CN105542696A - Preparation method of yellowing-resistant double-component ceramic repairing agent - Google Patents
Preparation method of yellowing-resistant double-component ceramic repairing agent Download PDFInfo
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- CN105542696A CN105542696A CN201610110063.1A CN201610110063A CN105542696A CN 105542696 A CN105542696 A CN 105542696A CN 201610110063 A CN201610110063 A CN 201610110063A CN 105542696 A CN105542696 A CN 105542696A
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- agent
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- repairing
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J163/00—Adhesives based on epoxy resins; Adhesives based on derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/36—Silica
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/54—Silicon-containing compounds
- C08K5/541—Silicon-containing compounds containing oxygen
- C08K5/5435—Silicon-containing compounds containing oxygen containing oxygen in a ring
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Abstract
The invention discloses a preparation method of a yellowing-resistant double-component ceramic repairing agent. The preparation method comprises steps as follows: Step one, selecting hydrogenated bisphenol A resin as a material A; Step two, selecting spherical silica powder as a material B; Step three, selecting a silane coupling agent as a material C; Step four, mixing the materials in proportion to form a mixture D; Step five, evenly mixing the mixture D, and dispersing the mixture D for two times to form a homogenous milky-white translucent dispersion E; Step six, evenly mixing an alicyclic amine epoxy curing agent ipda, a polyether amine epoxy curing agent d230 and hydrogenated bisphenol A resin to form a mixture F; Step seven, placing the dispersion E and the mixture F into integrated plastic packing rubber hoses with the volume ratio being 4:1 to be used during repair. With the adoption of the preparation method of the yellowing-resistant double-component ceramic repairing agent, the yellowing-resistant repairing agent capable of quickly and flexibly repairing tiny sintering defects such as pinholes, glaze crawling and the like on surfaces of ceramic products can be obtained, and the color of the repairing agent can be blended on site.
Description
Technical field
The present invention relates to the preparation method of a kind of color inhibition two-pack ceramics in repairing agent, belong to field of ceramic preparation technology.
Background technology
The various goods that pottery is is the material that main raw material is mixing, shaping through pulverizing and calcining is obtained with natural clay and various natural mineral; People were called pottery the article of high-temperature firing in special kiln be made into potter's clay in the past, and pottery is the general name of pottery and porcelain; Because ceramic fires to form under the high temperature of about 1300 DEG C, the generation of glaze plane defect is difficult to avoid, adopt simple, easy-operating later stage renovation technique is repaired these flaws, the yield rate of factory can be improved, factory can be reduced again defect ware is smashed, bury the expense of process, both increased the benefit for one beyond doubt, the new technology of energy-conserving and environment-protective again.
Summary of the invention
(1) technical problem that will solve
For solving the problem, the present invention proposes the preparation method of a kind of color inhibition two-pack ceramics in repairing agent, obtain a kind of on-the-spot adjustable color, ceramic surface slight flaws can be repaired as pin hole in fast and flexible ground, pinhole, the color inhibition renovation agent of the firing defects such as contracting glaze.
(2) technical scheme
The preparation method of color inhibition two-pack ceramics in repairing of the present invention agent, comprises the following steps:
The first step, selects Epalloy5000 Hydrogenated Bisphenol A resin to be material A;
Second step, selecting particle diameter to be the ball-shaped silicon micro powder of 600nm is material B;
3rd step, selects silane coupling agent 6040 for material C;
4th step, according to A:B:C=100g:130g:1g scalemic thereof material, forms mixture D;
5th step, first stirs mixture D with electric mixer, then with three roller dispersion mill dispersions twice, forms homogeneous milky white translucent dispersion E;
6th step, mixes aliphatic cyclic amine epoxy hardener ipda, polyetheramine epoxy hardener d230 and epalloy5000 according to Ipda:d230:Epalloy5000=100:30:50 ratio electric blender, forms mixture F;
7th step, is respectively charged into the mixture F in the dispersion E in the 5th step and the 6th step in the conjuncted plastic wrapping sebific duct that volumetric ratio is 4:1, uses time to be repaired.
Further, described dispersion E is the resin of repair materials.
Further, described mixture F is the solidifying agent of repair materials.
Further, the resin put in described conjuncted plastic wrapping sebific duct and curing agent component are than being 4:1.
The using method of color inhibition two-pack ceramics in repairing of the present invention agent, comprises the following steps:
The first step, the flaw part of pottery to be repaired of polishing with electric grinding machine, forms coarse pit;
Second step, appropriate healant extruded by the glue rifle supporting with conjuncted plastic wrapping sebific duct, mixes with choosing cutter;
3rd step, adds the color of colorant adjustment healant until consistent with porcelain surface color to be repaired;
4th step, scrapes into pit with thin blade by healant, makes it totally smooth;
5th step, reparation completes, and waits for spontaneous curing.
(3) beneficial effect
Compared with prior art, the preparation method of color inhibition two-pack ceramics in repairing of the present invention agent, cost is low, and repair materials of the present invention adopts resin to add the two-pack solidification pattern of solidifying agent, and dummy can spontaneous curing after finishing; Color inhibition, base mateiral selects the resin that ageing-resistant degree is high, charges and auxiliary agent, and the color inhibition phase of dummy can reach more than 15 years; Flexible to operation, on-the-spot can matching colors, without the need to applying for color customization to repair materials supplier, meeting ceramic color kind many but measure little individualized therapy demand; Repair materials, visually close to the texture of pottery, is convenient to form good repairing effect.
Embodiment
The preparation method of color inhibition two-pack ceramics in repairing of the present invention agent, comprises the following steps:
The first step, selects Epalloy5000 Hydrogenated Bisphenol A resin to be material A;
Second step, selecting particle diameter to be the ball-shaped silicon micro powder of 600nm is material B;
3rd step, selects silane coupling agent 6040 for material C;
4th step, according to A:B:C=100g:130g:1g scalemic thereof material, forms mixture D;
5th step, first stirs mixture D with electric mixer, then with three roller dispersion mill dispersions twice, forms homogeneous milky white translucent dispersion E;
6th step, mixes aliphatic cyclic amine epoxy hardener ipda, polyetheramine epoxy hardener d230 and epalloy5000 according to Ipda:d230:Epalloy5000=100:30:50 ratio electric blender, forms mixture F;
7th step, is respectively charged into the mixture F in the dispersion E in the 5th step and the 6th step in the conjuncted plastic wrapping sebific duct that volumetric ratio is 4:1, uses time to be repaired.
Described dispersion E is the resin of repair materials.
Described mixture F is the solidifying agent of repair materials.
The resin put in described conjuncted plastic wrapping sebific duct and curing agent component are than being 4:1.
The using method of color inhibition two-pack ceramics in repairing of the present invention agent, comprises the following steps:
The first step, the flaw part of pottery to be repaired of polishing with electric grinding machine, forms coarse pit;
Second step, appropriate healant extruded by the glue rifle supporting with conjuncted plastic wrapping sebific duct, mixes with choosing cutter;
3rd step, adds the color of colorant adjustment healant until consistent with porcelain surface color to be repaired;
4th step, scrapes into pit with thin blade by healant, makes it totally smooth;
5th step, reparation completes, and waits for spontaneous curing.
Embodiment recited above is only be described the preferred embodiment of the present invention, not limits the spirit and scope of the present invention.Under the prerequisite not departing from design concept of the present invention; the various modification that this area ordinary person makes technical scheme of the present invention and improvement; all should drop into protection scope of the present invention, the technology contents of request protection of the present invention, all records in detail in the claims.
Claims (5)
1. a preparation method for color inhibition two-pack ceramics in repairing agent, is characterized in that: comprise the following steps:
The first step, selects Epalloy5000 Hydrogenated Bisphenol A resin to be material A;
Second step, selecting particle diameter to be the ball-shaped silicon micro powder of 600nm is material B;
3rd step, selects silane coupling agent 6040 for material C;
4th step, according to A:B:C=100g:130g:1g scalemic thereof material, forms mixture D;
5th step, first stirs mixture D with electric mixer, then with three roller dispersion mill dispersions twice, forms homogeneous milky white translucent dispersion E;
6th step, mixes aliphatic cyclic amine epoxy hardener ipda, polyetheramine epoxy hardener d230 and Epalloy5000 according to Ipda:d230:Epalloy5000=100:30:50 ratio electric blender, forms mixture F;
7th step, is respectively charged into the mixture F in the dispersion E in the 5th step and the 6th step in the conjuncted plastic wrapping sebific duct that volumetric ratio is 4:1, uses time to be repaired.
2. the preparation method of color inhibition two-pack ceramics in repairing according to claim 1 agent, is characterized in that: described dispersion E is the resin of repair materials.
3. the preparation method of color inhibition two-pack ceramics in repairing according to claim 1 agent, is characterized in that: described mixture F is the solidifying agent of repair materials.
4. the preparation method of color inhibition two-pack ceramics in repairing according to claim 1 agent, is characterized in that: the resin put in described conjuncted plastic wrapping sebific duct and curing agent component are than being 4:1.
5. a using method for color inhibition two-pack ceramics in repairing agent, is characterized in that: comprise the following steps:
The first step, the flaw part of pottery to be repaired of polishing with electric grinding machine, forms coarse pit;
Second step, appropriate healant extruded by the glue rifle supporting with conjuncted plastic wrapping sebific duct, mixes with choosing cutter;
3rd step, adds the color of colorant adjustment healant until consistent with porcelain surface color to be repaired;
4th step, scrapes into pit with thin blade by healant, makes it totally smooth;
5th step, reparation completes, and waits for spontaneous curing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610110063.1A CN105542696A (en) | 2016-02-29 | 2016-02-29 | Preparation method of yellowing-resistant double-component ceramic repairing agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610110063.1A CN105542696A (en) | 2016-02-29 | 2016-02-29 | Preparation method of yellowing-resistant double-component ceramic repairing agent |
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| Publication Number | Publication Date |
|---|---|
| CN105542696A true CN105542696A (en) | 2016-05-04 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610110063.1A Pending CN105542696A (en) | 2016-02-29 | 2016-02-29 | Preparation method of yellowing-resistant double-component ceramic repairing agent |
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| CN (1) | CN105542696A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111962899A (en) * | 2020-07-14 | 2020-11-20 | 永旺永乐(江苏)物业服务有限公司 | Squat pit repairing process |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101314704A (en) * | 2007-05-31 | 2008-12-03 | 湖南神力实业有限公司 | Two-component epoxy resin adhesive for stone skin patching and preparation thereof |
| CN101608105A (en) * | 2008-06-17 | 2009-12-23 | 上海得荣电子材料有限公司 | Adhesive for packaging smart card module |
| CN101696264A (en) * | 2009-11-06 | 2010-04-21 | 中昊晨光化工研究院 | Epoxy resin sealing material and method for preparing same |
| CN101948667A (en) * | 2010-10-13 | 2011-01-19 | 湖南神力铃胶粘剂制造有限公司 | Adhesive for compounding marble veneer with base material and preparation method thereof |
| CN103756610A (en) * | 2013-05-13 | 2014-04-30 | 湖南柯盛新材料有限公司 | Double-component yellowing resistance epoxy resin adhesive and preparation method thereof |
| CN103756614A (en) * | 2014-01-14 | 2014-04-30 | 湖南柯盛新材料有限公司 | Modified epoxy stone back mesh adhesive and preparation method thereof |
-
2016
- 2016-02-29 CN CN201610110063.1A patent/CN105542696A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101314704A (en) * | 2007-05-31 | 2008-12-03 | 湖南神力实业有限公司 | Two-component epoxy resin adhesive for stone skin patching and preparation thereof |
| CN101608105A (en) * | 2008-06-17 | 2009-12-23 | 上海得荣电子材料有限公司 | Adhesive for packaging smart card module |
| CN101696264A (en) * | 2009-11-06 | 2010-04-21 | 中昊晨光化工研究院 | Epoxy resin sealing material and method for preparing same |
| CN101948667A (en) * | 2010-10-13 | 2011-01-19 | 湖南神力铃胶粘剂制造有限公司 | Adhesive for compounding marble veneer with base material and preparation method thereof |
| CN103756610A (en) * | 2013-05-13 | 2014-04-30 | 湖南柯盛新材料有限公司 | Double-component yellowing resistance epoxy resin adhesive and preparation method thereof |
| CN103756614A (en) * | 2014-01-14 | 2014-04-30 | 湖南柯盛新材料有限公司 | Modified epoxy stone back mesh adhesive and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111962899A (en) * | 2020-07-14 | 2020-11-20 | 永旺永乐(江苏)物业服务有限公司 | Squat pit repairing process |
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Application publication date: 20160504 |