CN105561879B - Prepare the container containing energy of three-dimensional grapheme cladding single-particle Nano diamond - Google Patents
Prepare the container containing energy of three-dimensional grapheme cladding single-particle Nano diamond Download PDFInfo
- Publication number
- CN105561879B CN105561879B CN201410539302.6A CN201410539302A CN105561879B CN 105561879 B CN105561879 B CN 105561879B CN 201410539302 A CN201410539302 A CN 201410539302A CN 105561879 B CN105561879 B CN 105561879B
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- China
- Prior art keywords
- housing
- containing energy
- nano diamond
- dimensional grapheme
- destressing
- Prior art date
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/04—Pressure vessels, e.g. autoclaves
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/05—Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30
Abstract
The invention discloses a kind of container containing energy for preparing three-dimensional grapheme cladding single-particle Nano diamond, by setting the housing of composite construction to buffer the surge of reaction moment；Simultaneously by eliminating the local stress of container in hull outside setting destressing band, the anti-pressure ability and its bearing strength of the container casing containing energy are improved, extends the life-span of the container containing energy；In addition, by setting up quick-opening device, make operating personnel while control the liquid feed valve and tapping valve of housing, simplify operating procedure, shorten the operating time, save labour, improve prouctiveness, so as to meet the needs of large-scale production.The present invention have be easily installed, reliability is high, be easily installed and the advantage such as safeguards, can improve containing can container quality, meet the needs mass produced.
Description
Technical field
The present invention relates to field of chemical equipment, prepares three-dimensional grapheme cladding single-particle more specifically to one kind and receives
The container containing energy of rice diamond.
Background technology
Energetic material, explosive, propellant and the class of pyrotechnic compound three are broadly divided into by purposes, are led in civilian, military and space etc.
Domain all plays very important effect, is to have obtained the specific function material of large-scale application.Now, with the hair of nanometer technology
Exhibition and progress, many new ideas are prepared by energetic material.
So that three-dimensional grapheme coats single-particle Nano diamond as an example, graphene is made up of individual layer SP2 hydbridized carbon atoms
The cellular two-dimensional structure of hexagonal lattice, its Stability Analysis of Structures, have excellent conductive and heat-conductive characteristic, good mechanical property, because
And extensive research is obtained.Graphene has been prepared out and applied in energy storage, transparency electrode, thermo-mechanical drive etc.
Field.In order to further develop the potential application of graphene, especially in energy stores conversion aspect, except two-dimensional graphene
Outside film, three-dimensional grapheme structure also has been able to prepare, also, three-dimensional grapheme is oxide coated in recent years, carbon materials
The composites such as material start to be widely studied, for example, three-dimensional grapheme coats single-particle Nano diamond, due to three-dimensional graphite
The cladding of alkene, significantly improves the conductance for the Nano diamond material being wrapped by, and combines the good characteristic of graphene,
The electric conductivity of these compounds can be dramatically increased, and excellent performance is also shown in terms of catalysis, capacitor and energy storage,
Turn into one of physics and the international forward position of semiconductor electronic research field and focus.
The method of energetic material synthesis three-dimensional grapheme cladding single-particle Nano diamond is to utilize high energy in the prior art
Energetic material, containing that can synthesize, is generally put into the container for filling with water by rich carbon energetic material under specific high-temperature and high-pressure conditions, then
Water container is hung in containing that can trigger reactor reaction in reaction vessel to prepare solution to be purified, then passes through purification system
Three-dimensional grapheme cladding single-particle Nano diamond is extracted from solution.Wherein, high energy richness carbon energetic material generally includes three
Nitrotoleune (TNT) and RDX (RDX) or Ao Suojin (HMX) etc. mix.
The existing container containing energy (as shown in Figure 1) includes：Spheroidal housing 1 containing upper and lower ends opening and for solid
Surely the support frame 9 of spheroidal housing 1 is supported, by the adpting flange lid 3 of changeover portion 2 at the upper end open of spheroidal housing 1, with shape
Into upper end charging hole, tapping valve 8 is provided with the lower ending opening of spheroidal housing 1；Wherein, be provided with blind flange 3 control valve 7 with
And air bleeding valve 10.
Due to have high pressure and high temperature (pressure reaches 5-6 MPas, and temperature reaches 2100 degrees Celsius) in the container containing energy, especially
In reaction moment, HTHP becomes apparent, and the existing container containing energy has the defects of structure：
1. the existing container containing energy is usually single layer structure, the material of single layer enclosure includes carbon steel, clad steel or titanium steel etc.,
In reaction moment, the shell of spheroidal housing 1 is because for single layer structure, its shell is more weak, container deformation easily occurs, even
The damaged situation of container；
2. the seam crossing stress concentration of changeover portion and spheroidal housing, bearing strength is low, lacks and subtracts flushing device, causes to contain energy
Container service life is short.
Received in view of the above-mentioned problems, those skilled in the art need a kind of new three-dimensional grapheme cladding single-particle for preparing of offer badly
The container containing energy of rice diamond, so as to improve the impact resistance of the container containing energy, extend the life-span of the container containing energy, meet extensive
The needs of production.
The content of the invention
It is an object of the invention to provide it is a kind of prepare three-dimensional grapheme cladding single-particle Nano diamond containing can container,
The anti-pressure ability of the shell of tank containing energy is improved, buffering reacts the surge of moment, improves the life-span of the container containing energy.
The present invention is in order to solve the above technical problems, technical scheme is as follows：
It is a kind of to prepare the container containing energy of three-dimensional grapheme cladding single-particle Nano diamond, including contain upper and lower ends opening
Hollow spheroidal housing, pass through changeover portion adpting flange lid at the upper end open of the housing, form upper end charging hole, ball
Tapping valve is provided with the lower ending opening of shape housing, the housing is in continuous wave including internal layer shell, outer casing and section
The steel plate of shape；The Interal fixation among the internal layer shell and outer casing, the wave base of the wavy steel plate with it is described
Internal layer shell is fixedly connected, and the wave crest of the wavy steel plate is fixedly connected with the outer casing；
The junction of the housing and the changeover portion is provided with destressing steel band, and the destressing steel band is consolidated by fastener
Determine and be coated on the lateral wall of the spheroidal housing；Wherein, the maximum stress threshold value of the fastener carrying is less than described
The maximum stress threshold value of destressing steel band carrying.
Preferably, it is provided between the inlet valve and the tapping valve and is used to control inlet valve and tapping valve to link and open simultaneously
The connecting rod closed, the connecting rod include the body of rod and two ends, and two ends are consolidated with the inlet valve and the tapping valve respectively
Fixed connection；Wherein, by applying external force in the connecting rod, so that the inlet valve and tapping valve are in and opened or closed simultaneously
State.
Preferably, the destressing steel band is at least two, and the destressing steel band encloses around the spheroidal housing one
And it is interspersed on the lateral wall of the spheroidal housing.
Preferably, the spheroidal housing includes two hemispherical shells symmetrical above and below, the company of two hemispherical shells
Meet place and be provided with destressing steel band, the destressing steel band encloses around the spheroidal housing one, and is fixed on institute by fastener
On the lateral wall for stating spheroidal housing.
Preferably, the wave base of the wavy steel plate is welded with the internal layer shell, and the wave crest of the wavy steel plate
Welded with the outer casing.
Preferably, the tapping valve is inverted cone-shaped structure, the outside dimension of the tapping valve and the spheroidal housing
Lower ending opening size is adapted.
Preferably, the material of the wavy steel plate is spring steel, and the thickness of the waveform steel plate is 1cm-20cm；Institute
It is double-decker to state internal layer shell；The material of the outer casing is mild steel Q345R.
Preferably, the internal layer shell includes mild steel Q345R layers and 304 stainless steel layers.
Preferably, the material of the destressing steel band is mild steel Q345R, its with a width of 2cm~8cm, thickness be 1mm~
6mm。
The container provided by the invention containing energy for preparing three-dimensional grapheme cladding single-particle Nano diamond, it is compound by setting
The housing of structure has buffered the surge of reaction moment, by the part that container is eliminated in hull outside setting destressing band
Stress, the anti-pressure ability and its bearing strength of the container casing containing energy are improved, extend the life-span of the container containing energy；The present invention has
Be easily installed, reliability is high, be easily installed and the advantage such as safeguards, can improve containing can container quality, meet what is mass produced
Need.In addition, by setting up quick-opening device, make operating personnel while control the liquid feed valve and tapping valve of housing, i.e., by pair
Connecting rod applies external force, and inlet valve and tapping valve simplify operating procedure, when shortening operation simultaneously in the state that opens or closes
Between, labour is saved, improves prouctiveness, so as to meet the needs of large-scale production.
Brief description of the drawings
Technical scheme in order to illustrate the embodiments of the present invention more clearly, it will use below required in embodiment
Accompanying drawing is briefly described, it should be apparent that, drawings in the following description are only some embodiments of the present invention, for ability
For the those of ordinary skill of domain, on the premise of not paying creative work, it can also be obtained according to these accompanying drawings other attached
Figure.
Fig. 1 is the existing structural representation for preparing three-dimensional grapheme and coating the container containing energy of single-particle Nano diamond；
Fig. 2 is that the present invention prepares the structural representation that three-dimensional grapheme coats the container containing energy of single-particle Nano diamond；
Fig. 3 is that the present invention prepares the top view that three-dimensional grapheme coats the container containing energy of single-particle Nano diamond.
[detailed description of main elements]：
1st, housing, 2, changeover portion, 3, blind flange, 4, charging hole, 5, destressing steel band；6th, fastener, 7, inlet valve, 8, row
Liquid valve, 9, support frame, 10, air bleeding valve, 11, internal layer shell, 12, outer casing, 13, steel plate, 14 connecting rods.
Embodiment
To make present disclosure more clear understandable, below in conjunction with Figure of description, present disclosure is made into one
Walk explanation.Certainly the invention is not limited in the specific embodiment, the general replacement known to those skilled in the art
Cover within the scope of the present invention.Secondly, the present invention has carried out detailed statement using schematic diagram, real the present invention is described in detail
During example, for convenience of description, schematic diagram, should not be in this, as limitation of the invention not according to general proportion partial enlargement.
It is that the present invention prepares the container containing energy that three-dimensional grapheme coats single-particle Nano diamond to refer to Fig. 2,3, Fig. 2
Structural representation；Fig. 3 is that the present invention prepares the top view that three-dimensional grapheme coats the container containing energy of single-particle Nano diamond.
As shown in Figure 2,3, present invention offer is a kind of prepares containing and holding for three-dimensional grapheme cladding single-particle Nano diamond
Device, including the hollow spheroidal housing 1 containing upper and lower ends opening, pass through the adpting flange of changeover portion 2 at the upper end open of housing 1
Lid 3, forms upper end charging hole 4, is provided with tapping valve 8 at the lower ending opening of spheroidal housing 1, and housing 1 includes internal layer shell 11, outside
Layer housing 12 and section are in continuous wavy steel plate 13；Steel plate 13 is fixed among internal layer shell 11 and outer casing 12,
The wave base of wavy steel plate 13 is fixedly connected with internal layer shell 11, and the wave crest of wavy steel plate 13 is fixed with outer casing 12 and connected
Connect；The junction of housing 1 and changeover portion 2 is provided with destressing steel band 5, and destressing steel band 5 is fixed by fastener 6 and is coated on circle
On the lateral wall of spherical shell 1；Wherein, the maximum stress threshold value that the fastener 6 carries carries most less than destressing steel band 5
Big stress threshold.By setting the housing 1 of composite construction to buffer the surge of reaction moment, by being set in the outside of housing 1
The local stress that destressing band 5 eliminates container is put, the anti-pressure ability and its bearing strength of the container containing energy is improved, extends and contain
The life-span of energy container.
Specifically, in the present embodiment, destressing steel band 5 is at least two, and the quantity of destressing steel band 5 and position can bases
Actual conditions are arranged in the side wall of spherical shell 1.The bandwidth of destressing steel band 5 is preferably 2cm~8cm, and thickness is preferably 1mm
~6mm；The material of destressing steel band 5 is preferably mild steel Q345R.Destressing steel band 5 encloses around the spheroidal housing 1 one,
Also the regional area that spherical shell 1 can be arranged at according to being actually needed, destressing steel band 5 are interspersed in the outer of spherical shell 1
In side wall or madial wall, or the madial wall of spherical shell 1 or lateral wall set destressing steel band 5 simultaneously.In addition, fastener 6 is held
The maximum stress threshold value of load is less than the maximum stress threshold value that destressing steel band 5 carries, and can make the moment in blast, fastener 6
Preferably it is broken relative to destressing steel band 5, so as to avoid changing destressing steel band 5, that is, changes fastener 6, reduce economical
Cost, reduce loss.
Wherein, the seam crossing of spheroidal housing 1 can be provided with destressing steel band 5, and spheroidal housing 1 generally includes about two
Symmetrical hemispherical shell, and the generally connection of the junction of two hemispherical shells is more weak, therefore two hemispherical shells
Junction can be provided with destressing steel band 5, the destressing steel band 5 encloses around the spheroidal housing 1 one, and passes through fastener
6 are fixed on the lateral wall of the spheroidal housing 5, and destressing steel band 5 may also set up on the madial wall of spheroidal housing 1,
Or the madial wall or lateral wall of spheroidal housing 1 are set simultaneously.By setting destressing band, it is ensured that in detonation moment, eliminate
The local stress of container, make the bearing strength of detonation container uniform, improve the quality of detonation container.
In the present embodiment, wave base and the internal layer shell 11 of wavy steel plate 13 weld, and the wave crest of wavy steel plate 13 with
Outer casing 12 welds, and wavy steel plate 13 is fixed among inner layer case 11 and outer casing 12 with this, preferably welding side
Formula is fixed, the firm convenient quickly, and cost is relatively low simultaneously of the fixed form.In addition, the material of wavy steel plate 13 is included but not
It is limited to spring steel, its thickness is preferably 1cm-20cm；The material of outer casing 12 is preferably mild steel Q345R；The inner layer case
Body 11 is double-decker, and it includes mild steel Q345R layers and 304 stainless steel layers.By setting the housing 1 of composite construction, delay
The surge of punching reaction moment, improve life-span and the quality of the container containing energy.
In addition, in order to simplify staff's operating procedure, shorten the time, improve prouctiveness, inlet valve 7 and tapping valve 8
Between be provided with and be used to control the connecting rod 14 of inlet valve 7 and the open-shut linkage of tapping valve 8 simultaneously, connecting rod 14 includes the body of rod and two ends
Portion, two ends are fixedly connected with inlet valve 7 and tapping valve 8 respectively；Wherein, by applying external force in connecting rod 14, so that charging
Valve 7 and tapping valve 8 are in simultaneously opens or closes state.
In process of production, operating personnel apply external force in connecting rod 14, and connecting rod 14 is lifted up, then inlet valve 7 and
Tapping valve 8 is in open mode, and now, tapping valve 8 discharges the liquid in housing 1, and operating personnel will contain explosive simultaneously
Put into containing water receptacle to housing 1.Treat that discharge opeing finishes, the input containing water receptacle containing explosive finishes, operating personnel apply again
External force is added to be pressed down on connecting rod 14, then inlet valve 7 and tapping valve 8 are in closed mode, so as to carry out down in connecting rod 14
One step.Therefore, because being additionally arranged quick-opening device, while the switch of tapping valve 8 and inlet valve 7 is controlled, simplifies operating procedure,
Shorten the operating time, so as to improve prouctiveness.
The support frame 9 for fixed support spheroidal housing 1, the supporting surface of support frame 9 are additionally provided with below the container containing energy
Match with the lateral wall of spheroidal housing 1.The preferably inverted cone-shaped structure of tapping valve 8, the outside dimension and spheroidal of tapping valve 8
The lower ending opening size of housing 1 is adapted.When exploding energetic material, hang in container, lead to after high energy richness carbon explosive is assembled
Initiator detonating charge is crossed, contains energy solution to prepare, then extracts the particle containing energy from solution by purification system.
In summary, the container provided by the invention containing energy for preparing three-dimensional grapheme cladding single-particle Nano diamond, leads to
The surge for setting the housing of composite construction to buffer reaction moment is crossed, by setting destressing band to eliminate in hull outside
The local stress of container, the anti-pressure ability and its bearing strength of the container casing containing energy are improved, extend the life-span of the container containing energy；
The present invention have be easily installed, reliability is high, be easily installed and the advantage such as safeguards, can improve containing can container quality, meet greatly
The needs of large-scale production.In addition, by setting up quick-opening device, make operating personnel while control liquid feed valve and the discharge opeing of housing
Valve, i.e., by applying external force to connecting rod, inlet valve and tapping valve simplify operating procedure simultaneously in the state that opens or closes,
Shorten the operating time, save labour, improve prouctiveness, so as to meet the needs of large-scale production.
It is understood that although the present invention is disclosed as above with preferred embodiment, but above-described embodiment and it is not used to
Limit the present invention.For any those skilled in the art, without departing from the scope of the technical proposal of the invention,
Many possible changes and modifications are all made to technical solution of the present invention using the technology contents of the disclosure above, or are revised as
With the equivalent embodiment of change.Therefore, every content without departing from technical solution of the present invention, the technical spirit pair according to the present invention
Any simple modifications, equivalents, and modifications made for any of the above embodiments, still fall within the scope of technical solution of the present invention protection
It is interior.
Claims (8)
1. the container containing energy of three-dimensional grapheme cladding single-particle Nano diamond is prepared a kind of, including contains upper and lower ends opening
Hollow spheroidal housing, pass through changeover portion adpting flange lid at the upper end open of the housing, form upper end charging hole, spheroidal
Tapping valve is provided with the lower ending opening of housing, it is characterised in that
It is in continuous wavy steel plate that the housing, which includes internal layer shell, outer casing and section,；The Interal fixation is in institute
State among internal layer shell and outer casing, the wave base of the wavy steel plate is fixedly connected with the internal layer shell, and the ripple
The wave crest of wave-like steel plate is fixedly connected with the outer casing；
The junction of the housing and the changeover portion is provided with least two destressing steel bands, and the destressing steel band is around described
Spheroidal housing one is enclosed and is interspersed on the lateral wall of the spheroidal housing, and the destressing steel band is consolidated by fastener
Determine and be coated on the lateral wall of the spheroidal housing；Wherein, the maximum stress threshold value of the fastener carrying is less than described
The maximum stress threshold value of destressing steel band carrying, for protecting the destressing steel band.
2. the container according to claim 1 containing energy for preparing three-dimensional grapheme cladding single-particle Nano diamond, its feature
It is, the connecting rod for being used for controlling inlet valve and tapping valve open-shut linkage simultaneously is provided between the inlet valve and the tapping valve,
The connecting rod includes the body of rod and two ends, and two ends are fixedly connected with the inlet valve and the tapping valve respectively；Its
In, by applying external force in the connecting rod, so that the inlet valve and tapping valve are in and open or close state simultaneously.
3. the container according to claim 1 containing energy for preparing three-dimensional grapheme cladding single-particle Nano diamond, its feature
It is, the spheroidal housing includes two hemispherical shells symmetrical above and below, and the junction of two hemispherical shells, which is provided with, to be gone
Stress steel band, the destressing steel band encloses around the spheroidal housing one, and is fixed on the spheroidal shell by fastener
On the lateral wall of body.
4. the container according to claim 1 containing energy for preparing three-dimensional grapheme cladding single-particle Nano diamond, its feature
It is, wave base and the internal layer shell of the wavy steel plate weld, and the wave crest of the wavy steel plate and the outer layer
Case weld.
5. the container according to claim 1 containing energy for preparing three-dimensional grapheme cladding single-particle Nano diamond, its feature
It is, the tapping valve is the lower ending opening chi of inverted cone-shaped structure, the outside dimension of the tapping valve and the spheroidal housing
It is very little to be adapted.
6. the container according to claim 1 containing energy for preparing three-dimensional grapheme cladding single-particle Nano diamond, its feature
It is, the material of the wavy steel plate is spring steel, and the thickness of the waveform steel plate is 1cm-20cm；The internal layer shell
For double-decker；The material of the outer casing is mild steel Q345R.
7. the container according to claim 6 containing energy for preparing three-dimensional grapheme cladding single-particle Nano diamond, its feature
It is, the internal layer shell includes mild steel Q345R layers and 304 stainless steel layers.
8. the container according to claim 1 containing energy for preparing three-dimensional grapheme cladding single-particle Nano diamond, its feature
It is, the material of the destressing steel band is mild steel Q345R, and, with a width of 2cm~8cm, thickness is 1mm~6mm for it.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410539302.6A CN105561879B (en) | 2014-10-13 | 2014-10-13 | Prepare the container containing energy of three-dimensional grapheme cladding single-particle Nano diamond |
| PCT/CN2014/089418 WO2016058216A1 (en) | 2014-10-13 | 2014-10-24 | Energetic container for preparing three-dimensional graphene-covered single-particle nanodiamonds |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410539302.6A CN105561879B (en) | 2014-10-13 | 2014-10-13 | Prepare the container containing energy of three-dimensional grapheme cladding single-particle Nano diamond |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105561879A CN105561879A (en) | 2016-05-11 |
| CN105561879B true CN105561879B (en) | 2018-02-23 |
Family
ID=55746002
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410539302.6A Active CN105561879B (en) | 2014-10-13 | 2014-10-13 | Prepare the container containing energy of three-dimensional grapheme cladding single-particle Nano diamond |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN105561879B (en) |
| WO (1) | WO2016058216A1 (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108816157A (en) * | 2018-06-25 | 2018-11-16 | 江苏亮盈科技股份有限公司 | A kind of pressure vessel tooling for graphene production |
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Also Published As
| Publication number | Publication date |
|---|---|
| WO2016058216A1 (en) | 2016-04-21 |
| CN105561879A (en) | 2016-05-11 |
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