CN105529121B - Production technology process for flexible composite insulating material - Google Patents

Production technology process for flexible composite insulating material Download PDF

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Publication number
CN105529121B
CN105529121B CN201510870884.0A CN201510870884A CN105529121B CN 105529121 B CN105529121 B CN 105529121B CN 201510870884 A CN201510870884 A CN 201510870884A CN 105529121 B CN105529121 B CN 105529121B
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Prior art keywords
film
component
speed
insulating materials
technological process
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CN105529121A (en
Inventor
朱永明
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Jiangsu Yuming New Material Co ltd
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Taizhou Yu New Materials Co Ltd
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B19/00Apparatus or processes specially adapted for manufacturing insulators or insulating bodies
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B17/00Insulators or insulating bodies characterised by their form
    • H01B17/56Insulating bodies
    • H01B17/60Composite insulating bodies
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B3/00Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
    • H01B3/18Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
    • H01B3/30Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
    • H01B3/303Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups H01B3/38 or H01B3/302
    • H01B3/305Polyamides or polyesteramides
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B3/00Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
    • H01B3/18Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
    • H01B3/30Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
    • H01B3/303Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups H01B3/38 or H01B3/302
    • H01B3/306Polyimides or polyesterimides
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B3/00Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
    • H01B3/18Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
    • H01B3/30Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
    • H01B3/42Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes polyesters; polyethers; polyacetals
    • H01B3/421Polyesters

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  • Physics & Mathematics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Insulating Materials (AREA)
  • Laminated Bodies (AREA)

Abstract

The invention discloses a production technology process for a flexible composite insulating material. The production technology process comprises the following steps: firstly, gluing on double surface of a film for electrical purposes; secondly, heating and drying; thirdly, adding fiber paper above and below the film for electrical purposes, and heating, laminating and compounding; fourthly, rolling and curing; and fifthly, carrying out rewinding testing. The production technology process for the flexible composite insulating material disclosed by the invention has the advantages that the fiber paper and the film for electrical purposes can be compounded to form the flexible composite material, various requirements such as dielectric strength, mechanical property and application process performance can be met, and the production technology process is suitable for slot insulation, insulation between phases, wire insulation and gasket insulation of motors, electrical appliances, transformers and other high-voltage electrical apparatuses.

Description

The flexible compound insulating materials technological process of production
Technical field
The present invention relates to a kind of flexible compound insulating materials technological process of production.
Background technology
Fibrous paper has between good adsorptivity and coil and cell wall good tack, it is to avoid occur during operation Displacement, but its dielectric strength is relatively low;Films for electrical purposes have good dielectric properties, but its tack is poor.Therefore they Respective weak point has been used as insulating materials.
The content of the invention
The present invention mainly solves the technical problem existing for prior art, so as to provide one kind can composite fibre paper and Films for electrical purposes form composite flexible material, can meet various requirements such as dielectric strength, mechanical property and technique for applying performance, fit For the soft of the slot insulation of motor, electrical equipment, transformer and other High-Voltage Electrical Appliances, phase insulation, wire insulation and liner insulation The property composite insulating material technological process of production.
What the above-mentioned technical problem of the present invention was mainly addressed by following technical proposals:
A kind of flexible compound insulating materials technological process of production, comprises the following steps:
First, in the double spread water of films for electrical purposes;
2nd, heat drying;
3rd, increase fibrous paper above and below the films for electrical purposes and to heat pressurization compound;
4th, wind and solidify;
5th, rewinding test.
Used as preferred embodiments of the present invention, described films for electrical purposes are polyester film or Kapton.
Used as preferred embodiments of the present invention, described fibrous paper is nonwoven polyester fabric or aromatic polyamide paper.
Used as preferred embodiments of the present invention, described glue is polyurethane binder.
Used as preferred embodiments of the present invention, described adhesive is polyester-type carbamic acid resin, by first component and second Component reconciles and forms, and first component is PEPA, and second component is isocyanate addition product;First component acts primarily as adhesive effect, Second component accelerates the adhering and solidifying speed of product;
Diluent is ethyl acetate.
Used as preferred embodiments of the present invention, the solid content of described first component is 30% ± 2% or 50% ± 2%;It is described Second component solid content be 60% ± 2%, isocyanide acid content be 11% ~ 13%.
As preferred embodiments of the present invention,
When room temperature is 25 DEG C ~ 36 DEG C, the weight percent of first component, second component and diluent in described polyurethane binder Than being respectively:57.5%、7.3%、35.2%;
When room temperature is 10 DEG C ~ 25 DEG C, the weight percent of first component, second component and diluent in described polyurethane binder Than being respectively:60.3%、8.6%、31.1%;
When room temperature is -10 DEG C ~ 10 DEG C, the weight hundred of first component, second component and diluent in described polyurethane binder Ratio is divided to be respectively:62.5%、8.9%、28.6%.
Used as preferred embodiments of the present invention, described step two is carried out in an oven;In first temperature rise period, baking oven The temperature of leading portion, stage casing and tail end be followed successively by:90 DEG C, 100 DEG C, 80 DEG C;In normal operation, the leading portion of baking oven, stage casing and The temperature of tail end is followed successively by:120 DEG C, 130 DEG C, 110 DEG C;When running in the first temperature rise period and normally, the speed of film with it is thin The thickness of film is directly proportional, and when the thickness of film is identical, during normal operation, the speed of film will be faster than just temperature rise period film Speed.
As preferred embodiments of the present invention,
In the first temperature rise period, the thickness of film is as shown in the table with the corresponding relation of speed:
Film thickness/millimeter 0.15 0.18 0.20 0.23 0.25 0.30 0.35 0.40 0.5
Film speed/m/min 8 8.6 9.2 9.8 9.8 9.8 9.8 9.8 9.8
In normal operation, the thickness of film is as shown in the table with the corresponding relation of speed:
Film thickness/millimeter 0.15 0.18 0.20 0.23 0.25 0.30 0.35 0.40 0.5
Film speed/m/min 13.2 13.8 14.4 15 15 15.6 15.6 16.2 16.2
As preferred embodiments of the present invention, in the cure stage of step 4,
When room temperature >=10 DEG C, clean, dry, ventilation place is stored in, standing puts 24 hours;
When 10 DEG C of room temperature <, first it is stored in the solidification room that temperature is 25 DEG C, standing is put 48 hours, takes from solidification room After going out, then 12 hours are put in ventilation.
The advantage of the flexible compound insulating materials technological process of production of the present invention is:Being capable of composite fibre paper and films for electrical purposes Composite flexible material is formed, various requirements such as dielectric strength, mechanical property and technique for applying performance can be met, it is adaptable to electricity The insulation of the slot insulation of mechanical, electrical device, transformer and other High-Voltage Electrical Appliances, phase insulation, wire insulation and liner.
Specific embodiment
Below in conjunction with the accompanying drawings the preferred embodiments of the present invention are described in detail, so that advantages and features of the invention energy It is easier to be readily appreciated by one skilled in the art, apparent clearly defines so as to make to protection scope of the present invention.
The advantage of the flexible compound insulating materials technological process of production of the present invention is:Being capable of composite fibre paper and films for electrical purposes Composite flexible material is formed, various requirements such as dielectric strength, mechanical property and technique for applying performance can be met, it is adaptable to electricity The insulation of the slot insulation of mechanical, electrical device, transformer and other High-Voltage Electrical Appliances, phase insulation, wire insulation and liner.
A kind of flexible compound insulating materials technological process of production, comprises the following steps:
First, in the double spread water of films for electrical purposes;
2nd, heat drying;
3rd, increase fibrous paper above and below the films for electrical purposes and to heat pressurization compound;
4th, wind and solidify;
5th, rewinding test.
The films for electrical purposes are polyester film or Kapton.
The fibrous paper is nonwoven polyester fabric or aromatic polyamide paper.
The glue is polyurethane binder.
The adhesive is polyester-type carbamic acid resin, is reconciled by first component and second component and is formed, and first component is that polyester is more First alcohol, second component are isocyanate addition products;First component acts primarily as adhesive effect, and second component accelerates the adhering and solidifying speed of product Degree;
Diluent is ethyl acetate.
The solid content of the first component is 30% ± 2% or 50% ± 2%;The solid content of the second component is 60% ± 2%, isocyanic acid Content is 11% ~ 13%.
When room temperature is 25 DEG C ~ 36 DEG C, the weight percent score of first component, second component and diluent in the polyurethane binder It is not:57.5%、7.3%、35.2%;
When room temperature is 10 DEG C ~ 25 DEG C, the weight percent score of first component, second component and diluent in the polyurethane binder It is not:60.3%、8.6%、31.1%;
When room temperature is -10 DEG C ~ 10 DEG C, the percentage by weight of first component, second component and diluent in the polyurethane binder Respectively:62.5%、8.9%、28.6%.
The step 2 is carried out in an oven;In the first temperature rise period, the temperature of the leading portion of baking oven, stage casing and tail end is successively For:90 DEG C, 100 DEG C, 80 DEG C;In normal operation, the temperature of the leading portion of baking oven, stage casing and tail end is followed successively by:120 DEG C, 130 DEG C, 110 DEG C;When running in the first temperature rise period and normally, the speed of film is directly proportional to the thickness of film, and in the thickness of film When spending identical, during normal operation, the speed of film will be faster than the speed of just temperature rise period film.
In the first temperature rise period, the thickness of film is as shown in the table with the corresponding relation of speed:
Film thickness/millimeter 0.15 0.18 0.20 0.23 0.25 0.30 0.35 0.40 0.5
Film speed/m/min 8 8.6 9.2 9.8 9.8 9.8 9.8 9.8 9.8
In normal operation, the thickness of film is as shown in the table with the corresponding relation of speed:
Film thickness/millimeter 0.15 0.18 0.20 0.23 0.25 0.30 0.35 0.40 0.5
Film speed/m/min 13.2 13.8 14.4 15 15 15.6 15.6 16.2 16.2
In the cure stage of step 4,
When room temperature >=10 DEG C, clean, dry, ventilation place is stored in, standing puts 24 hours;
When 10 DEG C of room temperature <, first it is stored in the solidification room that temperature is 25 DEG C, standing is put 48 hours, takes from solidification room After going out, then 12 hours are put in ventilation.
It is only the mentality of designing of some embodiments of the present invention above, in the case where system is allowed, the present invention can To expand to while external more functional modules, so as to extend its function to greatest extent.
The above, the only specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, any The change or replacement expected without creative work, should all be included within the scope of the present invention.Therefore, it is of the invention The protection domain that protection domain should be limited by claims is defined.

Claims (8)

1. a kind of flexible compound insulating materials technological process of production, it is characterised in that:Comprise the following steps:
First, in the double spread water of films for electrical purposes;
2nd, heat drying;
3rd, increase fibrous paper above and below the films for electrical purposes and to heat pressurization compound;
4th, wind and solidify;
5th, rewinding test;
Described step two is carried out in an oven;In the first temperature rise period, the temperature of the leading portion of baking oven, stage casing and tail end is successively For:90 DEG C, 100 DEG C, 80 DEG C;In normal operation, the temperature of the leading portion of baking oven, stage casing and tail end is followed successively by:120 DEG C, 130 DEG C, 110 DEG C;When running in the first temperature rise period and normally, the speed of film is directly proportional to the thickness of film, and in the thickness of film When spending identical, during normal operation, the speed of film will be faster than the speed of just temperature rise period film;
In the first temperature rise period, the thickness of film is as shown in the table with the corresponding relation of speed:
Film thickness/millimeter 0.15 0.18 0.20 0.23 0.25 0.30 0.35 0.40 0.5 Film speed/m/min 8 8.6 9.2 9.8 9.8 9.8 9.8 9.8 9.8
In normal operation, the thickness of film is as shown in the table with the corresponding relation of speed:
Film thickness/millimeter 0.15 0.18 0.20 0.23 0.25 0.30 0.35 0.40 0.5 Film speed/m/min 13.2 13.8 14.4 15 15 15.6 15.6 16.2 16.2
2. the flexible compound insulating materials technological process of production according to claim 1, it is characterised in that:Described electrician is thin Film is polyester film or Kapton.
3. the flexible compound insulating materials technological process of production according to claim 1, it is characterised in that:Described fibrous paper For nonwoven polyester fabric or aromatic polyamide paper.
4. the flexible compound insulating materials technological process of production according to claim 1, it is characterised in that:Described glue is Polyurethane binder.
5. the flexible compound insulating materials technological process of production according to claim 4, it is characterised in that:Described adhesive It is polyester-type carbamic acid resin, is reconciled by first component and second component and formed, first component is PEPA, and second component is isocyanide Acid esters addition product;First component acts primarily as adhesive effect, and second component accelerates the adhering and solidifying speed of product;
Diluent is ethyl acetate.
6. the flexible compound insulating materials technological process of production according to claim 5, it is characterised in that:Described first component Solid content be 30% ± 2% or 50% ± 2%;The solid content of described second component be 60% ± 2%, isocyanide acid content be 11% ~ 13%。
7. the flexible compound insulating materials technological process of production according to claim 6, it is characterised in that:
When room temperature is 25 DEG C ~ 36 DEG C, the weight percent score of first component, second component and diluent in described polyurethane binder It is not:57.5%、7.3%、35.2%;
When room temperature is 10 DEG C ~ 25 DEG C, the weight percent score of first component, second component and diluent in described polyurethane binder It is not:60.3%、8.6%、31.1%;
When room temperature is -10 DEG C ~ 10 DEG C, the percentage by weight of first component, second component and diluent in described polyurethane binder Respectively:62.5%、8.9%、28.6%.
8. the flexible compound insulating materials technological process of production according to claim 1, it is characterised in that:Consolidating in step 4 The change stage,
When room temperature >=10 DEG C, clean, dry, ventilation place is stored in, standing puts 24 hours;
When 10 DEG C of room temperature <, first it is stored in the solidification room that temperature is 25 DEG C, standing is put 48 hours, takes out from solidification room Afterwards, then in ventilation 12 hours are put.
CN201510870884.0A 2015-12-02 2015-12-02 Production technology process for flexible composite insulating material Active CN105529121B (en)

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Publication number Priority date Publication date Assignee Title
CN110349717B (en) * 2019-07-15 2020-08-14 瑞安复合材料(深圳)有限公司 High-temperature stable flame-retardant insulating composite material for generator

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101804715A (en) * 2010-04-15 2010-08-18 河南许绝电工绝缘材料有限公司 Method for manufacturing electric flexible polyester composite material
CN201845618U (en) * 2010-07-21 2011-05-25 株洲市绝缘材料有限责任公司 Composite material of polyimide film and aramid fiber paper
CN103085441A (en) * 2013-03-04 2013-05-08 株洲时代电气绝缘有限责任公司 Manufacturing method of flexible composite material
CN103818067A (en) * 2014-03-18 2014-05-28 温岭市第二绝缘材料厂 Insulation paper applicable to motor and production process of insulation paper
CN104448705A (en) * 2014-11-20 2015-03-25 绵阳润缘电工材料有限公司 Preparation method of nanomaterial modified DMD soft composite

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103547548A (en) * 2011-03-23 2014-01-29 密苏里大学学监 High dielectric constant composite materials and methods of manufacture

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101804715A (en) * 2010-04-15 2010-08-18 河南许绝电工绝缘材料有限公司 Method for manufacturing electric flexible polyester composite material
CN201845618U (en) * 2010-07-21 2011-05-25 株洲市绝缘材料有限责任公司 Composite material of polyimide film and aramid fiber paper
CN103085441A (en) * 2013-03-04 2013-05-08 株洲时代电气绝缘有限责任公司 Manufacturing method of flexible composite material
CN103818067A (en) * 2014-03-18 2014-05-28 温岭市第二绝缘材料厂 Insulation paper applicable to motor and production process of insulation paper
CN104448705A (en) * 2014-11-20 2015-03-25 绵阳润缘电工材料有限公司 Preparation method of nanomaterial modified DMD soft composite

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Effective date of registration: 20170216

Address after: 225300 Jiangsu Taizhou City Hailing Industrial Park Yingchun Road No. 98 Building 1 room 232 Hailing District hi tech Innovation Service Center in

Applicant after: TAIZHOU YUMING NEW MATERIAL CO.,LTD.

Address before: 225300 Jiangsu Province, Taizhou City Hailing Industrial Park Road on the north side of No. 11 spring

Applicant before: TAIZHOU NO.3 INSULATING MATERIAL FACTORY

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Address after: Room 232, building 1, No. 98, Yingchun East Road, hailing Industrial Park, Taizhou City, Jiangsu Province

Patentee after: Jiangsu Yuming New Material Co.,Ltd.

Address before: Room 232, building 1, No. 98, East Yingchun Road, hailing Industrial Park, Taizhou, Jiangsu

Patentee before: TAIZHOU YUMING NEW MATERIAL Co.,Ltd.

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Denomination of invention: Production process flow of flexible composite insulation materials

Effective date of registration: 20231221

Granted publication date: 20170322

Pledgee: Bank of Nanjing Co.,Ltd. Taizhou Branch

Pledgor: Jiangsu Yuming New Material Co.,Ltd.

Registration number: Y2023980072907