example 2 is 4, uses the skin of whitening facial treatment mask in embodiment 3Skin brightness degree is 6. Can find out, embodiment 3 is the preferred embodiment in above embodiment. UseIn embodiment 4, the skin brightness grade of whitening facial treatment mask is 5. Use whitening and skin-protecting face in embodiment 5The skin brightness grade of film is 8, can find out, has added trans dioxy morin, motherwort powder, AsiaOleic acid, simultaneously as adjutant, can promote the absorption of monarch drug in a prescription and ministerial drug, makes whitening effect better. UseIn embodiment 6 the skin brightness grade of whitening facial treatment mask be 10, used whitening in embodiment 7The skin brightness grade of facial treatment mask is 10. Can find out, although trans dioxy morin, motherwortPowder, linoleic value difference do not affect skin brightness grade, but with respect to embodiment 1 to 5,Improve to a great extent skin brightness grade.
As shown in Figure 1, the embodiment of the present invention also provides a kind of whitening and skin-protecting based on based on natural extractThe preparation method of facial mask, its umber that comprises the steps: that following steps occur is weight ratio,
The blueberry of S1, the purple grape of getting 50-80 part, 50-100 part, the mulberries of 40-60 part, be placed inIn container, and the water that adds 100-160 part, undertaken forming for stirring to pulp 30-60 minute by mixerPulp mixed liquor, is controlled at 4-6 DEG C by temperature, and rotating speed is 400-450 rev/min. Temperature is controlled at4-6 DEG C, can farthest preserve the delicate flavour of purple grape, blueberry, mulberries. Meanwhile, willThe time of making beating is controlled at 30-60 minute, and rotating speed is controlled at 400-450 rev/min, and the one, energyEnough realization fully ground, and the 2nd, the heat of having avoided too high rotating speed to bring destroys each in above-mentioned fruitPlant the activity of nutritional labeling. Rotating speed is controlled to 400-450 rev/min, can takes into account admirably grindingEffect and avoid heating. In purple grape, be rich in superoxide dismutase, blueberry is rich in anthocyanidin, and mulberryIn Shen, resveratrol oligomer class is higher compared to other fruit.
S2, the pulp mixed liquor of purple grape, blueberry and mulberries is carried out to traditional vacuum processing obtain slurries;In slurries, add 3-4 part cellulase to carry out enzymolysis, the temperature of enzymolysis is at 22-25 DEG C, slurries enzymolysisAfter fermentation 5-10 days, extremely residual monose is less than 3%, separates tank switching and obtains zymotic fluid. By to purple grape,The pulp mixed liquor of blueberry and mulberries carries out traditional vacuum processing, can more fill purple grape and blueberryThe mixing dividing. By cellulase, the polysaccharide in slurries can be converted into monose, simultaneously by fermentation,Monose in the zymotic fluid that is can be less than 3% (weight ratio), concrete, can pass through gas-chromatographyDetermination method is measured the contents of monosaccharides in zymotic fluid. Reduce the interference of sugar to whitening composition.
S3, by zymotic fluid leave standstill 4-7 hour, temperature is controlled at 4-6 DEG C; Get the zymotic fluid after leaving standstillSupernatant liquor; Supernatant liquor is transferred to container for evaporation and carry out heating evaporation, by the air pressure in container for evaporationBe controlled at 1800 to 2600 handkerchiefs, until water content drops in the supernatant liquor in container for evaporation10-15% forms the first paste. Temperature is controlled to 4-6 DEG C, the oxidation of the zymotic fluid that can slow down, andAnd the air pressure in container for evaporation is controlled to 1800 to 2600 handkerchiefs, can makes at the bar less than 10 DEG CUnder part, zymotic fluid evaporates rapidly. The standard of supernatant liquor is the impurity that is invisible to the naked eye.
S4, the first paste is taken out to put into storage vessel for subsequent use, the temperature control by storage in vesselAt 12-18 DEG C, the airborne oxygen content amount of storage vessel is controlled at 2% to 3%. This step can be very bigThe oxidation that delays the first paste.
S5, get the patter of rain haematococcus of 30-60 part, and by the patter of rain haematococcus shady and cool ventilation at 28-26 DEG C3-5 days is placed at place, gets the reticulate millettia of 40-50 part, and haematococcus pluvialis and reticulate millettia mixed grinding are formedParticle diameter is the mixed-powder of 0.05-0.1mm; To in mixed-powder, add the water-soluble solution of 80-100 part,And filter and obtain the red ball of the patter of rain with the filter membrane that aperture is 0.30-0.35um after traditional vacuum is processedThe hybrid filtering liquid of algae and reticulate millettia. In patter of rain haematococcus, be rich in astaxanthin, astaxanthin is the strongest in the worldOne of natural, effectively the oxygen radical in scavenger-cell, strengthens cytothesis ability, maintainsThe accumulation of organism balance and minimizing senile cell, Cell protection and DNA health from inside to outside, thus protectProtect skin health, instead of be only the effect that plays whitening. In reticulate millettia, be rich in formoononetin, thornMethoxyl group isoflavones in onocerin can make DOPA in melanocyte be converted back into tyrosine, fromAnd the generation of check melanin.
S6, the pH value of the hybrid filtering liquid of patter of rain haematococcus and reticulate millettia is adjusted to 7.15-7.25After again filter and obtained cleaner liquid with the filter membrane that aperture is 0.30-0.35um, can filter out assortedMatter. Carry out heating evaporation by container for evaporation to crossing cleaner liquid, the air pressure in container for evaporation is controlled at1000 to 1400 handkerchiefs are crossed cleaner liquid and can under the condition less than 10 DEG C, be steamed rapidly under this air pressureSend out, avoid destroying the active ingredient of whitening, until the water content in cleaner liquid of crossing in container for evaporation drops to20-35% forms the second paste, has avoided too low the first paste and the second paste of causing of water contentBad mixing, is also unlikely to the too high low defect of finished product concentration causing of water content.
S7, get 30-35 part LUMBRICUS and 2-3 part fruit of Chinese magnoliavine is ground, form particle diameter and beThe mixed powder powder of 0.05-0.1mm; To in mixed powder powder, add the ether dissolution of 30-50 part,Remove undissolved impurity and obtain, and ether evaporation is obtained to the solid matter after evaporation. In LUMBRICUSEarthworm peptide can irritation cell substrates collagen secretion, but the easily skin to face of too high levelsStimulate, the LUMBRICUS of therefore selecting 30-35 part is most suitable. The boiling point of ether is only 34.6 DEG C,Therefore the middle whitening active ingredient of extracting LUMBRICUS and the fruit of Chinese magnoliavine by ether, can effectively not become whiteningDivide and damage.
The first paste of S8, mixed merga pass agitator whipping step S3, the second cream of step S6Solid matter in xanthans, 5-10 part white fungus powder and the step S7 of shape thing, 10-15 part, and addEnter emulsifying agent 15-18 part, stir and within 2-4 hour, form whitening and skin-protecting facial mask composition finished product, the speed of stirringFor 700-800 rev/min, the temperature in agitator is controlled to 12-18 DEG C; And stir after by U.S.The whitening and skin-protecting facial mask finished product that it is 0.3-1.2mm that white facial treatment mask composition finished product flattens as thickness. StirSpeed is 700-800 rev/min, and the temperature in agitator is controlled to 12-18 DEG C, can avoid stirringThe waste heat that causes of excessive velocities, whitening composition is produced and is destroyed.
In the preparation method of the whitening and skin-protecting facial mask based on based on natural extract of the present invention,After step S8, also comprise:
S9, whitening and skin-protecting facial mask finished product is positioned in airtight container, the condition in airtight container is as follows:Airborne oxygen content amount is controlled at 2% to 3%, and passes into helium and remain on a standard atmospheric pressure,Atmospheric pressure error is in positive and negative 5 percent, and relative air humidity is at 40%-45%, and temperature scope is12-18 DEG C. This step, by replacing oxygen with this inert gas of helium, can be avoided whitening and skin-protectingCost-effectively in facial mask is oxidized and lost efficacy.
S10, by ultraviolet ray to airtight container sterilizing 60-120 minute, the intensity of ultraviolet disinfection isEvery square centimeter of 100-110 microwatt. This step has been avoided growing of microorganism, and whitening cost-effectively is madeBecome to destroy. Preferably, can also separate bag to the finished product of whitening and skin-protecting facial mask by sealing inner wrappingDress, and extract the air in packaging.
In the preparation method of the whitening and skin-protecting facial mask based on based on natural extract of the present invention,
While stirring, also add trans dioxy morin 2.5-2.6 part, motherwort powder in described step S84-8 part, linoleic acid 1.3-1.7 part.
Be understandable that, for the person of ordinary skill of the art, can be according to skill of the present inventionOther various corresponding changes and distortion is made in art design, and all these change and distortion all should belong to thisThe protection domain of invention claim.
Claims (6)
1. the whitening and skin-protecting facial mask based on natural extract, is characterized in that, it comprises following groupPoint, below component be weight ratio:
Superoxide dismutase 0.4-0.6 part, anthocyanidin 1-3 part, fruit of Chinese magnoliavine 0.2-0.25 part, earthwormPeptide 0.30-0.35 part, catalase 0.3-0.4 part, astaxanthin 1-3 part, resveratrol oligomer class3-5 part, formoononetin 6-7 part, emulsifying agent 15-18 part, xanthans 10-15 part, white fungus powder 5-10Part.
2. the whitening and skin-protecting facial mask based on natural extract as claimed in claim 1, is characterized in that,It also comprises following component, below component be weight ratio:
Trans dioxy morin 2.5-2.6 part, motherwort powder 4-8 part, linoleic acid 1.3-1.7 part.
3. the whitening and skin-protecting facial mask based on natural extract as claimed in claim 1 or 2, its featureBe,
Described emulsifying agent is the mixture of the hard ester alcohol of spermaceti, stearic acid, inulin lauryl carbamate;The ratio of the hard ester alcohol of described spermaceti, stearic acid, inulin lauryl carbamate is 2:2:3.
4. a preparation method for the whitening and skin-protecting facial mask based on based on natural extract, is characterized in that,Its umber that comprises the steps: that following steps occur is weight ratio,
The blueberry of S1, the purple grape of getting 50-80 part, 50-100 part, the mulberries of 40-60 part, be placed inIn container, and the water that adds 100-160 part, undertaken forming for stirring to pulp 30-60 minute by mixerPulp mixed liquor, is controlled at 4-6 DEG C by temperature, and rotating speed is 400-450 rev/min;
S2, the pulp mixed liquor of purple grape, blueberry and mulberries carried out to traditional vacuum processing obtain slurries,For again mixing pulp mixed liquor and remove the pulp slag of purple grape, blueberry and mulberries; In slurriesAdd 3-4 part cellulase to carry out enzymolysis, the temperature of enzymolysis is at 22-25 DEG C, slurries enzymolysis 5-10 days,Extremely residual monose is less than 3%, separates tank switching and obtains zymotic fluid;
S3, by zymotic fluid leave standstill 4-7 hour, temperature is controlled at 4-6 DEG C; Get the zymotic fluid after leaving standstillSupernatant liquor; Supernatant liquor is transferred to container for evaporation and carry out heating evaporation, by the air pressure in container for evaporationBe controlled at 1800 to 2600 handkerchiefs, until water content drops in the supernatant liquor in container for evaporation10-15% forms the first paste;
S4, the first paste is taken out to put into storage vessel for subsequent use, the temperature control by storage in vesselAt 12-18 DEG C, the airborne oxygen content amount of storage vessel is controlled at 2% to 3%;
S5, get the patter of rain haematococcus of 30-60 part, and by the patter of rain haematococcus shady and cool ventilation at 28-26 DEG C3-5 days is placed at place, gets the reticulate millettia of 40-50 part, and haematococcus pluvialis and reticulate millettia mixed grinding are formedParticle diameter is the mixed-powder of 0.05-0.1mm; To in mixed-powder, add the water-soluble solution of 80-100 part,And filter and obtain the red ball of the patter of rain with the filter membrane that aperture is 0.30-0.35um after traditional vacuum is processedThe hybrid filtering liquid of algae and reticulate millettia;
S6, the pH value of the hybrid filtering liquid of patter of rain haematococcus and reticulate millettia is adjusted to 7.15-7.25After again filter and obtained cleaner liquid with the filter membrane that aperture is 0.30-0.35um, pass through container for evaporationCarry out heating evaporation to crossing cleaner liquid, the air pressure in container for evaporation be controlled to 1000 to 1400 handkerchiefs,Until the water content of crossing in cleaner liquid in container for evaporation drops to 20-35% and forms the second paste;
S7, get 30-35 part LUMBRICUS and 2-3 part fruit of Chinese magnoliavine is ground, form particle diameter and beThe mixed powder powder of 0.05-0.1mm; To in mixed powder powder, add the ether dissolution of 30-50 part,Remove undissolved impurity and obtain, and ether evaporation is obtained to the solid matter after evaporation;
The first paste of S8, mixed merga pass agitator whipping step S3, the second cream of step S6Solid matter in xanthans, 5-10 part white fungus powder and the step S7 of shape thing, 10-15 part, and addEnter emulsifying agent 15-18 part, stir and within 2-4 hour, form whitening and skin-protecting facial mask composition finished product, the speed of stirringFor 700-800 rev/min, the temperature in agitator is controlled to 12-18 DEG C; And stir after by U.S.The whitening and skin-protecting facial mask finished product that it is 0.3-1.2mm that white facial treatment mask composition finished product flattens as thickness.
5. the preparation side of the whitening and skin-protecting facial mask based on based on natural extract as claimed in claim 4Method, is characterized in that, after step S8, also comprises:
S9, whitening and skin-protecting facial mask finished product is positioned in airtight container, the condition in airtight container is as follows:Airborne oxygen content amount is controlled at 2% to 3%, and passes into helium and remain on a standard atmospheric pressure,Atmospheric pressure error is in positive and negative 5 percent, and relative air humidity is at 40%-45%, and temperature scope is12-18℃；
S10, by ultraviolet ray to airtight container sterilizing 60-120 minute, the intensity of ultraviolet disinfection isEvery square centimeter of 100-110 microwatt.
6. the preparation side of the whitening and skin-protecting facial mask based on based on natural extract as claimed in claim 5Method, is characterized in that,
While stirring, also add trans dioxy morin 2.5-2.6 part, motherwort powder in described step S84-8 part, linoleic acid 1.3-1.7 part.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106619175A (en) * | 2016-11-10 | 2017-05-10 | 陕西慧康生物科技有限责任公司 | Genetic recombination superoxide dismutase mask |
| CN107028831A (en) * | 2017-04-27 | 2017-08-11 | 苏州唐基生物科技有限公司 | A kind of Chinese medicine beauty and skin care preparation and preparation method thereof |
| CN109419712A (en) * | 2017-09-03 | 2019-03-05 | 大德仟年生物技术有限公司 | A kind of preparation method containing fresh leonurus and haematococcus pluvialis facial mask |
| CN113509416A (en) * | 2021-07-13 | 2021-10-19 | 无限极（中国）有限公司 | Composition with function of enhancing catalase activity and application of composition in cosmetics |
| CN114652619A (en) * | 2022-05-09 | 2022-06-24 | 中国科学院烟台海岸带研究所 | Active oil-soluble anthocyanin and preparation method and application thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106619175A (en) * | 2016-11-10 | 2017-05-10 | 陕西慧康生物科技有限责任公司 | Genetic recombination superoxide dismutase mask |
| CN107028831A (en) * | 2017-04-27 | 2017-08-11 | 苏州唐基生物科技有限公司 | A kind of Chinese medicine beauty and skin care preparation and preparation method thereof |
| CN109419712A (en) * | 2017-09-03 | 2019-03-05 | 大德仟年生物技术有限公司 | A kind of preparation method containing fresh leonurus and haematococcus pluvialis facial mask |
| CN113509416A (en) * | 2021-07-13 | 2021-10-19 | 无限极（中国）有限公司 | Composition with function of enhancing catalase activity and application of composition in cosmetics |
| CN114652619A (en) * | 2022-05-09 | 2022-06-24 | 中国科学院烟台海岸带研究所 | Active oil-soluble anthocyanin and preparation method and application thereof |
| CN114652619B (en) * | 2022-05-09 | 2023-12-12 | 中国科学院烟台海岸带研究所 | Active oil-soluble anthocyanin as well as preparation method and application thereof |
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