CN105401296A - Manufacturing method for wool spinning fabric containing soybean fibers - Google Patents
Manufacturing method for wool spinning fabric containing soybean fibers Download PDFInfo
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- CN105401296A CN105401296A CN201510686599.3A CN201510686599A CN105401296A CN 105401296 A CN105401296 A CN 105401296A CN 201510686599 A CN201510686599 A CN 201510686599A CN 105401296 A CN105401296 A CN 105401296A
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
- D03D15/533—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads antistatic; electrically conductive
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
- D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
- D02G3/04—Blended or other yarns or threads containing components made from different materials
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D13/00—Woven fabrics characterised by the special disposition of the warp or weft threads, e.g. with curved weft threads, with discontinuous warp threads, with diagonal warp or weft
- D03D13/004—Woven fabrics characterised by the special disposition of the warp or weft threads, e.g. with curved weft threads, with discontinuous warp threads, with diagonal warp or weft with weave pattern being non-standard or providing special effects
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B13/00—Treatment of textile materials with liquids, gases or vapours with aid of vibration
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/14—Wool
- D06P3/148—Wool using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
- D06M2101/12—Keratin fibres or silk
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2211/00—Protein-based fibres, e.g. animal fibres
- D10B2211/01—Natural animal fibres, e.g. keratin fibres
- D10B2211/02—Wool
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2211/00—Protein-based fibres, e.g. animal fibres
- D10B2211/20—Protein-derived artificial fibres
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/16—Physical properties antistatic; conductive
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
Abstract
The invention relates to a manufacturing method for a wool spinning fabric containing soybean fibers. The fabric contains non-shrinkable wool whose specifications are 70 S-80 S of fineness and 60-70 mm of length, and soybean fibers whose specification is 4-5 dtex*(65-70) mm. Mass percentage of the two components of the non-shrinkable wool and the soybean fibers is 30-60% to 70-40%. The method comprises: dyeing non-shrinkable wool balls into color wool tops, dyeing soybean yarns, through silver blending, the yarns being woven into spun yarns, and through posterior spinning, fine yarns being obtained, a wool spinning fabric being made by the manufacturing method, and the fabric being made into the wool spinning fabric containing soybean fibers through two-time soaking and binding fabric processing. The fabric and the manufacturing method can effectively improve transmittance, moisture permeability and air permeability. The fabric has good soft hand feeling, tender luster like silk, heat retention property of cotton, and good skin-friendly and other excellent properties. The fabric has obvious bacteriostasis function, fastness to rubbing, color fastness to washing, and has good antistatic property, flame retardant property, and permeability, and has health care effect.
Description
Technical field
The present invention relates to weaving face fabric production art field, be specifically related to a kind of manufacture method containing fibre and soya wool spinning fabric.
Background technology
Wool fibre is the deformations of the skin of sheep, and warmth retention property is splendid, is used for the clothes of autumn and winter season, but very easily damages by worms, and the time of dress has been grown and easily grown various germ.Weaving wool fibre is main is sheep's wool, so-called wool, or claims wool fibre, or is called for short hair.Wool is natural protein fibre, and main component makes the protein of angle protein form, and angle protein content accounts for 97%, and inorganic matter accounts for 1 ~ 3%, and the essential element of wool angle protein is C, O, N, H, S.
Because wool surface has scale layer, in washing process, easily produce shrinkage, shape is unstable, have much the treatable research of wool fibre, be divested by physics, chemical method or weaken the scale layer of wool fibre mostly, thus improve the shortcoming of its shrinkage; But adopt Chemical Physics method inevitably to use various physics and chemistry reagent, it not only can residue in wool fibre, also pollute the environment, produce a large amount of industrial wastewaters, such as, in prior art conventional chloridizing and permanganimetric method (as CN201010269379).Along with the development of biological zymetology, the defect utilizing zymetology technology to change wool fibre is problem more popular in recent years.Chinese patent CN200810059502 and CN201010127072, all employs enzyme preparation, but in said method, many places employ chemical reagent equally, easily causes environmental pollution, and can partly residue in wool fibre, works the mischief to human body.
How utilizing merely enzyme preparation to process wool fibre, and reach the object of wrinkle resistant environmental protection, is prior art technical problem anxious to be resolved.
Current in addition, adopt colloidal sol to carry out functionalization to textiles in the prior art to arrange and mainly realized by following approach: first prepare Nano sol by sol-gel process, then its gelation is made, then by gel drying with remove the inside organic principle, under the high temperature of 300 ~ 800 DEG C, ultra-fine nano-powder is made in roasting again, and the functional modification finally nano-powder being applied to textiles arranges.
Wool spinning fabric is the important fabric with making high-grade business shirt, and wool spinning fabric good hand touch is comfortable and easy to wear, dark liking by consumers in general.But carry out health care arrangement to it at present, thus meet people and have to it function energy sexual demand had containing fibre and soya, need further research and development.
Summary of the invention
The object of the invention is to overcome defect of the prior art, design one effectively can improve transmitance, vapor transfer rate and air penetrability, there is good soft feel, fastness to rubbing, color fastness to washing, and there is good antistatic behaviour, fire resistance and gas permeability, also have the manufacture method of health-care effect containing fibre and soya wool spinning fabric.
For achieving the above object, the technical solution adopted in the present invention is:
Containing a manufacture method for fibre and soya wool spinning fabric, described fabric comprises: specification is fineness 70
s~ 80
s, length is the non-shrinkable wool of 60 ~ 70mm; Specification is the fibre and soya of 4 ~ 5dtexX (65 ~ 70) mm; The mass percent of non-shrinkable wool and fibre and soya two components is 30 ~ 60%:70 ~ 40%; By non-shrinkable wool hair ball dyeing make coloured wool top, soybean yarn is dyeed, adopt strip mixing be spun into spun yarn, then through after spin to obtain spun yarn, manufacture containing fibre and soya wool spinning fabric by manufacturing technique; The concrete steps of described manufacture method comprise:
S1, by non-shrinkable wool hair ball bar dye recombing: by pine group, dyeing, combing, obtain wool yarn;
S2, produce fibre and soya strip: by fibre and soya dyeing yarn, obtain fibre and soya vitta;
S3, rove spin: wool yarn and fibre and soya vitta adopt wool top to mix and be spun into rove;
S4, after spin: through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting, obtain spun yarn; Described yarn steaming temperature is 75 ~ 90 DEG C, 80 ~ 120 minutes time; The speed of a motor vehicle of described high speed doubling is 500 ~ 700 ms/min, and the double twisting speed of a motor vehicle is 5000 ~ 8000 revs/min;
S5, by fabric manufacturing process and finishing technique, make the worsted fabric of wool fibre and fibre and soya blending;
S6, first time dip fabric: the worsted fabric of wool fibre and fibre and soya blending two is soaked two and rolls in coloured Nano silica sol, and pressure is 0.5 ~ 2.5kg/cm
2, pick-up is 75 ~ 85%, preliminary drying under the temperature conditions of 70 ~ 90 DEG C, then under the temperature conditions of 120 ~ 180 DEG C, bake 3 ~ 5 minutes;
S7, second time dip fabric: dip the fabric after oven dry by through first time, then put into the scented tea wood aqueous solution two and soak and two to roll, and pressure is 1 ~ 3kg/cm
2, pick-up is 60 ~ 80%, preliminary drying under the temperature conditions of 60 ~ 80 DEG C, then under the temperature conditions of 100 ~ 160 DEG C, bake 2 ~ 3 minutes; Through washing, after naturally drying, obtain containing fibre and soya wool spinning fabric.
Preferred technical scheme is, described in state the dyeing of non-shrinkable wool hair ball and adopt REACTIVE DYES, described fibre and soya dyeing yarn adopts DISPERSE DYES.
Preferred technical scheme also has, and the number of described worsted yarn is 90 ~ 120/2.
Preferred technical scheme also has, and the fabric construction of described fabric to adopt on plain weave, two once twill or cassimere twill.
Preferred technical scheme also has, and described coloured Nano silica sol is in molar ratio, ethanol: ethyl silicate 40 is 2 ~ 11:1, water: ethyl silicate 40 is 5 ~ 20:0.5, FeCl
36H2O: ethyl silicate 40 is 0.6 ~ 0.8:0.6, is prepared from.
Preferred technical scheme also has further, described coloured Nano silica sol adopts sol-gel process preparation, step comprises: by even to ethyl silicate 40, ethanol and mixed in hydrochloric acid, slowly drip the iron ion aqueous solution under agitation, 50 ~ 70 DEG C are warming up to again after dropwising, stir 2.5 ~ 3 hours, namely obtain a kind of coloured Nano silica sol.
Preferred technical scheme also has, and the making of the described scented tea wood aqueous solution comprises:
The preparation of scented tea material water, producer in Tea Production process is savored tealeaves to select the tea rim charges such as rear remaining tea head, tea stalk, tea dust, Lao Ye and mix after preliminary cleaning, boil 3 ~ 4 hours with the temperature of 90 DEG C ~ 100 DEG C, then obtain scented tea material water by filtering, distilling;
The preparation of incense wood material water, by the incense wood material for preparing through preliminary cleaning, digesting apparatus boiling is put into after draining, first with 60 DEG C of temperature boilings 3 hours, be warming up to 120 DEG C and continue boiling about 3 ~ 4 hours, until wooden aromatic flavour and do not have the smell of burning, period repeatedly can stir the dissolving that short raw material promote incense wood material, is then filtered, distills and obtain incense wood material water;
Mixing, mixes scented tea material water and incense wood material water by weight 60% ~ 80%:40% ~ 20% proportioning and both obtains the wooden aqueous solution of scented tea.
Preferred technical scheme also has, and first time of described S6 step dips second time that fabric and S7 walk and dips in fabric process and need respectively to carry out microwave treatment, and microwave frequency is 130MHz ~ 280MHz, and microwave treatment time is 6 ~ 8min.
Advantage of the present invention and beneficial effect are: the described manufacture method containing fibre and soya wool spinning fabric can make up the deficiency of wool fibre, and developing can at the health care wool worsted fabric being applicable to take each season.Breakthrough wool worsted fabric is taken limitation in season by the present invention, expands the scope of application of wool worsted fabric, also can meet consumer in spring, autumn, wear the demand of high-grade woolen winter.Innovated by raw material simultaneously, by fibre and soya and fleece fibre blended spinning, hand over also, interweave, give flexibility, skin-friendly that fabric is lasting.Because fibre and soya has, fineness is thin, light specific gravity, TENSILE STRENGTH are high, acid-fast alkali-proof is strong, Moisture absorption & moisture conductivity is good.And be better than the feel of cashmere, gloss can compare favourably with silk, the premium properties such as cotton warmth retention property and good skin-friendly, also have obvious bacteria resistance function, be described as " the healthy comfortable environment-protection fiber of new century ", thus overcome the shortcoming of current wool bacteriostasis property difference, what expand wool takes scope, improve the added value of wool product, be conducive to the development of wool textile industry, meet modern textiles trend.
In addition owing to selecting ethyl silicate 40 to be the sol solutions of precursor power containing iron ion, sol solutions is coloured, nontoxic, and sol particles is uniformly dispersed and stablizes; Adopt and roll the method for sorting curing this applicable textiles, only need carry out the heat treatment of 100 ~ 160 DEG C to fabric, can be formed at fabric face and adsorb firmly gel film.Fabric after arrangement not only has the color compared with high color fastness, have also obtained excellent antistatic behaviour, anti-flammability and gas permeability simultaneously.
After have employed scented tea wood again mixed liquor dipping, make the weaving woollen internal penetration aromatic odor of tea material and timber, effectively can remove the pollutants such as formaldehyde in air, clean air, make fabric have cleaning efficacy; Fabric itself can give out unique tea wood mixing natural flavor, can calm the nerves salubrious, have health care effectiveness, and fragrance is prolonged does not fall apart.
The present invention not only solves the potential pollution problem of existing hair side material, more effectively improve effect and the quality of existing hair side material, also solve a large amount of tea rim charge simultaneously, wood boundary material leave unused, the problem such as production waste and environmental pollution that processing procedure is brought, be environmental protection, health care, comfortableness the technical scheme of depositing.
Detailed description of the invention
Below in conjunction with embodiment, the specific embodiment of the present invention is further described.Following examples only for technical scheme of the present invention is clearly described, and can not limit the scope of the invention with this.
Embodiment 1
The present invention is a kind of manufacture method containing fibre and soya wool spinning fabric, and described fabric comprises: specification is fineness 70
s, length is the non-shrinkable wool of 60mm; Specification is the fibre and soya of 4dtexX65mm; The mass percent of non-shrinkable wool and fibre and soya two components is 30%:70%; By non-shrinkable wool hair ball dyeing make coloured wool top, soybean yarn is dyeed, adopt strip mixing be spun into spun yarn, then through after spin to obtain spun yarn, manufacture containing fibre and soya wool spinning fabric by manufacturing technique; The concrete steps of described manufacture method comprise:
S1, by non-shrinkable wool hair ball bar dye recombing: by pine group, dyeing, combing, obtain wool yarn;
S2, produce fibre and soya strip: by fibre and soya dyeing yarn, obtain fibre and soya vitta;
S3, rove spin: wool yarn and fibre and soya vitta adopt wool top to mix and be spun into rove;
S4, after spin: through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting, obtain spun yarn; Described yarn steaming temperature is 75 DEG C, 80 minutes time; The speed of a motor vehicle of described high speed doubling is 500 ms/min, and the double twisting speed of a motor vehicle is 5000 revs/min;
S5, by fabric manufacturing process and finishing technique, make the worsted fabric of wool fibre and fibre and soya blending;
S6, first time dip fabric: the worsted fabric of wool fibre and fibre and soya blending two is soaked two and rolls in coloured Nano silica sol, and pressure is 1.5kg/cm
2, pick-up is 75%, preliminary drying under the temperature conditions of 70 DEG C, then under the temperature conditions of 120 DEG C, bake 3 minutes;
S7, second time dip fabric: dip the fabric after oven dry by through first time, then put into the scented tea wood aqueous solution two and soak and two to roll, and pressure is 1kg/cm
2, pick-up is 60%, preliminary drying under the temperature conditions of 60 DEG C, then under the temperature conditions of 100 DEG C, bake 2 minutes; Through washing, after naturally drying, obtain containing fibre and soya wool spinning fabric.
The preferred embodiment of the invention is, described in state the dyeing of non-shrinkable wool hair ball and adopt REACTIVE DYES, described fibre and soya dyeing yarn adopts DISPERSE DYES.
The preferred embodiment of the invention also has, and the number of described worsted yarn is 90/2.
The preferred embodiment of the invention also has, and the fabric construction of described fabric to adopt on plain weave, two once twill or cassimere twill.
The preferred embodiment of the invention also has, and described coloured Nano silica sol is in molar ratio, ethanol: ethyl silicate 40 is 2:1, water: ethyl silicate 40 is 5:0.5, FeCl
36H2O: ethyl silicate 40 is 0.6:0.6, is prepared from.
Further preferred embodiment of the present invention also has, described coloured Nano silica sol adopts sol-gel process preparation, step comprises: by even to ethyl silicate 40, ethanol and mixed in hydrochloric acid, slowly drip the iron ion aqueous solution under agitation, 50 DEG C are warming up to again after dropwising, stir 2.5 hours, namely obtain a kind of coloured Nano silica sol.
41.7gTEOS, 27.6gEtOH and appropriate HCl are joined in 500ml tri-mouthfuls of round-bottomed flasks successively, regulates pH to be 2 ~ 3.Stir under the rotating speed of 100 revs/min, mix the iron ion aqueous solution (5.42gFeCl36H2O+7.2gH2O) while stirring, and at 50 DEG C, continue stirring 2.5 hours.Namely transparent, coloured and uniform nanometer coloured silicasol system is obtained.Wool spinning fabric first time two leaching two in nanometer coloured silicasol is rolled, pressure 1kg/cm
2, pick-up 80%.Then 60 DEG C of preliminary dryings in convection oven, bake 3 minutes after washings, naturally dry at 130 DEG C.
First there is poly-condensation and hydrolysis in ethyl silicate 40, generate sol particles in alcohol solvent; Mix iron ion, form the coloured Nano silica sol of tool.Be adsorbed onto fully on fabric by this colloidal sol by the mode of padding, in follow-up heating process, colloidal sol changes xerogel into and at the surface filming of fabric, and this film can firmly cover at web surface, to realize arranging the functional modification of fabric.
The preferred embodiment of the invention also has, and the making of the described scented tea wood aqueous solution comprises:
The preparation of scented tea material water, producer in Tea Production process is savored tealeaves to select the tea rim charges such as rear remaining tea head, tea stalk, tea dust, Lao Ye and mix after preliminary cleaning, boil 3 hours with the temperature of 90 DEG C, then obtain scented tea material water by filtering, distilling;
The preparation of incense wood material water, by the incense wood material for preparing through preliminary cleaning, digesting apparatus boiling is put into after draining, first with 60 DEG C of temperature boilings 3 hours, be warming up to 120 DEG C and continue boiling about 3 hours, until wooden aromatic flavour and do not have the smell of burning, period repeatedly can stir the dissolving that short raw material promote incense wood material, is then filtered, distills and obtain incense wood material water;
Mixing, mixes scented tea material water and incense wood material water by weight 60%:40% proportioning and both obtains the wooden aqueous solution of scented tea.
The preferred technical scheme of the present invention also has, and first time of described S6 step dips second time that fabric and S7 walk and dips in fabric process and need respectively to carry out microwave treatment, and microwave frequency is 130MHz, and microwave treatment time is 6min.
Embodiment 2
The present invention is a kind of manufacture method containing fibre and soya wool spinning fabric, and described fabric comprises: specification is fineness 75
s, length is the non-shrinkable wool of 65mm; Specification is the fibre and soya of 4dtexX65mm; The mass percent of non-shrinkable wool and fibre and soya two components is 45%:55%; By non-shrinkable wool hair ball dyeing make coloured wool top, soybean yarn is dyeed, adopt strip mixing be spun into spun yarn, then through after spin to obtain spun yarn, manufacture containing fibre and soya wool spinning fabric by manufacturing technique; The concrete steps of described manufacture method comprise:
S1, by non-shrinkable wool hair ball bar dye recombing: by pine group, dyeing, combing, obtain wool yarn;
S2, produce fibre and soya strip: by fibre and soya dyeing yarn, obtain fibre and soya vitta;
S3, rove spin: wool yarn and fibre and soya vitta adopt wool top to mix and be spun into rove;
S4, after spin: through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting, obtain spun yarn; Described yarn steaming temperature is 80 DEG C, 100 minutes time; The speed of a motor vehicle of described high speed doubling is 600 ms/min, and the double twisting speed of a motor vehicle is 6500 revs/min;
S5, by fabric manufacturing process and finishing technique, make the worsted fabric of wool fibre and fibre and soya blending;
S6, first time dip fabric: the worsted fabric of wool fibre and fibre and soya blending two is soaked two and rolls in coloured Nano silica sol, and pressure is 0.5kg/cm
2, pick-up is 85%, preliminary drying under the temperature conditions of 90 DEG C, then under the temperature conditions of 180 DEG C, bake 5 minutes;
S7, second time dip fabric: dip the fabric after oven dry by through first time, then put into the scented tea wood aqueous solution two and soak and two to roll, and pressure is 2kg/cm
2, pick-up is 70%, preliminary drying under the temperature conditions of 70 DEG C, then under the temperature conditions of 130 DEG C, bake 2 minutes; Through washing, after naturally drying, obtain containing fibre and soya wool spinning fabric.
The preferred embodiment of the invention is, described in state the dyeing of non-shrinkable wool hair ball and adopt REACTIVE DYES, described fibre and soya dyeing yarn adopts DISPERSE DYES.
The preferred embodiment of the invention also has, and the number of described worsted yarn is 100/2.
The preferred embodiment of the invention also has, and the fabric construction of described fabric to adopt on plain weave, two once twill or cassimere twill.
The preferred embodiment of the invention also has, and described coloured Nano silica sol is in molar ratio, ethanol: ethyl silicate 40 is 2:1, water: ethyl silicate 40 is 5:0.5, FeCl
36H2O: ethyl silicate 40 is 0.6:0.6, is prepared from.
Further preferred embodiment of the present invention also has, described coloured Nano silica sol adopts sol-gel process preparation, step comprises: by even to ethyl silicate 40, ethanol and mixed in hydrochloric acid, slowly drip the iron ion aqueous solution under agitation, 60 DEG C are warming up to again after dropwising, stir 2.5 hours, namely obtain a kind of coloured Nano silica sol.
41.7gTEOS, 73.6gEtOH and appropriate HCl are joined in 500ml tri-mouthfuls of round-bottomed flasks successively, regulates pH to be 2 ~ 3.Stir under the rotating speed of 250 revs/min, mix the iron ion aqueous solution (5.42gFeCl36H2O+36.0gH2O) while stirring, and at 70 DEG C, continue stirring 2 hours.Namely transparent, coloured and uniform nanometer coloured silicasol system is obtained.Wool spinning fabric two leachings two in nanometer coloured silicasol are rolled, pressure 2kg/cm
2, pick-up 70%, then 60 DEG C of preliminary dryings in convection oven, bake 2 minutes after washings, naturally dry at 150 DEG C.
First there is poly-condensation and hydrolysis in ethyl silicate 40, generate sol particles in alcohol solvent; Mix iron ion, form the coloured Nano silica sol of tool.Be adsorbed onto fully on fabric by this colloidal sol by the mode of padding, in follow-up heating process, colloidal sol changes xerogel into and at the surface filming of fabric, and this film can firmly cover at web surface, to realize arranging the functional modification of fabric.
The preferred embodiment of the invention also has, and the making of the described scented tea wood aqueous solution comprises:
The preparation of scented tea material water, producer in Tea Production process is savored tealeaves to select the tea rim charges such as rear remaining tea head, tea stalk, tea dust, Lao Ye and mix after preliminary cleaning, boil 3.5 hours with the temperature of 95 DEG C, then obtain scented tea material water by filtering, distilling;
The preparation of incense wood material water, by the incense wood material for preparing through preliminary cleaning, digesting apparatus boiling is put into after draining, first with 60 DEG C of temperature boilings 3 hours, be warming up to 120 DEG C and continue boiling about 3 hours, until wooden aromatic flavour and do not have the smell of burning, period repeatedly can stir the dissolving that short raw material promote incense wood material, is then filtered, distills and obtain incense wood material water;
Mixing, mixes scented tea material water and incense wood material water by weight 70%:30% proportioning and both obtains the wooden aqueous solution of scented tea.
The preferred technical scheme of the present invention also has, and first time of described S6 step dips second time that fabric and S7 walk and dips in fabric process and need respectively to carry out microwave treatment, and microwave frequency is 200MHz, and microwave treatment time is 7min.
Embodiment 3
The present invention is a kind of manufacture method containing fibre and soya wool spinning fabric, and described fabric comprises: specification is fineness 80
s, length is the non-shrinkable wool of 70mm; Specification is the fibre and soya of 4dtexX70mm; The mass percent of non-shrinkable wool and fibre and soya two components is 60%:40%; By non-shrinkable wool hair ball dyeing make coloured wool top, soybean yarn is dyeed, adopt strip mixing be spun into spun yarn, then through after spin to obtain spun yarn, manufacture containing fibre and soya wool spinning fabric by manufacturing technique; The concrete steps of described manufacture method comprise:
S1, by non-shrinkable wool hair ball bar dye recombing: by pine group, dyeing, combing, obtain wool yarn;
S2, produce fibre and soya strip: by fibre and soya dyeing yarn, obtain fibre and soya vitta;
S3, rove spin: wool yarn and fibre and soya vitta adopt wool top to mix and be spun into rove;
S4, after spin: through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting, obtain spun yarn; Described yarn steaming temperature is 90 DEG C, 120 minutes time; The speed of a motor vehicle of described high speed doubling is 700 ms/min, and the double twisting speed of a motor vehicle is 8000 revs/min;
S5, by fabric manufacturing process and finishing technique, make the worsted fabric of wool fibre and fibre and soya blending;
S6, first time dip fabric: the worsted fabric of wool fibre and fibre and soya blending two is soaked two and rolls in coloured Nano silica sol, and pressure is 2.5kg/cm
2, pick-up is 80%, preliminary drying under the temperature conditions of 80 DEG C, then under the temperature conditions of 150 DEG C, bake 4 minutes;
S7, second time dip fabric: dip the fabric after oven dry by through first time, then put into the scented tea wood aqueous solution two and soak and two to roll, and pressure is 3kg/cm
2, pick-up is 80%, preliminary drying under the temperature conditions of 80 DEG C, then under the temperature conditions of 160 DEG C, bake 3 minutes; Through washing, after naturally drying, obtain containing fibre and soya wool spinning fabric.
The preferred embodiment of the invention is, described in state the dyeing of non-shrinkable wool hair ball and adopt REACTIVE DYES, described fibre and soya dyeing yarn adopts DISPERSE DYES.
The preferred embodiment of the invention also has, and the number of described worsted yarn is 120/2.
The preferred embodiment of the invention also has, and the fabric construction of described fabric to adopt on plain weave, two once twill or cassimere twill.
The preferred embodiment of the invention also has, and described coloured Nano silica sol is in molar ratio, ethanol: ethyl silicate 40 is 11:1, water: ethyl silicate 40 is 20:0.5, FeCl
36H2O: ethyl silicate 40 is 0.8:0.6, is prepared from.
Further preferred embodiment of the present invention also has, described coloured Nano silica sol adopts sol-gel process preparation, step comprises: by even to ethyl silicate 40, ethanol and mixed in hydrochloric acid, slowly drip the iron ion aqueous solution under agitation, 70 DEG C are warming up to again after dropwising, stir 3 hours, namely obtain a kind of coloured Nano silica sol.
41.7gTEOS, 119.6gEtOH and appropriate HCl are joined in 500ml tri-mouthfuls of round-bottomed flasks successively, regulates pH to be 2 ~ 3.Stir under the rotating speed of 500 revs/min, mix the iron ion aqueous solution (5.42gFeCl36H2O+57.6gH2O) while stirring, and at 70 DEG C, continue stirring 2 hours.Namely transparent, coloured and uniform nanometer coloured silicasol system is obtained.Wool spinning fabric two leachings two in the nanometer coloured silicasol prepared are rolled, pressure 3kg/cm
2, pick-up 90%.Then 70 DEG C of preliminary dryings in convection oven, bake 2 minutes after washings, naturally dry at 150 DEG C.
First there is poly-condensation and hydrolysis in ethyl silicate 40, generate sol particles in alcohol solvent; Mix iron ion, form the coloured Nano silica sol of tool.Be adsorbed onto fully on fabric by this colloidal sol by the mode of padding, in follow-up heating process, colloidal sol changes xerogel into and at the surface filming of fabric, and this film can firmly cover at web surface, to realize arranging the functional modification of fabric.
The preferred embodiment of the invention also has, and the making of the described scented tea wood aqueous solution comprises:
The preparation of scented tea material water, producer in Tea Production process is savored tealeaves to select the tea rim charges such as rear remaining tea head, tea stalk, tea dust, Lao Ye and mix after preliminary cleaning, boil 4 hours with the temperature of 100 DEG C, then obtain scented tea material water by filtering, distilling;
The preparation of incense wood material water, by the incense wood material for preparing through preliminary cleaning, digesting apparatus boiling is put into after draining, first with 60 DEG C of temperature boilings 3 hours, be warming up to 120 DEG C and continue boiling about 4 hours, until wooden aromatic flavour and do not have the smell of burning, period repeatedly can stir the dissolving that short raw material promote incense wood material, is then filtered, distills and obtain incense wood material water;
Mixing, mixes scented tea material water and incense wood material water by weight 80%:20% proportioning and both obtains the wooden aqueous solution of scented tea.
The preferred technical scheme of the present invention also has, and first time of described S6 step dips second time that fabric and S7 walk and dips in fabric process and need respectively to carry out microwave treatment, and microwave frequency is 280MHz, and microwave treatment time is 8min.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (8)
1., containing a manufacture method for fibre and soya wool spinning fabric, it is characterized in that, described fabric comprises: specification is fineness 70
s~ 80
s, length is the non-shrinkable wool of 60 ~ 70mm; Specification is the fibre and soya of 4 ~ 5dtexX (65 ~ 70) mm; The mass percent of non-shrinkable wool and fibre and soya two components is 30 ~ 60%:70 ~ 40%; By non-shrinkable wool hair ball dyeing make coloured wool top, soybean yarn is dyeed, adopt strip mixing be spun into spun yarn, then through after spin to obtain spun yarn, manufacture containing fibre and soya wool spinning fabric by manufacturing technique; The concrete steps of described manufacture method comprise:
S1, by non-shrinkable wool hair ball bar dye recombing: by pine group, dyeing, combing, obtain wool yarn;
S2, produce fibre and soya strip: by fibre and soya dyeing yarn, obtain fibre and soya vitta;
S3, rove spin: wool yarn and fibre and soya vitta adopt wool top to mix and be spun into rove;
S4, after spin: through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting, obtain spun yarn; Described yarn steaming temperature is 75 ~ 90 DEG C, 80 ~ 120 minutes time; The speed of a motor vehicle of described high speed doubling is 500 ~ 700 ms/min, and the double twisting speed of a motor vehicle is 5000 ~ 8000 revs/min;
S5, by fabric manufacturing process and finishing technique, make the worsted fabric of wool fibre and fibre and soya blending;
S6, first time dip fabric: the worsted fabric of wool fibre and fibre and soya blending two is soaked two and rolls in coloured Nano silica sol, and pressure is 0.5 ~ 2.5kg/cm
2, pick-up is 75 ~ 85%, preliminary drying under the temperature conditions of 70 ~ 90 DEG C, then under the temperature conditions of 120 ~ 180 DEG C, bake 3 ~ 5 minutes;
S7, second time dip fabric: dip the fabric after oven dry by through first time, then put into the scented tea wood aqueous solution two and soak and two to roll, and pressure is 1 ~ 3kg/cm
2, pick-up is 60 ~ 80%, preliminary drying under the temperature conditions of 60 ~ 80 DEG C, then under the temperature conditions of 100 ~ 160 DEG C, bake 2 ~ 3 minutes; Through washing, after naturally drying, obtain containing fibre and soya wool spinning fabric.
2. the manufacture method containing fibre and soya wool spinning fabric as claimed in claim 1, is characterized in that, described in state the dyeing of non-shrinkable wool hair ball and adopt REACTIVE DYES, described fibre and soya dyeing yarn adopts DISPERSE DYES.
3. the manufacture method containing fibre and soya wool spinning fabric as claimed in claim 1, it is characterized in that, the number of described worsted yarn is 90 ~ 120/2.
4. the manufacture method containing fibre and soya wool spinning fabric as claimed in claim 1, is characterized in that, the fabric construction of described fabric to adopt on plain weave, two once twill or cassimere twill.
5. the manufacture method containing fibre and soya wool spinning fabric as claimed in claim 1, it is characterized in that, described coloured Nano silica sol is in molar ratio, ethanol: ethyl silicate 40 is 2 ~ 11:1, water: ethyl silicate 40 is 5 ~ 20:0.5, FeCl
36H2O: ethyl silicate 40 is 0.6 ~ 0.8:0.6, is prepared from.
6. the manufacture method containing fibre and soya wool spinning fabric as claimed in claim 5, it is characterized in that, described coloured Nano silica sol adopts sol-gel process preparation, step comprises: by even to ethyl silicate 40, ethanol and mixed in hydrochloric acid, slowly drip the iron ion aqueous solution under agitation, be warming up to 50 ~ 70 DEG C again after dropwising, stir 2.5 ~ 3 hours, namely obtain a kind of coloured Nano silica sol.
7. the manufacture method containing fibre and soya wool spinning fabric as claimed in claim 1, is characterized in that, the making of the described scented tea wood aqueous solution comprises:
The preparation of scented tea material water, producer in Tea Production process is savored tealeaves to select the tea rim charges such as rear remaining tea head, tea stalk, tea dust, Lao Ye and mix after preliminary cleaning, boil 3 ~ 4 hours with the temperature of 90 DEG C ~ 100 DEG C, then obtain scented tea material water by filtering, distilling;
The preparation of incense wood material water, by the incense wood material for preparing through preliminary cleaning, digesting apparatus boiling is put into after draining, first with 60 DEG C of temperature boilings 3 hours, be warming up to 120 DEG C and continue boiling about 3 ~ 4 hours, until wooden aromatic flavour and do not have the smell of burning, period repeatedly can stir the dissolving that short raw material promote incense wood material, is then filtered, distills and obtain incense wood material water;
Mixing, mixes scented tea material water and incense wood material water by weight 60% ~ 80%:40% ~ 20% proportioning and both obtains the wooden aqueous solution of scented tea.
8. the manufacture method containing fibre and soya wool spinning fabric as claimed in claim 1, it is characterized in that, first time of described S6 step dips second time that fabric and S7 walk and dips in fabric process and need respectively to carry out microwave treatment, microwave frequency is 130MHz ~ 280MHz, and microwave treatment time is 6 ~ 8min.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110453340A (en) * | 2019-09-04 | 2019-11-15 | 江苏阳光股份有限公司 | A kind of production technology of mercerized wool soybean fiber worsted fabric |
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