CN105461416A - Fermented water retention type sustained-release preparation and preparation method - Google Patents

Fermented water retention type sustained-release preparation and preparation method Download PDF

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Publication number
CN105461416A
CN105461416A CN201410422403.5A CN201410422403A CN105461416A CN 105461416 A CN105461416 A CN 105461416A CN 201410422403 A CN201410422403 A CN 201410422403A CN 105461416 A CN105461416 A CN 105461416A
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parts
fermentation
moisture
sustained release
release formulation
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CN201410422403.5A
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Inventor
刘泽华
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Qingdao Xin Runtu Nursery Stock Specialty Co-Operative Organization
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Qingdao Xin Runtu Nursery Stock Specialty Co-Operative Organization
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Abstract

The invention discloses a fermented water retention type sustained-release preparation and a preparation method thereof. The sustained-release preparation is characterized by comprising the following raw materials by weight: 100 parts of acrylic acid, 15-20 parts of straw fermentation broth, 5-7 parts of urea, 2-3 parts of trifluralin, 3-4 parts of fomesafen, 8-12 parts of sepiolite, 0.07-0.08 part of an initiator, 0.08-0.12 part of a crosslinking agent, 4-6 parts of sawdust, 3-4 parts of borax, 3-4 parts of polyvinyl alcohol, and 1.5-1.8 parts of guar gum. According to the invention, the weeding and insecticidal effective organic components and the organic fermentation broth are integrated, the fermentation broth provides sufficient organic matters for plant growth, the crop resistance to diseases is improved, the water absorption and drainage capacity is strong, the water permeability and air permeability of soil are enhanced, and the sustained-release effect of fertilizer is enhanced, the fermented water retention type sustained-release preparation has good biocompatibility, and is beneficial to sustainable development of resources.

Description

The moisture-retention sustained release formulation of a kind of fermentation and making method
Technical field
The invention belongs to fertilizer manufacture technology field, be specifically related to the moisture-retention sustained release formulation of a kind of fermentation and making method.
Background technology
In agriculture production, harmful organism be one of important factor causing grain drop in production, and spraying pesticide be prevention and elimination of disease and pests, improve grain yield, guarantee agricultural high yield effective way.There is the shortcomings such as effective constituent release rate is fast, drug effect efficiency time is short, dosage is large in traditional conventional type pesticide preparation, utilization ratio generally only has 20% ~ 30%.In order to maintain certain drug effect, just must spray higher than effective dose of medicine amount, or increase spraying times.Both easily produce poisoning like this, increase pesticide residue, harm humans health, contaminate environment, time-consuming again, very uneconomical.In addition, though agricultural water-loss reducer now has very strong water absorbing and retaining properties, not there is the necessary nutrient of crop growth.
Organic fertilizer fermentation is mainly derived from plant, imposing on soil to provide plant nutrition is the carbonaceous material of its major function, through biological substance, animals and plants waste, plant residue processing, eliminate hazardous and noxious substances wherein, be rich in a large amount of benefit materials, can increase and upgrade the soil organism, promote microbial reproduction, improving physico-chemical property and the biological activity of soil, is the Main Nutrients of pollution-free food production.
Therefore, how to produce the moisture-retention sustained release formulation of a kind of fermentation, water-holding agent and organic fermented liquid are harmonious, full nutrition can be provided for farm crop, there is strong water absorbing and retaining properties, and fertilizer efficiency be long simultaneously, nutrient loss is few, advantages of environment protection, is the technical problem to be solved in the present invention.
Summary of the invention
For problems of the prior art, the object of the present invention is to provide the moisture-retention sustained release formulation of a kind of fermentation and making method, by herbicide pesticide etc., effectively organic composition and organic fermented liquid merge the moisture-retention sustained release formulation that the present invention obtains, fermented liquid is that the growth of plant provides sufficient organic matter, improve the disease-resistant performance of crop, the ability that discharges water that absorbs water is strong, soil water permeability, ventilation property strengthen, enhance the slow release effect of fertilizer, there is good biocompatibility, be beneficial to the Sustainable development of resource.
The technical scheme that the present invention takes is:
The moisture-retention sustained release formulation of a kind of fermentation, it is characterized in that, feed components is composed as follows according to weight fraction:
Linking agent 0.08-0.12 part that initiator 0.07-0.08 part that 100 parts, vinylformic acid, stalk fermentation liquid 15-20 part, urea 5-7 part, trifluralin 2-3 part, fomesafen 3-4 part, sepiolite 8-12 part, Sodium Persulfate and trolamine form according to weight ratio 2:3, epoxy chloropropane and dimethyl diallyl ammonium chloride form according to weight ratio 2:3, wood chip 4-6 part, borax 3-4 part, polyvinyl alcohol 3-4 part, guar gum 1.5-1.8 part.
Further, the making method of described stalk fermentation liquid is for being that 3:1:5 gets stalk, animal excrement and water composition mixture according to weight ratio, soak 8-10h, add the bacterial classification of the 0.3-0.5% be made up of according to weight ratio 2:2:1 genus bacillus, sporotrichum thermophile, yeast, add the humic acids of 3-5%, control leavening temperature is 38-40 DEG C, and interval 2h passes into a sterile air, gas material volume ratio is regulated to be 1:2,3-4 days before fermentation.
To ferment the making method of moisture-retention sustained release formulation, it is characterized in that, specifically comprise the steps:
(1) solid-liquid mixtures processed: getting urea, trifluralin, fomesafen and water preparation mass percent according to proportioning raw materials is the pesticidal emulsion of 16-18%, slowly adds sepiolite, linking agent, mixing and stirring in emulsion;
(2) integument particle processed: in the reactor, vinylformic acid mass concentration is the solution of potassium carbonate neutralization of 25%, part acrylic acid is made to be converted into potassium acrylate, add above-mentioned obtained solid-liquid mixtures, initiator successively, stir, be warming up to 60-65 ° of C, reaction keeps 4-5h to obtain gel polymerisate, drying, grinding, excessively 200 eye mesh screens;
(3) coating process: in granulating disc; put into above-mentioned obtained integument particle; open air blast feeder; add ultra-fine wood chip powder on the integument particle rolled, make it evenly be wrapping to particle surface, with the mixture of the nozzles spray borax of pressure >=0.4MPa, polyvinyl alcohol and guar gum; consumption accounts for the 1.5-3% of integument particle; temperature maintains 55 ° of C, and Hot-blast Heating, is cooled to room temperature.
Beneficial effect of the present invention is:
By herbicide pesticide etc., effectively organic composition and organic fermented liquid merge the moisture-retention sustained release formulation that the present invention obtains, fermented liquid is that the growth of plant provides sufficient organic matter, the output of the crop of improving, the effective components such as trifluralin make the resistant to diseases and insects of plant improve, improve the disease-resistant performance of crop, indirectly improve the quality of crop.
Product of the present invention is divided into inside and outside two-layer, inner sepiolite and outside wood chip all act as the effect of water conservation carrier, can improve the utilization ratio of moisture and nutrient simultaneously, and the ability that discharges water that absorbs water is strong, and it can form crumb structure in soil, soil water permeability, ventilation property are strengthened;
The present invention makes full use of stalk the like waste, turns waste into wealth, and has good biocompatibility, is beneficial to the Sustainable development of resource.
The envelope components such as polyvinyl alcohol, guar gum, enhances the slow release effect of fertilizer, improves the utilization ratio of fertilizer, nutrient can need fertile slow releasing by crop, can Soil structure be regulated, reduce the antagonism between ion, thus improve effective specific absorption of plant, reduce applying quantity of chemical fertilizer.
Embodiment
Embodiment 1
The making method of stalk fermentation liquid is for being that 3:1:5 gets stalk, animal excrement and water composition mixture according to weight ratio, soak 8-10h, add the bacterial classification be made up of according to weight ratio 2:2:1 genus bacillus, sporotrichum thermophile, yeast of 0.3-0.5%, add the humic acids of 3-5%, control leavening temperature is 38-40 DEG C, interval 2h passes into a sterile air, regulates gas material volume ratio to be 1:2,3-4 days before fermentation.
To ferment the making method of moisture-retention sustained release formulation, it is characterized in that, specifically comprise the steps:
(1) solid-liquid mixtures processed: getting urea 5-7 part, trifluralin 2-3 part, fomesafen 3-4 part and water preparation mass percent according to proportioning raw materials is the pesticidal emulsion of 16-18%, linking agent 0.08-0.12 part that sepiolite 8-12 part, epoxy chloropropane and dimethyl diallyl ammonium chloride form according to weight ratio 2:3 is slowly added, mixing and stirring in emulsion;
(2) integument particle processed: in the reactor, 100 parts, vinylformic acid is the solution of potassium carbonate neutralization of 25% by mass concentration, part acrylic acid is made to be converted into potassium acrylate, add initiator 0.07-0.08 part that above-mentioned obtained solid-liquid mixtures, Sodium Persulfate and trolamine form according to weight ratio 2:3 successively, stir, be warming up to 60-65 ° of C, reaction keeps 4-5h to obtain gel polymerisate, drying, grinding, excessively 200 eye mesh screens;
(3) coating process: in granulating disc; put into above-mentioned obtained integument particle; open air blast feeder; add ultra-fine wood chip powder on the integument particle rolled, make it evenly be wrapping to particle surface, with the mixture of nozzles spray borax 3-4 part of pressure >=0.4MPa, polyvinyl alcohol 3-4 part, guar gum 1.5-1.8 part; consumption accounts for the 1.5-3% of integument particle; temperature maintains 55 ° of C, and Hot-blast Heating, is cooled to room temperature.
Embodiment 2
The making method of stalk fermentation liquid is for being that 3:1:5 gets stalk, animal excrement and water composition mixture according to weight ratio, soak 8-10h, add the bacterial classification be made up of according to weight ratio 2:2:1 genus bacillus, sporotrichum thermophile, yeast of 0.3-0.5%, add the humic acids of 3-5%, control leavening temperature is 38-40 DEG C, interval 2h passes into a sterile air, regulates gas material volume ratio to be 1:2,3-4 days before fermentation.
To ferment the making method of moisture-retention sustained release formulation, it is characterized in that, specifically comprise the steps:
(1) solid-liquid mixtures processed: getting urea 5-7 part, trifluralin 2-3 part, fomesafen 3-4 part and water preparation mass percent according to proportioning raw materials is the pesticidal emulsion of 16-18%, linking agent 0.08-0.12 part that sepiolite 8-12 part, epoxy chloropropane and dimethyl diallyl ammonium chloride form according to weight ratio 2:3 is slowly added, mixing and stirring in emulsion;
(2) integument particle processed: in the reactor, 100 parts, vinylformic acid is the solution of potassium carbonate neutralization of 25% by mass concentration, part acrylic acid is made to be converted into potassium acrylate, add initiator 0.07-0.08 part that above-mentioned obtained solid-liquid mixtures, Sodium Persulfate and trolamine form according to weight ratio 2:3 successively, stir, be warming up to 60-65 ° of C, reaction keeps 4-5h to obtain gel polymerisate, drying, grinding, excessively 200 eye mesh screens;
(3) coating process: in granulating disc; put into above-mentioned obtained integument particle; open air blast feeder; add ultra-fine wood chip powder on the integument particle rolled, make it evenly be wrapping to particle surface, with the mixture of nozzles spray borax 3-4 part of pressure >=0.4MPa, polyvinyl alcohol 3-4 part, guar gum 1.5-1.8 part; consumption accounts for the 1.5-3% of integument particle; temperature maintains 55 ° of C, and Hot-blast Heating, is cooled to room temperature.
Embodiment 3
The making method of stalk fermentation liquid is for being that 3:1:5 gets stalk, animal excrement and water composition mixture according to weight ratio, soak 8-10h, add the bacterial classification be made up of according to weight ratio 2:2:1 genus bacillus, sporotrichum thermophile, yeast of 0.3-0.5%, add the humic acids of 3-5%, control leavening temperature is 38-40 DEG C, interval 2h passes into a sterile air, regulates gas material volume ratio to be 1:2,3-4 days before fermentation.
To ferment the making method of moisture-retention sustained release formulation, it is characterized in that, specifically comprise the steps:
(1) solid-liquid mixtures processed: getting urea 5-7 part, trifluralin 2-3 part, fomesafen 3-4 part and water preparation mass percent according to proportioning raw materials is the pesticidal emulsion of 16-18%, linking agent 0.08-0.12 part that sepiolite 8-12 part, epoxy chloropropane and dimethyl diallyl ammonium chloride form according to weight ratio 2:3 is slowly added, mixing and stirring in emulsion;
(2) integument particle processed: in the reactor, 100 parts, vinylformic acid is the solution of potassium carbonate neutralization of 25% by mass concentration, part acrylic acid is made to be converted into potassium acrylate, add initiator 0.07-0.08 part that above-mentioned obtained solid-liquid mixtures, Sodium Persulfate and trolamine form according to weight ratio 2:3 successively, stir, be warming up to 60-65 ° of C, reaction keeps 4-5h to obtain gel polymerisate, drying, grinding, excessively 200 eye mesh screens;
(3) coating process: in granulating disc; put into above-mentioned obtained integument particle; open air blast feeder; add ultra-fine wood chip powder on the integument particle rolled, make it evenly be wrapping to particle surface, with the mixture of nozzles spray borax 3-4 part of pressure >=0.4MPa, polyvinyl alcohol 3-4 part, guar gum 1.5-1.8 part; consumption accounts for the 1.5-3% of integument particle; temperature maintains 55 ° of C, and Hot-blast Heating, is cooled to room temperature.

Claims (6)

1. ferment a moisture-retention sustained release formulation, and it is characterized in that, feed components is composed as follows according to weight fraction:
100 parts, vinylformic acid, stalk fermentation liquid 15-20 part, urea 5-7 part, trifluralin 2-3 part, fomesafen 3-4 part, sepiolite 8-12 part, initiator 0.07-0.08 part, linking agent 0.08-0.12 part, wood chip 4-6 part, borax 3-4 part, polyvinyl alcohol 3-4 part, guar gum 1.5-1.8 part.
2. the moisture-retention sustained release formulation of a kind of fermentation according to claim 1, it is characterized in that, the making method of described stalk fermentation liquid is for being that 3:1:5 gets stalk, animal excrement and water composition mixture according to weight ratio, soak 8-10h, add the bacterial classification of 0.3-0.5%, add the humic acids of 3-5%, control leavening temperature is 38-40 DEG C, interval 2h passes into a sterile air, regulates gas material volume ratio to be 1:2,3-4 days before fermentation.
3. the moisture-retention sustained release formulation of a kind of fermentation according to claim 1, is characterized in that, the mixed strains that described bacterial classification selects genus bacillus, sporotrichum thermophile, yeast to form according to weight ratio 2:2:1.
4. the moisture-retention sustained release formulation of a kind of fermentation according to claim 1, it is characterized in that, described linking agent is the mixture that epoxy chloropropane and dimethyl diallyl ammonium chloride form according to weight ratio 2:3.
5. the moisture-retention sustained release formulation of a kind of fermentation according to claim 1, it is characterized in that, described initiator is the mixture that Sodium Persulfate and trolamine form according to weight ratio 2:3.
6. a making method for the moisture-retention sustained release formulation of fermentation, is characterized in that, specifically comprise the steps:
(1) solid-liquid mixtures processed: getting urea, trifluralin, fomesafen and water preparation mass percent according to proportioning raw materials is the pesticidal emulsion of 16-18%, slowly adds sepiolite, linking agent, mixing and stirring in emulsion;
(2) integument particle processed: in the reactor, vinylformic acid mass concentration is the solution of potassium carbonate neutralization of 25%, part acrylic acid is made to be converted into potassium acrylate, add above-mentioned obtained solid-liquid mixtures, initiator successively, stir, be warming up to 60-65 ° of C, reaction keeps 4-5h to obtain gel polymerisate, drying, grinding, excessively 200 eye mesh screens;
(3) coating process: in granulating disc; put into above-mentioned obtained integument particle; open air blast feeder; add ultra-fine wood chip powder on the integument particle rolled, make it evenly be wrapping to particle surface, with the mixture of the nozzles spray borax of pressure >=0.4MPa, polyvinyl alcohol and guar gum; consumption accounts for the 1.5-3% of integument particle; temperature maintains 55 ° of C, and Hot-blast Heating, is cooled to room temperature.
CN201410422403.5A 2014-08-26 2014-08-26 Fermented water retention type sustained-release preparation and preparation method Pending CN105461416A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106590677A (en) * 2016-12-02 2017-04-26 重庆市江津区森德家庭农场 Multifunctional soil improvement agent and preparation method thereof
CN106748100A (en) * 2016-12-15 2017-05-31 涓ュ垢 A kind of low cost, the environmentally friendly film-coated and slow release fertilizer with water retaining function and preparation method thereof
CN107176881A (en) * 2017-06-28 2017-09-19 常州麒通国际贸易有限公司 A kind of Water-retaining slow-release fertilizer and preparation method thereof
CN108101626A (en) * 2017-12-14 2018-06-01 成都新柯力化工科技有限公司 A kind of ecology sustained release organic film fertilizer and preparation method

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CN101050147A (en) * 2007-05-24 2007-10-10 武汉市海格尔科技有限公司 Water retaining slow-release / controled fertilizer, and preparation method
CN101062878A (en) * 2006-04-30 2007-10-31 中国科学院过程工程研究所 Degradable natural organic matter bundled slow-releasing fertilizer and preparation method and usage thereof
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CN102617249A (en) * 2012-03-31 2012-08-01 山东喜丰田生态肥业有限公司 Novel polysaccharide gel water retaining and slow release fertilizer
CN103819276A (en) * 2014-03-12 2014-05-28 许自霖 Slow-release seaweed fertilizer with high water-retaining property and preparation method thereof
CN103897112A (en) * 2012-12-26 2014-07-02 青岛鑫垚保水高新材料有限公司 Preparation method of super absorbent polymer (nitrogen) aquasorb-fertilizer

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1074206A (en) * 1993-01-14 1993-07-14 北京化工学院 Coated slow release fertilizer and method for making thereof
CN1587211A (en) * 2004-09-20 2005-03-02 中国农业科学院土壤肥料研究所 Process for producing water preserving type film coated urea fertilizer
CN1810732A (en) * 2006-01-23 2006-08-02 石家庄天源淀粉衍生物有限公司 Multifunctional fertilizer and pesticide slow/controlled releasing agent and its prepn process
CN101062878A (en) * 2006-04-30 2007-10-31 中国科学院过程工程研究所 Degradable natural organic matter bundled slow-releasing fertilizer and preparation method and usage thereof
CN101050147A (en) * 2007-05-24 2007-10-10 武汉市海格尔科技有限公司 Water retaining slow-release / controled fertilizer, and preparation method
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CN102617249A (en) * 2012-03-31 2012-08-01 山东喜丰田生态肥业有限公司 Novel polysaccharide gel water retaining and slow release fertilizer
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106590677A (en) * 2016-12-02 2017-04-26 重庆市江津区森德家庭农场 Multifunctional soil improvement agent and preparation method thereof
CN106748100A (en) * 2016-12-15 2017-05-31 涓ュ垢 A kind of low cost, the environmentally friendly film-coated and slow release fertilizer with water retaining function and preparation method thereof
CN107176881A (en) * 2017-06-28 2017-09-19 常州麒通国际贸易有限公司 A kind of Water-retaining slow-release fertilizer and preparation method thereof
CN108101626A (en) * 2017-12-14 2018-06-01 成都新柯力化工科技有限公司 A kind of ecology sustained release organic film fertilizer and preparation method

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