CN105541501A - Slow/controlled-release fertilizer containing organic matters and preparation method of fertilizer - Google Patents
Slow/controlled-release fertilizer containing organic matters and preparation method of fertilizer Download PDFInfo
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- CN105541501A CN105541501A CN201610131878.8A CN201610131878A CN105541501A CN 105541501 A CN105541501 A CN 105541501A CN 201610131878 A CN201610131878 A CN 201610131878A CN 105541501 A CN105541501 A CN 105541501A
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- release
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- endoplasm
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C9/00—Fertilisers containing urea or urea compounds
- C05C9/02—Fertilisers containing urea or urea compounds containing urea-formaldehyde condensates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/30—Layered or coated, e.g. dust-preventing coatings
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Fertilizers (AREA)
Abstract
The invention relates to the technical field of slow-release fertilizer, in particular to slow/controlled-release fertilizer containing organic matters. The fertilizer comprises 65-80 parts of urea formaldehyde powder, 10-20 parts of Abamectin dregs and 5-15 parts of rice husk charcoal. Firstly, master batches are prepared from urea formaldehyde powder and 2/3 of Abamectin dregs, then the rest 1/3 Abamectin dregs and rice husk charcoal cover the master batches, and fertilizer granules are prepared. The slow-release fertilizer contains urea formaldehyde powder, Abamectin dregs and rice husk charcoal, is seldom released before 10 days and a little release before 20 days, reaches the high-speed release period after 20 days, still has efficiency after 70 days, is slow-release nitrogen fertilizer with an excellent slow-release effect, can be used for various grain crops, cash crops, vegetables and fruits, and provides richer nutrition for crops due to addition of Abamectin dregs and organic matters.
Description
Technical field
The present invention relates to slow release fertilizer technical field, particularly a kind of endoplasm slow-release or control-release fertilizer, also relate to the preparation method of described endoplasm slow-release or control-release fertilizer.
Background technology
Current agriculture main fertilizer is based on the chemical fertilizer of nitrogenous, phosphorus, potassium, can play the effect of supplementary respective element, have certain effect of increasing production to crop after using.But the utilization ratio of fertilizer is but in low-down level always, a large amount of nitrogen, phosphorus, potassium element, because release is improper for opportunity, can not be effectively utilized by crop and be trapped in soil, and nutritive element waste is serious, and causes environmental pollution.After soil life-time service chemical fertilizer, soil compaction is serious, and organic microbial reduces, even contaminated, causes soil quality to decline, and crop yield declines.
Using slowly/controlled releasing fertilizer is one of effective way alleviating fertile element loss, and the comparable common utilization rate of nitrogen fertilizer of usual slowly/controlled releasing fertilizer improves 10% ~ 30%, reduces rate of fertilizer application 15% ~ 20%.Owing to there is plurality of advantages, slowly/controlled releasing fertilizer has become the focus of fertilizer research in recent years, slowly/controlled releasing fertilizer in China's development rapidly, and achieve certain economic benefit and ecological benefits, compare the method for agronomic measures and biological pathway raising utilization rate of fertilizer, better effects if on raising utilization rate of fertilizer is promoted in the research and development of slowly/controlled releasing fertilizer, has larger advantage.Wherein urea aldehydes slow-release nitrogen fertilizer is developed successfully the earliest, realizes business-like slow release fertilizer at first, but still be the slow release fertilizer that in current world wide, amount of application is maximum, becomes the slow-release nitrogen fertilizer kind received much concern.
But now for organic fertilizer but do not have corresponding inhibition fertilizer or slow releasing function effect poor, and urea-formaldehyde fertilizer lacks natural biomass, cause there are relative merits separately, therefore, studying a kind of inhibition fertilizer containing organic fertilizer, is that in fertilizer field, demand is the most urgent.
Summary of the invention
In order to solve the problem that both that exist in above existing slow release fertilizer and organic fertilizer can not combine very well, this application provides a kind of containing organic and there is the endoplasm slow-release or control-release fertilizer of corrosion mitigating effect.
Present invention also provides the preparation method of described endoplasm slow-release or control-release fertilizer.
The present invention is achieved by the following measures:
A kind of endoplasm slow-release or control-release fertilizer, raw material weight proportioning is as follows:
Urea aldehyde powder 65-80 part, avermectin slag 10-20 part, rice hull carbon 5-15 part;
Urea aldehyde powder is obtained by following steps:
Urea is soluble in water, pH7.5-8 is regulated by buffer system, add furfural, the mol ratio of urea and furfural is 1.9:1, feeds in raw material while stir, keep temperature of reaction system 50-55 DEG C, insulation 1h, then rises to 70 DEG C by temperature of reaction system, regulation system pH5-5.5, stirring reaction 1h, by product drying and crushing to 100-200 order and get final product.
Described endoplasm slow-release or control-release fertilizer, preferred feedstock weight proportion is as follows:
Urea aldehyde powder 70-75 part, avermectin slag 13-17 part, rice hull carbon 8-12 part.
Described endoplasm slow-release or control-release fertilizer, containing organic more than 75% in preferred avermectin slag.
Described endoplasm slow-release or control-release fertilizer, preferred rice hull carbon particle diameter is 100 orders.
Described endoplasm slow-release or control-release fertilizer, preferred feedstock weight proportion is as follows:
70 parts, urea aldehyde powder, avermectin slag 17 parts, rice hull carbon 8 parts.
Described endoplasm slow-release or control-release fertilizer, preferred feedstock weight proportion is as follows:
75 parts, urea aldehyde powder, avermectin slag 13 parts, rice hull carbon 12 parts.
Described endoplasm slow-release or control-release fertilizer, preferred feedstock weight proportion is as follows:
73 parts, urea aldehyde powder, avermectin slag 15 parts, rice hull carbon 10 parts.
The preparation method of described endoplasm slow-release or control-release fertilizer, first makes master batch by the avermectin slag of urea aldehyde powder and 2/3rds, more remaining 1/3rd avermectin slags and rice hull carbon is wrapped in outside master batch and makes fertiliser granulates.
Described preparation method, preferred master batch particle diameter is 0.8-2mm.
Described preparation method, preferred fertiliser granulates particle diameter is 1-3mm.
Beneficial effect of the present invention:
Containing urea aldehyde powder, avermectin slag, rice hull carbon in the slow-release fertilizer of the application, before 10 days, release seldom, before 20 days, burst size is also little, the high speed pay-out phase is entered after 20 days, still effective after 70 days, be a kind of slow-release nitrogen fertilizer of slow release effect excellence, can use in various food crop and cash crop and veterinary antibiotics, and due to adding of avermectin slag, add organic matter, for crop provides abundanter nutrition.
Embodiment
For a better understanding of the present invention, further illustrate below in conjunction with specific embodiment.
embodiment 1:
A kind of endoplasm slow-release or control-release fertilizer, raw material weight proportioning is as follows:
65 parts, urea aldehyde powder, avermectin slag 20 parts, rice hull carbon 5 parts;
Urea aldehyde powder is obtained by following steps:
Urea is soluble in water, pH7.5-8 is regulated by buffer system, add furfural, the mol ratio of urea and furfural is 1.9:1, feeds in raw material while stir, keep temperature of reaction system 50-55 DEG C, insulation 1h, then rises to 70 DEG C by temperature of reaction system, regulation system pH5-5.5, stirring reaction 1h, by product drying and crushing to 100-200 order and get final product.
The avermectin slag of urea aldehyde powder and 2/3rds is first made the master batch that particle diameter is 0.8-2mm, more remaining 1/3rd avermectin slags and rice hull carbon are wrapped in outside master batch make the fertiliser granulates that particle diameter is 1-3mm.
embodiment 2:
A kind of endoplasm slow-release or control-release fertilizer, raw material weight proportioning is as follows:
80 parts, urea aldehyde powder, avermectin slag 10 parts, rice hull carbon 15 parts;
The preparation method of urea aldehyde powder and endoplasm slow-release or control-release fertilizer is with embodiment 1.
embodiment 3:
A kind of endoplasm slow-release or control-release fertilizer, raw material weight proportioning is as follows:
70 parts, urea aldehyde powder, avermectin slag 17 parts, rice hull carbon 8 parts;
The preparation method of urea aldehyde powder and endoplasm slow-release or control-release fertilizer is with embodiment 1.
embodiment 4:
A kind of endoplasm slow-release or control-release fertilizer, raw material weight proportioning is as follows:
75 parts, urea aldehyde powder, avermectin slag 13 parts, rice hull carbon 12 parts;
The preparation method of urea aldehyde powder and endoplasm slow-release or control-release fertilizer is with embodiment 1.
embodiment 5:
A kind of endoplasm slow-release or control-release fertilizer, raw material weight proportioning is as follows:
73 parts, urea aldehyde powder, avermectin slag 15 parts, rice hull carbon 10 parts;
The preparation method of urea aldehyde powder and endoplasm slow-release or control-release fertilizer is with embodiment 1.
comparative example 1:
Compare with embodiment 1, all urea aldehyde powder, avermectin slag, rice hull carbon are mixed together even granulation by endoplasm slow-release or control-release fertilizer in the preparation.
comparative example 2:
Compare with embodiment 1, not containing rice hull carbon in endoplasm slow-release or control-release fertilizer, the preparation method of urea aldehyde powder is with embodiment 1, the avermectin slag of urea aldehyde powder and 2/3rds is first made the master batch that particle diameter is 0.8-2mm, more remaining 1/3rd avermectin slags are wrapped in outside master batch make the fertiliser granulates that particle diameter is 1-3mm.
the water dissolution test of nitrogen
Adopt the standard in GB/T23348-2009 to carry out the lixiviate of inhibition fertilizer nutrient, in the nylon gauze of 150 μm (100 orders), take slow release fertilizer be about 10g, make pouch, pouch is sealed, 200mL water is added in 250mL Plastic Bottle or vial, cultivate in the biochemical constant incubator of 25 DEG C after sealing, sample time is 24h, 2d, 4d, 7d, 10d, 20d, 30d, 50d, 70d.The detection method of nitrogen is the method for comparative maturity in prior art, just repeats no more at this.In above-described embodiment 1-5 and comparative example 1-2 nitrogen water-soluble go out result as following table.
As can be seen from upper table data, adopt containing urea aldehyde powder, avermectin slag, rice hull carbon in slow-release fertilizer, before 10 days, release seldom, and before 20 days, burst size is also little, enters the high speed pay-out phase after 20 days, still effective after 70 days.To comparative example 1,2, there is obvious slowly-releasing advantage.
Above-described embodiment is the present invention's preferably embodiment; but embodiments of the present invention are not by the restriction of embodiment; other is any do not deviate from spirit of the present invention and principle under make change, modification, combination, substitute, simplify and all should be equivalent substitute mode, be included within protection scope of the present invention.
Claims (10)
1. an endoplasm slow-release or control-release fertilizer, is characterized in that raw material weight proportioning is as follows:
Urea aldehyde powder 65-80 part, avermectin slag 10-20 part, rice hull carbon 5-15 part;
Urea aldehyde powder is obtained by following steps:
Urea is soluble in water, pH7.5-8 is regulated by buffer system, add furfural, the mol ratio of urea and furfural is 1.9:1, feeds in raw material while stir, keep temperature of reaction system 50-55 DEG C, insulation 1h, then rises to 70 DEG C by temperature of reaction system, regulation system pH5-5.5, stirring reaction 1h, by product drying and crushing to 100-200 order and get final product.
2. endoplasm slow-release or control-release fertilizer according to claim 1, is characterized in that raw material weight proportioning is as follows:
Urea aldehyde powder 70-75 part, avermectin slag 13-17 part, rice hull carbon 8-12 part.
3. endoplasm slow-release or control-release fertilizer according to claim 1, is characterized in that in avermectin slag containing organic more than 75%.
4. endoplasm slow-release or control-release fertilizer according to claim 1, is characterized in that rice hull carbon particle diameter is 100 orders.
5. endoplasm slow-release or control-release fertilizer according to claim 1, is characterized in that raw material weight proportioning is as follows:
70 parts, urea aldehyde powder, avermectin slag 17 parts, rice hull carbon 8 parts.
6. endoplasm slow-release or control-release fertilizer according to claim 1, is characterized in that raw material weight proportioning is as follows:
75 parts, urea aldehyde powder, avermectin slag 13 parts, rice hull carbon 12 parts.
7. endoplasm slow-release or control-release fertilizer according to claim 1, is characterized in that raw material weight proportioning is as follows:
73 parts, urea aldehyde powder, avermectin slag 15 parts, rice hull carbon 10 parts.
8. the preparation method of the endoplasm slow-release or control-release fertilizer described in a claim 1-6, it is characterized in that the avermectin slag of urea aldehyde powder and 2/3rds first to make master batch, more remaining 1/3rd avermectin slags and rice hull carbon are wrapped in outside master batch make fertiliser granulates.
9. preparation method according to claim 8, is characterized in that master batch particle diameter is 0.8-2mm.
10. preparation method according to claim 8, is characterized in that fertiliser granulates particle diameter is 1-3mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610131878.8A CN105541501A (en) | 2016-03-09 | 2016-03-09 | Slow/controlled-release fertilizer containing organic matters and preparation method of fertilizer |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610131878.8A CN105541501A (en) | 2016-03-09 | 2016-03-09 | Slow/controlled-release fertilizer containing organic matters and preparation method of fertilizer |
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| CN105541501A true CN105541501A (en) | 2016-05-04 |
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| CN201610131878.8A Pending CN105541501A (en) | 2016-03-09 | 2016-03-09 | Slow/controlled-release fertilizer containing organic matters and preparation method of fertilizer |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110423163A (en) * | 2019-09-03 | 2019-11-08 | 河北农业大学 | A kind of corn slow-release or control-release fertilizer |
| CN111470906A (en) * | 2020-05-21 | 2020-07-31 | 山东省农业科学院生物技术研究中心 | Special controlled-release microbial fertilizer for peanuts in continuous cropping field and preparation method thereof |
| CN111517897A (en) * | 2020-05-21 | 2020-08-11 | 山东省农业科学院生物技术研究中心 | Controlled-release bacterial fertilizer special for peanuts and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101462909A (en) * | 2009-01-14 | 2009-06-24 | 黑龙江八一农垦大学 | Preparation of avermectin slag fertilizer |
| CN102603429A (en) * | 2012-03-31 | 2012-07-25 | 孙玉珂 | Crop fertilizer applicable to saline-alkali soil and preparation method of crop fertilizer |
| CN104447063A (en) * | 2014-12-24 | 2015-03-25 | 上海大洋生态有机肥有限公司 | Urea formaldehyde carbon base compound fertilizer and clearance type preparation method thereof |
| CN104973929A (en) * | 2015-05-05 | 2015-10-14 | 马鞍山科邦生态肥有限公司 | Biomass charcoal-enveloped controlled-release fertilizer and preparation method thereof |
-
2016
- 2016-03-09 CN CN201610131878.8A patent/CN105541501A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101462909A (en) * | 2009-01-14 | 2009-06-24 | 黑龙江八一农垦大学 | Preparation of avermectin slag fertilizer |
| CN102603429A (en) * | 2012-03-31 | 2012-07-25 | 孙玉珂 | Crop fertilizer applicable to saline-alkali soil and preparation method of crop fertilizer |
| CN104447063A (en) * | 2014-12-24 | 2015-03-25 | 上海大洋生态有机肥有限公司 | Urea formaldehyde carbon base compound fertilizer and clearance type preparation method thereof |
| CN104973929A (en) * | 2015-05-05 | 2015-10-14 | 马鞍山科邦生态肥有限公司 | Biomass charcoal-enveloped controlled-release fertilizer and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110423163A (en) * | 2019-09-03 | 2019-11-08 | 河北农业大学 | A kind of corn slow-release or control-release fertilizer |
| CN111470906A (en) * | 2020-05-21 | 2020-07-31 | 山东省农业科学院生物技术研究中心 | Special controlled-release microbial fertilizer for peanuts in continuous cropping field and preparation method thereof |
| CN111517897A (en) * | 2020-05-21 | 2020-08-11 | 山东省农业科学院生物技术研究中心 | Controlled-release bacterial fertilizer special for peanuts and preparation method thereof |
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Application publication date: 20160504 |
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