CN105401436A - Preparation method for flame-retardation finishing liquid for fabrics - Google Patents

Preparation method for flame-retardation finishing liquid for fabrics Download PDF

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Publication number
CN105401436A
CN105401436A CN201510949701.4A CN201510949701A CN105401436A CN 105401436 A CN105401436 A CN 105401436A CN 201510949701 A CN201510949701 A CN 201510949701A CN 105401436 A CN105401436 A CN 105401436A
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China
Prior art keywords
weight
parts
weight portion
stir
flame
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
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CN201510949701.4A
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Chinese (zh)
Inventor
俞佳美
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SUZHOU FUMEI TEXTILE TECHNOLOGY Co Ltd
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SUZHOU FUMEI TEXTILE TECHNOLOGY Co Ltd
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Priority to CN201510949701.4A priority Critical patent/CN105401436A/en
Publication of CN105401436A publication Critical patent/CN105401436A/en
Pending legal-status Critical Current

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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53Polyethers
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/68Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
    • D06M11/70Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
    • D06M11/71Salts of phosphoric acids
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/188Monocarboxylic acids; Anhydrides, halides or salts thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/248Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
    • D06M13/262Sulfated compounds thiosulfates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46Compounds containing quaternary nitrogen atoms
    • D06M13/463Compounds containing quaternary nitrogen atoms derived from monoamines
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03Polysaccharides or derivatives thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/30Flame or heat resistance, fire retardancy properties
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50Modified hand or grip properties; Softening compositions

Abstract

A disclosed preparation method for a flame-retardation finishing liquid for fabrics comprises the following steps: 1) 1-2 parts by weight of polyoxyethylene monolaurate, 1.1 parts by weight of gum acacia powder, 1.3 parts by weight of bis(2-hydroxyethyl)dimethylammonium chloride fatty acid ester, 0.9 part by weight of iso-tridecanol polyoxyethylene ether into 17 parts by mass of deionized water, and stirring uniformly; and 2) simultaneously pouring 1.3 parts by weight of RHIZOMA COPTIDIS extraction liquid, 2.2 parts by weight of acrylic acid, 1.7 parts by weight of dimethyl sulfate, and 0.3 part by weight of aluminium phosphate, and continuing to stir until the mixture is fully mixed, so as to prepare the finishing liquid. The prepared finishing solution is good in hydrophilicity and good in permeability. The fabrics finished by using the finishing solution possesses excellent flame resistance, mildew resistance, moth resistance, bacteria resistance and static electricity resistance, and is strong in washing fastness and soft in handfeel.

Description

The preparation method of flame-retardant fabric finishing liquid
Technical field
The present invention relates to the preparation method of flame-retardant fabric finishing liquid.
Background technology
The function singleness of existing dressing liquid, can not meet fire-retardant, the mildew-resistant of fabric panel, mothproof, antibacterial, antistatic washable arrangement requirement, and fabric panel feel after arranging is soft not.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of flame-retardant fabric finishing liquid, dressing liquid good hydrophilic property, the good penetrability of preparation, fabric panel after using this dressing liquid to arrange has excellent fire-retardant, mildew-resistant, mothproof, antibacterial, antistatic property, and washability is strong, soft.
For achieving the above object, technical scheme of the present invention designs a kind of preparation method of flame-retardant fabric finishing liquid, comprises the steps:
1) two to 1 ~ 2 weight portion laurate polyoxyethylene ester, 1.1 weight portion gum arabic powder, 1.3 weight portions-(2-ethoxy)-alkyl dimethyl ammonium chloride fatty acid ester, 0.9 weight portion isomerous tridecanol polyoxyethylene ether are dropped in 17 parts by mass deionized waters successively, stir;
2) drop into 1.3 weight portion rhizoma extracting liquids, 2.2 weight portion propionic acid, 1.7 parts sulfuric acid dimethyl esters, 0.3 parts by weight of phosphoric acid three aluminium more simultaneously, continue to stir, to fully mixing, obtained dressing liquid.
Preferably, the preparation method of flame-retardant fabric finishing liquid, comprises the steps:
1) two to 1 weight portion laurate polyoxyethylene ester, 1.1 weight portion gum arabic powder, 1.3 weight portions-(2-ethoxy)-alkyl dimethyl ammonium chloride fatty acid ester, 0.9 weight portion isomerous tridecanol polyoxyethylene ether are dropped in 17 parts by mass deionized waters successively, stir;
2) drop into 1.3 weight portion rhizoma extracting liquids, 2.2 weight portion propionic acid, 1.7 parts sulfuric acid dimethyl esters, 0.3 parts by weight of phosphoric acid three aluminium more simultaneously, continue to stir, to fully mixing, obtained dressing liquid.
Preferably, the preparation method of flame-retardant fabric finishing liquid, comprises the steps:
1) two to 2 weight portion laurate polyoxyethylene ester, 1.1 weight portion gum arabic powder, 1.3 weight portions-(2-ethoxy)-alkyl dimethyl ammonium chloride fatty acid ester, 0.9 weight portion isomerous tridecanol polyoxyethylene ether are dropped in 17 parts by mass deionized waters successively, stir;
2) drop into 1.3 weight portion rhizoma extracting liquids, 2.2 weight portion propionic acid, 1.7 parts sulfuric acid dimethyl esters, 0.3 parts by weight of phosphoric acid three aluminium more simultaneously, continue to stir, to fully mixing, obtained dressing liquid.
Advantage of the present invention and beneficial effect are: the preparation method providing a kind of flame-retardant fabric finishing liquid, dressing liquid good hydrophilic property, the good penetrability of preparation, fabric panel after using this dressing liquid to arrange has excellent fire-retardant, mildew-resistant, mothproof, antibacterial, antistatic property, and washability is strong, soft.
Detailed description of the invention
Below in conjunction with embodiment, the specific embodiment of the present invention is further described.Following examples only for technical scheme of the present invention is clearly described, and can not limit the scope of the invention with this.
The technical scheme that the present invention specifically implements is:
Embodiment 1
A preparation method for flame-retardant fabric finishing liquid, comprises the steps:
1) two to 1 ~ 2 weight portion laurate polyoxyethylene ester, 1.1 weight portion gum arabic powder, 1.3 weight portions-(2-ethoxy)-alkyl dimethyl ammonium chloride fatty acid ester, 0.9 weight portion isomerous tridecanol polyoxyethylene ether are dropped in 17 parts by mass deionized waters successively, stir;
2) drop into 1.3 weight portion rhizoma extracting liquids, 2.2 weight portion propionic acid, 1.7 parts sulfuric acid dimethyl esters, 0.3 parts by weight of phosphoric acid three aluminium more simultaneously, continue to stir, to fully mixing, obtained dressing liquid.
Embodiment 2
The preparation method of flame-retardant fabric finishing liquid, comprises the steps:
1) two to 1 weight portion laurate polyoxyethylene ester, 1.1 weight portion gum arabic powder, 1.3 weight portions-(2-ethoxy)-alkyl dimethyl ammonium chloride fatty acid ester, 0.9 weight portion isomerous tridecanol polyoxyethylene ether are dropped in 17 parts by mass deionized waters successively, stir;
2) drop into 1.3 weight portion rhizoma extracting liquids, 2.2 weight portion propionic acid, 1.7 parts sulfuric acid dimethyl esters, 0.3 parts by weight of phosphoric acid three aluminium more simultaneously, continue to stir, to fully mixing, obtained dressing liquid.
Embodiment 3
The preparation method of flame-retardant fabric finishing liquid, comprises the steps:
1) two to 2 weight portion laurate polyoxyethylene ester, 1.1 weight portion gum arabic powder, 1.3 weight portions-(2-ethoxy)-alkyl dimethyl ammonium chloride fatty acid ester, 0.9 weight portion isomerous tridecanol polyoxyethylene ether are dropped in 17 parts by mass deionized waters successively, stir;
2) drop into 1.3 weight portion rhizoma extracting liquids, 2.2 weight portion propionic acid, 1.7 parts sulfuric acid dimethyl esters, 0.3 parts by weight of phosphoric acid three aluminium more simultaneously, continue to stir, to fully mixing, obtained dressing liquid.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.

Claims (3)

1. the preparation method of flame-retardant fabric finishing liquid, is characterized in that, comprises the steps:
1) two to 1 ~ 2 weight portion laurate polyoxyethylene ester, 1.1 weight portion gum arabic powder, 1.3 weight portions-(2-ethoxy)-alkyl dimethyl ammonium chloride fatty acid ester, 0.9 weight portion isomerous tridecanol polyoxyethylene ether are dropped in 17 parts by mass deionized waters successively, stir;
2) drop into 1.3 weight portion rhizoma extracting liquids, 2.2 weight portion propionic acid, 1.7 parts sulfuric acid dimethyl esters, 0.3 parts by weight of phosphoric acid three aluminium more simultaneously, continue to stir, to fully mixing, obtained dressing liquid.
2. the preparation method of flame-retardant fabric finishing liquid according to claim 1, is characterized in that, comprises the steps:
1) two to 1 weight portion laurate polyoxyethylene ester, 1.1 weight portion gum arabic powder, 1.3 weight portions-(2-ethoxy)-alkyl dimethyl ammonium chloride fatty acid ester, 0.9 weight portion isomerous tridecanol polyoxyethylene ether are dropped in 17 parts by mass deionized waters successively, stir;
2) drop into 1.3 weight portion rhizoma extracting liquids, 2.2 weight portion propionic acid, 1.7 parts sulfuric acid dimethyl esters, 0.3 parts by weight of phosphoric acid three aluminium more simultaneously, continue to stir, to fully mixing, obtained dressing liquid.
3. the preparation method of flame-retardant fabric finishing liquid according to claim 1, is characterized in that, comprises the steps:
1) two to 2 weight portion laurate polyoxyethylene ester, 1.1 weight portion gum arabic powder, 1.3 weight portions-(2-ethoxy)-alkyl dimethyl ammonium chloride fatty acid ester, 0.9 weight portion isomerous tridecanol polyoxyethylene ether are dropped in 17 parts by mass deionized waters successively, stir;
2) drop into 1.3 weight portion rhizoma extracting liquids, 2.2 weight portion propionic acid, 1.7 parts sulfuric acid dimethyl esters, 0.3 parts by weight of phosphoric acid three aluminium more simultaneously, continue to stir, to fully mixing, obtained dressing liquid.
CN201510949701.4A 2015-12-18 2015-12-18 Preparation method for flame-retardation finishing liquid for fabrics Pending CN105401436A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510949701.4A CN105401436A (en) 2015-12-18 2015-12-18 Preparation method for flame-retardation finishing liquid for fabrics

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510949701.4A CN105401436A (en) 2015-12-18 2015-12-18 Preparation method for flame-retardation finishing liquid for fabrics

Publications (1)

Publication Number Publication Date
CN105401436A true CN105401436A (en) 2016-03-16

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101765629A (en) * 2007-07-28 2010-06-30 化学制造布敦海姆两合公司 Halogen-free flame-proofing agent
CN102803456A (en) * 2010-04-01 2012-11-28 赢创德固赛有限公司 Fabric softener active composition
CN103194893A (en) * 2013-04-24 2013-07-10 广州市番禺区协运来化工用品有限公司 Softener and preparation method thereof
CN103643483A (en) * 2013-12-04 2014-03-19 江苏博士邦尼时装有限公司 Production technology of anti-bacterial underwear fabric
CN103835126A (en) * 2013-12-12 2014-06-04 青岛无为保温材料有限公司 Novel mildew preventive for textile, and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101765629A (en) * 2007-07-28 2010-06-30 化学制造布敦海姆两合公司 Halogen-free flame-proofing agent
CN102803456A (en) * 2010-04-01 2012-11-28 赢创德固赛有限公司 Fabric softener active composition
CN103194893A (en) * 2013-04-24 2013-07-10 广州市番禺区协运来化工用品有限公司 Softener and preparation method thereof
CN103643483A (en) * 2013-12-04 2014-03-19 江苏博士邦尼时装有限公司 Production technology of anti-bacterial underwear fabric
CN103835126A (en) * 2013-12-12 2014-06-04 青岛无为保温材料有限公司 Novel mildew preventive for textile, and preparation method thereof

Non-Patent Citations (6)

* Cited by examiner, † Cited by third party
Title
刘程等: "《表面活性剂应用手册 第三版》", 30 September 2004 *
宋国艾等: "《化妆品原料技术规格》", 31 July 2000 *
廖双全等: "《热塑性弹性体及其应用》", 30 April 2014 *
张敏民: "《生态家用纺织品》", 31 July 2006 *
朱平: "《功能纤维及功能纺织品》", 31 August 2006 *
肖学福等: "《车辆装备封存技术》", 30 April 2013 *

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Application publication date: 20160316