CN105541196A - High-strength copper artware clay sculpture material and preparation method thereof - Google Patents
High-strength copper artware clay sculpture material and preparation method thereof Download PDFInfo
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- CN105541196A CN105541196A CN201510939941.6A CN201510939941A CN105541196A CN 105541196 A CN105541196 A CN 105541196A CN 201510939941 A CN201510939941 A CN 201510939941A CN 105541196 A CN105541196 A CN 105541196A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00956—Uses not provided for elsewhere in C04B2111/00 for making sculptures or artistic casts
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- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
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Abstract
The invention discloses a high-strength copper artware clay sculpture material and a preparation method thereof. The preparation method comprises 1, immersing straw and cotton in a nitric acid solution, filtering the solution and carrying out cleaning to obtain filter cake, 2, mixing loess, kaolin, bentonite, corn flour, polyvinyl alcohol, xanthan gum, stearin, 3-methyl-1-butyn-2-ol and water and carrying out aging to obtain an aging product, and 3, mixing the aging product, the filter cake, methylcellulose and borax, carrying out stewing and carrying out cooling to obtain the high-strength copper artware clay sculpture material. A clay sculpture product obtained through the high-strength copper artware clay sculpture material has excellent mechanical strength.
Description
Technical field
The present invention relates to clay sculpture, particularly, relate to a kind of high-strength copper skill clay sculpture material and preparation method thereof.
Background technology
Clay sculpture is a requisite process in copper artware making processes, the predecessor of every part copper artware needs a clay sculpture prototype, clay sculpture be all through sculptors repeatedly try to figure out on the basis of Original Architectural Design original text, weigh after carry out create again, the moulding quality of clay sculpture, the embodiment of romantic charm are whether, the expression of intention presents directly impact product quality from now on, and an outstanding copper is carved product and be unable to do without outstanding sculptors.Clay sculpture concrete operation step has, sculpture clay get the raw materials ready screening, water spray wake up mud, take and make skeleton, holder mud device, upper large mud, moulding.From then on the stage start clay sculpture constantly spray water keep do not ftracture, the halfway general holiday wants covered with plastic film to carry out moisturizing until sculpture mould completes, and finally carries out drying in the shade with obtained clay sculpture finished product.
At present, often there is the situation of breaking in the clay sculpture finished product obtained by aforesaid method, and then substantially increase production cost in the process of carrying or turning over molding jig.
Summary of the invention
The object of this invention is to provide a kind of high-strength copper skill clay sculpture material and preparation method thereof, the clay sculpture goods obtained by this clay sculpture material have excellent mechanical strength.
To achieve these goals, the invention provides a kind of preparation method of high-strength copper skill clay sculpture material, comprising:
1) straw and cotton are soaked in salpeter solution, then filter, clean to obtain filter cake;
2) ripening is carried out with obtained ageing product by after loess, white clay, wilkinite, Semen Maydis powder, polyvinyl alcohol, xanthan gum, stearin, 3-methyl isophthalic acid-butine-3-alcohol and water mixing;
3) ageing product, filter cake, methylcellulose gum are mixed with borax, and carry out boiling, then cool with obtained high-strength copper skill clay sculpture material.
Present invention also offers a kind of high-strength copper skill clay sculpture material, this high-strength copper skill clay sculpture material is obtained by the preparation of above-mentioned method.
By technique scheme, the present invention makes the high-strength copper skill clay sculpture material obtained by the synergy of straw, cotton, loess, white clay, wilkinite, Semen Maydis powder, polyvinyl alcohol, xanthan gum, stearin, 3-methyl isophthalic acid-butine-3-alcohol, methylcellulose gum and borax and water, ripening and boiling.The clay sculpture goods mechanical strength obtained by this clay sculpture material, to prevent the generation of the situation of breaking, drastically increases the working efficiency of operator, also plays the effect reducing production cost simultaneously.
Other features and advantages of the present invention are described in detail in embodiment part subsequently.
Embodiment
Below the specific embodiment of the present invention is described in detail.Should be understood that, embodiment described herein, only for instruction and explanation of the present invention, is not limited to the present invention.
The invention provides a kind of preparation method of high-strength copper skill clay sculpture material, comprising:
1) straw and cotton are soaked in salpeter solution, then filter, clean to obtain filter cake;
2) ripening is carried out with obtained ageing product by after loess, white clay, wilkinite, Semen Maydis powder, polyvinyl alcohol, xanthan gum, stearin, 3-methyl isophthalic acid-butine-3-alcohol and water mixing;
3) ageing product, filter cake, methylcellulose gum are mixed with borax, and carry out boiling, then cool with obtained high-strength copper skill clay sculpture material.
In step 1 of the present invention) in, the consumption of each material can be selected in wide scope, but in order to improve the obtained clay sculpture goods mechanical strength of this clay sculpture material further, preferably, in step 1) in, relative to the straw of 1 weight part, the consumption of cotton is 0.7-1.4 weight part, and the pH of salpeter solution is 4.5-6.Further preferably, relative to the straw of 1 weight part, the consumption of salpeter solution is 20-30 weight part.
In step 1 of the present invention) in, the condition of soaking can be selected in wide scope, but in order to improve the obtained clay sculpture goods mechanical strength of this clay sculpture material further, preferably, soak and at least meet the following conditions: soaking temperature is 15-35 DEG C, and soak time is 10-15h.
In step 2 of the present invention) in, the consumption of each material can be selected in wide scope, but in order to improve the obtained clay sculpture goods mechanical strength of this clay sculpture material further, preferably, in step 2) in, relative to the loess of 100 weight parts, the consumption of white clay is 9-15 weight part, bentonitic consumption is 15-18 weight part, the consumption of Semen Maydis powder is 6-7 weight part, the consumption of polyvinyl alcohol is 15-23 weight part, the consumption of xanthan gum is 1.2-3.2 weight part, the consumption of stearin is 1.1-1.9 weight part, the consumption of 3-methyl isophthalic acid-butine-3-alcohol is 0.5-1.1 weight part, the consumption of water is 120-150 weight part.
In step 2 of the present invention) in, the weight-average molecular weight of loess, white clay and bentonitic particle diameter and polyvinyl alcohol can be selected in wide scope, but in order to improve the obtained clay sculpture goods mechanical strength of this clay sculpture material further, preferably, in loess, white clay and wilkinite, the particle diameter of any one or many persons is 20-30 μm; The weight-average molecular weight of polyvinyl alcohol is 3000-4500.
In step 2 of the present invention) in, the condition of ripening can be selected in wide scope, but in order to improve the obtained clay sculpture goods mechanical strength of this clay sculpture material further, preferably, ripening at least meets the following conditions: Aging Temperature is 35-45 DEG C, and digestion time is 2-3 days.
In step 3 of the present invention) in, the consumption of each material can be selected in wide scope, but in order to improve the obtained clay sculpture goods mechanical strength of this clay sculpture material further, preferably, in step 3) in, relative to the ageing product of 100 weight parts, the consumption of filter cake is 16-21 weight part, the consumption of methylcellulose gum is 6.5-8 weight part, and the consumption of borax is 3-8 weight part.
In step 3 of the present invention) in, the condition of boiling can be selected in wide scope, but in order to improve the obtained clay sculpture goods mechanical strength of this clay sculpture material further, preferably, boiling at least meets the following conditions: boiling temperature is 150-200 DEG C, and cooking time is 5-6h.
In step 3 of the present invention) in, the temperature of cooling can be selected in wide scope, but in order to improve the obtained clay sculpture goods mechanical strength of this clay sculpture material further, preferably, the temperature of cooling is 15-35 DEG C.
Present invention also offers a kind of high-strength copper skill clay sculpture material, this high-strength copper skill clay sculpture material is obtained by the preparation of above-mentioned method.
Below will be described the present invention by embodiment
Embodiment 1
1) at 25 DEG C, straw, cotton and salpeter solution (pH is 5) mixed according to the weight ratio of 1:1:25 and soak 13h, then filtering, clean to obtain filter cake;
2) loess (particle diameter is 25 μm), white clay (particle diameter is 25 μm), wilkinite (particle diameter is 25 μm), Semen Maydis powder, polyvinyl alcohol, xanthan gum, stearin, 3-methyl isophthalic acid-butine-3-alcohol and water are mixed according to the weight ratio of 100:12:16:6.5:19:2:1.5:0.8:130, then at 40 DEG C ripening 2.5 days with obtained ageing product;
3) described ageing product, filter cake, methylcellulose gum are mixed with the weight ratio of borax according to 100:18:7:6, and carry out boiling 5.5h in 180 DEG C, then cool at 25 DEG C with obtained high-strength copper skill clay sculpture materials A 1.
Embodiment 2
1) at 15 DEG C, straw, cotton and salpeter solution (pH is 4.5) mixed according to the weight ratio of 1:0.7:20 and soak 10h, then filtering, clean to obtain filter cake;
2) loess (particle diameter is 20 μm), white clay (particle diameter is 20 μm), wilkinite (particle diameter is 20 μm), Semen Maydis powder, polyvinyl alcohol, xanthan gum, stearin, 3-methyl isophthalic acid-butine-3-alcohol and water are mixed according to the weight ratio of 100:9:15:6:15:1.2:1.1:0.5:120, then at 35 DEG C ripening 2 days with obtained ageing product;
3) described ageing product, filter cake, methylcellulose gum are mixed with the weight ratio of borax according to 100:16:6.5:3, and carry out boiling 5h in 150 DEG C, then cool at 15 DEG C with obtained high-strength copper skill clay sculpture materials A 2.
Embodiment 3
1) at 35 DEG C, straw, cotton and salpeter solution (pH is 6) mixed according to the weight ratio of 1:1.4:30 and soak 15h, then filtering, clean to obtain filter cake;
2) loess (particle diameter is 30 μm), white clay (particle diameter is 30 μm), wilkinite (particle diameter is 30 μm), Semen Maydis powder, polyvinyl alcohol, xanthan gum, stearin, 3-methyl isophthalic acid-butine-3-alcohol and water are mixed according to the weight ratio of 100:15:18:7:23:3.2:1.9:1.1:150, then at 45 DEG C ripening 3 days with obtained ageing product;
3) described ageing product, filter cake, methylcellulose gum are mixed with the weight ratio of borax according to 100:21:8:8, and carry out boiling 6h in 200 DEG C, then cool at 35 DEG C with obtained high-strength copper skill clay sculpture materials A 3.
Comparative example 1
Carry out obtained copper skill clay sculpture material B 1 according to the method for embodiment 1, unlike, step 1) in do not use straw.
Comparative example 2
Carry out obtained copper skill clay sculpture material B 2 according to the method for embodiment 1, unlike, step 1) in do not use cotton.
Comparative example 3
Carry out obtained copper skill clay sculpture material B 3 according to the method for embodiment 1, unlike, step 1) in do not use white clay.
Comparative example 4
Carry out obtained copper skill clay sculpture material B 4 according to the method for embodiment 1, unlike, step 1) in do not use wilkinite.
Comparative example 5
Carry out obtained copper skill clay sculpture material B 5 according to the method for embodiment 1, unlike, step 1) in do not use Semen Maydis powder.
Comparative example 6
Carry out obtained copper skill clay sculpture material B 6 according to the method for embodiment 1, unlike, step 1) in do not use xanthan gum.
Comparative example 7
Carry out obtained copper skill clay sculpture material B 7 according to the method for embodiment 1, unlike, step 1) in do not use methylcellulose gum.
Application examples 1
First copper skill clay sculpture material and water to be sprayed water the mud 24h that wakes up according to the weight ratio of 100:50 by above-mentioned copper skill clay sculpture material, then carry out moulding, then surface sprinkling moisturizing (4 times/day is carried out, continue 3 days, relative to the copper skill clay sculpture material of 100g, each injection flow rate is 5-10g), dry in the shade at being finally placed in 15 DEG C, within 20 days, detect the ultimate compression strength (MPa) of each clay sculpture afterwards, concrete outcome is in table 1.
Table 1
Known by above-described embodiment, comparative example and application examples, copper skill clay sculpture material provided by the invention has excellent mechanical strength characteristics.
More than describe the preferred embodiment of the present invention in detail; but the present invention is not limited to the detail in above-mentioned embodiment, within the scope of technical conceive of the present invention; can carry out multiple simple variant to technical scheme of the present invention, these simple variant all belong to protection scope of the present invention.
It should be noted that in addition, each concrete technical characteristic described in above-mentioned embodiment, in reconcilable situation, can be combined by any suitable mode, in order to avoid unnecessary repetition, the present invention illustrates no longer separately to various possible array mode.
In addition, also can carry out arbitrary combination between various different embodiment of the present invention, as long as it is without prejudice to thought of the present invention, it should be considered as content disclosed in this invention equally.
Claims (10)
1. a preparation method for high-strength copper skill clay sculpture material, is characterized in that, comprising:
1) straw and cotton are soaked in salpeter solution, then filter, clean to obtain filter cake;
2) ripening is carried out with obtained ageing product by after loess, white clay, wilkinite, Semen Maydis powder, polyvinyl alcohol, xanthan gum, stearin, 3-methyl isophthalic acid-butine-3-alcohol and water mixing;
3) described ageing product, filter cake, methylcellulose gum are mixed with borax, and carry out boiling, then cool with obtained high-strength copper skill clay sculpture material.
2. preparation method according to claim 1, wherein, in step 1) in, relative to the described straw of 1 weight part, the consumption of described cotton is 0.7-1.4 weight part, and the pH of described salpeter solution is 4.5-6.
3. preparation method according to claim 2, wherein, relative to the described straw of 1 weight part, the consumption of described salpeter solution is 20-30 weight part;
Preferably, described immersion at least meets the following conditions: soaking temperature is 15-35 DEG C, and soak time is 10-15h.
4. according to the preparation method in claim 1-3 described in any one, wherein, in step 2) in, relative to the described loess of 100 weight parts, the consumption of described white clay is 9-15 weight part, described bentonitic consumption is 15-18 weight part, the consumption of described Semen Maydis powder is 6-7 weight part, the consumption of described polyvinyl alcohol is 15-23 weight part, the consumption of described xanthan gum is 1.2-3.2 weight part, the consumption of described stearin is 1.1-1.9 weight part, the consumption of described 3-methyl isophthalic acid-butine-3-alcohol is 0.5-1.1 weight part, the consumption of described water is 120-150 weight part.
5. preparation method according to claim 4, wherein, in described loess, white clay and wilkinite, the particle diameter of any one or many persons is 20-30 μm; The weight-average molecular weight of described polyvinyl alcohol is 3000-4500.
6. preparation method according to claim 5, wherein, described ripening at least meets the following conditions: Aging Temperature is 35-45 DEG C, and digestion time is 2-3 days.
7. according to the preparation method in claim 1-3,5 and 6 described in any one, wherein, in step 3) in, relative to the described ageing product of 100 weight parts, the consumption of described filter cake is 16-21 weight part, the consumption of described methylcellulose gum is 6.5-8 weight part, and the consumption of described borax is 3-8 weight part.
8. preparation method according to claim 7, wherein, described boiling at least meets the following conditions: boiling temperature is 150-200 DEG C, and cooking time is 5-6h.
9. preparation method according to claim 7, wherein, the temperature of described cooling is 15-35 DEG C.
10. a high-strength copper skill clay sculpture material, is characterized in that, described high-strength copper skill clay sculpture material is obtained by the method preparation in claim 1-9 described in any one.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510939941.6A CN105541196A (en) | 2015-12-15 | 2015-12-15 | High-strength copper artware clay sculpture material and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510939941.6A CN105541196A (en) | 2015-12-15 | 2015-12-15 | High-strength copper artware clay sculpture material and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE20002125U1 (en) * | 2000-02-07 | 2000-05-18 | Sackschewski, Petra, 47918 Tönisvorst | Figures made of plant pot elements |
| CN1600575A (en) * | 2003-09-24 | 2005-03-30 | 谢海军 | Method for fabricating copper plated sculpture at size of 1-1.5 m from steel, sculpture clay and resin glue daub |
| CN104261794A (en) * | 2014-09-16 | 2015-01-07 | 吴持跃 | Handicraft clay sculpture material and preparation method thereof |
| CN104261777A (en) * | 2014-09-16 | 2015-01-07 | 吴持跃 | Clay sculpture Buddha repair material and preparation method thereof |
-
2015
- 2015-12-15 CN CN201510939941.6A patent/CN105541196A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE20002125U1 (en) * | 2000-02-07 | 2000-05-18 | Sackschewski, Petra, 47918 Tönisvorst | Figures made of plant pot elements |
| CN1600575A (en) * | 2003-09-24 | 2005-03-30 | 谢海军 | Method for fabricating copper plated sculpture at size of 1-1.5 m from steel, sculpture clay and resin glue daub |
| CN104261794A (en) * | 2014-09-16 | 2015-01-07 | 吴持跃 | Handicraft clay sculpture material and preparation method thereof |
| CN104261777A (en) * | 2014-09-16 | 2015-01-07 | 吴持跃 | Clay sculpture Buddha repair material and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 朱洪法: "《催化剂载体制备及应用技术（第二版）》", 31 October 2014 * |
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Application publication date: 20160504 |