CN105562164B - A kind of ball grinder - Google Patents

A kind of ball grinder Download PDF

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Publication number
CN105562164B
CN105562164B CN201610121418.7A CN201610121418A CN105562164B CN 105562164 B CN105562164 B CN 105562164B CN 201610121418 A CN201610121418 A CN 201610121418A CN 105562164 B CN105562164 B CN 105562164B
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CN
China
Prior art keywords
ball milling
ball
tank body
chamber
milling chamber
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CN201610121418.7A
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Chinese (zh)
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CN105562164A (en
Inventor
赵怀周
陈小龙
谷林
李善明
曹丙磊
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Institute of Physics of CAS
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Institute of Physics of CAS
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Priority to CN201610121418.7A priority Critical patent/CN105562164B/en
Publication of CN105562164A publication Critical patent/CN105562164A/en
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/04Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with unperforated container
    • B02C17/06Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with unperforated container with several compartments
    • B02C17/07Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with unperforated container with several compartments in radial arrangement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/10Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with one or a few disintegrating members arranged in the container
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/04Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with unperforated container
    • B02C17/06Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with unperforated container with several compartments
    • B02C2017/065Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with unperforated container with several compartments with several compartments in the form of multiwell blocks

Abstract

It the present invention relates to a kind of ball grinder, including at least two tank bodies, is fixedly connected between tank body, forms multiple ball milling units between adjacent two tank bodies, multiple ball milling units are mutually independent seal cavity.Ball grinder provided by the invention includes multiple ball milling units, can disposably complete the ball-milling treatment of multiple batches of material sample.And collaboration vibration may be implemented between multiple ball milling units, substantially increase grinding efficiency.Closer, the design of multiple ball milling units can ensure to carry out micro or low-volume samples the sample yield of ball milling, simultaneously, since each ball milling unit is all under identical ball milling condition, so the consistency that ball grinder provided by the invention can also ensure the repeatability of experiment and entirely test.

Description

A kind of ball grinder
Technical field
The present invention relates to ball grinding technique field, especially a kind of ball grinder.
Background technology
High throughput synthesis is the forefront project of material science development now, and core is the high-throughput efficient material of development Expect synthetic method, technology and sophisticated equipment.And solid material is most important member in material science family, including metal And alloy, inorganic non-metallic material, organic polymer material etc..The synthetic method of wherein solid inorganic material is varied, but It is the diffusion-sintering that most important synthesis technology must include the mixing and reactant of raw material.The two is mutual indepedent technique step Suddenly, high-throughput materials synthesis is finally realized, it is necessary to all be realized in terms of the two steps high-throughput.
Traditional material mixing often realizes that as shown in Figure 1, 2, the ball grinder for commonly using ball mill includes tank body by ball mill 11, end cap 12 and attachment device 13, end cap 12 are fixed to the open end of tank body 11, but the ball of this structure by attachment device 13 Grinding jar generally only includes a ball milling chamber, once can be only done a kind of mixing of material, and yield is relatively low, cannot be satisfied primary The demand that property handles multiple batches of sample.Meanwhile being also not easy to ensure the consistency of multiple batches of experiment.
Invention content
In view of this, the purpose of the present invention is to provide a kind of ball grinder, make its can solve the deficiency of traditional technology and It disclosure satisfy that the requirement of high-throughput material preparation.
The present invention is for a kind of ball grinder, which is characterized in that including at least two tank bodies, it is fixedly connected between tank body, it is adjacent Two tank bodies between form multiple ball milling units, multiple ball milling units are mutually independent seal cavity.
Preferably, the first ball milling chamber and the second ball milling chamber, the first ball milling chamber is respectively set on two adjacent tank bodies It is spliced to form the ball milling unit with the second ball milling chamber.
Preferably, the open edge of the first ball milling chamber or the second ball milling chamber is provided with sealing mechanism.
Preferably, the ball milling unit is elliposoidal cavity.
Preferably, a length of 1-3cm of long axis of the elliposoidal cavity, a length of 1-2cm of short axle.
Preferably, the 6-10 ball milling units are formed between two tank bodies.
Preferably, including the first tank body, the second tank body and third tank body, second tank body are arranged in first tank body Between third tank body, and multiple ball milling units are respectively formed between first tank body and third tank body.
Preferably, the first ball milling chamber is set on an end face of first tank body, second tank body is opposite The first ball milling chamber and the second ball milling chamber are respectively set on two end faces, on an end face of the third tank body described in setting Second ball milling chamber.
Preferably, second tank body is provided with one or more.
Preferably, pass through connecting rod or threaded connection between tank body.
Ball grinder provided by the invention includes multiple ball milling units, can disposably be completed at the ball milling of multiple batches of material sample Reason.And collaboration vibration may be implemented between multiple ball milling units, substantially increase grinding efficiency.Closer, multiple ball millings The design of unit can ensure to carry out micro or low-volume samples the sample yield of ball milling, simultaneously as each ball milling unit All under identical ball milling condition, so, ball grinder provided by the invention can also ensure the repeated and entire reality of experiment The consistency tested.
Description of the drawings
By referring to the drawings to the description of the embodiment of the present invention, above-mentioned and other purposes of the invention, feature and Advantage will be apparent from, in the accompanying drawings:
Fig. 1 is prior art ball grinder structural schematic diagram;
Fig. 2 is prior art ball grinder schematic cross-sectional view;
Fig. 3 is ball grinder structural schematic diagram of the present invention;
Fig. 4 is ball grinder schematic cross-sectional view of the present invention;
Fig. 5 is sealed structural representation at the first ball milling chamber.
Specific implementation mode
Hereinafter reference will be made to the drawings is more fully described various embodiments of the present invention.In various figures, identical element It is indicated using same or similar reference numeral.For the sake of clarity, the various pieces in attached drawing are not necessarily to scale.
The present invention provides a kind of ball grinder that can be realized and disposably complete multiple batches of material sample ball-milling treatment.Such as Fig. 3 Shown, ball grinder provided by the invention includes the first tank body 101, the second tank body 102 and third tank body 103, second tank body 102 are arranged between first tank body 101 and third tank body 103, first tank body 101, the second tank body 102 and third tank Body 103 is connected by connecting rod 104 or other modes, such as is threadedly coupled.As shown in figure 4, ball grinder group provided by the invention After the completion of dress, second tank body 102 forms multiple ball milling lists between first tank body 101 and third tank body 103 respectively Member 105, multiple ball milling units 105 are distributed with single-layer or multi-layer, it is preferable that and the ball milling unit 105 is elliposoidal cavity, Its long axis is 2cm, short axle 1.5cm.Each described ball milling unit 105 is an independent closed ball milling chamber, makes this The ball grinder that invention provides can realize the sample ball-milling treatment for disposably completing multiple batches.Ball grinder tank provided by the invention Body is especially 105 inside of the ball milling unit and uses stainless steel, converted steel or other high hardness wear-resisting materials, ensures the ball Grind the wearability of unit 105.
As shown in Figure 3,4, first tank body 101 includes the first ball milling portion 111 and first support 112, first ball Mill portion 111 is with certain thickness column construction, and preferably cylindrical structure is arranged on an end face of the cylinder There is the first ball milling chamber 151, the first ball milling chamber 151 is provided with multiple, and multiple first ball milling chambers 151 are with described first The center of 111 end face of ball milling portion is symmetrical centre distribution in a center of symmetry, it is preferable that the first ball milling chamber 151 is provided with 6- 10.The first support 112 is fixedly attached to the outer rim in first ball milling portion 111, is provided in the first support 112 First connecting hole 113 is used for the positioning and installation of the connecting rod 104, first connecting hole 113 be provided with it is multiple, and along institute The circumferential direction for stating the first ball milling portion 111 is uniformly distributed.Preferably, first connecting hole 113 is threaded hole.
Second tank body 102 include the second ball milling portion 121 and second support 122, second ball milling portion 121 for institute The identical column construction of 111 end surface shape of the first ball milling portion is stated, second is provided in the first end face in second ball milling portion 121 Ball milling chamber 152, the second ball milling chamber 152 and shape, position and quantity with the first ball in first ball milling portion 111 Mill chamber 151 is corresponding, as shown in figure 4, the first ball milling chamber 151 and the second ball milling chamber 152 are spliced to form the ball milling unit 105, it is preferable that the open edge of the first ball milling chamber 151 or the second ball milling chamber 152 is provided with sealing structure 153, makes described Ball milling unit 105 is the cavity of sealing, as shown in figure 5, the sealing structure 153 preferably in the first ball milling chamber 151 or The seal groove that the open edge of second ball milling chamber 152 is circumferentially formed along it, the interior setting sealing ring of the seal groove are sealed, institute It is preferably high quality Wear-resistant, high-temperature resistant rubber ring to state sealing ring.Second ball milling portion 121 opposite with its first end face second The first ball milling chamber 151 is provided on end face, it is preferable that the first ball milling chamber 151 and second in second ball milling portion 121 The position of ball milling chamber 152 and quantity are corresponding.Circumferentially fixed connection of the second support 122 along second ball milling portion 121 To the outer rim in second ball milling portion 121, the second connecting hole 123 is provided in the second support 122 for the connecting rod 104 positioning and installation, the quantity of second connecting hole 123 and position and the first connecting hole on first tank body 101 113 is corresponding.
The third tank body 103 include third ball milling portion 131 and third holder 132, third ball milling portion 131 for institute The first ball milling portion 111 and the identical column construction of 121 end surface shape of the second ball milling portion are stated, is provided on one end face described Second ball milling chamber 152, the second ball milling chamber 152 in third ball milling portion 131 and first ball milling portion 111 and the second ball milling The first ball milling chamber 151 in portion 121 is corresponding.Circumferentially fixed connection of the third holder 132 along third ball milling portion 131 To the outer rim in third ball milling portion 131, third connecting hole 133 is provided on the third holder 132 for the connecting rod 104 positioning and installation, it is preferable that the third connecting hole 133 is that counterbore, installation position and quantity are connect with described first Hole 113 and the second connecting hole 123 are corresponding.
The height of ball grinder provided by the invention is 7.5cm, a diameter of 5.2cm, includes at least 20 ball milling units 105.Alternatively, in other preferred embodiments, the ball grinder can also only include first tank body 101 and third tank body 103, Or it is arranged as required to one or more second tank bodies 102.
The application method of ball grinder provided by the invention:
The sample of experiment material is put into each described first ball milling chamber 151, then in the first ball milling chamber 151 Inside it is put into abrading-ball, it is preferable that be put into a diameter and be preferably the abrading-ball of 0.64cm, or be put into the smaller multiple mills of diameter The total volume of ball, the abrading-ball for being put at least one abrading-ball, and being put into each described ball milling chamber 151 is not more than institute State the one third of 105 cavity volume of ball milling unit.Experiment material put well after according to sequence from down to up successively by described One tank body 101, the second tank body 102 and third tank body 103 are stacked together, and make first connecting hole 113, the second connecting hole 123 and third connecting hole 133 be aligned, the first ball milling chamber 151 is aligned just with the second ball milling chamber 152 at this time.By the company Extension bar 104 is penetrated successively in the third connecting hole 133, the second connecting hole 123 and the first connecting hole 113, and three tank bodies are connected It is connected to and forms ball grinder together, the ball grinder is then attached to progress ball milling experiment on ball mill.
Ball grinder provided by the invention include multiple ball milling units 105, it can be achieved that disposable multiple batches of material sample ball Mill processing, meanwhile, collaboration vibration can also be realized between multiple ball milling units 105, greatly improve vibration and grinding efficiency. And the ball milling unit 105 is designed to that elliposoidal cavity can increase the kinetic energy of abrading-ball in the cavity, so as to meet The smaller abrading-ball of use quality under the premise of demand.
It should be noted that herein, relational terms such as first and second and the like are used merely to a reality Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those Element, but also include other elements that are not explicitly listed, or further include for this process, method, article or equipment Intrinsic element.In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that There is also other identical elements in process, method, article or equipment including the element.
Finally it should be noted that:Obviously, the above embodiment is merely an example for clearly illustrating the present invention, and simultaneously The non-restriction to embodiment.For those of ordinary skill in the art, it can also do on the basis of the above description Go out other various forms of variations or variation.There is no necessity and possibility to exhaust all the enbodiments.And thus drawn The obvious changes or variations that Shen goes out are still in the protection scope of this invention.

Claims (7)

1. a kind of ball grinder, which is characterized in that including the first tank body, the second tank body and third tank body, the second tank body setting Between first tank body and third tank body, and multiple ball milling lists are respectively formed between first tank body and third tank body Member, multiple ball milling units are mutually independent seal cavity;
First ball milling chamber is set on one end face of first tank body, and second tank body is set respectively on two opposite end faces The first ball milling chamber and the second ball milling chamber are set, the second ball milling chamber, first ball milling are set on an end face of the third tank body Chamber and the second ball milling chamber are spliced to form the ball milling unit.
2. ball grinder according to claim 1, which is characterized in that the opening edge of the first ball milling chamber or the second ball milling chamber Edge is provided with sealing mechanism.
3. ball grinder according to claim 1, which is characterized in that the ball milling unit is elliposoidal cavity.
4. ball grinder according to claim 3, which is characterized in that a length of 1-3cm of long axis of the elliposoidal cavity, short axle A length of 1-2cm.
5. ball grinder according to claim 1, which is characterized in that form the 6-10 ball millings between two adjacent tank bodies Unit.
6. ball grinder according to claim 1, which is characterized in that second tank body is provided with one or more.
7. ball grinder according to claim 1, which is characterized in that pass through connecting rod or threaded connection between adjacent tank body.
CN201610121418.7A 2016-03-03 2016-03-03 A kind of ball grinder Active CN105562164B (en)

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Application Number Priority Date Filing Date Title
CN201610121418.7A CN105562164B (en) 2016-03-03 2016-03-03 A kind of ball grinder

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Application Number Priority Date Filing Date Title
CN201610121418.7A CN105562164B (en) 2016-03-03 2016-03-03 A kind of ball grinder

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CN105562164B true CN105562164B (en) 2018-08-10

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106694108A (en) * 2016-12-19 2017-05-24 天津雪赢世纪专利技术有限公司 Grinding machine for cosmetics
CN111151342A (en) * 2020-01-09 2020-05-15 合肥科晶材料技术有限公司 High-flux centrifugal ball-milling tank

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EP1323472A3 (en) * 2000-07-07 2006-05-10 Symyx Technologies, Inc. Methods and apparatus for preparing an array of catalysis material
US7410804B2 (en) * 2000-07-18 2008-08-12 Uop Llc Process of parallel sample presentation
US6817558B1 (en) * 2002-04-23 2004-11-16 Uop Llc Parallel sizing, dosing and transfer assembly and method of use
ZA200504494B (en) * 2004-06-01 2006-04-26 Smith International Methods for manufacturing ultrahard cutting elements
US7763112B2 (en) * 2005-04-29 2010-07-27 Transform Pharmaceuticals, Inc. Methods and systems for co-crystal synthesis
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CN203764341U (en) * 2014-03-05 2014-08-13 山东科技大学 High-pressure ball mill
CN204503223U (en) * 2014-12-23 2015-07-29 江苏泽龙石英有限公司 A kind of ball mill of nanometer quartz powder
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