CN105534712A - Industrialized processing technology of traditional Chinese medicine decoction pieces simmering fresh ginger - Google Patents
Industrialized processing technology of traditional Chinese medicine decoction pieces simmering fresh ginger Download PDFInfo
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- CN105534712A CN105534712A CN201510912346.3A CN201510912346A CN105534712A CN 105534712 A CN105534712 A CN 105534712A CN 201510912346 A CN201510912346 A CN 201510912346A CN 105534712 A CN105534712 A CN 105534712A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
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Abstract
The invention discloses an industrialized processing technology of traditional Chinese medicine decoction pieces simmering fresh ginger. The processing method comprises: taking fresh ginger, selecting and grading, cleaning the fresh ginger by clear water, draining water, using wet paper to pack the fresh ginger, the top ends or small ends facing upward in a unified manner, placing the fresh ginger on the object placing frame in an automatic temperature controlled traditional Chinese medicine roasting processing stove, adding a heat-transfer medium until the stove body of the roasting processing stove is fully filled, according to differences of the top ends and the small ends of the fresh ginger, respectively heating assemblies distributed on the upper and lower parts and/or left and right parts, to heat, wherein the temperature setting of the heating assembly on the side close to the top end of the fresh ginger is higher than that of the heating assembly on the side of the small end, starting a temperature control unit, setting time and temperature according to a temperature programming method, simmering to specified processing time, after cooling to room temperature, taking the fresh ginger out, removing the paper, cutting the fresh ginger into thick slices in thickness of 2-3 mm, screening out dusts, to obtain simmered fresh ginger. The processing temperature can be accurately controlled, production environment is closed, and production environment satisfies GMP requirements, and the method is beneficial for improving production efficiency.
Description
Technical field
The invention belongs to pharmaceutical technology sectors, relate to a kind of processing procedure simmering Chinese medicine processed, be specifically related to a kind of prepared slices of Chinese crude drugs and simmer the industrialized processing procedure of Rhizoma Zingiberis Recens.
Background technology
Stewing method is the concocting method often used in Chinese medicine processing, is directly or with wetted surface, l Water Paper to be wrapped up by medicine, is embedded in showing tremendous enthusiasm ash, or Pulvis Talci, or the concocting method of slowly heating in Testa Tritici is called stewing method.Its object mainly reduces toxic and side effects, or relaxes the property of medicine, or strengthens drug effect.Roast Rhizoma Zingiberis Recens is the Rhizoma Zingiberis Recens processed product adopting simmer method to prepare." Zhenglei Bencao " carries: " simmer Rhizoma Zingiberis Recens silk floss to wrap up in, receive in bottom, cold namely easily it." " pavilion qi rescues just opinion " say: " the warm taste of stewing person master, property master keeps." " book on Chinese herbal medicine is just read " cloud: " simmer ripe, without the property of dispersing.But can warming middle-JIAO to send down the adverse QI.Control cold stagnant stomachache." the stupid Zeng Yun of stone: " and Rhizoma Zingiberis Recens is simmered ripe, falls and does not rise, only stomachache let out profit, hold up temper, loose pathogen, therefore XIAOYAO POWDER uses it." Wu Yiluo also cloud: " Roast Rhizoma Zingiberis Recens and middle preventing or arresting vomiting, fear it with Rhizoma Zingiberis Recens and fall apart, and fears that it is dry with Rhizoma Zingiberis, and only this is slightly not dry loose." Roast Rhizoma Zingiberis Recens is extensive at Popular Utilization.Namely Rhizoma Zingiberis Recens to induce sweat declines after simmering system, and some volatile and stimulating component in removing medicine, make its property of medicine relax, and is mainly used in warming middle-JIAO to arrest vomiting and stomachache is had loose bowels.There are some researches show, Rhizoma Zingiberis Recens can significantly shorten mice bleeding time and clotting time after simmering, and is conducive to the generation of hemostatic compositions in Rhizoma Zingiberis Recens.But, owing to still adopting Conventional wisdom method when simmering system processing medical material, it concocts the duration and degree of heating and the time is not easily grasped, simmer technological parameter processed to be difficult to quantize, easily burn, burn out medical material, do not meet current Good and produce GMP requirement, be difficult to realize industrialized great production, cause stewing method to be on the verge of in modern Chinese medicine processing technique lost.Therefore, the stewing Rhizoma Zingiberis Recens industrialization processing procedure that exploitation adapts to modern GMP requirement is a difficult problem urgently to be resolved hurrily, simmers method processing technique have important practice significance to Inheritance＆ development Chinese medicine.
Summary of the invention
For above-mentioned the deficiencies in the prior art, the invention provides a kind of prepared slices of Chinese crude drugs and simmer the industrialization processing procedure of Rhizoma Zingiberis Recens, there is parameter controllable precise, production technology favorable reproducibility and meet the features such as national GMP production requirement.
The technical solution used in the present invention is:
An industrialization processing procedure for Rhizoma Zingiberis Recens simmered by the prepared slices of Chinese crude drugs, and concocting method is as follows:
(1), get Rhizoma Zingiberis Recens, select stepping, clear water is cleaned, and drain the water to obtain the obtained thing of step (1);
(2), the obtained thing l Water Paper of step (1) is wrapped, with top or unified upward with small end, be placed on the rack in temperature automatically controlled Chinese medicine stewing stove processed, add heat transfer medium and simmer furnace body processed to filling, different according to Rhizoma Zingiberis Recens top and small end, arrange up and down and/or the heating-up temperature of the heating component of left and right distribution respectively, heating component temperature wherein near side, Rhizoma Zingiberis Recens top is arranged need higher than its small end side, open temp control unit simultaneously, follow procedure heating mode setup times and temperature, simmer the concocted time of system to regulation, to be cooled to room temperature, take out Rhizoma Zingiberis Recens, removing paper, obtain the obtained thing of step (2),
(3), get the obtained thing of step (2), cut 2-3mm sheet, sieve dedust bits, to obtain final product.
Further, in step (2), Rhizoma Zingiberis Recens top upward, small end down, on the rack, adopt temperature-programmed mode, the stewing time and the temperature that arrange heating component are 0-1 hour, 110-130 DEG C in even placement, 1-2 hour, 160-200 DEG C, 2-5 hour, 270-330 DEG C; The stewing time of lower heating component and temperature are 0-1 hour, 90-120 DEG C, 1-2 hour, 140-180 DEG C, 2-5 hour, 240-300 DEG C.
Preferably, upper and lower heating component temperature is set to, the stewing time of upper heating component and temperature are 0-1 hour, 115-125 DEG C, 1-2 hour, 170-190 DEG C, 2-5 hour, 290-310 DEG C; The stewing time of lower heating component and temperature are 0-1 hour, 100-110 DEG C, 1-2 hour, 150-170 DEG C, 2-5 hour, 270-290 DEG C.
Heat transfer medium is preferably plant ashes, and more preferably thin bran is grey.
This technique simmers stove processed by temperature automatically controlled Chinese medicine to realize.Temperature automatically controlled Chinese medicine is simmered stove processed and is comprised cover plate, body of heater and heating system, in body of heater up and down and/or left and right be provided with heating component, each heating component comprises heating part and temperature sensing portion, the control circuit of heating component and control chamber connects to form heating system, each heating component has independently temperature control unit, control chamber is arranged on the outside of body of heater, is provided with rack in body of heater, rack put the thing scope of operation between each heating component.
Preferably have on inboard wall of furnace body and be respectively provided with a set of heating component, the thing scope of operation of putting of rack is overlapped between the heating part of heating components upper and lower two.Thermal insulation layer is provided with between body of heater body wall.Rack is evenly provided with and puts thing hole.
Between the heating part of upper and lower two cover heating components, spacing distance is 8-50cm up and down.
The heating part of heating component is electrothermal tube, and the temperature sensing portion of heating component is temperature sensor; A temperature sensor and an electrothermal tube composition one independently heating component, independently heating component is connected with the independently temperature control unit circuit of control chamber.Electrothermal tube is U-shaped, W type, snakelike, screw type heating tube or finned, flange form, threaded heating tube.
Advantage of the present invention:
(1) production environment adapts to GMP requirement.Traditional method bran coat is fuel, and greatly, production environment is severe, and cannot meet the clean requirement of GMP to pharmaceutical production environment, traditional method is on the verge of lost for smog and dust.The thermal source of temperature automatically controlled stewing stove processed adopts electric heating, and production environment is airtight, and production environment can meet GMP requirement.
(2) processing parameter controls.The technological parameter of traditional method depends on the experience of operator, obviously random, especially cannot grasp firepower size during bran coat burning, and the little then Rhizoma Zingiberis Recens difficulty of fire is simmered thoroughly, and the too large then easy carbonization of Rhizoma Zingiberis Recens of fire, so product difference between batch is large.Temperature automatically controlled stewing stove processed by upper and lower two can accurate temperature controlling heating tube heat, the processing parameter such as firepower, time is accurately controlled, and product difference between batch obviously reduces, and easily meets GMP production requirement, can realize suitability for industrialized production.
(3) labor intensity significantly reduces.Adopt traditional method to need a few individual to supervise stewing process in turn, need pay close attention to the change of firepower, add bran coat in time, labor intensity is large.And adopting temperature automatically controlled stewing stove processed only to need people watch-dog ruuning situation at any time, labor intensity is little, and production cost declines.
Accompanying drawing explanation
Fig. 1 is that embodiment of the present invention 16-gingerol reference substance HPLC schemes.
Fig. 2 is the embodiment of the present invention 1 Rhizoma Zingiberis Recens raw product decoction pieces HPLC figure.
Fig. 3 is that Rhizoma Zingiberis Recens (Traditional Method) decoction pieces HPLC figure simmers in the embodiment of the present invention 1 Jianchang side.
Fig. 4 is that side stewing Rhizoma Zingiberis Recens (modern method) decoction pieces HPLC in the embodiment of the present invention 1 Jianchang schemes.
Fig. 5 is the structural representation that stove processed simmered by temperature automatically controlled Chinese medicine.
Fig. 6 is the structural representation of rack.
Reference numeral: A is 6-gingerol, cover plate 1, body of heater 2, thermal insulation layer 3, temperature sensor 4, electrothermal tube 5, control chamber 6, display window 7, switch 8, and thing hole 10 put by rack 9.
Detailed description of the invention
Tie with specific embodiment that the present invention is described further below.
Embodiment 1
One, in the present embodiment, the stewing control equipment of employing is that stove processed simmered by temperature automatically controlled Chinese medicine
In the body of heater simmering stove processed, be provided with the two cover heating components distributed up and down, be wherein placed with moveable Chinese medicine rack 9.Be fixedly connected with two cover on and off switch 8 and display window 7 on body of heater side, control two cover heating components respectively.According to Chinese medicine characteristic and Chinese medicine tradition concocting method or existing legal processing standard, select suitable process of preparing Chinese medicine material as heat transfer medium.The thin bran ash of the heat transfer medium wherein added.Its layout structure as Fig. 5 and Fig. 6, primarily of cover plate 1, body of heater 2, thermal insulation layer 3, temperature sensor 4, electrothermal tube 5, control chamber 6, display window 7, switch 8, rack 9 forms, and is provided with thermal insulation layer 3 between described body of heater 2 body wall, described rack 9 is evenly provided with and puts thing hole 10.Wherein, need rack 9 to put in stove case before processing, ensure that its four feets are steadily placed at body of heater inner bottom part, the upper plane of rack 9 is just in time between two electrothermal tubes 5.
The heating tubes such as the electrothermal tube 5 distributed up and down in body of heater is U-shaped, W type, snakelike, screw type or finned, flange form, threaded; The upper and lower distribution distance of two cover heating tubes is 8-50cm.
Two, the preparation of different ginger product:
1. adopt traditional method preparation to simmer Rhizoma Zingiberis Recens (Traditional Method):
(1) get Rhizoma Zingiberis Recens, clean with clear water, with l Water Paper parcel, put to enclose in stove and imbed quantitative dry bran, light, simmer and take out to when the most ash cooling of bran, paper zoom, micro-Jiao of Rhizoma Zingiberis Recens crust, center buff; (2) remove paper, hit sheet, and sieve dedust bits, to obtain final product.
2. adopt the preparation of temperature automatically controlled stewing stove processed to simmer Rhizoma Zingiberis Recens (modern method):
(1) get Rhizoma Zingiberis Recens, select stepping, clear water is cleaned, and drains the water; (2) wrap with l Water Paper, top upward, small end down, be placed on temperature automatically controlled stewing stove rack processed, add thin bran ash and simmer furnace body processed to filling, adopt temperature-programmed mode, the stewing time and the temperature that arrange heating component are 0-1 hour, 120 DEG C, 1-2 hour, 180 DEG C, 2-5 hour, 300 DEG C; The stewing time of lower heating component and temperature are 0-1 hour, 100 DEG C, 1-2 hour, 160 DEG C, 2-5 hour, 280 DEG C, and system of simmering is to the stipulated time; (3) treat ash cooling, take out Rhizoma Zingiberis Recens, removing paper, cuts 2-3mm sheet, and sieve dedust bits, to obtain final product.
Three, Comparative Analysis on Quality---adopt HPLC method to measure 6-gingerol content in Rhizoma Zingiberis Recens
1. the preparation of solution
(1) preparation of reference substance solution
Get 6-gingerol reference substance appropriate, accurately weighed, add methanol and make the solution of every 1ml containing 0.154mg, to obtain final product.
(2) preparation of need testing solution
Get the broken end of this product about 0.8g, accurately weighed, put in tool plug conical flask, precision adds methanol 25ml, weighed weight, and reflux 30 minutes, lets cool, more weighed weight, supplies the weight of less loss, shake up with methanol, filters, gets subsequent filtrate, to obtain final product.
2. chromatographic condition
Chromatographic column: VenusilXBP-C
18post (5 μm, 4.6 × 250mm); Mobile phase: acetonitrile-methanol-water (40:5:55); Flow velocity: 1.0ml/min; Determined wavelength: 280nm; Column temperature: 35 DEG C.
3. linear relationship is investigated
Accurate absorption reference substance solution 0.5ml, 1ml, 2ml, 4ml, 8ml, 10ml put in 10ml measuring bottle respectively, add methanol dilution to scale, shake up, and accurate absorption 10 μ l, successively injection liquid chromatography, measure respectively.With sample size X(μ g) linear regression is carried out to peak area A, regression equation is: A=1.194x10
6x-1.188x10
4, r=0.9999.Known 6-gingerol peak area and sample size within the scope of 0.0772 ~ 1.543 μ g are good linear relation.
4. precision test
Draw the mixing reference substance solution 10 μ l of same concentration, repeat sample introduction and measure 5 times, record chromatogram, the RSD of result 6-gingerol peak area is 0.72%.
5. stability test
Precision takes simmers Rhizoma Zingiberis Recens sample (modern method) 0.8g, by legal system available test sample solution below (2) item, difference sampling and measuring after room temperature places 0h, 2h, 4h, 8h and 24h, the RSD of result 6-gingerol peak area is 1.10%, shows that need testing solution is stable in 24h.
6. replica test
Precision takes 5 parts, the stewing Rhizoma Zingiberis Recens sample (modern method) of 0.8g, by legal system available test sample solution below (2) item, measures in accordance with the law, in results sample 6-gingerol content be 0.37%, RSD2.45%.
7. average recovery test
Precision takes stewing Rhizoma Zingiberis Recens sample (modern method) 0.4g of 6 parts of known content, every part respectively precision add reference substance 6-gingerol 1.50mg, by legal system available test sample solution below (2) item, measure in accordance with the law.Result 6-gingerol average recovery rate is: 96.69%, RSD2.18%.
8. sample size measures
Precision takes Rhizoma Zingiberis Recens, simmers Rhizoma Zingiberis Recens sample (Traditional Method), simmers Rhizoma Zingiberis Recens sample (modern method), by legal system available test sample solution below (2) item respectively.Accurate absorption mixes reference substance solution 10 μ l and each 20 μ l of need testing solution, injection liquid chromatography, record chromatogram.By external standard method, with 6-gingerol content in calculated by peak area sample.The results are shown in Table 1.
6-gingerol assay result (￣ X ± S) in table 1 sample
| Sample | Sample number | 6-gingerol/% |
| Rhizoma Zingiberis Recens | 10 | （0.11±0.10） |
| Simmer Rhizoma Zingiberis Recens (Traditional Method) | 10 | （0.36±0.27） |
| Simmer Rhizoma Zingiberis Recens (modern method) | 10 | （0.38±0.08） |
Because working substance basis of inducing sweat in Rhizoma Zingiberis Recens is mainly wherein some volatile and stimulating component, after the system of simmering, these volatility and stimulating component easily scatter and disappear, cause its declines that induces sweat, but the 6-gingerol of warming middle-JIAO effect of wherein having is relatively better to heat stability, not easily decompose after adding fire bending, i.e. warming middle-JIAO to arrest vomiting power victory.This experiment is containing surveying index with 6-gingerol, and result shows a few zero difference of stewing Quality of Ginger adopting traditional method and temperature automatically controlled method of simmering stove processed to prepare, and the stewing Rhizoma Zingiberis Recens namely adopting stewing stove processed to prepare can reach the quality standard that side tradition in Jianchang simmers Rhizoma Zingiberis Recens; It is little compared with the fluctuation of Traditional Method content, and namely differences between batches are little.
Claims (5)
1. an industrialization processing procedure for Rhizoma Zingiberis Recens simmered by the prepared slices of Chinese crude drugs, and it is characterized in that, concocting method is as follows:
(1), get Rhizoma Zingiberis Recens, select stepping, clear water is cleaned, and drain the water to obtain the obtained thing of step (1);
(2), the obtained thing l Water Paper of step (1) is wrapped, with top or unified upward with small end, be placed on the rack (9) in temperature automatically controlled Chinese medicine stewing stove processed, add heat transfer medium and simmer furnace body processed to filling, different according to Rhizoma Zingiberis Recens top and small end, arrange up and down and/or the heating-up temperature of the heating component of left and right distribution respectively, heating component temperature wherein near side, Rhizoma Zingiberis Recens top is arranged need higher than its small end side, open temp control unit simultaneously, follow procedure heating mode setup times and temperature, simmer the concocted time of system to regulation, to be cooled to room temperature, take out Rhizoma Zingiberis Recens, removing paper, obtain the obtained thing of step (2),
(3), get the obtained thing of step (2), cut 2-3mm sheet, sieve dedust bits, to obtain final product.
2. the industrialization processing procedure of Rhizoma Zingiberis Recens simmered by a kind of prepared slices of Chinese crude drugs according to claim 1, it is characterized in that, in step (2), Rhizoma Zingiberis Recens top upward, small end down, evenly be placed on rack (9), adopt temperature-programmed mode, the stewing time and the temperature that arrange heating component are 0-1 hour, 110-130 DEG C, 1-2 hour, 160-200 DEG C, 2-5 hour, 270-330 DEG C; The stewing time of lower heating component and temperature are 0-1 hour, 90-120 DEG C, 1-2 hour, 140-180 DEG C, 2-5 hour, 240-300 DEG C.
3. the industrialization processing procedure of Rhizoma Zingiberis Recens simmered by a kind of prepared slices of Chinese crude drugs according to claim 2, it is characterized in that, upper and lower heating component temperature is set to, and the stewing time of upper heating component and temperature are 0-1 hour, 115-125 DEG C, 1-2 hour, 170-190 DEG C, 2-5 hour, 290-310 DEG C; The stewing time of lower heating component and temperature are 0-1 hour, 100-110 DEG C, 1-2 hour, 150-170 DEG C, 2-5 hour, 270-290 DEG C.
4. the industrialization processing procedure of Rhizoma Zingiberis Recens simmered by a kind of prepared slices of Chinese crude drugs according to claim 1, and it is characterized in that, heat transfer medium is plant ashes.
5. the industrialization processing procedure of Rhizoma Zingiberis Recens simmered by a kind of prepared slices of Chinese crude drugs according to claim 4, it is characterized in that, plant ashes are thin bran ash.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2147861Y (en) * | 1993-01-20 | 1993-12-01 | 刘延林 | Multifunctional traditional Chinese medicine preparing machine |
| CN2537385Y (en) * | 2002-04-16 | 2003-02-26 | 程桂俊 | Automatic regulating and preparing Chinese medicine furnace |
| CN201727740U (en) * | 2009-12-11 | 2011-02-02 | 杭州海善制药设备有限公司 | High-temperature control traditional Chinese medicament calcining furnace |
| CN203354916U (en) * | 2013-07-25 | 2013-12-25 | 尚勇 | Electric-heating braising and calcining device for preparing Chinese herb medicine |
| CN103585017A (en) * | 2013-09-22 | 2014-02-19 | 王小平 | Industrialized preparing process for traditional Chinese medicine decoction pieces simmered monkshood and automatic temperature-control simmering furnace |
-
2015
- 2015-12-11 CN CN201510912346.3A patent/CN105534712A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2147861Y (en) * | 1993-01-20 | 1993-12-01 | 刘延林 | Multifunctional traditional Chinese medicine preparing machine |
| CN2537385Y (en) * | 2002-04-16 | 2003-02-26 | 程桂俊 | Automatic regulating and preparing Chinese medicine furnace |
| CN201727740U (en) * | 2009-12-11 | 2011-02-02 | 杭州海善制药设备有限公司 | High-temperature control traditional Chinese medicament calcining furnace |
| CN203354916U (en) * | 2013-07-25 | 2013-12-25 | 尚勇 | Electric-heating braising and calcining device for preparing Chinese herb medicine |
| CN103585017A (en) * | 2013-09-22 | 2014-02-19 | 王小平 | Industrialized preparing process for traditional Chinese medicine decoction pieces simmered monkshood and automatic temperature-control simmering furnace |
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Application publication date: 20160504 |