CN105561824A - Mixer - Google Patents

Mixer Download PDF

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Publication number
CN105561824A
CN105561824A CN201410532202.0A CN201410532202A CN105561824A CN 105561824 A CN105561824 A CN 105561824A CN 201410532202 A CN201410532202 A CN 201410532202A CN 105561824 A CN105561824 A CN 105561824A
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China
Prior art keywords
pipe
feed pipe
catalyst
catalyst commissioning
feed
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Granted
Application number
CN201410532202.0A
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Chinese (zh)
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CN105561824B (en
Inventor
张英民
李德华
徐�明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
QINGDAO DOUBLE-PEACH SPECIALITY CHEMICALS GROUP Co Ltd
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QINGDAO DOUBLE-PEACH SPECIALITY CHEMICALS GROUP Co Ltd
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Application filed by QINGDAO DOUBLE-PEACH SPECIALITY CHEMICALS GROUP Co Ltd filed Critical QINGDAO DOUBLE-PEACH SPECIALITY CHEMICALS GROUP Co Ltd
Priority to CN201410532202.0A priority Critical patent/CN105561824B/en
Publication of CN105561824A publication Critical patent/CN105561824A/en
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Publication of CN105561824B publication Critical patent/CN105561824B/en
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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

The invention relates to a mixer. The mixer comprises a mixer cylinder body, a first feeding tube and a catalyst feeding tube, one end of the catalyst feeding tube stretches into the first feeding tube, the mixer cylinder body is provided with a cylinder body top cover, one end of the first feeding tube is fixedly arranged in the center position of the cylinder top cover and is connected with the mixer cylinder body, the one end of the catalyst feeding tube stretching into the first feeding tube is fixedly provided with a supporting device, and the supporting device is overlapped to the inner wall of the first feeding tube. The mixer effectively prevents impact of a catalyst to mixer sealing flanges due to fracture of the catalyst feeding tube through avoiding the fracture of the catalyst feeding tube, and also prevents corrosion of phosphoric acid to the sealing flanges, induced by satisfactory uniformity of mixing of the catalyst and acetic acid steam after the fracture of the catalyst feeding tube, so the service life of the sealing flanges is prolonged, and the mixing effect is improved.

Description

A kind of blender
Technical field
The present invention relates to a kind of mixing arrangement, particularly a kind of blender.
Background technology
Current acetic acid steam and diammonium hydrogen phosphate catalyst solution reach average and mix and need to use blender, and blender catalyst commissioning pipe one end of the prior art is stretched in the first feed pipe and fed intake, and finds that catalyst commissioning pipe easily produces fracture after Long-Time Service.The reason of its fracture is catalyst commissioning pipe is that one end is fixed, and the one end stretched in the first feed pipe is not fixed, and catalyst commissioning pipe defines the longer cantilever beam of length, vibrates and rupture under the flow velocity that acetic acid steam is higher impacts.After its fracture, diammonium hydrogen phosphate catalyst solution can impact the cover flange of blender, cause cover flange to corrode, diammonium hydrogen phosphate catalyst solution after the fracture of catalyst commissioning pipe and acetic acid steam do not reach the uniformity and form phosphoric acid, exacerbate the corrosion of cover flange.Middle discovery is used on average within every 2 to 3 months, to need to change the cover flange be once corroded.
Summary of the invention
Main purpose of the present invention is to solve the problem, and provides one that catalyst commissioning pipe can be avoided to rupture, and improves the blender of blender cover flange life cycle and the mixed effect of catalyst in acetic acid steam.
For achieving the above object, technical scheme of the present invention is:
A kind of blender, comprise mixer tube, the first feed pipe and catalyst commissioning pipe, one end of described catalyst commissioning pipe is stretched in described first feed pipe, described mixer tube is provided with cylinder top cover, one end of described first feed pipe is fixed on the center of described cylinder top cover and is communicated with described mixer tube, the one end stretching into the first feed pipe at described catalyst commissioning pipe is fixed with bracing or strutting arrangement, and the inwall of described bracing or strutting arrangement and described first feed pipe overlaps.
Further, described cylinder top cover is cover flange, and described mixer tube is by being arranged on shell flange on cylinder body outer wall and cover flange is fixed, and one end of described first feed pipe is fixed on the home position of described cover flange.
Further, described first feed pipe is bend pipe, and the part that described first feed pipe and cylinder top cover are fixed is reduced pipe.
Further, also comprise the second feed pipe, described second feed pipe is fixed on described first feed pipe outer wall, in described second feed pipe, be provided with described catalyst commissioning pipe, termination and described second feed pipe of described catalyst commissioning pipe one end are fixed, and the other end stretches in described first feed pipe.
Further, the outer diameter of described catalyst commissioning pipe is equal with the inner diameter of the second feed pipe.
Further, the termination that described catalyst commissioning pipe stretches into described first feed pipe one end is arranged on the pipe axial location of described first feed pipe, and the discharging direction of described catalyst commissioning pipe is parallel with the discharging direction of the first feed pipe.
Further, between described catalyst commissioning pipe and described first feed pipe, there is certain angle, one end that described catalyst commissioning pipe stretches into described first feed pipe bends in the pipe axial location of described first feed pipe, and the part after described catalyst commissioning pipe bending is along the pipe Axis Extension of the first feed pipe.
Further, the termination of described catalyst commissioning pipe is provided with fog-spray nozzle.
Further, described bracing or strutting arrangement comprises two supports, the end winding support of every root support one end and described catalyst commissioning pipe, and the inwall of the other end and described first feed pipe overlaps, and two described supports angle is in the horizontal direction 180 °.
Further, described bracing or strutting arrangement comprises three supports, the end winding support of every root support one end and described catalyst commissioning pipe, and the inwall of the other end and described first feed pipe overlaps, and every two described supports angle is in the horizontal direction 120 °.
To sum up content, a kind of blender of the present invention, tool has the following advantages:
1, by stretching into one end fixed support device of the first feed pipe at catalyst commissioning pipe, thus make catalyst commissioning pipe change simply supported beam form into by original cantilever beam form, effectively avoid the fracture of catalyst commissioning pipe.
2, be connected by the interference fit between catalyst commissioning pipe with the second feed pipe, the cantilever beam of catalyst commissioning pipe is made to shorten (its cantilever beam length is only the part stretching into the first feed pipe), if bracing or strutting arrangement cannot support catalyst commissioning pipe, so catalyst commissioning pipe also can be effectively avoided to rupture because cantilever beam is shorter.
3, by avoiding catalyst commissioning pipe to rupture, effectively prevent because the fracture of catalyst commissioning pipe makes catalyst to the impact of blender cover flange, and prevent catalyst after the fracture of catalyst commissioning pipe and acetic acid steam does not reach the uniformity and forms the corrosion of phosphoric acid to cover flange, improve the service life of cover flange.
4, bent by the pipe axial location of catalyst commissioning pipe at the first feed pipe, and along pipe Axis Extension, make catalyst solution after the outflow of catalyst commissioning pipe, be positioned at the shaft core position of the first feed pipe, and it is parallel with the acetic acid steam steam flow direction of the first feed pipe, be conducive to mixing of catalyst solution and acetic acid steam, improve mixed effect.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention.
As shown in Figure 1, the first feed pipe 1, second feed pipe 2, catalyst commissioning pipe 3, support 4, fog-spray nozzle 5, mixer tube 6, shell flange 7, cover flange 8, mounting flange 9.
Detailed description of the invention
Below in conjunction with accompanying drawing and detailed description of the invention, the present invention is described in further detail:
As shown in Figure 1, a kind of blender, comprise mixer tube 6, first feed pipe 1, second feed pipe 2 and catalyst commissioning pipe 3, wherein the first feed pipe 1 is for carrying acetic acid steam, second feed pipe 2 is for carrying diammonium hydrogen phosphate catalyst solution, and mixer tube 6 is for both mixing.
Mixer tube 6 is fixed with cover flange 8 by the shell flange 7 be arranged on cylinder body outer wall, the first feed pipe 1 is fixed at cover flange 8 home position, first feed pipe 1 is communicated with mixer tube 6, and acetic acid steam enters mixer tube 6 by the first feed pipe 1.The outer wall of the first feed pipe 1 is fixed the second feed pipe 2, second feed pipe 2 is arranged by certain angle of inclination, catalyst commissioning pipe 3 is provided with in the second feed pipe 2, the top of catalyst commissioning pipe 3 and the top of the second feed pipe 2 are fixed by mounting flange 9, the bottom of catalyst commissioning pipe 3 is stretched in the first feed pipe 1, and diammonium hydrogen phosphate catalyst solution is conveyed into mixer tube 6.
First feed pipe 1 is bend pipe, shape is circular arc, and one end of the first feed pipe 1 is fixed on the home position of cover flange 8, and the part that the first feed pipe 1 is fixed with cover flange 8 is reduced pipe, the tube wall diameter of reduced pipe reduces gradually to inner side outside cover flange 8, tapered setting.
Bracing or strutting arrangement is fixed with in the tip position of the bottom of catalyst commissioning pipe 3, bracing or strutting arrangement comprises two supports 4, the bottom of support 4 one end and catalyst commissioning pipe 3 is welded and fixed, and the inwall of the other end and the first feed pipe 1 overlaps, and two supports 4 angle is in the horizontal direction 180 °.The bottom of catalyst commissioning pipe 3 is enable to be overlapped on the inwall of the first feed pipe 1 by two supports 4, thus make catalyst commissioning pipe 3 change simply supported beam form into by original cantilever beam form, can not produce when the first feed pipe 1 acetic acid steam flow rate is larger and rock, effectively avoid the fracture of catalyst commissioning pipe 3.
Bracing or strutting arrangement can also be three supports 4, and the bottom of every root support 4 one end and catalyst commissioning pipe 3 is welded and fixed, and the inwall of the other end and the first feed pipe 1 overlaps, and every two supports 4 angle is in the horizontal direction 120 °.Adopt three supports 4 that overlap joint can be made more firm.Support 4 should not arrange too much, and too much support 4 can affect the charging effect of the first feed pipe 1.
Support 4 and the first feed pipe 1 overlap but not are welded and fixed, because the acetic acid vapor (steam) temperature of the first feed pipe 1 reaches 300-400 DEG C, because acetic acid vapor (steam) temperature is higher, cause solder joint to rupture so support 4 can produce to expand with heat and contract with cold, and easily cause the corrosion of the first feed pipe 1 inwall and cover flange 8 after solder joint fracture.
The outer diameter of catalyst commissioning pipe 3 is equal with the inner diameter of the second feed pipe 2, by the interference fit of catalyst commissioning pipe 3 and the second feed pipe 2 support, make catalyst commissioning pipe 3 dilation connect in the second feed pipe 2, the cantilever beam of catalyst commissioning pipe 3 shortens, its cantilever beam length is only the part stretching into the first feed pipe 1, if bracing or strutting arrangement damages and cannot support for catalyst commissioning pipe 3, so because the shorter catalyst commissioning pipe 3 of also can effectively avoiding of cantilever beam of catalyst commissioning pipe 3 ruptures.
The termination that catalyst commissioning pipe 3 stretches into first feed pipe 1 one end is arranged on the pipe axial location of the first feed pipe 1, the discharging direction of catalyst commissioning pipe 3 is parallel with the discharging direction of the first feed pipe 1, make the shaft core position of catalyst solution from the position that catalyst commissioning pipe 3 flows out at the first feed pipe 1, and the discharging direction after catalyst solution flows out from the first feed pipe 1 from the discharging direction after catalyst commissioning pipe 3 flows out with acetic acid steam is parallel, is conducive to mixing of catalyst and acetic acid steam.
As shown in Figure 1, due in the present embodiment, second feed pipe 2 and catalyst commissioning pipe 3 are arranged by certain angle of inclination, and there is certain angle between the first feed pipe 1, the acetic acid steam flowed out from the first feed pipe 1 and the catalyst flowed out from catalyst commissioning pipe 3 flowing to when mixing not parallel, have impact on mixed effect, so in the present embodiment, one end that catalyst commissioning pipe 3 stretches into the first feed pipe 1 bends in the pipe axial location of the first feed pipe 1, catalyst commissioning pipe 3 after bending is along the pipe Axis Extension of the first feed pipe 1, namely catalyst commissioning pipe 3 bends the axis of rear section and the pipe dead in line of the first feed pipe 1.Catalyst solution is flowed out by this structure from catalyst commissioning pipe 3 after, be not only positioned at the shaft core position of the first feed pipe 1, also parallel with the discharging direction of the acetic acid steam flowed out from the first feed pipe 1, be conducive to mixing of catalyst and acetic acid steam.
Bracing or strutting arrangement also serves certain booster action at this, ensure that catalyst commissioning pipe 3 does not rock by bracing or strutting arrangement, enables the termination of catalyst commissioning pipe 3 remain on the pipe axial location of the first feed pipe 1.
The part that catalyst commissioning pipe 3 bends rear extension stretches in mixer tube 6, stretches on the termination in mixer tube 6 be provided with fog-spray nozzle 5 at catalyst commissioning pipe 3, and the spray direction of fog-spray nozzle 5 is identical with the discharging direction of the first feed pipe 1.
In sum, this blender is owing to arranging bracing or strutting arrangement, make catalyst commissioning pipe 3 not easy fracture, rupture by avoiding catalyst commissioning pipe 3, make catalyst solution when entering blender, torrent impact can not be carried out to the first feed pipe 1 and cover flange 8, and not rupture due to catalyst commissioning pipe 3 thus to make to mix, the mixing of acetic acid steam and catalyst is made to reach the uniformity, thus formation ammonium phosphate, avoiding corroding cover flange 8 because mixing uneven formation phosphoric acid, greatly improving the service life of cover flange 8.Bent by the pipe axial location of catalyst commissioning pipe 3 at the first feed pipe 1, and along pipe Axis Extension, make catalyst solution after catalyst commissioning pipe 3 outflow, be positioned at the shaft core position of the first feed pipe 1, and it is parallel with the acetic acid steam steam flow direction of the first feed pipe 1, be conducive to mixing of catalyst solution and acetic acid steam, improve mixed effect.
As mentioned above, plan content given by reference to the accompanying drawings, can derive similar technical scheme.In every case be the content not departing from technical solution of the present invention, any simple modification done above embodiment according to technical spirit of the present invention, equivalent variations and modification, all still belong in the scope of technical solution of the present invention.

Claims (10)

1. a blender, comprise mixer tube (6), first feed pipe (1) and catalyst commissioning pipe (3), one end of described catalyst commissioning pipe (3) is stretched in described first feed pipe (1), it is characterized in that: on described mixer tube (6), be provided with cylinder top cover, one end of described first feed pipe (1) is fixed on the center of described cylinder top cover and is communicated with described mixer tube (6), the one end stretching into the first feed pipe (1) described catalyst commissioning pipe (3) is fixed with bracing or strutting arrangement, the inwall of described bracing or strutting arrangement and described first feed pipe (1) overlaps.
2. a kind of blender according to claim 1, it is characterized in that: described cylinder top cover is cover flange (8), described mixer tube (6) is fixed with cover flange (8) by the shell flange (7) be arranged on cylinder body outer wall, and one end of described first feed pipe (1) is fixed on the home position of described cover flange (8).
3. a kind of blender according to claim 1, is characterized in that: described first feed pipe (1) is bend pipe, and the part that described first feed pipe (1) is fixed with cylinder top cover is reduced pipe.
4. a kind of blender according to claim 1, it is characterized in that: also comprise the second feed pipe (2), described second feed pipe (2) is fixed on described first feed pipe (1) outer wall, described catalyst commissioning pipe (3) is provided with in described second feed pipe (2), the termination of described catalyst commissioning pipe (3) one end and described second feed pipe (2) are fixed, and the other end stretches in described first feed pipe (1).
5. a kind of blender according to claim 4, is characterized in that: the outer diameter of described catalyst commissioning pipe (3) is equal with the inner diameter of the second feed pipe (2).
6. a kind of blender according to claim 1, it is characterized in that: the termination that described catalyst commissioning pipe (3) stretches into described first feed pipe (1) one end is arranged on the pipe axial location of described first feed pipe (1), and the discharging direction of described catalyst commissioning pipe (3) is parallel with the discharging direction of the first feed pipe (1).
7. a kind of blender according to claim 6, it is characterized in that: between described catalyst commissioning pipe (3) and described first feed pipe (1), there is certain angle, one end that described catalyst commissioning pipe (3) stretches into described first feed pipe (1) bends in the pipe axial location of described first feed pipe (1), and the part after described catalyst commissioning pipe (3) bending is along the pipe Axis Extension of the first feed pipe (1).
8. a kind of blender according to claim 1, is characterized in that: the termination of described catalyst commissioning pipe (3) is provided with fog-spray nozzle (5).
9. a kind of blender according to claim 1, it is characterized in that: described bracing or strutting arrangement comprises two supports (4), the end winding support of every root support (4) one end and described catalyst commissioning pipe (3), the inwall of the other end and described first feed pipe (1) overlaps, and two described supports (4) angle is in the horizontal direction 180 °.
10. a kind of blender according to claim 1, it is characterized in that: described bracing or strutting arrangement comprises three supports (4), the end winding support of every root support (4) one end and described catalyst commissioning pipe (3), the inwall of the other end and described first feed pipe (1) overlaps, and every two described supports (4) angle is in the horizontal direction 120 °.
CN201410532202.0A 2014-10-10 2014-10-10 A kind of mixer Active CN105561824B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410532202.0A CN105561824B (en) 2014-10-10 2014-10-10 A kind of mixer

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Application Number Priority Date Filing Date Title
CN201410532202.0A CN105561824B (en) 2014-10-10 2014-10-10 A kind of mixer

Publications (2)

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CN105561824A true CN105561824A (en) 2016-05-11
CN105561824B CN105561824B (en) 2018-07-20

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0477846A1 (en) * 1990-09-25 1992-04-01 Praxair Technology, Inc. Improved in-line gas/liquid dispersion
CN1265338A (en) * 1999-01-26 2000-09-06 英国石油化学品有限公司 Apparatus for adding fluid into process material flow
CN201678720U (en) * 2010-05-17 2010-12-22 朝阳金达钛业有限责任公司 Titanium sponge reactor feeding tube structure
CN202161980U (en) * 2011-06-13 2012-03-14 苏州浩波科技股份有限公司 Mixing device of acetic acid and catalysts in acetic acid thermal cracking reaction
CN204093334U (en) * 2014-10-10 2015-01-14 青岛双桃精细化工(集团)有限公司 A kind of blender

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0477846A1 (en) * 1990-09-25 1992-04-01 Praxair Technology, Inc. Improved in-line gas/liquid dispersion
CN1265338A (en) * 1999-01-26 2000-09-06 英国石油化学品有限公司 Apparatus for adding fluid into process material flow
CN201678720U (en) * 2010-05-17 2010-12-22 朝阳金达钛业有限责任公司 Titanium sponge reactor feeding tube structure
CN202161980U (en) * 2011-06-13 2012-03-14 苏州浩波科技股份有限公司 Mixing device of acetic acid and catalysts in acetic acid thermal cracking reaction
CN204093334U (en) * 2014-10-10 2015-01-14 青岛双桃精细化工(集团)有限公司 A kind of blender

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Inventor after: Zhang Yingmin

Inventor after: Li Dehua

Inventor after: Yang Gang

Inventor after: Tian Zhiying

Inventor before: Zhang Yingmin

Inventor before: Li Dehua

Inventor before: Xu Ming

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