CN105363231B - It can prevent catalyst from gluing the centrifugal spray drying device of wall - Google Patents

It can prevent catalyst from gluing the centrifugal spray drying device of wall Download PDF

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Publication number
CN105363231B
CN105363231B CN201510842151.6A CN201510842151A CN105363231B CN 105363231 B CN105363231 B CN 105363231B CN 201510842151 A CN201510842151 A CN 201510842151A CN 105363231 B CN105363231 B CN 105363231B
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China
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air
drying
tower
drying tower
frequency conversion
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CN201510842151.6A
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CN105363231A (en
Inventor
吴敏
李伟杰
曾平川
周宇骋
杨黛
张仲琨
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Nanjing Jingwei Environmental Protection Technology Co ltd
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NANJING WEIAN NEW MATERIAL SCIENCE & TECHNOLOGY Co Ltd
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Abstract

The present invention relates to a kind of centrifugal spray drying device for preventing catalyst from gluing wall, including centrifugal drying tower, feeding device, heater, cool down blanking device, dedusting emptier and intelligent control box, spiral case hot-air distributor and frequency conversion centrifugal atomizer are provided with the middle part of the tower top of drying tower, heater connects the air inlet of spiral case hot-air distributor by hot air duct, cool down the bottom that blanking device is arranged on drying tower, cloth envelop collector room is provided with the tower internal upper part side wall of drying tower, the bottom of cloth envelop collector room is open, the outside of drying tower is provided with a cooling sandwith layer, intelligent control box connects frequency conversion centrifugal atomizer by wire, dehvery pump, heater, cool down blanking device, exhaust fan, air-introduced machine and electric butterfly valve, the running parameter of whole drying device is accurately controlled.The device rate of drying is fast, stabilization simple to operate, and material wall sticking phenomenon hardly occurs, and effectively increases the quality of catalyst drying and the continuity of drying process.

Description

It can prevent catalyst from gluing the centrifugal spray drying device of wall
Technical field
The present invention relates to catalyst preparation technical field, and in particular to a kind of catalyst is dry and the spray drying of granulation fills Put, more particularly to a kind of centrifugal spray drying that can effectively prevent catalyst feed from wall sticking phenomenon occurring in drying tower dress Put.
Background technology
Catalyst has irreplaceable status in modern chemical industry, there are about 80% chemical reaction and catalyst In the presence of relevant.Existing catalyst is mostly nanoscale or micron-sized granular powder, Presence of an interface tension force between particle and solution, Particle aggregation is easily produced, therefore during solution reaction prepares catalyst powder, drying is extremely critical process.Spray It is that a kind of most common dry technology for liquid being dried to powder-product, its operation principle are in chemical engineering industry that mist, which is dried,:With Material is sprayed into droplet dispersion in hot-air by the method for spraying, and material and hot-air are mutual in a manner of cocurrent, adverse current or mixed flow It is in contact, moisture is evaporated rapidly, reaches dry purpose.Using this drying means, concentration, filtering can be saved, crushed Operated Deng unit, and drying time short (general drying time is 5~30s), the active ingredient to dried material destroy less.But Be existing catalyst drying device during being spray-dried, often occur by dry material adhering to drying tower Phenomenon on inwall, because viscous wall material is relatively difficult to be taken out of drying tower in time, so as to cause adhesion material to burn or the shadow that goes bad Ring the quality of catalyst powder;In order to improve the quality of product, the viscous wall material in drying tower is removed, it has to which midway stops dry It is dry, operation cycle length is in turn resulted in, production efficiency is low, continuous operation is difficult.
The content of the invention
The present invention is exactly for technical problem present in prior art, there is provided a kind of centrifugation for preventing catalyst from gluing wall Spray-drying installation, the device overall construction design is ingenious, and automaticity is high, can effectively avoid dry catalyst in drying tower The interior phenomenon that viscous wall occurs, improve the quality of finished catalyst.
To achieve these goals, the technical solution adopted by the present invention is a kind of centrifugation for preventing catalyst from gluing wall spray Mist drying device, including the centrifugal drying tower of vertical upper cylinder and lower circular cone composite construction, feeding device, heater, cooling Blanking device, dedusting emptier and intelligent control box, be provided with the middle part of the tower top of drying tower spiral case hot-air distributor and frequency conversion from Heart atomizer, the upper wind deflector of the spiral case hot-air distributor and lower wind deflector are arranged in cone, the upper wind deflector with The angle of cone axis is 25~30 °, and the angle of lower wind deflector and cone axis is 0 °, and the quantity of upper wind deflector is lower wind-guiding Twice of plate quantity, so enabling to hot blast to enter in drying tower can be uniformly distributed and ensure that hot blast rotates, from And extend hot blast and the time of contact being atomized between feed liquid, promote hot blast and the heat and mass being atomized between feed liquid complete in Best Times Into, effectively avoid wet stock glue wall phenomenon occur.The nozzle of the frequency conversion centrifugal atomizer passes through spiral case hot-air distributor Cone is extended to inside drying tower;The length that the cone of the spiral case hot-air distributor is stretched into drying tower is 100~200mm, The length that the nozzle of the frequency conversion centrifugal atomizer is stretched into drying tower is 200~250mm, can so prevent that being atomized feed liquid exists Dry column overhead because too high hot blast temperature cause it is over-drying form coke powder.
The front end of the heater is provided with air cleaner, and air passes through air-supply after air cleaner filtering Machine is delivered to and forms hot blast in electric heater after heating, and helically state enters drying to hot blast after the distribution of spiral case hot-air distributor In tower and the atomization feed liquid with being sprayed from the nozzle of frequency conversion centrifugal atomizer carries out hot exchanging with matter.The covering radius of hot blast Larger and distribution is more uniform, can substantially effectively be combined with atomization feed liquid, rapidly be evaporated the moisture being atomized in feed liquid.It is described The air inlet of spiral case hot-air distributor is provided with EAT sensor, and leaving air temp is provided with the air outlet of spiral case hot-air distributor Sensor, the electric heater are provided with temperature controller, EAT sensor, leaving air temp sensor and temperature controller It is connected by wire with intelligent control box, and then accomplishes the drying temperature in accurate control drying tower, is improved catalyst and dry Effect.The material-storage jar of the feeding device is connected to the charging aperture of frequency conversion centrifugal atomizer by dehvery pump, dehvery pump with Feeding pipe between frequency conversion centrifugal atomizer is provided with filter, for the crude fibre in filter material and bulky grain debris, To prevent the distributing device of feed blocking frequency conversion centrifugal atomizer and atomizing disk passage, so that material shape leaves mist into droplet The moment for changing disk just forms uniform atomization feed liquid, improves catalyst powder or granulation uniformity.The heater passes through heat Wind pipeline connects the air inlet of spiral case hot-air distributor, and the cooling blanking device is arranged on the bottom of drying tower and gone out with drying tower Material mouth connects, and the dedusting emptier includes the dust removing purifier and exhaust fan being connected, the dust removing purifier connection The evacuation port of drying tower;Cloth envelop collector room is provided with the tower internal upper part side wall of drying tower, drying tower evacuation port is opened in cloth bag In the side wall of filter chamber, the bottom of cloth envelop collector room is open, and multiple dismountable cloth bags are provided with cloth envelop collector room Filter;The outside of the drying tower is provided with a cooling sandwith layer, and open up on the cooling sandwith layer at tower top one it is cold Wind air-vent, the cold wind air-vent connects air-introduced machine by cold air duct, and electric butterfly valve is provided with cold air duct;The intelligence Energy control cabinet passes through wire and connects frequency conversion centrifugal atomizer, dehvery pump, heater, cooling blanking device, exhaust fan, air-introduced machine And electric butterfly valve, the running parameter of whole drying device is accurately controlled.The ingenious practicality of the whole Technical Design, Control and manage convenient for production, can effectively avoid material from gluing the phenomenon of wall, catalyst powder purity after drying is high, quality It is good.
Wherein, the dehvery pump uses membrane pump, and ball face sealing, sealing are used between the valve seat and valve ball of the membrane pump Can be good, and the uniformity into material in frequency conversion centrifugal atomizer has been effectively ensured, it is continuous so as to improve charging rate and charging Property.
The dry inner wall of tower and the inside and outside wall of cloth envelop collector room are provided with a floor hydrophobic layer, the contact of hydrophobic layer Angle is more than 90 °;The material selection polytetrafluoroethylene (PTFE) of the hydrophobic layer is made, drying temperature is 0~250 in its tolerable tower ℃。
The frequency conversion centrifugal atomizer uses associated mode high speed centrifugal atomization device, and the nozzle of the frequency conversion centrifugal atomizer is adopted It is made of thyrite, due to the material with high temperature resistant, to acid-alkali salt with good corrosion resistance and well Chemical stability the advantages that so that nozzle operation have in drying tower environment relatively low wear rate and it is good chemically Can, so as to improve the service life of frequency conversion centrifugal atomizer, the uniformity coefficient of atomization feed liquid has also been effectively ensured.And it is atomized Variable-frequency motor on device is directly connected to by shaft coupling and the rotary shaft on atomizing disk top, so as to effectively avoid atomizing disk from revolving The phenomenon to be deflected during turning, so as to ensure that the nozzle of atomizing disk bottom does not shift, is effectively avoided because of nozzle Tilt and caused local material wall sticking phenomenon.And shaft coupling is fixedly mounted on atomizing disk top, atomizing disk by bearing block Substantially influence not vibrated in rotary shaft rotation process, the phenomenon that material glues wall is further avoided the occurrence of.
Relative to prior art, advantages of the present invention is as follows, 1) overall construction design of this drying device is ingenious, dismounting group Convenient maintenance and replacement is filled, cost is relatively low and rate of drying is fast, and feed liquid surface area after atomization greatly increases, the wink in hot-air flow Between can evaporate 95% to 99% moisture content, completing the dry time only needs more than ten seconds to arrive several tens of seconds, is catalyzed through drying gained Epigranular, good fluidity, the dissolubility of agent powder be good and product purity is high, quality is good;2) stabilization simple to operate of the device, Drying temperature, feed rate, discharge velocity, intake air temperature, air outlet temperature only need to be pre-set in intelligent control box Deng the Drying Technology Parameter of correlation, whole device enters the state automatically continuously to work after start, and whole drying process is by intelligence Control cabinet carries out full-automatic centralized Control, and control and management are convenient, effectively reduce the labor intensity of operating personnel;3) centrifuging Cloth envelop collector room is set in drying tower, effectively prevent the rewinding dust arrester being arranged in the past outside drying tower to drying tower The influence of interior dry gas stream, so that it is guaranteed that atomization feed liquid dries abundant degree in tower, and material wall sticking phenomenon is avoided to occur;Together When cloth envelop collector room in set the recyclable attritive powder being entrained by the flow of air of cloth envelop collector, and reclaim after powder due to The powder that the effect of self gravitation falls to the cone bottom discharge mouth of drying tower and fallen after drying again is discharged outside tower together, Waste gas by exhaust fan after evacuation port removing dust clarifier dust separation by being discharged into air;4) as a result of air-supply uniformity The good frequency conversion centrifugal atomizer of good spiral case hot-air distributor and atomizing effect, in addition on drying tower inner wall of tower liner contact The setting of cooling sandwith layer on hydrophobic layer and outer wall of the angle more than 90 °, when carrying out catalyst drying process using this drying device Material wall sticking phenomenon hardly occurs, effectively increases the quality of catalyst drying and the continuity of drying process, significantly The economic benefit of enterprise is added while improving drying efficiency.
Brief description of the drawings
Fig. 1 is the overall structure diagram of the present invention.
Fig. 2 is the structural representation of spiral case hot-air distributor of the present invention.
Fig. 3 is the structural representation of frequency conversion centrifugal atomizer of the present invention.
In figure:1- centrifugal drying towers, 2- frequency conversion centrifugal atomizers, 3- spiral case hot-air distributors, 4- material-storage jars, 5- conveyings Pump, 6- filters, 7- cooling blanking devices, 8- pressure fan, 9- air cleaners, 10- electric heaters, 11- cloth envelop collectors room, 12- cloth envelop collectors, 13- dust removing purifiers, 14- exhaust fans, 15- intelligent control box, 16- air-introduced machines, 17- electric butterfly valves, 18- air inlets, the upper wind deflectors of 19-, 20- cones, wind deflector under 21-, 22- conical shells, 23- air outlets, 24- variable-frequency motors, 25- connection Axle device, 26- bearing blocks, 27- rotary shafts, 28- atomizing disks, 29- cooling sandwith layers.
Embodiment
In order to deepen the understanding of the present invention and understanding, the invention will be further described below in conjunction with the accompanying drawings and introduces.
Embodiment 1:Such as Fig. 1-Fig. 3, a kind of centrifugal spray drying device for preventing catalyst from gluing wall, including it is vertical on The centrifugal drying tower 1 of cylinder and lower circular cone composite construction, feeding device, heater, cooling blanking device 7, dedusting emptier With intelligent control box 15, spiral case hot-air distributor 3 and frequency conversion centrifugal atomizer 2, the snail are provided with the middle part of the tower top of drying tower 1 The upper wind deflector 19 of shell hot-air distributor 3 and lower wind deflector 21 are arranged in cone 20, the upper wind deflector 19 and cone 20 The angle of axis is 25~30 °, and the angle of lower wind deflector 21 and the axis of cone 20 is 0 °, and the quantity of upper wind deflector 19 be under lead Twice of the quantity of aerofoil 21, so enabling to hot blast to enter in drying tower 1 can be uniformly distributed and ensure that hot blast does rotation fortune It is dynamic, so as to the time of contact for extending hot blast and being atomized between feed liquid, promote hot blast and the heat and mass being atomized between feed liquid when optimal Interior completion, effectively avoid wet stock from gluing the phenomenon of wall and occur.The nozzle of the frequency conversion centrifugal atomizer 2 divides through spiral case hot blast The cone 20 of orchestration 3 is extended to inside drying tower 1;The material-storage jar 4 of the feeding device is connected to frequency conversion by dehvery pump 5 and centrifuged The charging aperture of atomizer 2, the heater connects the air inlet 18 of spiral case hot-air distributor 3 by hot air duct, described cold But blanking device 7 is arranged on the bottom of drying tower 1 and connected with the discharging opening of drying tower 1, and the dedusting emptier includes being connected Dust removing purifier 13 and exhaust fan 14, the dust removing purifier 13 connects the evacuation port of drying tower 1;The heater Front end is provided with air cleaner 9, and air is delivered in electric heater 10 after the air cleaner 9 filtering by pressure fan 8 Form hot blast after heating, hot blast after the distribution of spiral case hot-air distributor 3 helically state enter in drying tower 1 and with from frequency conversion The atomization feed liquid progress heat sprayed in the nozzle of centrifugal atomizer 2 exchanges with matter.The covering radius of hot blast it is larger and distribution compared with To be uniform, it can substantially effectively be combined with atomization feed liquid, be rapidly evaporated the moisture being atomized in feed liquid.The spiral case hot blast distribution The air inlet 18 of device 3 is provided with EAT sensor, is sensed in the air outlet 23 of spiral case hot-air distributor 3 provided with leaving air temp Device, the electric heater 10 are provided with temperature controller, and EAT sensor, leaving air temp sensor and temperature controller are equal It is connected by wire with intelligent control box 15, and then accomplishes the drying temperature in accurate control drying tower 1, is improved catalyst and dry Effect.Cloth envelop collector room 11 is provided with the tower internal upper part side wall of drying tower 1, the evacuation port of drying tower 1 is opened in Bag filter In the side wall of device room 11, the bottom of cloth envelop collector room 11 is open, and multiple dismountable cloth are provided with cloth envelop collector room 11 Bag type filter 12;The outside of the drying tower 1 is provided with a cooling sandwith layer 29, and is opened on the cooling sandwith layer 29 at tower top If a cold wind air-vent, the cold wind air-vent connects air-introduced machine 16 by cold air duct, and provided with electronic on cold air duct Butterfly valve 17;The intelligent control box 15 connects frequency conversion centrifugal atomizer 2, dehvery pump 5, heater, cooling blanking by wire Device 7, exhaust fan 14, air-introduced machine 16 and electric butterfly valve 17, the running parameter of whole drying device is accurately controlled.It is described The whole ingenious practicality of Technical Design, controls and manages convenient for production, can effectively avoid material from gluing the phenomenon of wall, through drying Catalyst powder purity afterwards is high, quality better.
Filter 6 is provided with feeding pipe between dehvery pump 5 and frequency conversion centrifugal atomizer 2, in filter material Crude fibre and bulky grain debris, to prevent the distributing device of feed blocking frequency conversion centrifugal atomizer 2 and the passage of atomizing disk 28, so as to So that material shape into droplet and moment for leaving atomizing disk 28 just forms uniform atomization feed liquid, improve catalyst powder or particle The uniformity.
The dehvery pump 5 uses membrane pump, and ball face sealing, sealing property are used between the valve seat and valve ball of the membrane pump It is good, and the uniformity into material in frequency conversion centrifugal atomizer 2 has been effectively ensured, it is continuous so as to improve charging rate and charging Property.
The length that the cone 20 of the spiral case hot-air distributor 3 is stretched into drying tower 1 is 100~200mm, the frequency conversion from The length that the nozzle of heart atomizer 2 is stretched into drying tower 1 is 200~250mm, can so prevent from being atomized feed liquid in drying tower 1 Tower top because too high hot blast temperature cause it is over-drying form coke powder.
The inwall of drying tower 1 and the inside and outside wall of cloth envelop collector room 11 are provided with a floor hydrophobic layer, described in making The material selection polytetrafluoroethylene (PTFE) of hydrophobic layer, drying temperature is 0~250 DEG C in its tolerable tower.
The frequency conversion centrifugal atomizer 2 uses associated mode high speed centrifugal atomization device, and the variable-frequency motor 24 on atomizer passes through Shaft coupling 25 and the rotary shaft 27 on the top of atomizing disk 28 are directly connected to, so as to effectively avoid atomizing disk 28 from being sent out in rotary course The phenomenon of raw deflection, so as to ensure that the nozzle of the bottom of atomizing disk 28 does not shift, effectively avoids producing because of nozzle inclination Raw local material wall sticking phenomenon.And shaft coupling 25 is fixedly mounted on the top of atomizing disk 28, atomizing disk 28 by bearing block 26 Substantially not vibrated influence in the rotation process of rotary shaft 27, the phenomenon that material glues wall is further avoided the occurrence of.
The nozzle of the frequency conversion centrifugal atomizer 2 is made of thyrite, due to the material have high temperature resistant, There is good corrosion resistance and good chemical stability to acid-alkali salt so that nozzle operation is in the ring of drying tower 1 There is relatively low wear rate and good chemical property in border, so as to improve the service life of frequency conversion centrifugal atomizer 2, also have Effect ensure that the uniformity coefficient of atomization feed liquid.
It should be noted that above-described embodiment, is not used for limiting protection scope of the present invention, in above-mentioned technical proposal On the basis of made equivalents or replacement each fall within the scope that the claims in the present invention are protected.

Claims (1)

  1. A kind of 1. centrifugal spray drying device for preventing catalyst from gluing wall, it is characterised in that:Including vertical upper cylinder and lower circle Centrifugal drying tower, feeding device, heater, cooling blanking device, dedusting emptier and the intelligent control box of composite construction are bored, Spiral case hot-air distributor and frequency conversion centrifugal atomizer are provided with the middle part of the tower top of drying tower, is led on the spiral case hot-air distributor Aerofoil and lower wind deflector are arranged in the cone of spiral case hot-air distributor, and the angle of the upper wind deflector and cone axis is 25 ~30 °, the angle of lower wind deflector and cone axis is 0 °, and the quantity of upper wind deflector is twice of lower wind deflector quantity, described The cone of the nozzle of frequency conversion centrifugal atomizer through spiral case hot-air distributor is extended to inside drying tower;The spiral case hot blast distribution The length that the cone of device is stretched into drying tower is 100~200mm, and the nozzle of the frequency conversion centrifugal atomizer is stretched into drying tower Length is 200~250mm, and the material-storage jar of the feeding device is connected to the charging aperture of frequency conversion centrifugal atomizer by dehvery pump, And filter is provided with the feeding pipe between dehvery pump and frequency conversion centrifugal atomizer, the dehvery pump uses membrane pump, should Ball face sealing is used between the valve seat and valve ball of membrane pump, the heater connects spiral case hot-air distributor by hot air duct Air inlet, the cooling blanking device is arranged on the bottom of drying tower and connects with drying tower discharging opening, dedusting emptying dress Put dust removing purifier and exhaust fan including being connected, the evacuation port of the dust removing purifier connection drying tower;The heating The front end of device is provided with air cleaner, and air is delivered in electric heater after air cleaner filtering by pressure fan Form hot blast after heating, hot blast after the distribution of spiral case hot-air distributor helically state enter in drying tower and with from frequency conversion from The atomization feed liquid progress heat sprayed in the nozzle of heart atomizer exchanges with matter;The frequency conversion centrifugal atomizer is high using associated mode Fast centrifugal atomizer, the nozzle of frequency conversion centrifugal atomizer are made of thyrite, and the variable-frequency motor on atomizer leads to Cross shaft coupling and the rotary shaft on atomizing disk top is directly connected to, and shaft coupling is fixedly mounted on atomizing disk by bearing block Portion;The air inlet of the spiral case hot-air distributor is provided with EAT sensor, is provided with the air outlet of spiral case hot-air distributor Leaving air temp sensor, the electric heater are provided with temperature controller, EAT sensor, leaving air temp sensor and temperature Degree controller is connected by wire with intelligent control box;Cloth envelop collector room is provided with the tower internal upper part side wall of drying tower, is done Dry tower evacuation port is opened in the side wall of cloth envelop collector room, and the bottom of cloth envelop collector room is open, in cloth envelop collector room Provided with multiple dismountable cloth envelop collectors;One is equipped with the dry inner wall of tower and the inside and outside wall of cloth envelop collector room Layer hydrophobic layer, and the hydrophobic layer is made from polytetrafluoroethylmaterial material, the contact angle of hydrophobic layer is more than 90 °;The drying tower Outside be provided with a cooling sandwith layer, and a cold wind air-vent is opened up on the cooling sandwith layer at tower top, the cold wind draws Air port connects air-introduced machine by cold air duct, and electric butterfly valve is provided with cold air duct;The intelligent control box passes through wire Frequency conversion centrifugal atomizer, dehvery pump, heater, cooling blanking device, exhaust fan, air-introduced machine and electric butterfly valve are connected, to whole The running parameter of individual drying device is accurately controlled.
CN201510842151.6A 2015-11-28 2015-11-28 It can prevent catalyst from gluing the centrifugal spray drying device of wall Expired - Fee Related CN105363231B (en)

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CN106766818B (en) * 2017-01-10 2023-06-16 楚雄医药高等专科学校 Energy-saving efficient airflow dryer for Yi medicine extracts and drying method thereof
CN106732173A (en) * 2017-01-11 2017-05-31 陆文光 Anti- molten atomizing granulating and drying machine and its method of work
CN108096863A (en) * 2017-12-28 2018-06-01 无锡市桑莱特干燥设备有限公司 A kind of spray dryer using magnetic suspension atomizer
CN110812866A (en) * 2019-11-14 2020-02-21 佛山市和利环保科技有限公司 Spray drier
CN112619190B (en) * 2020-12-09 2022-04-19 加沃农(江苏)农业科技有限公司 Spray drying equipment for fertilizer production and fertilizer production method
CN114504834B (en) * 2022-02-24 2023-03-07 华夏生生药业(北京)有限公司 Calcium gluconate solution purification equipment and process thereof
CN114768277B (en) * 2022-04-29 2023-09-05 湖南东健药业有限公司 Spray drying system for traditional Chinese medicine preparation

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Granted publication date: 20180406