CN105582384A - Foot bath powder containing folium artemisiae argyi residue and with cold dispelling and menstruation regulating functions and preparation method thereof - Google Patents
Foot bath powder containing folium artemisiae argyi residue and with cold dispelling and menstruation regulating functions and preparation method thereof Download PDFInfo
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Abstract
The invention relates to the technical field of healthcare products and particularly relates to foot bath powder containing folium artemisiae argyi residue and with cold dispelling and menstruation regulating functions and a preparation method thereof. The foot bath powder comprises the following raw materials in parts by weight: 50-80 parts of folium artemisiae argyi residue, 10-25 parts of towel gourd stem, 1-10 parts of hibiscus rosa-sinensis, 5-20 parts of herba lycopi, 5-20 parts of fresh aloe leaf, 5-20 parts of star anise, 10-25 parts of corn stigma, 0.5-6 parts of sodium sesquicarbonate and 2-10 parts of sodium chloride. The foot bath powder provided by the invention has the advantages of easily available raw materials, low cost, no skin irritation and remarkable cold dispelling and menstruation regulating functions and can be used for effectively preventing and treating the symptoms such as cold hands and feet, irregular menstruation and dysmenorrhea caused by female uterus cold.
Description
Technical field
The present invention relates to health product technology field, be specifically related to a kind of lavipeditum containing the tarragon dregs of a decoction with dispelling cold menstruation regulating effectPowder and preparation method thereof.
Background technology
On tcm clinical practice, " palace is cold " singly do not refer to a certain symptom, but traditional Chinese medicine is to the varied clinical condition of patientThe summary of shape, as the menstrual cycle is delayed, Hypomenorrhea and look black, has clot, and even amenorrhea is not all right; The moon is premenstrual or menstrual period are littleAbdomen pain; Clear and thin leucorrhea amount is many etc. Ancient medicine is early recognized palace is cold, as " Synopsis Golden Chamber " the miscellaneous internal diseases in woman section carries: " married woman itDisease, because of empty, long-pending cold, knot gas, for Zhu Jingshui breaks off, over the years to having, pathogenic cold coagulating with blood, uterus injured by cold, meridian and collateral being blocked. "
Except irregular menstruation, palace is cold returns women and brings other many harm, as: 1) disorder of qi and blood, interior free yl is extremely aliveJump, old and feeble age age ratio normal female shifts to an earlier date, and easily forms the facial problem such as color spot, acne; 2) menstrual period or its front and back underbelly painUnbearably, feel restless, have a strong impact on work and study and daily life; 3), due to cold uterus, make women's shortage of heat, healthAutomatically hoard fat, thereby cause and get fat, and with shortness of breath and fatigue, insomnia and dreamful sleep, the symptom such as do not ovulate; 4) pain, lower abdomen is coldColdly sometimes have a pain, premenstrual underbelly has falling inflation sense, and occurs the phenomenons such as leucorrhea increasing, the soreness of waist or pain, two mammary swelling pains, and minority has insteadStomach, the reaction of feeling sick; 5) trick is ice-cold; 6) as long as Gong Hanke causes the effect in uterus to reduce even to lose efficacy, can cause in uterusEach conveying and the alluvial of nutrition pipeline or stop up, also can cause the burden in uterus, causes female acyesis.
The factors such as the traditional Chinese medical science thinks that Gong Hanyu suffers from a deficiency of the kidney, insufficiency of the spleen, the deficiency of blood, liver depression, phlegm are wet, blood stasis are relevant. Its etiology and pathogenesis can be returnedReceive as what time following: 1) congenital constitution is partially cold, the insufficiency of both the spleen and the kindey, causes that palace is cold; 2) occupy for a long time moist cold environment or summer air-conditioning coldIn gas, cold-evil enters from flesh table, and the yang-energy of hurting sb.'s feelings causes palace cold; 3) cold food such as cold drink, iced tea, melon and fruit is too many, causes yang-energy consumptionToo much, raw in cold-evil, cause palace cold; 4) after menstrual period, postpartum or how pregnant fecund, overworked, lose in taking good care of oneself, kidney yang virtual loss, orDiseases caused by external factors cold-evil's yang-energy consumes for a long time, and uterus loses in warm, causes palace cold; 5) plain body liver depression or feelings are not smooth when anything crops up, causes stagnation of QI-blood for a long time,The dysfunction of the spleen in transport, raw in phlegm is wet, passages through which vital energy circulates is obstructed, and yang-energy does not reach, and causes palace cold. At present, for the cold all diseases that cause in palace, clinically stillTaking oral drugs or dietotherapy as main, food therapy weak curative effect and cycle are long, and oral drugs not only exist liver first-pass effect and stomach and intestineRoad stimulates, and has also increased the weight of patient's liver kidney burden.
Footbath with traditional Chinese medicines therapy is one of therapy the most frequently used in motherland's medical science external therapy. Medical science ancient books and records have cloud: " people hasPin, still, like the root that has of tree, sets withered and first exhausts, and people is old, and pin first declines. " people's both feet have countless nerve endings to be closely connected with brain,And be connected with body of gland with all organs. According to theory of traditional Chinese medical science, human five internal organs's six internal organs have homolographic projection on pin. Foot is foot threeThe starting point of yin channel (the spleen channel, Liver Channel, kidney channel), is again the terminal of the three yang channels of foots (urinary bladder channel, stomach warp, gallbladder channel), below ankle-joint, hasMore than 60 acupuncture point, stimulates these acupuncture points, can improve the function of each organ, strengthens blood vessels operation, conditioning viscera, and logical channels and collaterals relax.Select suitable medicine decocting foot bath according to the principle of tcm treatment according to syndrome differentiation, can stimulate the each acupuncture point of foot, promote QI-blood circulation, dredgeStimulate the menstrual flow network, improve metabolism, allow effective ingredient pass through mucosa absorption under the warm-heat effect of water and mechanism simultaneouslyPenetrate into blood circulation of human body with skin, give full play to the effect of medicine, thereby reach the effect of prevention and treatment disease.Footbath with traditional Chinese medicines therapy for treating palace is cold with the obvious advantage, has a extensive future.
Chinese patent application 201410585817.X discloses a kind of women's lavipeditum powder, with radix bupleuri, the root of large-flowered skullcap, Radix Angelicae Sinensis, sweetGrass, the radix paeoniae rubrathe, the root of herbaceous peony, rhizoma cyperi, the bighead atractylodes rhizome and Fructus meliae toosendan are that bulk drug is prepared from. This lavipeditum powder formula is simple, have regulating menstruation and activating blood,Effect that the dissipation stasis of blood is stagnant, but it is in dispelling cold menstruation regulating, and the aspect effects such as treatment brothers are ice-cold, irregular menstruation, dysmenorrhoea are not remarkable.
Summary of the invention
In order to overcome the deficiencies in the prior art, the invention provides a kind of foot containing the tarragon dregs of a decoction with dispelling cold menstruation regulating effectBath powder. Lavipeditum powder raw material provided by the invention is easy to get, with low cost, easy to use, also has dispelling cold menstruation regulating simultaneously, invigorates blood circulationEffect of stagnation resolvation, the regulation of qi and blood, warm kidney Gu Mai and dispersing stagnated hepatoqi, can effectively prevent and treat the cold trick ice causing in women palaceThe symptoms such as cool, irregular menstruation, dysmenorrhoea. In addition, the present invention also provides this lavipeditum powder corresponding preparation method.
The technical scheme that the present invention solves the problems of the technologies described above is as follows:
There is the lavipeditum powder of dispelling cold menstruation regulating effect containing the tarragon dregs of a decoction, comprise the raw materials of following weight portion: the tarragon dregs of a decoction50-80 part, luffa vine 10-25 part, Flos Hibisci Rosae-Sinensis 1-10 part, Herba Lycopi 5-20 part, Fresh leaf of aloe 5-20 part, Chinese anise 5-20 part,Corn stigma 10-25 part, concentrated crystal soda 0.5-6 part and sodium chloride 2-10 part.
Preferably, described lavipeditum powder comprises the raw materials of following weight portion: tarragon dregs of a decoction 55-65 part, luffa vine 15-20Part, Flos Hibisci Rosae-Sinensis 3-8 part, Herba Lycopi 10-15 part, Fresh leaf of aloe 8-15 part, Chinese anise 10-20 part, corn stigma 10-20 part, sesquialterSodium carbonate 2-4 part and sodium chloride 4-8 part.
Preferably, described lavipeditum powder comprises the raw materials of following weight portion: 60 parts of the tarragon dregs of a decoction, 18 parts of luffa vines, hold up5 parts, mulberry, 13 parts of Herba Lycopi, 12 parts of Fresh leaf of aloe, 15 parts of Chinese anises, 15 parts of corn stigmas, 3 parts of concentrated crystal sodas and sodium chloride 5Part.
Preferably, the described tarragon dregs of a decoction are the dregs of a decoction of tarragon after supercritical carbon dioxide extracts P-Cymene.
Preferably, the preparation method of the described tarragon dregs of a decoction comprises the following steps: will be dried after tarragon is pulverized and fill extraction kettle,The upper pressure of setting extraction kettle is 25MPa, presses down as 27MPa, and temperature is 48 DEG C, and the pressure of setting extraction-container is 5MPa, and temperature is60 DEG C, then pass into CO 2 fluid extraction, collect medicinal extract at extraction-container, in the time that reaching 2.5%, output stops, retaining after extractionThe dregs of a decoction, drying under reduced pressure, obtains the tarragon dregs of a decoction.
The present invention also provides a kind of preparation containing the tarragon dregs of a decoction with the lavipeditum powder of dispelling cold menstruation regulating effect of the present inventionMethod, comprises the following steps:
S1: will be dried after tarragon is pulverized and fill extraction kettle, the upper pressure of setting extraction kettle is 25MPa, presses down as 27MPa, and temperature is48 DEG C, the pressure of setting extraction-container is 5MPa, and temperature is 60 DEG C, then passes into CO 2 fluid extraction, collects at extraction-containerMedicinal extract stops in the time that output reaches 2.5%, retains the dregs of a decoction after extraction, and drying under reduced pressure, obtains the tarragon dregs of a decoction;
S2: get Fresh leaf of aloe, cleaning and chopping, pulverizes making beating for colloidal liquid, and colloidal liquid is carried out to press filtration and retains aloeFilter residue, the liquid obtaining after press filtration is aloe gel juice;
S3: get luffa vine, Herba Lycopi, Flos Hibisci Rosae-Sinensis, Chinese anise and corn stigma, impurity elimination, the aloe filter residue of cleaning afterwards and described in S2 mixClose, drying under reduced pressure, mixes with the tarragon dregs of a decoction described in S1, pulverizes, and crosses 80-100 mesh sieve, adds medicinal powder weight 8-10 doubly to measure volumeMark is the ethanol of 70-85%, refluxing extraction 2-3 time, and each 1-2h, filters and retains mixture filter residue; Merging filtrate, decompressionEthanol is removed in distillation, is evaporated to the thick paste that at 60 DEG C, relative density is 1.30-1.35;
S4: get the mixture filter residue described in S3, add with after distilled water washing 2-3 time the distilled water that former medicinal powder weight 10-12 doubly measuresSoak 30-60min, decoct 2-3h, filter; The decocting that filter residue adds medicinal powder weight 8-10 doubly to measure boils 1-2h, filters; Merge twiceFiltrate, is evaporated to the thick paste that at 60 DEG C, relative density is 1.30-1.35;
S5: the thick paste described in S3 and S4 is mixed with the aloe gel juice described in S2, and vacuum freeze drying obtains solid, with sesquialterSodium carbonate and sodium chloride mix rear ultramicro grinding to 200-300 order powder, obtain lavipeditum powder of the present invention.
In addition, the present invention also provides the user containing the tarragon dregs of a decoction with the lavipeditum powder of dispelling cold menstruation regulating effect of the present inventionMethod, comprises the following steps: take fully bath powder, add its weight 100-150 doubly to measure the warm water of 40-50 DEG C, after fully dissolving by bipedBe placed in warm water, more than the water yield will there be ankle, soak 20-30min, add in right amount during this time hot water to regulate water temperature, make water temperatureRemain on 40-50 DEG C.
Lavipeditum powder of the present invention is to extract the dregs of a decoction after essential oil as primary raw material taking tarragon, adds luffa vine, Flos Hibisci Rosae-Sinensis, poolOrchid, Fresh leaf of aloe, Chinese anise and 6 kinds of common Chinese medicine materials of corn stigma and concentrated crystal soda and two kinds of composite forming of salt of sodium chloride.In the tarragon dregs of a decoction, do not extract completely volatile oil except containing, also contain flavonoids, tannin class, polysaccharide, alkaloid and chlorogenic acidDeng active ingredient of Chinese herbs, there is warming channel and expelling cold, recuperating qi-blood, antibacterial, anti-oxidant and strengthen the effects such as immunity; Luffa vine is calabashThe rattan of Lu Ke plant sponge gourd, taste is sweet, and property is flat, has the effects such as clearing and activating the channels and collaterals, invigorating the spleen, records it: " and blood in " it is former that book on Chinese herbal medicine is asked "Arteries and veins, the grain of living, grows water, only cloudy pain, bowl spares invigorating the spleen, consumer edema. Control blood depletion few, waist knee numb limb, postpartum infantile convulsion, menstruation regulating "; Hold upMulberry is the flower of Malvaceae plant Chinese Hibiscu, and taste is sweet, and property is flat, has effect of clearing lung and eliminating phlegm, removing pattogenic heat from the blood and toxic material from the body, main cough with lung heat,Spitting of blood, nosebleed epistaxis, uterine bleeding, leukorrhea, dysentery, reddish and whitish turbid urine and carbuncle pyogenic infections sore etc.; Herba Lycopi is the dry of labiate hair leaf lycopus lucidusDry aerial part, bitter, pungent, slightly warm in nature, have promoting blood circulation and removing blood stasis, effect of line water detumescence, for irregular menstruation, through closing, dysmenorrhoea,Postpartum blood stasis stomachache, oedema etc.; Fresh leaf of aloe is the fresh leaf of liliaceous plant stripe aloe vera or aloe barbadensis Miller, bitter,Puckery, cold in nature, tool purging intense heat, stimulates the menstrual flow, desinsection, and effect of removing toxic substances, controls gonorrhoea, hematuria, women is through closing, being with down, pediatric epilepsy scared, infantile malnutrition due to digestive disturbances or intestinalparasites,Scald, hemorrhoid, scabies, carbuncle is swollen etc.; Chinese anise is the dry mature fruit of Magnoliacea plant Chinese anise, and taste is pungent, warm in nature, toolWarming yang for dispelling cold, effect of regulating qi-flowing for relieving pain, " medical center bun will " records it: " kidney tonifying of profit kidney, the edema with the liver involved of relaxing, reach gloomy, relaxing muscles and tendons, lower to pinGas "; Corn stigma is style and the fresh idea of grass family Zea plant corn, and taste is sweet, light, and property is flat, and " the southern regions of the Yunnan Province book on Chinese herbal medicine " records it:" gas under wide intestines, controls married woman's breast knot, alactation, and congestion and swelling pain, the heating of being afraid of cold, headache body is tired "; Concentrated crystal soda and sodium chlorideThe interpolation of two kinds of salt has the effect of clean, antipruritic, antibacterial and fine and smooth pedal skin on the one hand, is conducive to blood circulation and fitnessSkin, also helps lend some impetus on the other hand Chinese medicine and dissolves fast in water. Lavipeditum powder reasonable recipe provided by the invention, each groupPoint synergy, reaches effect of dispelling cold menstruation regulating, promoting blood circulation and removing blood stasis, the regulation of qi and blood, warm kidney Gu Mai and dispersing stagnated hepatoqi jointly, can be effectiveThe symptoms such as the cold trick causing of prevention and treatment women palace is ice-cold, irregular menstruation, dysmenorrhoea.
Compared with prior art, beneficial effect of the present invention is:
(1) lavipeditum powder that has dispelling cold menstruation regulating effect containing the tarragon dregs of a decoction provided by the invention is taking the tarragon dregs of a decoction as primary raw material,Composite other compositions are prepared from, and are the further exploitation to the tarragon dregs of a decoction; Utilize the tarragon dregs of a decoction to prepare lavipeditum powder, will endThe leaf dregs of a decoction are turned waste into wealth, and make full use of the active ingredient in the tarragon dregs of a decoction, have higher economic benefit;
(2) the lavipeditum powder reasonable recipe containing the tarragon dregs of a decoction with dispelling cold menstruation regulating effect provided by the invention, each component synergy,Jointly reach effect of dispelling cold menstruation regulating, promoting blood circulation and removing blood stasis, the regulation of qi and blood, warm kidney Gu Mai and dispersing stagnated hepatoqi, can effectively prevent and treatThe symptoms such as the cold trick causing in women palace is ice-cold, irregular menstruation, dysmenorrhoea;
(3) the lavipeditum powder raw material that has dispelling cold menstruation regulating effect containing the tarragon dregs of a decoction provided by the invention is easy to get, with low cost, simultaneously thisThe preparation method that invention provides can fully extract and retain the active ingredient of medicinal material, and medicinal material availability is high, the lavipeditum preparingPowder active constituents of medicine content is high.
Detailed description of the invention
Further describe the present invention by detailed description of the invention below, but the present invention is not limited only to following examples. ?In scope of the present invention or not departing from content of the present invention, spirit and scope, the present invention is suitably improved, replacedThe component that effect is identical, will become apparent to those skilled in the art that they are all deemed to be included in of the present inventionWithin scope.
Embodiment 1
The lavipeditum powder that the embodiment of the present invention 1 has dispelling cold menstruation regulating effect containing the tarragon dregs of a decoction comprises the raw materials of following weight portion:50 parts of the tarragon dregs of a decoction, 25 parts of luffa vines, 10 parts of Flos Hibisci Rosae-Sinensis, 10 parts of Herba Lycopi, 10 parts of Fresh leaf of aloe, 5 parts of Chinese anises, corn stigma 20Part, 4 parts, 2 parts of concentrated crystal sodas and sodium chloride.
Preparation method:
S1: will be dried after tarragon is pulverized and fill extraction kettle, the upper pressure of setting extraction kettle is 25MPa, presses down as 27MPa, and temperature is48 DEG C, the pressure of setting extraction-container is 5MPa, and temperature is 60 DEG C, then passes into CO 2 fluid extraction, collects at extraction-containerMedicinal extract stops in the time that output reaches 2.5%, retains the dregs of a decoction after extraction, and drying under reduced pressure, obtains the tarragon dregs of a decoction;
S2: get Fresh leaf of aloe, cleaning and chopping, pulverizes making beating for colloidal liquid, and colloidal liquid is carried out to press filtration and retains aloeFilter residue, the liquid obtaining after press filtration is aloe gel juice;
S3: get luffa vine, Herba Lycopi, Flos Hibisci Rosae-Sinensis, Chinese anise and corn stigma, impurity elimination, the aloe filter residue of cleaning afterwards and described in S2 mixClose, drying under reduced pressure, mixes with the tarragon dregs of a decoction described in S1, pulverizes, and crosses 80 mesh sieves, adds 8 times of amount volume fractions of medicinal powder weight to be70% ethanol, refluxing extraction 2 times, each 1.5h, filters and retains mixture filter residue; Merging filtrate, second is removed in decompression distillationAlcohol, is evaporated to the thick paste that at 60 DEG C, relative density is 1.30;
S4: get the mixture filter residue described in S3, with the distilled water immersion that adds 10 times of amounts of former medicinal powder weight after distilled water washing 3 times30min, decocts 2h, filters; Filter residue adds the decocting of 8 times of amounts of medicinal powder weight to boil 1.5h, filters; Merge filtrate twice, reduce pressure denseBe reduced to the thick paste that at 60 DEG C, relative density is 1.30;
S5: the thick paste described in S3 and S4 is mixed with the aloe gel juice described in S2, and vacuum freeze drying obtains solid, with sesquialterSodium carbonate and sodium chloride mix rear ultramicro grinding to 200 order powder, obtain lavipeditum powder of the present invention.
Embodiment 2
The lavipeditum powder that the embodiment of the present invention 2 has dispelling cold menstruation regulating effect containing the tarragon dregs of a decoction comprises the raw materials of following weight portion:65 parts of the tarragon dregs of a decoction, 15 parts of luffa vines, 5 parts of Flos Hibisci Rosae-Sinensis, 15 parts of Herba Lycopi, 15 parts of Fresh leaf of aloe, 10 parts of Chinese anises, corn stigma 10Part, 6 parts, 4 parts of concentrated crystal sodas and sodium chloride.
Preparation method:
S1: will be dried after tarragon is pulverized and fill extraction kettle, the upper pressure of setting extraction kettle is 25MPa, presses down as 27MPa, and temperature is48 DEG C, the pressure of setting extraction-container is 5MPa, and temperature is 60 DEG C, then passes into CO 2 fluid extraction, collects at extraction-containerMedicinal extract stops in the time that output reaches 2.5%, retains the dregs of a decoction after extraction, and drying under reduced pressure, obtains the tarragon dregs of a decoction;
S2: get Fresh leaf of aloe, cleaning and chopping, pulverizes making beating for colloidal liquid, and colloidal liquid is carried out to press filtration and retains aloeFilter residue, the liquid obtaining after press filtration is aloe gel juice;
S3: get luffa vine, Herba Lycopi, Flos Hibisci Rosae-Sinensis, Chinese anise and corn stigma, impurity elimination, the aloe filter residue of cleaning afterwards and described in S2 mixClose, drying under reduced pressure, mixes with the tarragon dregs of a decoction described in S1, pulverizes, and crosses 100 mesh sieves, adds 10 times of amount volume fractions of medicinal powder weightBe 85% ethanol, refluxing extraction 2 times, each 2h, filters and retains mixture filter residue; Merging filtrate, second is removed in decompression distillationAlcohol, is evaporated to the thick paste that at 60 DEG C, relative density is 1.30;
S4: get the mixture filter residue described in S3, with the distilled water immersion that adds 12 times of amounts of former medicinal powder weight after distilled water washing 3 times60min, decocts 3h, filters; Filter residue adds the decocting of 10 times of amounts of medicinal powder weight to boil 2h, filters; Merge filtrate twice, reduced pressure concentrationTo the thick paste that is 1.30 of relative density at 60 DEG C;
S5: the thick paste described in S3 and S4 is mixed with the aloe gel juice described in S2, and vacuum freeze drying obtains solid, with sesquialterSodium carbonate and sodium chloride mix rear ultramicro grinding to 300 order powder, obtain lavipeditum powder of the present invention.
Embodiment 3
The lavipeditum powder that the embodiment of the present invention 3 has dispelling cold menstruation regulating effect containing the tarragon dregs of a decoction comprises the raw materials of following weight portion:60 parts of the tarragon dregs of a decoction, 18 parts of luffa vines, 5 parts of Flos Hibisci Rosae-Sinensis, 13 parts of Herba Lycopi, 12 parts of Fresh leaf of aloe, 15 parts of Chinese anises, corn stigma 15Part, 5 parts, 3 parts of concentrated crystal sodas and sodium chloride.
Preparation method:
S1: will be dried after tarragon is pulverized and fill extraction kettle, the upper pressure of setting extraction kettle is 25MPa, presses down as 27MPa, and temperature is48 DEG C, the pressure of setting extraction-container is 5MPa, and temperature is 60 DEG C, then passes into CO 2 fluid extraction, collects at extraction-containerMedicinal extract stops in the time that output reaches 2.5%, retains the dregs of a decoction after extraction, and drying under reduced pressure, obtains the tarragon dregs of a decoction;
S2: get Fresh leaf of aloe, cleaning and chopping, pulverizes making beating for colloidal liquid, and colloidal liquid is carried out to press filtration and retains aloeFilter residue, the liquid obtaining after press filtration is aloe gel juice;
S3: get luffa vine, Herba Lycopi, Flos Hibisci Rosae-Sinensis, Chinese anise and corn stigma, impurity elimination, the aloe filter residue of cleaning afterwards and described in S2 mixClose, drying under reduced pressure, mixes with the tarragon dregs of a decoction described in S1, pulverizes, and crosses 100 mesh sieves, adds 9 times of amount volume fractions of medicinal powder weight to be80% ethanol, refluxing extraction 2 times, each 2h, filters and retains mixture filter residue; Merging filtrate, ethanol is removed in decompression distillation,Be evaporated to the thick paste that at 60 DEG C, relative density is 1.30;
S4: get the mixture filter residue described in S3, with the distilled water immersion that adds 12 times of amounts of former medicinal powder weight after distilled water washing 3 times40min, decocts 2.5h, filters; Filter residue adds the decocting of 8 times of amounts of medicinal powder weight to boil 2h, filters; Merge filtrate twice, reduce pressure denseBe reduced to the thick paste that at 60 DEG C, relative density is 1.30;
S5: the thick paste described in S3 and S4 is mixed with the aloe gel juice described in S2, and vacuum freeze drying obtains solid, with sesquialterSodium carbonate and sodium chloride mix rear ultramicro grinding to 300 order powder, obtain lavipeditum powder of the present invention.
Embodiment 4
The lavipeditum powder that the embodiment of the present invention 4 has dispelling cold menstruation regulating effect containing the tarragon dregs of a decoction comprises the raw materials of following weight portion:60 parts of the tarragon dregs of a decoction, 20 parts of luffa vines, 3 parts of Flos Hibisci Rosae-Sinensis, 15 parts of Herba Lycopi, 8 parts of Fresh leaf of aloe, 10 parts of Chinese anises, corn stigma 10Part, 4 parts, 2 parts of concentrated crystal sodas and sodium chloride.
Preparation method is with embodiment 3.
Comparative example 1
Comparative example 1 lavipeditum powder comprises the raw materials of following weight portion:
60 parts of the tarragon dregs of a decoction, 18 parts of luffa vines, 5 parts of Flos Hibisci Rosae-Sinensis, 13 parts of Herba Lycopi, 12 parts of Fresh leaf of aloe, 15 parts, ginger, corn stigma 15Part, 5 parts, 3 parts of concentrated crystal sodas and sodium chloride.
Preparation method is similar to Example 3.
Comparative example 2
Comparative example 2 lavipeditum powders comprise the raw materials of following weight portion:
60 parts of the tarragon dregs of a decoction, 18 parts of luffa vines, 5 parts of Flos Hibisci Rosae-Sinensis, 13 parts of Herba Lycopi, 12 parts of Fresh leaf of aloe, 15 parts of Chinese anises, corn8 parts, 15 parts of palpuses and sodium chloride.
Preparation method is similar to Example 3.
Comparative example 3
Comparative example 3 lavipeditum powder formulas are with embodiment 3.
Preparation method:
S1: will be dried after tarragon is pulverized and fill extraction kettle, the upper pressure of setting extraction kettle is 23MPa, presses down as 25MPa, and temperature is45 DEG C, the pressure of setting extraction-container is 5MPa, and temperature is 58 DEG C, then passes into CO 2 fluid extraction, collects at extraction-containerMedicinal extract stops in the time that output reaches 2%, gets the dregs of a decoction after extraction, and drying under reduced pressure obtains the tarragon dregs of a decoction;
S2: get luffa vine, Flos Hibisci Rosae-Sinensis, Herba Lycopi, Fresh leaf of aloe, Chinese anise and corn stigma, impurity elimination, clean rear drying under reduced pressure, withThe tarragon dregs of a decoction, concentrated crystal soda and sodium chloride mix, and are crushed to 100 order powder, obtain comparative example 3 lavipeditum powders of the present invention.
Test example one, lavipeditum powder irritation test of the present invention
Test is according in " technological guidance's principle of Chinese medicine, natural drug excitant and hemolytic research " " irritation test "Related request carry out.
Get 40 of healthy adult new zealand rabbit regular grade, body weight 2.0-2.5kg, male and female half and half. Be divided at random 10 groups, everyOrganize 4 rabbits, each 5 groups of intact skin group and damaged skin group. 24h before administration, backbone both sides, back are used after surgical scissors cropping,Again with 8% vulcanized sodium depilation, left and right 5% of the body surface area that is of depilation area. Damaged skin group skin degerming, weares and teares with sand paperExtremely slight oozing of blood is degree. Respectively get the lavipeditum powder of the 3g embodiment of the present invention 1, embodiment 3, comparative example 1, comparative example 2 and comparative example 3,Fully dissolve rear cooling for subsequent use with 12mL40-50 DEG C of warm water. Adopt consubstantiality left and right sides self-contrast method, get tested lavipeditum powder solution2mL is directly coated on the skin of unhairing of rabbit left side, then covers with two layers of gauze and one deck glassine paper, then uses nonirritant yarnCloth and bandage are fixed; Opposite side is coated with isometric purified water as blank. Application time is 4h, sticks endAfter, remove tested material and with the clean medicine-feeding part of warm water. Once a day, stick 4h, continuously same position administration 14 days at every turn.Remove after medicine 1h at every turn and again stick front observation and record erythema and whether oedema, coating part have pigmentation, go outBlood point, pachylosis or epidermatic atrophy situation and time of origin and regression time, and erythema and oedema are marked. Last pastesAfter applying, removing 30-60min after medicine, 24h, 48h and 72h visually observe and record coating part and have or not erythema and oedema etc.Situation.
Result: rabbit skin gives the lavipeditum of the embodiment of the present invention 1, embodiment 3 and comparative example 1, comparative example 2, comparative example 3After powder solution (0.25g/mL), intact skin and damaged skin are showed no to the reaction of the skin irritation such as erythema, oedema, use 2After week, embodiment of the present invention group rabbit skin polishes, and has no the situation such as pigmentation and pachylosis.
Test example two, lavipeditum powder effect test of the present invention
1, palace sympotoms caused by cold factors shape: 1) leukorrhea amount is many, rare clearly; 2) irregular menstruation, dysmenorrhoea; 3) sexual apathy, multithread are produced; 4) underbelly not warm, fourLimb is ice-cold, dizzy, breast distent before menstruation; 5) chloasma, acne; 6) sleepy pain in the back, dim complexion, eyelid swelled.
Meet the above-described the 1st), 2) two kinds of symptoms for once palace is cold, meet the 1st), 2) two kinds of symptoms and appointing belowA symptom of meaning be that two degree palaces are cold, meet the 1st), 2) two kinds of symptoms and below arbitrarily binomial and above be the most seriousThree degree palaces are cold.
2, subjects: invite 600 female volunteers with palace sympotoms caused by cold factors shape to participate in this test.
In 600 volunteers, age 18-45 year, wherein, once 153 of the cold volunteers in palace, the two cold volunteers 286 in degree palacesName, three 161 of the cold volunteers in degree palace. By all volunteers be divided at random 1 group of embodiment, 3 groups of embodiment, comparative example 1-3 group and6 groups of positive controls, every group of 100 people, every group of volunteer learns by statistics and processes equal nothing at aspects such as age, the course of disease, the cold situations in palaceSignificant difference, has comparativity.
2,1 group of test method: embodiment, 3 groups of embodiment, comparative example 1-3 organize each group of volunteer and use respectively the present invention realExecute the lavipeditum powder of example 1, embodiment 3, comparative example 1-3, before sleeping every day, lavipeditum 1 time, is used 2 months continuously.
Lavipeditum method: get 15g lavipeditum powder, add 2000mL40-50 DEG C of warm water, after fully dissolving, biped is placed in to warm waterIn, more than the water yield will there be ankle, soak 30min, add in right amount during this time hot water to regulate water temperature, make water temperature remain on 40-50℃。
Positive controls is directly used 400mL40-50 DEG C of emerge in worm water both feet 30min.
3, effect evaluation method:
Cure: symptom disappears completely;
Effective: transference cure >=2/3;
Effective: transference cure >=1/3;
Invalid: transference cure < 1/3;
Recurrence: follow up a case by regular visits to after healing 6 months, reappear palace sympotoms caused by cold factors shape.
Recurrence rate=recurrence number of cases/healing number of cases × 100%
4, result for the treatment of, in table 1 and table 2.
The total effects that table 1 lavipeditum powder of the present invention is cold to palace
The result for the treatment of of table 2 lavipeditum powder of the present invention to the cold cardinal symptom in palace
5, conclusion (of pressure testing)
Result from table 1 and table 2:
(1) lavipeditum powder that the present invention has dispelling cold menstruation regulating effect containing the tarragon dregs of a decoction has significant dispelling cold menstruation regulating effect, can be effectiveThe symptoms such as the cold trick causing of prevention and treatment women palace is ice-cold, irregular menstruation, dysmenorrhoea, recurrence rate after healing is low;
(2) difference of comparative example 1 and comparative example 2 lavipeditum powder formulas and the embodiment of the present invention 3 lavipeditum powder formulas is in comparative example 1The ginger close with effect with nature and flavor replaces the Chinese anise in the embodiment of the present invention 3, and in comparative example 2, increases the use of sodium chlorideMeasure but do not add concentrated crystal soda, from result of the test, compared with comparative example 1, comparative example 2, prepared by the embodiment of the present invention 3Lavipeditum powder is more excellent to the cold result for the treatment of in palace, can effectively cure the gentle palace sympotoms caused by cold factors shapes such as trick is ice-cold, irregular menstruation, dysmenorrhoea of separating,Lavipeditum powder reasonable recipe of the present invention is described, between each component, there is synergy;
(3) comparative example 3 lavipeditum powder formulas are consistent with the embodiment of the present invention 3 formulas, but preparation method's difference, can from result of the testKnow, lavipeditum powder prepared by the embodiment of the present invention 3 is significantly better than 3 groups of comparative examples to the cold result for the treatment of in palace, and lavipeditum of the present invention is describedThe preparation method of powder can fully extract and retain the active ingredient of Chinese medicine, and medicinal material availability is high, the lavipeditum powder medicine preparingThing active component content is high, more remarkable treatment effect.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention. Any ripeThe personage who knows this technology all can, under spirit of the present invention and category, modify or change above-described embodiment. CauseThis, have in technical field under such as conventionally know the knowledgeable do not depart under disclosed spirit and technological thought completeAll equivalences that become are modified or change, and must be contained by claim of the present invention.
Claims (7)
1. a lavipeditum powder containing the tarragon dregs of a decoction with dispelling cold menstruation regulating effect, is characterized in that, described lavipeditum powder comprises following heavyThe raw materials of amount part: tarragon dregs of a decoction 50-80 part, luffa vine 10-25 part, Flos Hibisci Rosae-Sinensis 1-10 part, Herba Lycopi 5-20 part, Fresh leaf of aloe5-20 part, Chinese anise 5-20 part, corn stigma 10-25 part, concentrated crystal soda 0.5-6 part and sodium chloride 2-10 part.
2. the lavipeditum powder containing the tarragon dregs of a decoction with dispelling cold menstruation regulating effect as claimed in claim 1, is characterized in that described lavipeditumPowder comprises the raw materials of following weight portion: tarragon dregs of a decoction 55-65 part, luffa vine 15-20 part, Flos Hibisci Rosae-Sinensis 3-8 part, Herba Lycopi 10-15 parts, Fresh leaf of aloe 8-15 part, Chinese anise 10-20 part, corn stigma 10-20 part, concentrated crystal soda 2-4 part and sodium chloride 4-8Part.
3. the lavipeditum powder containing the tarragon dregs of a decoction with dispelling cold menstruation regulating effect as claimed in claim 1, is characterized in that described lavipeditumPowder comprises the raw materials of following weight portion: 60 parts of the tarragon dregs of a decoction, 18 parts of luffa vines, 5 parts of Flos Hibisci Rosae-Sinensis, 13 parts of Herba Lycopi, aloe are fresh5 parts, 12 parts, leaf, 15 parts of Chinese anises, 15 parts of corn stigmas, 3 parts of concentrated crystal sodas and sodium chloride.
4. the lavipeditum powder containing the tarragon dregs of a decoction with dispelling cold menstruation regulating effect as claimed in claim 1, is characterized in that described tarragonThe dregs of a decoction are the dregs of a decoction of tarragon after supercritical carbon dioxide extracts P-Cymene.
5. the lavipeditum powder containing the tarragon dregs of a decoction with dispelling cold menstruation regulating effect as claimed in claim 4, is characterized in that described tarragonThe preparation method of the dregs of a decoction comprises the following steps: will be dried after tarragon is pulverized and fill extraction kettle, the upper pressure of setting extraction kettle is25MPa, presses down as 27MPa, and temperature is 48 DEG C, and the pressure of setting extraction-container is 5MPa, and temperature is 60 DEG C, then passes into titanium dioxideCarbon fluid extraction, collects medicinal extract at extraction-container, in the time that output reaches 2.5%, stops, and retains the dregs of a decoction after extraction, and drying under reduced pressure, to obtain final productThe tarragon dregs of a decoction.
6. one kind has the preparation side of the lavipeditum powder of dispelling cold menstruation regulating effect containing the tarragon dregs of a decoction as described in as arbitrary in claim 1-5Method, is characterized in that, described preparation method comprises the following steps:
S1: will be dried after tarragon is pulverized and fill extraction kettle, the upper pressure of setting extraction kettle is 25MPa, presses down as 27MPa, and temperature is48 DEG C, the pressure of setting extraction-container is 5MPa, and temperature is 60 DEG C, then passes into CO 2 fluid extraction, collects at extraction-containerMedicinal extract stops in the time that output reaches 2.5%, retains the dregs of a decoction after extraction, and drying under reduced pressure, obtains the tarragon dregs of a decoction;
S2: get Fresh leaf of aloe, cleaning and chopping, pulverizes making beating for colloidal liquid, and colloidal liquid is carried out to press filtration and retains aloeFilter residue, the liquid obtaining after press filtration is aloe gel juice;
S3: get luffa vine, Herba Lycopi, Flos Hibisci Rosae-Sinensis, Chinese anise and corn stigma, impurity elimination, the aloe filter residue of cleaning afterwards and described in S2 mixClose, drying under reduced pressure, mixes with the tarragon dregs of a decoction described in S1, pulverizes, and crosses 80-100 mesh sieve, adds medicinal powder weight 8-10 doubly to measure volumeMark is the ethanol of 70-85%, refluxing extraction 2-3 time, and each 1-2h, filters and retains mixture filter residue; Merging filtrate, decompressionEthanol is removed in distillation, is evaporated to the thick paste that at 60 DEG C, relative density is 1.30-1.35;
S4: get the mixture filter residue described in S3, add with after distilled water washing 2-3 time the distilled water that former medicinal powder weight 10-12 doubly measuresSoak 30-60min, decoct 2-3h, filter; The decocting that filter residue adds medicinal powder weight 8-10 doubly to measure boils 1-2h, filters; Merge twiceFiltrate, is evaporated to the thick paste that at 60 DEG C, relative density is 1.30-1.35;
S5: the thick paste described in S3 and S4 is mixed with the aloe gel juice described in S2, and vacuum freeze drying obtains solid, with sesquialterSodium carbonate and sodium chloride mix rear ultramicro grinding to 200-300 order powder, obtain lavipeditum powder of the present invention.
7. one kind has the user of the lavipeditum powder of dispelling cold menstruation regulating effect containing the tarragon dregs of a decoction as described in as arbitrary in claim 1-6Method, is characterized in that, described using method comprises the following steps: take fully bath powder, add its weight 100-150 doubly to measure 40-50DEG C warm water, after fully dissolving, biped is placed in to warm water, more than the water yield will there be ankle, soak 20-30min, appropriate during this timeAdd hot water to regulate water temperature, make water temperature remain on 40-50 DEG C.
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| CN108355037A (en) * | 2018-05-15 | 2018-08-03 | 黄巧明 | The Chinese medicine bathing instant granular of improvement women palace cold dysmenorrhoea and preparation and application method |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104147276A (en) * | 2014-08-27 | 2014-11-19 | 刘卫明 | Foot bath powder |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104147276A (en) * | 2014-08-27 | 2014-11-19 | 刘卫明 | Foot bath powder |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108355037A (en) * | 2018-05-15 | 2018-08-03 | 黄巧明 | The Chinese medicine bathing instant granular of improvement women palace cold dysmenorrhoea and preparation and application method |
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