CN105379771A - Plant-derived pesticide and its preparation method and use - Google Patents

Plant-derived pesticide and its preparation method and use Download PDF

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Publication number
CN105379771A
CN105379771A CN201510937787.9A CN201510937787A CN105379771A CN 105379771 A CN105379771 A CN 105379771A CN 201510937787 A CN201510937787 A CN 201510937787A CN 105379771 A CN105379771 A CN 105379771A
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plant
plant insecticide
leaf
ash
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罗永城
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/38Solanaceae [Potato family], e.g. nightshade, tomato, tobacco or chilli pepper
    • A01N65/385Tobacco
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Mycology (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a plant-derived pesticide and its preparation method and use and belongs to the technical field of pesticide preparation. The plant-derived pesticide is prepared from tobacco, common threewingnut root, capsicum, rhizome of Chinese monkshood, pyrethrum, Azadirachta indica, tea leaves, patrinia herb, bitter herbs, wormwood, ash bark, radix sophorae flavescentis, Euphorbia songarica Boiss, Derris fordii Oliv., Chinese prickly ash, purslane, mandala, Anabasis Aphylla L., leaves of Salix babylonica, leaves of Pterocarya stenoptera and water. The plant-derived pesticide is prepared by soup extraction, condensation, drying, crushing, sieving and disinfection. The plant-derived pesticide is nontoxic and harmless, does not produce residues, is harmless, is environmentally friendly, does not pollute the environment, can effectively prevent and control injurious insects such as yellow spider, arrowhead scales, leaf roller moth and fruit fly, has a one-step killing rate of 95.41% or more, has no drug resistance and can be used for 4-6 years.

Description

A kind of plant insecticide, preparation method and application thereof
Technical field
The invention belongs to insecticide preparing technical field, be specifically related to a kind of plant insecticide, preparation method and application thereof.
Background technology
Current control pest all use chemical insecticide mostly, along with the raising of living standards of the people, require high, not only will eat, and will eat health agricultural product quality.The Pesticide Residue that high malicious chemical pesticide causes more and more becomes the focus of social concerns.High-toxic pesticide is the core and the key that affect agricultural product quality and safety, not only affects agricultural product quality, directly endangers the healthy of the people, also affects increasing peasant income.Because the toxicity of high-toxic pesticide is large, the event of person poultry poisoning was caused to happen occasionally in the past.Very big on the impact of women and children, the children that teratogenesis is disabled are a lot.In addition, along with the protective awareness of countries in the world to environment for human survival and natural, ecological strengthens day by day, high malicious high residue insecticide will be restricted further.The quality safety of unreasonable use to agricultural product of agricultural chemicals constitutes a threat to, therefore, reduce Pesticide use particularly high-toxic pesticide use, to raising agricultural product quality and the market competitiveness, promote China's agricultural sustainable development, ensure the life security of broad masses of the people and very great meaning of building a harmonious society.
Because chemical pesticide is easy to the pesticide resistance causing insect; dosage is made in order to control efficiency well constantly increases; a lot of natural enemy and beneficial organism are murdered; and pollute us and to depend on for existence living environment; the more and more attention of Environmental protection; will be further strict to the Detecting Pesticide in agricultural product, therefore, greatly develop the direction that non-toxic and non-pollution high-efficiency plant source pesticide is Agrochemicals from now on.
Summary of the invention
The invention provides a kind of plant insecticide, preparation method and application thereof, use chemical pesticide control insect to cause the problem such as pest resistance to insecticide and contaminated environment to solve, plant insecticide composition of the present invention is nontoxic, noresidue, nuisanceless, environmental protection, can not bring environmental pollution; Plant insecticide of the present invention can effectively prevent and treat the plant insects such as yellow spider, arrowhead scales, leaf roller, trypetid, and one time killing rate all reaches more than 95.41%, and does not have drug resistance.
For solving above technical problem, the present invention by the following technical solutions:
A kind of plant insecticide, in units of weight portion, comprise following raw material: tobacco 20-50 part, thunder godvine 20-50 part, capsicum 20-50 part, rhizome of Chinese monkshood 30-40 part, Dalmatian chrysanthemum 30-40 part, print chinaberry 30-40 part, tea free 20-30 part, field pennycress 20-30 part, bitter dish 20-30 part, absinth 15-25 part, bark of ash 15-25 part, kuh-seng 15-25 part, Roots of Euphorbia soongarica 12-20 part, poison trifoliate jewelvine 12-20 part, Chinese prickly ash 12-20 part, kitchen garden 10-15 part, datura 10-15 part, Herba Anabasis aphyllae 10-15 part, weeping willow leaf 6-12 part, leaf of Pterocarya Stenoptera 6-12 part, water 1300-5600 part.
Preferably, described plant insecticide, in units of weight portion, comprise following raw material: tobacco 30-40 part, thunder godvine 30-40 part, capsicum 30-40 part, rhizome of Chinese monkshood 32-38 part, Dalmatian chrysanthemum 32-38 part, print chinaberry 32-38 part, tea free 22-28 part, field pennycress 22-28 part, bitter dish 22-28 part, absinth 18-22 part, bark of ash 18-22 part, kuh-seng 18-22 part, Roots of Euphorbia soongarica 14-18 part, poison trifoliate jewelvine 14-18 part, Chinese prickly ash 14-18 part, kitchen garden 12-14 part, datura 12-14 part, Herba Anabasis aphyllae 12-14 part, weeping willow leaf 8-10 part, leaf of Pterocarya Stenoptera 8-10 part, water 2000-5000 part.
Preferably, described plant insecticide, in units of weight portion, comprise following raw material: tobacco 35 parts, thunder godvine 35 parts, 35 parts, capsicum, the rhizome of Chinese monkshood 35 parts, Dalmatian chrysanthemum 35 parts, print chinaberry 35 parts, tea free 25 parts, field pennycress 25 parts, bitter dish 25 parts, absinth 20 parts, the bark of ash 20 parts, kuh-seng 20 parts, Roots of Euphorbia soongarica 16 parts, malicious trifoliate jewelvine 16 parts, 16 parts, Chinese prickly ash, kitchen garden 12 parts, datura 12 parts, Herba Anabasis aphyllae 12 parts, 9 parts, weeping willow leaf, leaf of Pterocarya Stenoptera 9 parts, 3500 parts, water.
The present invention also provides a kind of preparation method of plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish, absinth, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, malicious trifoliate jewelvine, Chinese prickly ash, kitchen garden, datura, Herba Anabasis aphyllae, weeping willow leaf, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 140-180W, concentration of alcohol is 55%-75%, Extracting temperature is 55-65 DEG C, and extraction time is 30-50min;
S2: by medical filtration obtained for step S1, concentrated, obtain mixture B, gained mixture B be dry, pulverize, sieve, sterilizing, obtained plant insecticide.
Preferably, step S2 herb liquid filters, and is concentrated into water content≤25%.
Preferably, in step S2, mixture B is dry at 90-100 DEG C.
More preferably, described mixture B is dried to water content≤6% at 90-100 DEG C.
Preferably, the condition of sieving in step S2 is: cross 100-200 mesh sieve.
Preferably, the condition of sterilizing in step S2 is: temperature is 134-136 DEG C, and pressure is 210-230KPa, and the time is 3-5min.
The application of described plant insecticide in one or more plant insects of control yellow spider, arrowhead scales, leaf roller, trypetid.
Pharmacology of the present invention is as follows:
Tobacco has the effects such as promoting qi circulation and relieving pain, eliminating dampness, detumescence, removing toxic substances desinsection.
Thunder godvine can be dispeled the wind, removing toxic substances, desinsection.External application treating rheumatic arthritis, skin is itched, and kills maggot, wriggler, water-snail eradication, malicious mouse.
Capsicum can alleviate chest abdomen crymodynia, prevents dysentery, kills and presses down stomach abdomen entozoa, controls cardiopathy and coronary sclerosis, the function such as have sterilization, anticorrosion, seasoning, nutrition, dispel cold.
The aconitine of aconite extract has suppression or killing action to staphylococcus aureus, shigella dysenteriae, typhoid bacillus, Pseudomonas aeruginosa.
Dalmatian chrysanthemum containing 4 kinds of insecticidal constituents, pyrethrin (pyrethrin) I, II and cinerin (cinerin) I, II, Dalmatian chrysanthemum to various insects as mosquito, fly, bedbug and cockroach etc. have toxic action.
Print Melia, in Meliaceae, comes from Southeast Asia, and containing print chinaberry, solannin etc., have good disinsection efficiency, insect is once contact, and growth will be suppressed.
The extract of tea free has potent bactericidal action, and tea tree can effectively tackle for various mycotic infection, can kill staphylococcus aureus, diphtheria bacillus.
Field pennycress, with root-like stock and root, all herbal medicine, belongs to antipyretic and antidotal type medicine in Chinese medicine, cool in nature, taste is pungent, bitter.Return liver, stomach, large intestine channel, have effect that is clearing heat and detoxicating, removing blood stasis and expelling pus.Modern pharmacy is thought, it is containing volatile oil, Patrinia scaniosaefolia saponin and β-sterol glucose formula, have anti-inflammatory, antibacterial, calm, protect the liver the effect with cardiac stimulant diuresis.Field pennycress has suppression or killing action to staphylococcus aureus, shigella dysenteriae, typhoid bacillus, Pseudomonas aeruginosa.
Containing the composition such as taraxasterol, choline in bitter dish, stronger bactericidal action is had to staphylococcus aureus resistance bacterial strain, hemolytic streptococcus, also there is certain lethal effect to Diplococcus pneumopniae, meningococcus, diphtheria bacillus, Pseudomonas aeruginosa, shigella dysenteriae etc., therefore all have certain curative effect to icterepatitis, sphagitis, bacillary dysentery, cold, fever and chronic bronchitis, tonsillitis etc.
Absinth bitter, cold in nature, poisonous, there is heat-clearing and damp-drying drug, drive ascarid, stomach invigorating, the effect such as antibacterial desinsection, all have suppression and killing action to multiple coccus, bacillus, fungi and virus etc.
The bark of ash has antibacterial insecticidal action, has obvious inhibitory action, be usually used in controlling bacillary dysentery clinically to staphylococcus aureus, bacillus subtilis, Escherichia coli, brewer's yeast, bacterium wine yeast etc., enteritis, leukorrhea, chronic bronchitis, red eye, swell pain etc.
Kuh-seng belongs to herbaceos perennial; Be taken as the substitute of monkshood and radix aconiti agrestis at the Northwest's kuh-seng and use, simultaneously the traditional medicine of the ethnic group such as Ye Shi Kazak, the Hui ethnic group, is mainly used in pain relieving, dehumidifying, cold-dispelling.
Roots of Euphorbia soongarica is herbaceos perennial, main product in Gansu, the ground such as Xinjiang and Russia, the substitute in new thick area as the root of Beijing euphorbia uses, and has effect of removing water retention by purgation, dispersing swelling and dissipating binds.
Poison trifoliate jewelvine dicotyledon medicine leguminous plant, extract bitter, very toxic, there is killing parasites to relieve itshing, by effects such as arthritis with fixed pain caused by dampness.
Chinese prickly ash can alleviate chest abdomen crymodynia, prevents dysentery, kills and presses down stomach abdomen entozoa, controls cardiopathy and coronary sclerosis, the function such as have sterilization, anticorrosion, seasoning, nutrition, dispel cold.
Kitchen garden is cold in nature, the sweet acid of taste, and have clearing heat and detoxicating, Li Shui dries, and loose blood detumescence, dust-collection sterilization, anti-inflammatory analgetic, effects such as cool blood of stopping blooding, have stronger inhibitory action to shigella dysenteriae, typhoid bacillus and Escherichia coli.
Datura is botanical pesticide, has extremely strong sterilization, insecticidal action.
Herba Anabasis aphyllae belongs to chenopod, is dicotyledon, has the effects such as clearing heat and detoxicating, anti-inflammation, pain relieving desinsection, can be used for rural area preparation agricultural chemicals of eliminating the four pests--rats, bedbugs, flies and mosquitoes, the use of disinfestation and deratization.
Weeping willow leaf has the effect such as clearing heat and detoxicating, expelling wind and removing dampness, anti-inflammation, maggot of going out, infanticide Jue.
Chinese ash has the effects such as antibacterial, desinsection, removing toxic substances, and leaf is poisonous, can used as pesticides insecticide.
The present invention has following beneficial effect:
(1) plant insecticide composition of the present invention is nontoxic, and noresidue is nuisanceless, environmental protection, can not bring environmental pollution;
(2) plant insecticide of the present invention can effectively prevent and treat the plant insects such as yellow spider, arrowhead scales, leaf roller, trypetid, and one time killing rate all reaches more than 95.41%, and does not have resistance to medical, can use by 4-6;
(3) vegetable source pesticide agent and process for producing same of the present invention is simple, and cost is low, easy to use, and effect is good, is conducive to applying.
Embodiment
Be specifically described below in conjunction with specific embodiment.
Embodiment 1
A kind of plant insecticide, in units of weight portion, comprise following raw material: tobacco 20 parts, thunder godvine 20 parts, 20 parts, capsicum, the rhizome of Chinese monkshood 30 parts, Dalmatian chrysanthemum 30 parts, print chinaberry 30 parts, tea free 20 parts, field pennycress 20 parts, bitter dish 20 parts, absinth 15 parts, the bark of ash 15 parts, kuh-seng 15 parts, Roots of Euphorbia soongarica 12 parts, malicious trifoliate jewelvine 12 parts, 12 parts, Chinese prickly ash, kitchen garden 10 parts, datura 10 parts, Herba Anabasis aphyllae 10 parts, 6 parts, weeping willow leaf, leaf of Pterocarya Stenoptera 6 parts, 1300 parts, water.
The preparation method of described plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish, absinth, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, malicious trifoliate jewelvine, Chinese prickly ash, kitchen garden, datura, Herba Anabasis aphyllae, weeping willow leaf, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 140W, concentration of alcohol is 55%, and Extracting temperature is 55 DEG C, and extraction time is 50min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 25%, and obtain mixture B, it is 6% that gained mixture B is dried to water content at 90 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 134 DEG C in temperature, pressure is sterilizing 5min under 210KPa, obtained plant insecticide.
Embodiment 2
A kind of plant insecticide, in units of weight portion, comprise following raw material: tobacco 50 parts, thunder godvine 50 parts, 50 parts, capsicum, the rhizome of Chinese monkshood 40 parts, Dalmatian chrysanthemum 40 parts, print chinaberry 40 parts, tea free 30 parts, field pennycress 30 parts, bitter dish 30 parts, absinth 25 parts, the bark of ash 25 parts, kuh-seng 25 parts, Roots of Euphorbia soongarica 20 parts, malicious trifoliate jewelvine 20 parts, 20 parts, Chinese prickly ash, kitchen garden 15 parts, datura 15 parts, Herba Anabasis aphyllae 15 parts, 12 parts, weeping willow leaf, leaf of Pterocarya Stenoptera 12 parts, 5600 parts, water.
The preparation method of described plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish, absinth, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, malicious trifoliate jewelvine, Chinese prickly ash, kitchen garden, datura, Herba Anabasis aphyllae, weeping willow leaf, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 180W, concentration of alcohol is 75%, and Extracting temperature is 65 DEG C, and extraction time is 30min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 18%, and obtain mixture B, it is 4% that gained mixture B is dried to water content at 100 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 136 DEG C in temperature, pressure is sterilizing 3min under 230KPa, obtained plant insecticide.
Embodiment 3
A kind of plant insecticide, in units of weight portion, comprise following raw material: tobacco 35 parts, thunder godvine 35 parts, 35 parts, capsicum, the rhizome of Chinese monkshood 35 parts, Dalmatian chrysanthemum 35 parts, print chinaberry 35 parts, tea free 25 parts, field pennycress 25 parts, bitter dish 25 parts, absinth 20 parts, the bark of ash 20 parts, kuh-seng 20 parts, Roots of Euphorbia soongarica 16 parts, malicious trifoliate jewelvine 16 parts, 16 parts, Chinese prickly ash, kitchen garden 12 parts, datura 12 parts, Herba Anabasis aphyllae 12 parts, 9 parts, weeping willow leaf, leaf of Pterocarya Stenoptera 9 parts, 3500 parts, water.
The preparation method of described plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish, absinth, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, malicious trifoliate jewelvine, Chinese prickly ash, kitchen garden, datura, Herba Anabasis aphyllae, weeping willow leaf, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 160W, concentration of alcohol is 65%, and Extracting temperature is 60 DEG C, and extraction time is 40min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 20%, and obtain mixture B, it is 5% that gained mixture B is dried to water content at 95 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 135 DEG C in temperature, pressure is sterilizing 4min under 220KPa, obtained plant insecticide.
Embodiment 4
A kind of plant insecticide, in units of weight portion, comprise following raw material: tobacco 30 parts, thunder godvine 30 parts, 30 parts, capsicum, the rhizome of Chinese monkshood 32 parts, Dalmatian chrysanthemum 32 parts, print chinaberry 32 parts, tea free 22 parts, field pennycress 22 parts, bitter dish 22 parts, absinth 18 parts, the bark of ash 18 parts, kuh-seng 18 parts, Roots of Euphorbia soongarica 14 parts, malicious trifoliate jewelvine 14 parts, 14 parts, Chinese prickly ash, kitchen garden 12 parts, datura 12 parts, Herba Anabasis aphyllae 12 parts, 8 parts, weeping willow leaf, leaf of Pterocarya Stenoptera 8 parts, 2000 parts, water.
The preparation method of described plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish, absinth, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, malicious trifoliate jewelvine, Chinese prickly ash, kitchen garden, datura, Herba Anabasis aphyllae, weeping willow leaf, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 150W, concentration of alcohol is 60%, and Extracting temperature is 55 DEG C, and extraction time is 45min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 22%, and obtain mixture B, it is 6% that gained mixture B is dried to water content at 90 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 134 DEG C in temperature, pressure is sterilizing 5min under 210KPa, obtained plant insecticide.
Embodiment 5
A kind of plant insecticide, in units of weight portion, comprise following raw material: tobacco 40 parts, thunder godvine 40 parts, 40 parts, capsicum, the rhizome of Chinese monkshood 38 parts, Dalmatian chrysanthemum 38 parts, print chinaberry 38 parts, tea free 28 parts, field pennycress 28 parts, bitter dish 28 parts, absinth 22 parts, the bark of ash 22 parts, kuh-seng 22 parts, Roots of Euphorbia soongarica 18 parts, malicious trifoliate jewelvine 18 parts, 18 parts, Chinese prickly ash, kitchen garden 14 parts, datura 14 parts, Herba Anabasis aphyllae 14 parts, 10 parts, weeping willow leaf, leaf of Pterocarya Stenoptera 10 parts, 5000 parts, water.
The preparation method of described plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish, absinth, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, malicious trifoliate jewelvine, Chinese prickly ash, kitchen garden, datura, Herba Anabasis aphyllae, weeping willow leaf, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 170W, concentration of alcohol is 70%, and Extracting temperature is 65 DEG C, and extraction time is 35min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 20%, and obtain mixture B, it is 5% that gained mixture B is dried to water content at 100 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 136 DEG C in temperature, pressure is sterilizing 3min under 230KPa, obtained plant insecticide.
Embodiment 6
A kind of plant insecticide, in units of weight portion, comprise following raw material: tobacco 45 parts, thunder godvine 45 parts, 45 parts, capsicum, the rhizome of Chinese monkshood 35 parts, Dalmatian chrysanthemum 35 parts, print chinaberry 35 parts, tea free 25 parts, field pennycress 25 parts, bitter dish 25 parts, absinth 23 parts, the bark of ash 23 parts, kuh-seng 23 parts, Roots of Euphorbia soongarica 18 parts, malicious trifoliate jewelvine 18 parts, 18 parts, Chinese prickly ash, kitchen garden 14 parts, datura 14 parts, Herba Anabasis aphyllae 14 parts, 11 parts, weeping willow leaf, leaf of Pterocarya Stenoptera 11 parts, 5400 parts, water.
The preparation method of described plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish, absinth, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, malicious trifoliate jewelvine, Chinese prickly ash, kitchen garden, datura, Herba Anabasis aphyllae, weeping willow leaf, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 160W, concentration of alcohol is 70%, and Extracting temperature is 60 DEG C, and extraction time is 45min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 23%, and obtain mixture B, it is 5% that gained mixture B is dried to water content at 95 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 136 DEG C in temperature, pressure is sterilizing 3min under 230KPa, obtained plant insecticide.
For verifying the effect of plant insecticide of the present invention, by following experimental verification.
Adopt the plant insecticide of embodiment 1-6, the ratio of joining 40g water in 1g plant insecticide uses, and once prevents and treats the test of the plant insects such as yellow spider, arrowhead scales, leaf roller, trypetid, the results are shown in following table.
From upper table, the plant insecticide of embodiment of the present invention 1-6 is to a killing rate of the plant insects such as yellow spider, arrowhead scales, leaf roller, trypetid all more than 95.41%, and result of use is good.Due to plant insecticide nonhazardous of the present invention, do not pollute, do not remain, it is efficient to add control efficiency, therefore, can widely popularize application.
Above content can not assert that the present invention specifically implements to be confined to these explanations; for general technical staff of the technical field of the invention; do not departing under concept thereof of the present invention; some simple deduction or replace can also be made, all should be considered as belonging to the scope of patent protection that the present invention is determined by submitted to claims.

Claims (10)

1. a plant insecticide, it is characterized in that, in units of weight portion, comprise following raw material: tobacco 20-50 part, thunder godvine 20-50 part, capsicum 20-50 part, rhizome of Chinese monkshood 30-40 part, Dalmatian chrysanthemum 30-40 part, print chinaberry 30-40 part, tea free 20-30 part, field pennycress 20-30 part, bitter dish 20-30 part, absinth 15-25 part, bark of ash 15-25 part, kuh-seng 15-25 part, Roots of Euphorbia soongarica 12-20 part, poison trifoliate jewelvine 12-20 part, Chinese prickly ash 12-20 part, kitchen garden 10-15 part, datura 10-15 part, Herba Anabasis aphyllae 10-15 part, weeping willow leaf 6-12 part, leaf of Pterocarya Stenoptera 6-12 part, water 1300-5600 part.
2. plant insecticide according to claim 1, it is characterized in that, in units of weight portion, comprise following raw material: tobacco 30-40 part, thunder godvine 30-40 part, capsicum 30-40 part, rhizome of Chinese monkshood 32-38 part, Dalmatian chrysanthemum 32-38 part, print chinaberry 32-38 part, tea free 22-28 part, field pennycress 22-28 part, bitter dish 22-28 part, absinth 18-22 part, bark of ash 18-22 part, kuh-seng 18-22 part, Roots of Euphorbia soongarica 14-18 part, poison trifoliate jewelvine 14-18 part, Chinese prickly ash 14-18 part, kitchen garden 12-14 part, datura 12-14 part, Herba Anabasis aphyllae 12-14 part, weeping willow leaf 8-10 part, leaf of Pterocarya Stenoptera 8-10 part, water 2000-5000 part.
3. plant insecticide according to claim 1, it is characterized in that, in units of weight portion, comprise following raw material: tobacco 35 parts, thunder godvine 35 parts, 35 parts, capsicum, the rhizome of Chinese monkshood 35 parts, Dalmatian chrysanthemum 35 parts, print chinaberry 35 parts, tea free 25 parts, field pennycress 25 parts, bitter dish 25 parts, absinth 20 parts, the bark of ash 20 parts, kuh-seng 20 parts, Roots of Euphorbia soongarica 16 parts, malicious trifoliate jewelvine 16 parts, 16 parts, Chinese prickly ash, kitchen garden 12 parts, datura 12 parts, Herba Anabasis aphyllae 12 parts, 9 parts, weeping willow leaf, leaf of Pterocarya Stenoptera 9 parts, 3500 parts, water.
4. a preparation method for the plant insecticide according to any one of claim 1-3, is characterized in that, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish, absinth, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, malicious trifoliate jewelvine, Chinese prickly ash, kitchen garden, datura, Herba Anabasis aphyllae, weeping willow leaf, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 140-180W, concentration of alcohol is 55%-75%, Extracting temperature is 55-65 DEG C, and extraction time is 30-50min;
S2: by medical filtration obtained for step S1, concentrated, obtain mixture B, gained mixture B be dry, pulverize, sieve, sterilizing, obtained plant insecticide.
5. the preparation method of plant insecticide according to claim 4, is characterized in that, step S2 herb liquid filters, and is concentrated into water content≤25%.
6. the preparation method of plant insecticide according to claim 4, is characterized in that, in step S2, mixture B is dry at 90-100 DEG C.
7. the preparation method of plant insecticide according to claim 6, is characterized in that, described mixture B is dried to water content≤6% at 90-100 DEG C.
8. the preparation method of plant insecticide according to claim 4, is characterized in that, the condition of sieving in step S2 is: cross 100-200 mesh sieve.
9. the preparation method of plant insecticide according to claim 4, is characterized in that, the condition of sterilizing in step S2 is: temperature is 134-136 DEG C, and pressure is 210-230KPa, and the time is 3-5min.
10. the application of the plant insecticide according to any one of claim 1-3 in one or more plant insects of control yellow spider, arrowhead scales, leaf roller, trypetid.
CN201510937787.9A 2015-12-16 2015-12-16 Plant-derived pesticide and its preparation method and use Pending CN105379771A (en)

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CN106561735A (en) * 2016-08-02 2017-04-19 章吉浦 Plant growth protection liquid and preparation method thereof
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CN107821482A (en) * 2017-11-27 2018-03-23 张莘蔓 A kind of dragon fruit plant insecticide and preparation method thereof
CN107873743A (en) * 2017-12-06 2018-04-06 昭平县科学技术实验场 Plant insecticide containing selfheal and preparation method thereof
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CN109258714A (en) * 2018-10-30 2019-01-25 大新县科学技术情报研究所 A kind of biological insecticides and preparation method thereof for preventing and treating vegetable aphid
CN109717211A (en) * 2017-10-27 2019-05-07 丹阳市景林园园艺有限公司 A kind of sweet osmanthus insecticide
CN109769616A (en) * 2019-03-07 2019-05-21 杭州市林业科学研究院(杭州市林业科技推广总站) The control method of Allomyrina dichotoma in a kind of officinal dendrobium stem plantation
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CN105994412A (en) * 2016-06-01 2016-10-12 蚌埠市宝煦家庭农场 Insecticide for control of black currant plume moth pest
CN106561735A (en) * 2016-08-02 2017-04-19 章吉浦 Plant growth protection liquid and preparation method thereof
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Application publication date: 20160309