CN105341244A - Series Clinacanthus nutans tea beverage and preparation method thereof - Google Patents

Series Clinacanthus nutans tea beverage and preparation method thereof Download PDF

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Publication number
CN105341244A
CN105341244A CN201510661472.6A CN201510661472A CN105341244A CN 105341244 A CN105341244 A CN 105341244A CN 201510661472 A CN201510661472 A CN 201510661472A CN 105341244 A CN105341244 A CN 105341244A
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China
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sorrow
escape
tea
tea beverage
careless tea
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CN105341244B (en
Inventor
杜明
冯立婷
刘猛
樊凤娇
涂茂林
石璞洁
谭晓怡
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Harbin Institute of Technology
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Harbin Institute of Technology
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00Tea; Tea substitutes; Preparations thereof
    • A23F3/34Tea substitutes, e.g. matè; Extracts or infusions thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00Tea; Tea substitutes; Preparations thereof
    • A23F3/06Treating tea before extraction; Preparations produced thereby
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00Tea; Tea substitutes; Preparations thereof
    • A23F3/06Treating tea before extraction; Preparations produced thereby
    • A23F3/12Rolling or shredding tea leaves
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00Tea; Tea substitutes; Preparations thereof
    • A23F3/16Tea extraction; Tea extracts; Treating tea extract; Making instant tea
    • A23F3/166Addition of, or treatment with, enzymes or microorganisms

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Microbiology (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Tea And Coffee (AREA)

Abstract

The invention relates to a series Clinacanthus nutans tea beverage and a preparation method thereof, belongs to the technical field of food processing, and aims to solve the problems of flocculation precipitation of the Clinacanthus nutans tea beverage, color changes of tea soup and bad smell of the tea soup. The series Clinacanthus nutans tea beverage disclosed by the invention relates to the series of a primary taste tea beverage, a fruit juice tea beverage, a milk tea beverage, a composite tea beverage and the like. The preparation method comprises the following steps of firstly, performing fixation on the Clinacanthus nutans leaves, baking the Clinacanthus nutans leaves after fixation, and stir-frying the baked Clinacanthus nutans leaves so as to obtain the Clinacanthus nutans tea; and mixing the Clinacanthus nutans tea and purified water so as to obtain a mixture, adding beta-cyclodextrin, preparing aqueous extract liquid, then performing enzymolysis treatment, and then adding vitamin C, citric acid, a stabilizing agent and seasoning, performing homogenizing treatment, and then performing disinfection so as to obtain the series Clinacanthus nutans tea beverage. The series Clinacanthus nutans tea beverage disclosed by the invention can still keep clear and transparent after being preserved for 12 months at normal atmospheric temperature after disinfection, flocculent precipitation and a supernatant do not exist, the smell has delicate fragrance, the series Clinacanthus nutans tea beverage has the flavor characteristic of the tea beverage, and the and organoleptic investigation result is good.

Description

Series sorrow is escaped careless tea beverage and preparation method thereof
Technical field
The invention belongs to food processing technology field, relating to a series of is tea beverage and preparation method thereof of raw material with sorrow grass of escaping.
Background technology
Sorrow escape grass for Acanthaceae (Acanthaceae) crocodile mouth Pittosporum crocodile mouth flower Clinacanthusnutans (Burm.F.) Lindau herb, range and turn round sequence Pittosporum, its another name has crocodile mouth flower, turns round sequence flower, blue or green arrow, Sabah snakeweed, soft thorn are careless.Growth, in low altitude area sparse woods or in shrubbery, is distributed widely in Malaysia, Indonesia, Thailand and south China to the west and south as areas such as Guangdong, Guangxi, Yunnan.In recent years, sorrow is escaped careless fashionable Southeast Asian countries, and reason is that the local cancer patient of Malaysia finds that edible sorrow grass of escaping has suitable effect to antitumor, and this report causes medical scientific research worker all over the world and pays close attention to, and then expands a series of research to it.Chinese scholars is separated, identifies number of chemical composition from sorrow escapes grass, comprises triterpenes, carbon glycosides flavonoids, sulfur-containing compound, phytosterol, pheophytin class, cerebroside, amino acid, trace element, alkaloid and multiple micromolecular compound etc.
The sorrow people in grass growth area blade of grass of often sorrow being escaped of escaping does vegetables and eats, and also useful Fresh leaves is squeezed the juice and drunk, and can strengthen the resistance of body.China market can being seen, escape careless tealeaves and sorrow of sorrow is escaped grass meal two kinds of products, but sorrow is escaped, careless drink has no correlative study or product.
Why the traditional beverages that tea is familiar with as China resident, be described as " state's drink " of the Chinese nation, and reason is in tea raw material containing abundant physiological activator.Tea is one of pandemic three large non-alcohol hobby property beverages, and the market scale of Related product as tea beverage also improves year by year.Along with the transformation of consumption idea and life style, tea beverage becomes one of Chinese Consumer's favorite drink category.Statistics shows, and tea-drinking consumption market has accounted for the share of about 20% of whole beverage consumption market.Under this overall background, develop the market prospects that novel tea beverage is significant and wide.Tea beverage is the tealeaves that is soaked in water, and adds water, the goods of the modulation such as liquid glucose, acid, flavoring essence, fruit juice or Sik (Valley) matter extract through techniques such as extracting, filtration, clarifications in the millet paste made or millet paste.
Although the Quality Control Technology relative maturity in existing tea beverage processing, but there is some difference for the composition that different raw materials is corresponding and content, this also just makes sorrow escape the product quality control method of careless drink can not be identical with tea beverage Quality Control Technology in the market, and that is the production key technology of the tea beverage such as existing green tea, black tea, oolong tea can not directly apply to sorrow grass of escaping is in the beverage exploitation of raw material.
The said goods is the drink that a kind of water-soluble extractive (abbreviation low cost vegetable plant water extract) of plant material is prepared into through techniques such as allotments after all, and the raising of product quality mainly contains the technology restriction of three aspects in the processing of these drinks, one is the stability of drink, one is the color and luster of drink, and another is the local flavor problem of drink.
(1) stability of drink controls relevant issues
Containing multiple water soluble ingredient in low cost vegetable plant water extract, as polyphenols, free amino acid, water soluble protein, pectin, caffeine etc.Protein, pectin etc., after low cost vegetable plant water extract cooling, can form flocculent deposit, simultaneously Polyphenols and oxidation product thereof also easily and soluble protein, caffeine produce and precipitate, also can form precipitation between protein, caffeine, the Ca in addition in water 2+, Mg 2+can be formed with polyphenols complexing Deng also and precipitate.
(2) the color and luster control problem of drink
Low cost vegetable plant water extract is a kind of system of instability, easily by the impact of oxygen, temperature, soup look is changed.The master operation affecting its change is extraction and sterilizing, in low cost vegetable plant water extract, polyphenol content is higher, Tea Polyphenols is a kind of strong reductant, very easily there is non-enzymatic autoxidation and generate coloured o-quinone material, and also easily oxidation further between o-quinone material, form sepia material, thus make the brown stain of soup look, especially, under high temperature and alkali condition, Tea Polyphenols oxidation rate is accelerated, thus affects the quality of low cost vegetable plant water extract.
The Another reason of low cost vegetable plant water extract brown stain is caused to cause due to low cost vegetable plant water extract Determination of Chlorophyll de-magging.Magnesium ion in chlorophyll molecule replace by ammonium ion, generate the pheophytin of black, thus show color and luster and deepen, even brown stain.Chlorophyllous de-magging effect is because when polyphenols oxidation generates o-quinone, in solution, hydrogen ion concentration can increase relatively, under the action of heat, can replace the magnesium in the green rope of leaf, thus makes it to form black product.
(3) the smell control problem of drink
Plant material contains a large amount of volatile flavor substances, and wherein the taste of some composition is not be popular.In reality processing, have plenty of to adopt and plant material is carried out frying, reduce bad flavor, the method increasing pleasant flavor substance content controls.Also the certain embedding techniques of the use had controls.
Summary of the invention
The present invention is directed to the processing technology of the careless drink that all do not find at present both at home and abroad to escape about sorrow, to escape the flocculation sediment problem of careless tea beverage to solve sorrow, the color and luster change of millet paste and the problem of bad smell of millet paste, and provide serial sorrow to escape careless tea beverage and preparation method thereof.
Sorrow of the present invention escape careless tea beverage raw material composition by mass percentage by 0.16% ~ 4% sorrow escape careless tea, account for sorrow escape careless tea quality 0.5% ~ 1.5% embedding medium, account for sorrow escape careless tea quality 2.5% ~ 5% enzyme, 0.02% ~ 0.1% vitamin C, 0.02% ~ 0.1% citric acid, 0.02% ~ 0.1% stabilizing agent, the flavor substance of 0.002% ~ 0.01%, the sweetener of 4% ~ 8% and surplus water form; Wherein said embedding medium is beta-schardinger dextrin-, and enzyme is one or several the mixture in protease, pectase, tannase, and flavor substance is essence.
The escape raw material composition of careless tea beverage of sorrow of the present invention to be escaped careless tea by the sorrow of 0.16% ~ 4% by mass percentage, account for sorrow escape careless tea quality 0.5% ~ 1.5% embedding medium, account for sorrow escape careless tea quality 2.5% ~ 5% enzyme, the vitamin C of 0.02% ~ 0.1%, the citric acid of 0.02% ~ 0.1%, the stabilizing agent of 0.02% ~ 0.1%, the flavor substance of 0.002% ~ 0.01%, the sweetener of 4% ~ 8%, the fruit juice of 5% ~ 10%, the edible fruity flavor of 0.002% ~ 0.01% and the water composition of surplus, wherein said embedding medium is beta-schardinger dextrin-, and enzyme is protease, pectase, tannase or its multiple mixture, and flavor substance is essence.
The escape raw material composition of careless tea beverage of sorrow of the present invention to be escaped careless tea by the sorrow of 0.16% ~ 4% by mass percentage, account for sorrow escape careless tea quality 0.5% ~ 1.5% embedding medium, account for sorrow escape careless tea quality 2.5% ~ 5% enzyme, the vitamin C of 0.02% ~ 0.1%, the citric acid of 0.02% ~ 0.1%, the stabilizing agent of 0.02% ~ 0.1%, the flavor substance of 0.002% ~ 0.01%, the sweetener of 4% ~ 8%, the breast of 5% ~ 15% or dairy products, the edible milk-taste essence of 0.002% ~ 0.01% and the water composition of surplus, wherein said embedding medium is beta-schardinger dextrin-, and enzyme is one or several the mixture in protease, pectase, tannase, and flavor substance is essence.
Sorrow of the present invention escape careless tea beverage raw material composition by mass percentage by 0.16% ~ 4% sorrow escape careless tea, account for sorrow escape careless tea quality 0.5% ~ 1.5% embedding medium, account for sorrow escape careless tea quality 2.5% ~ 5% enzyme, 0.02% ~ 0.1% vitamin C, 0.02% ~ 0.1% citric acid, 0.02% ~ 0.1% stabilizing agent, 0.002% ~ 0.01% flavor substance, the sweetener of 4% ~ 8%, the tea extract of 5% ~ 30% and surplus water form; Wherein said embedding medium is beta-schardinger dextrin-, and enzyme is one or several the mixture in protease, pectase, tannase, and flavor substance is essence, and tea extract is one or more in green-tea extract, black tea extract, oolong tea extract.
The escape preparation method of careless tea beverage follows these steps to realize the present invention's series sorrow:
One, pick out sorrow after plucking to escape blade of grass, naturally spread to moisture content 60% ~ 80% after impurity elimination, then put into cylinder, arranging bowl temperature is 200 ~ 350 DEG C, uses hot blast or steam to shake green grass or young crops 3 ~ 10min, obtains the sorrow after completing and to escape blade of grass;
Two, blade of grass of the sorrow after completing being escaped is put in kneading machine, and be 20 ~ 40 DEG C in temperature, rotating speed is knead under the condition of 30 ~ 60 revs/min, obtain the sorrow after kneading to escape blade of grass, after curing process, be put into re-roasting pot again carry out re-roasting, when to fry to moisture content be 3% ~ 6%, obtain sorrow and to escape careless tea;
Three, adopt pulverizer to carry out pulverization process the sorrow that step 2 obtains careless tea of escaping, collection of sieving obtains sorrow and to escape careless tea powder;
Four, careless tea powder of sorrow being escaped mixes with purifying waste water, obtain sorrow to escape careless tea solution, then add and account for sorrow and to escape the beta-schardinger dextrin-of careless tea solution weight 0.02% ~ 0.1%, 20 ~ 60min is extracted at the temperature of 50 ~ 80 DEG C, carry out centrifugal treating after filtration and collect centrifugal clear liquid, obtain water extract liquid;
Five, the pH adding acid regulator regulation and control water extract liquid is 5 ~ 7, then adds the enzyme accounting for water extract liquid weight 0.02% ~ 0.1% and carries out enzymolysis processing, obtain the clear liquid after enzymolysis processing;
Six, in the clear liquid after enzymolysis processing, add dilution of purifying waste water, adding acid regulator regulation system pH is 5 ~ 7, is then placed in temporary storage tank storage and obtains pretreatment mother liquor;
Seven, add the vitamin C, the citric acid of 0.02% ~ 0.1%, the stabilizing agent of 0.02% ~ 0.1% and the flavoring that account for pretreatment mother liquor weight 0.02% ~ 0.1% to pretreatment mother liquor, obtain seasoning liquid;
Eight, be 60 ~ 80 DEG C in temperature, pressure is carry out homogeneous process to seasoning liquid under the condition of 15 ~ 23MPa, obtains the seasoning liquid after homogeneous;
Nine, the seasoning liquid after homogeneous is filled in vial, and carries out sterilization processing, obtain serial sorrow and to escape careless tea beverage;
Enzyme wherein described in step 5 is one or several the mixture in protease, pectase, tannase, and the flavoring described in step 7 is one or more mixtures of fruit juice, sugar, sweetener, breast, dairy products, essence, green-tea extract, black tea extract or oolong tea extract.
The present invention uses tannase (hydrolase) to cut off the ester bond of catechol and gallic acid, the gallic acid anion discharged again can with other oxidation product of Polyphenols competition caffeine, form the hydrotrope of molecular weight, thus reduce the turbidity of low cost vegetable plant water extract.Soluble protein in the protease decomposable asymmetric choice net millet paste simultaneously added in low cost vegetable plant water extract generates amino acid, and the pectase decomposable asymmetric choice net pectic substance of interpolation generates monose.The generation of the small-molecule substance such as amino acid, monose, facilitates the formation of low cost vegetable plant water extract local flavor on the one hand, also reduces the amount participating in forming deposit simultaneously, thus reduces the turbidity of low cost vegetable plant water extract.
The present invention finds that pH value can affect sorrow and to escape the stability of catechin in careless water-soluble extractive, and when pH value is greater than 5 ~ 7, catechin brown stain will occur.By control ph, thus the carrying out of restriction dehydrogenation oxidation, make the color and luster of low cost vegetable plant water extract effectively can keep substantially constant under the condition of low ph value.
Low cost vegetable plant water extract along with the intensification of the degree of oxidation of polyphenols by green flavescence, even general red.Add Vc as strong reductant, its oxidation-reduction potential is lower than polyphenols, under identical external condition, can have precedence over first high with the electrode potential material of polyphenols as combinations such as oxygen.
Wherein the molecular structure of cyclodextrine makes the outer surface of its molecule have stronger hydrophily, the center of molecule then shows as hydrophobicity, and it can be made multiple compounds molecule be entered in molecular cavities whole or in part by Van der Waals force and form Inclusion Complexes.Adopt β-CD to have significant bury function to the material participating in being formed precipitation in low cost vegetable plant water extract, blocked the combination between Polyphenols and caffeine, protein, decreased the amount of substance forming precipitation, thus improve the clarity of millet paste.
In sum, sorrow is escaped in grass and is had multiple physiologically active ingredient, comprises flavonoids, triterpenes, sulfur-containing compound, phytosterol, pheophytin class, cerebroside, amino acid, trace element, alkaloid and multiple micromolecular compound etc.There is the good potential quality being developed to drink.Because escape composition and the content of these physiological activators in the material of grassland and current local tea variety of having illustrated of sorrow has certain difference, therefore the present invention is optimized from the aspect of raw material extraction, seasoning allotment, homogeneous, sterilization to the escape preparation technology of careless water-soluble extractive of sorrow.
The serial sorrow that the present invention obtains escape careless tea beverage after sterilization preservation under room temperature within 12 months, still keep as clear as crystal, without flocculent deposit and supernatant, smell delicate fragrance, have tea beverage flavor characteristics, results of sensory evaluation is excellent; The indices such as polyphenol content, caffeine, protein meet national standard.
The invention provides and a series ofly escape grass for the preparation method of the drink of raw material with sorrow, the sorrow variation of careless Related product, the sorrow exploitation of grass in functional food or health food of escaping of escaping are had great importance.
1, carried out sorrow first to escape the exploitation of various beverages that grass is raw material;
2, set forth serial sorrow to escape the processing technology of careless drink and parameter;
3, opening statement affects sorrow and to escape the various influence factor of careless drink stable system and control measure thereof;
4, the present invention sets forth sorrow from multiple angle and to escape the method for quality control of careless drink, and providing a series of is the preparation method of the beverage of raw material with sorrow grass of escaping.The present invention has great importance in the exploitation of functional food for the sorrow variation of careless Related product, sorrow grass of escaping of escaping, and Related product has wide market prospects.
Detailed description of the invention
Detailed description of the invention one: present embodiment sorrow escape careless tea beverage raw material composition by mass percentage by 0.16% ~ 4% sorrow escape careless tea, account for sorrow escape careless tea quality 0.5% ~ 1.5% embedding medium, account for sorrow escape careless tea quality 2.5% ~ 5% enzyme, 0.02% ~ 0.1% vitamin C, 0.02% ~ 0.1% citric acid, 0.02% ~ 0.1% stabilizing agent, the flavor substance of 0.002% ~ 0.01%, the sweetener of 4% ~ 8% and surplus water form; Wherein said embedding medium is beta-schardinger dextrin-, and enzyme is one or several the mixture in protease, pectase, tannase, and flavor substance is essence.
Detailed description of the invention two: the escape raw material composition of careless tea beverage of present embodiment sorrow to be escaped careless tea by the sorrow of 0.16% ~ 4% by mass percentage, account for sorrow escape careless tea quality 0.5% ~ 1.5% embedding medium, account for sorrow escape careless tea quality 2.5% ~ 5% enzyme, the vitamin C of 0.02% ~ 0.1%, the citric acid of 0.02% ~ 0.1%, the stabilizing agent of 0.02% ~ 0.1%, the flavor substance of 0.002% ~ 0.01%, the sweetener of 4% ~ 8%, the fruit juice of 5% ~ 10%, the edible fruity flavor of 0.002% ~ 0.01% and the water composition of surplus, wherein said embedding medium is beta-schardinger dextrin-, and enzyme is one or several the mixture in protease, pectase, tannase, and flavor substance is essence.
The sorrow that present embodiment obtains is escaped polyphenol content >=200mg/kg, content of caffeine >=35mg/kg in careless tea beverage.
Detailed description of the invention three: the escape raw material composition of careless tea beverage of present embodiment sorrow to be escaped careless tea by the sorrow of 0.16% ~ 4% by mass percentage, account for sorrow escape careless tea quality 0.5% ~ 1.5% embedding medium, account for sorrow escape careless tea quality 2.5% ~ 5% enzyme, the vitamin C of 0.02% ~ 0.1%, the citric acid of 0.02% ~ 0.1%, the stabilizing agent of 0.02% ~ 0.1%, the flavor substance of 0.002% ~ 0.01%, the sweetener of 4% ~ 8%, the breast of 5% ~ 15% or dairy products, the edible milk-taste essence of 0.002% ~ 0.01% and the water composition of surplus, wherein said embedding medium is beta-schardinger dextrin-, and enzyme is one or several the mixture in protease, pectase, tannase, and flavor substance is essence.
Detailed description of the invention four: the escape raw material composition of careless tea beverage of present embodiment sorrow to be escaped careless tea by the sorrow of 0.16% ~ 4% by mass percentage, account for sorrow escape careless tea quality 0.5% ~ 1.5% embedding medium, account for sorrow escape careless tea quality 2.5% ~ 5% enzyme, the vitamin C of 0.02% ~ 0.1%, the citric acid of 0.02% ~ 0.1%, the stabilizing agent of 0.02% ~ 0.1%, the flavor substance of 0.002% ~ 0.01%, the sweetener of 4% ~ 8%, the tea extract of 5% ~ 30% and the water composition of surplus, wherein said embedding medium is beta-schardinger dextrin-, and enzyme is one or several the mixture in protease, pectase, tannase, and flavor substance is essence, and tea extract is one or more in green-tea extract, black tea extract, oolong tea extract.
The sorrow that present embodiment obtains is escaped polyphenol content >=150mg/kg, content of caffeine >=325mg/kg in careless tea beverage.
Embedding medium described in detailed description of the invention one to four uses escaping to sorrow in careless extraction with aqueous solution process.
Detailed description of the invention five: one of present embodiment and detailed description of the invention one to four are escaped in careless tea beverage unlike sorrow and be also filled with carbon dioxide.
The content (20 DEG C of volume multiples) >=1.5 times of carbon dioxide in present embodiment.
Detailed description of the invention six: the escape preparation method of careless tea beverage follows these steps to implement present embodiment series sorrow:
One, pick out sorrow after plucking to escape blade of grass, naturally spread to moisture content 60% ~ 80% after impurity elimination, then put into cylinder, arranging bowl temperature is 200 ~ 350 DEG C, uses hot blast or steam to shake green grass or young crops 3 ~ 10min, obtains the sorrow after completing and to escape blade of grass;
Two, blade of grass of the sorrow after completing being escaped is put in kneading machine, and be 20 ~ 40 DEG C in temperature, rotating speed is knead under the condition of 30 ~ 60 revs/min, obtain the sorrow after kneading to escape blade of grass, after curing process, be put into re-roasting pot again carry out re-roasting, when to fry to moisture content be 3% ~ 6%, obtain sorrow and to escape careless tea;
Three, adopt pulverizer to carry out pulverization process the sorrow that step 2 obtains careless tea of escaping, collection of sieving obtains sorrow and to escape careless tea powder;
Four, careless tea powder of sorrow being escaped mixes with purifying waste water, obtain sorrow to escape careless tea solution, then add and account for sorrow and to escape the beta-schardinger dextrin-of careless tea solution weight 0.02% ~ 0.1%, 20 ~ 60min is extracted at the temperature of 50 ~ 80 DEG C, carry out centrifugal treating after filtration and collect centrifugal clear liquid, obtain water extract liquid;
Five, the pH adding acid regulator regulation and control water extract liquid is 5 ~ 7, then adds the enzyme accounting for water extract liquid weight 0.02% ~ 0.1% and carries out enzymolysis processing, obtain the clear liquid after enzymolysis processing;
Six, in the clear liquid after enzymolysis processing, add dilution of purifying waste water, adding acid regulator regulation system pH is 5 ~ 7, is then placed in temporary storage tank storage and obtains pretreatment mother liquor;
Seven, add the vitamin C, the citric acid of 0.02% ~ 0.1%, the stabilizing agent of 0.02% ~ 0.1% and the flavoring that account for pretreatment mother liquor weight 0.02% ~ 0.1% to pretreatment mother liquor, obtain seasoning liquid;
Eight, be 60 ~ 80 DEG C in temperature, pressure is carry out homogeneous process to seasoning liquid under the condition of 15 ~ 23MPa, obtains the seasoning liquid after homogeneous;
Nine, the seasoning liquid after homogeneous is filled in vial, and carries out sterilization processing, obtain serial sorrow and to escape careless tea beverage;
Enzyme wherein described in step 5 is one or several the mixture in protease, pectase, tannase, and the flavoring described in step 7 is one or more mixtures of fruit juice, sugar, sweetener, breast, dairy products, essence, green-tea extract, black tea extract or oolong tea extract.
Process of kneading described in present embodiment step 2 not only achieves kneads shaping, but also in the cooling procedure of the various compositions that sorrow is escaped in grass after completing, various physicochemical change occurs, improves quality.
Sorrow grass of escaping is a Plants, composition in leaf is different from the tealeaves that other can be used as beverage raw material, sorrow protocol of escaping contains crude protein about 46%, crude fat about 10%, crude fibre about 15%, ash content about 13%, wherein also containing a large amount of polyphenols, triterpene substance, sterols material.The contamination of these materials and common tealeaves (green tea, black tea, oolong tea) all have certain difference, and adopt different extraction processes, the ratio that these materials are dissolved is also different; Especially again through being deployed into dissimilar beverage (fruit juice, breast, etc.), more add the complexity of this system, and these are all the keys affecting product stability.The present invention adopts controlling extractive technique, controlling zymolysis technique, microcapsule embedded technology combine and add the multiple method such as specific stabilizing agent and make product of the present invention have good stability.
Present embodiment careless tea of sorrow being escaped is deployed into following four large class beverages, and namely sorrow is escaped careless tea beverage (millet paste), seasoning tea beverage, multiple (mix) conjunction tea beverage and tea concentrate four class.Seasoning tea beverage is divided into fruit juice tea beverage, fruity tea beverage, milk tea beverage, milk taste tea beverage, carbonic acid tea beverage and other seasoning tea beverages.
Detailed description of the invention seven: present embodiment and detailed description of the invention six are that blade of grass of the sorrow after kneading being escaped is spread out in the baking being lined with poromeric material and sieves unlike the processing procedure of curing described in step 2, leaf-spreading thickness is 1.5 ~ 2.5 centimetres, first cure process with the temperature of 70 ~ 110 DEG C, be cooled to 40 ~ 60 DEG C again, being dried to the escape moisture content of blade of grass of sorrow is 10% ~ 15%, completes and cure process after cooling.Other step and parameter identical with detailed description of the invention six.
Detailed description of the invention eight: present embodiment and detailed description of the invention six or seven are 40 ~ 60 DEG C unlike pot temperature during step 2 re-roasting.Other step and parameter identical with detailed description of the invention six or seven.
Detailed description of the invention nine: one of present embodiment and detailed description of the invention six to eight are crossed 60 mesh sieves unlike step 3 and carried out screening collection and obtain sorrow and to escape careless tea powder.Other step and parameter identical with one of detailed description of the invention six to eight.
Detailed description of the invention ten: one of present embodiment and detailed description of the invention six to nine are papain or bromelain unlike the protease described in step 5.Other step and parameter identical with one of detailed description of the invention six to nine.
Detailed description of the invention 11: one of present embodiment and detailed description of the invention six to ten adopt evaporation to concentrate unlike the pretreatment mother liquor obtained step 6 again.Other step and parameter identical with one of detailed description of the invention six to ten.
Detailed description of the invention 12: present embodiment and detailed description of the invention six unlike careless tea beverage of escaping when step 9 series sorrow be sorrow escape grassland flavor beverage time, flavoring described in step 7 is sucrose or sweetener, and the content of sucrose accounts for 0.02% ~ 0.1% of pretreatment mother liquor weight.Other step and parameter identical with detailed description of the invention six.
Detailed description of the invention 13: present embodiment and detailed description of the invention six unlike careless tea beverage of escaping when step 9 series sorrow be sorrow escape tsaoko flavor beverage time, the flavoring described in step 7 is fruit juice, edible fruity flavor, sugar and sweetener.Other step and parameter identical with detailed description of the invention six.
Detailed description of the invention 14: present embodiment and detailed description of the invention six unlike careless tea beverage of escaping when step 9 series sorrow be sorrow escape careless milk taste tea beverage time, the flavoring described in step 7 is breast, dairy products, sugar, sweetener and edible milk-taste essence.Other step and parameter identical with detailed description of the invention six.
Detailed description of the invention 15: present embodiment and detailed description of the invention six unlike careless tea beverage of escaping when step 9 series sorrow be sorrow escape careless compound tea beverage time, the flavoring described in step 7 is one or more mixture of green-tea extract, black tea extract or oolong tea extract.Other step and parameter identical with detailed description of the invention six.
Detailed description of the invention 16: present embodiment and detailed description of the invention six unlike careless tea beverage of escaping when step 9 series sorrow be sorrow escape careless soda time, in advance thermal sterilization is carried out to vitamin C, citric acid, calgon and flavoring that step 7 is added, and omit the sterilization processing in step 9.Other step and parameter identical with detailed description of the invention six.
Detailed description of the invention 17: present embodiment and detailed description of the invention six are carry out ultra high temperature short time sterilization in tubing heat exchanger unlike the sterilization processing described in step 9, temperature controls at 130 ~ 142 DEG C, time is 2 ~ 8s, carries out sterile filling after being cooled to normal temperature.Other step and parameter identical with detailed description of the invention six.
Embodiment one: the escape preparation method of careless tea beverage follows these steps to implement the present embodiment series sorrow:
One, pick out sorrow after plucking to escape blade of grass, naturally spread to moisture content 60% after impurity elimination, then put into cylinder, arrange bowl temperature 200 DEG C, serviceability temperature is 250 DEG C, and the hot blast of 600rpm shakes blue or green 5min, obtains the sorrow after completing and to escape blade of grass;
Two, blade of grass of the sorrow after completing being escaped is put in kneading machine, it is 30 DEG C in temperature, rotating speed is knead under the condition of 50 revs/min, obtain the sorrow after kneading to escape blade of grass, after curing process, be put into pot temperature is again that 50 DEG C of re-roasting pots carry out re-roasting, fry when being 5% to the obvious moisture content of fragrance, obtain sorrow and to escape careless tea;
Three, adopt pulverizer to carry out pulverization process the sorrow that step 2 obtains careless tea of escaping, cross 60 mesh sieve and carry out screening collection and obtain sorrow and to escape careless tea powder;
Four, careless tea powder of 20kg sorrow being escaped is purified waste water with 500kg and is mixed, obtain sorrow to escape careless tea solution, then add and account for sorrow and to escape the beta-schardinger dextrin-of careless tea solution weight 0.1%, 40min is extracted at the temperature of 70 DEG C, 100 eye mesh screens are adopted to carry out filtration treatment, collect centrifugal clear liquid with the centrifugation process of 6000rpm, obtain water extract liquid;
Five, the pH adding HCl regulation and control water extract liquid is 6, then adds the papain accounting for water extract liquid weight 0.05%% and carries out enzymolysis processing 2h, obtain the clear liquid after enzymolysis processing;
Six, in the clear liquid after enzymolysis processing, add 2 times of dilutions of purifying waste water, adding HCl regulation system pH is 6, is then placed in temporary storage tank storage and obtains pretreatment mother liquor;
Seven, to pretreatment mother liquor add account for pretreatment mother liquor weight 0.1% vitamin C, 0.1% citric acid, 0.1% calgon, the granulated sugar of 6%, the cider of 10% and 0.01% green apple essence, obtain seasoning liquid;
Eight, be 70 DEG C in temperature, pressure is carry out homogeneous process twice to seasoning liquid under the condition of 20MPa, obtains the seasoning liquid after homogeneous;
Nine, the seasoning liquid after homogeneous is filled in vial, sterilization processing 20min at 120 DEG C, obtains sorrow and to escape careless tea beverage.
Sorrow present embodiment prepared careless water-soluble extractive of escaping is placed 12 months at room temperature 25 DEG C, then Product Status is observed, and ask 15 experienced professional and technical personnel to form evaluation group, with reference to the subjective appreciation method of table 1, the organoleptic indicator of product is marked.Adopt 15 points of point systems processed, the weighted value of each index sees the following form, and by calculating the comprehensive acceptability of product, its value shows that more greatly the organoleptic quality of product is better; The escape sensory evaluation scores of careless tea beverage of sorrow prepared by result the present embodiment is 14.5.The polyphenol content contained in corresponding product is 235.6mg/kg, and caffeine content is 53.4mg/kg.
Table 1 sorrow is escaped careless water-soluble extractive subjective appreciation
Embodiment two: the escape preparation method of careless tea beverage follows these steps to implement the present embodiment series sorrow:
One, pick out sorrow after plucking to escape blade of grass, naturally spread to moisture content 80% after impurity elimination, then put into cylinder, arrange bowl temperature 300 DEG C, serviceability temperature is 300 DEG C, and the hot blast of 800rpm shakes blue or green 10min, obtains the sorrow after completing and to escape blade of grass;
Two, blade of grass of the sorrow after completing being escaped is put in kneading machine, it is 40 DEG C in temperature, rotating speed is knead under the condition of 60 revs/min, obtain the sorrow after kneading to escape blade of grass, after curing process, be put into pot temperature is again that 50 DEG C of re-roasting pots carry out re-roasting, fry when being 5% to the obvious moisture content of fragrance, obtain sorrow and to escape careless tea;
Three, adopt pulverizer to carry out pulverization process the sorrow that step 2 obtains careless tea of escaping, cross 60 mesh sieve and carry out screening collection and obtain sorrow and to escape careless tea powder;
Four, careless tea powder of 20kg sorrow being escaped is purified waste water with 300kg and is mixed, obtain sorrow to escape careless tea solution, then add and account for sorrow and to escape the beta-schardinger dextrin-of careless tea solution weight 0.05%, 60min is extracted at the temperature of 80 DEG C, 100 eye mesh screens are adopted to carry out filtration treatment, collect centrifugal clear liquid with the centrifugation process 20min of 8000rpm, obtain water extract liquid;
Five, the pH adding HCl regulation and control water extract liquid is 6, then adds the bromelain accounting for water extract liquid weight 0.1% and carries out enzymolysis processing 1.5h, obtain the clear liquid after enzymolysis processing;
Six, in the clear liquid after enzymolysis processing, add 3 times of dilutions of purifying waste water, adding HCl regulation system pH is 6, is then placed in temporary storage tank storage and obtains pretreatment mother liquor;
Seven, to pretreatment mother liquor add account for pretreatment mother liquor weight 0.05% vitamin C, 0.05% citric acid, 0.05% calgon, 5% granulated sugar, 10% skimmed milk (protein quality mark >=0.5%) and 0.01% milk-taste essence, obtain seasoning liquid;
Eight, be 80 DEG C in temperature, pressure is carry out homogeneous process twice to seasoning liquid under the condition of 23MPa, obtains the seasoning liquid after homogeneous;
Nine, get the liquid after homogeneous, in tubing heat exchanger, carry out ultra high temperature short time sterilization, temperature controls at 140 DEG C, time 4s.Carry out sterile filling after being cooled to normal temperature, obtain sorrow and to escape careless tea beverage.
Sorrow present embodiment prepared careless water-soluble extractive of escaping is placed 12 months at room temperature 25 DEG C, then Product Status is observed, and ask 15 experienced professional and technical personnel to form evaluation group, with reference to the subjective appreciation method of table 1, the organoleptic indicator of product is marked.Adopt 15 points of point systems processed, the weighted value of each index sees the above table, and by calculating the comprehensive acceptability of product, its value shows that more greatly the organoleptic quality of product is better; The escape sensory evaluation scores of careless tea beverage of sorrow prepared by result the present embodiment is 14.6.The polyphenol content contained in corresponding product is 221.6mg/kg, and caffeine content is 40.7mg/kg.Protein content is 0.85%.

Claims (10)

1. sorrow is escaped careless tea beverage, it is characterized in that this sorrow escape careless tea beverage raw material composition by mass percentage by 0.16% ~ 4% sorrow escape careless tea, account for sorrow escape careless tea quality 0.5% ~ 1.5% embedding medium, account for sorrow escape careless tea quality 2.5% ~ 5% enzyme, 0.02% ~ 0.1% vitamin C, 0.02% ~ 0.1% citric acid, 0.02% ~ 0.1% stabilizing agent, the flavor substance of 0.002% ~ 0.01%, the sweetener of 4% ~ 8% and surplus water form; Wherein said embedding medium is beta-schardinger dextrin-, and enzyme is one or several the mixture in protease, pectase, tannase, and flavor substance is essence.
2. sorrow is escaped careless tea beverage, it is characterized in that this sorrow escape careless tea beverage raw material composition by mass percentage by 0.16% ~ 4% sorrow escape careless tea, account for sorrow escape careless tea quality 0.5% ~ 1.5% embedding medium, account for sorrow escape careless tea quality 2.5% ~ 5% enzyme, 0.02% ~ 0.1% vitamin C, 0.02% ~ 0.1% citric acid, 0.02% ~ 0.1% stabilizing agent, 0.002% ~ 0.01% flavor substance, 4% ~ 8% sweetener, the fruit juice of 5% ~ 10%, the edible fruity flavor of 0.002% ~ 0.01% and surplus water form; Wherein said embedding medium is beta-schardinger dextrin-, and enzyme is one or several the mixture in protease, pectase, tannase, and flavor substance is essence.
3. sorrow is escaped careless tea beverage, it is characterized in that this sorrow escape careless tea beverage raw material composition by mass percentage by 0.16% ~ 4% sorrow escape careless tea, account for sorrow escape careless tea quality 0.5% ~ 1.5% embedding medium, account for sorrow escape careless tea quality 2.5% ~ 5% enzyme, the vitamin C of 0.02% ~ 0.1%, citric acid, the stabilizing agent of 0.02% ~ 0.1%, flavor substance, the sweetener of 4% ~ 8%, the breast of 5% ~ 15% or dairy products, the edible milk-taste essence of 0.002% ~ 0.01% and the water of surplus of 0.002% ~ 0.01% of 0.02% ~ 0.1% form; Wherein said embedding medium is beta-schardinger dextrin-, and enzyme is one or several the mixture in protease, pectase, tannase, and flavor substance is essence.
4. sorrow is escaped careless tea beverage, it is characterized in that this sorrow escape careless tea beverage raw material composition by mass percentage by 0.16% ~ 4% sorrow escape careless tea, account for sorrow escape careless tea quality 0.5% ~ 1.5% embedding medium, account for sorrow escape careless tea quality 2.5% ~ 5% enzyme, 0.02% ~ 0.1% vitamin C, 0.02% ~ 0.1% citric acid, 0.02% ~ 0.1% stabilizing agent, 0.002% ~ 0.01% flavor substance, the sweetener of 4% ~ 8%, the tea extract of 5% ~ 30% and surplus water form; Wherein said embedding medium is beta-schardinger dextrin-, enzyme is one or several the mixture in protease, pectase, tannase, flavor substance is essence, and tea extract is the mixture of one or more in green-tea extract, black tea extract, oolong tea extract.
5. to escape careless tea beverage according to the sorrow one of Claims 1-4 Suo Shu, it is characterized in that also being filled with carbon dioxide in sorrow escapes careless tea beverage.
6. serial sorrow is escaped the preparation method of careless tea beverage, it is characterized in that following these steps to realize:
One, pick out sorrow after plucking to escape blade of grass, naturally spread to moisture content 60% ~ 80% after impurity elimination, then put into cylinder, arranging bowl temperature is 200 ~ 350 DEG C, uses hot blast or steam to shake green grass or young crops 3 ~ 10min, obtains the sorrow after completing and to escape blade of grass;
Two, blade of grass of the sorrow after completing being escaped is put in kneading machine, and be 20 ~ 40 DEG C in temperature, rotating speed is knead under the condition of 30 ~ 60 revs/min, obtain the sorrow after kneading to escape blade of grass, after curing process, be put into re-roasting pot again carry out re-roasting, when to fry to moisture content be 3% ~ 6%, obtain sorrow and to escape careless tea;
Three, adopt pulverizer to carry out pulverization process the sorrow that step 2 obtains careless tea of escaping, collection of sieving obtains sorrow and to escape careless tea powder;
Four, careless tea powder of sorrow being escaped mixes with purifying waste water, obtain sorrow to escape careless tea solution, then add and account for sorrow and to escape the beta-schardinger dextrin-of careless tea solution weight 0.02% ~ 0.1%, 20 ~ 60min is extracted at the temperature of 50 ~ 80 DEG C, carry out centrifugal treating after filtration and collect centrifugal clear liquid, obtain water extract liquid;
Five, the pH adding acid regulator regulation and control water extract liquid is 5 ~ 7, then adds the enzyme accounting for water extract liquid weight 0.02% ~ 0.1% and carries out enzymolysis processing, obtain the clear liquid after enzymolysis processing;
Six, in the clear liquid after enzymolysis processing, add dilution of purifying waste water, adding acid regulator regulation system pH is 5 ~ 7, is then placed in temporary storage tank storage and obtains pretreatment mother liquor;
Seven, add the vitamin C, the citric acid of 0.02% ~ 0.1%, the stabilizing agent of 0.02% ~ 0.1% and the flavoring that account for pretreatment mother liquor weight 0.02% ~ 0.1% to pretreatment mother liquor, obtain seasoning liquid;
Eight, be 60 ~ 80 DEG C in temperature, pressure is carry out homogeneous process to seasoning liquid under the condition of 15 ~ 23MPa, obtains the seasoning liquid after homogeneous;
Nine, the seasoning liquid after homogeneous is filled in vial, and carries out sterilization processing, obtain serial sorrow and to escape careless tea beverage;
Enzyme wherein described in step 5 is one or several the mixture in protease, pectase, tannase, and the flavoring described in step 7 is one or more mixtures of fruit juice, sugar, sweetener, breast, dairy products, essence, green-tea extract, black tea extract or oolong tea extract.
7. serial sorrow according to claim 6 is escaped the preparation method of careless tea beverage, it is characterized in that the protease described in step 5 is papain or bromelain.
8. serial sorrow according to claim 6 is escaped the preparation method of careless tea beverage, it is characterized in that the pretreatment mother liquor obtained step 6 adopts evaporation to concentrate again.
9. serial sorrow according to claim 6 is escaped the preparation method of careless tea beverage, it is characterized in that when step 9 series sorrow escape careless tea beverage be sorrow escape grassland flavor beverage time, flavoring described in step 7 is sucrose or sweetener, and the content of sucrose accounts for 0.02% ~ 0.1% of pretreatment mother liquor weight.
10. serial sorrow according to claim 6 is escaped the preparation method of careless tea beverage, it is characterized in that when the sterilization processing described in step 9 carries out ultra high temperature short time sterilization in tubing heat exchanger, temperature controls at 130 ~ 142 DEG C, and the time is 2 ~ 8s, carries out sterile filling after being cooled to normal temperature.
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CN106472758A (en) * 2016-09-30 2017-03-08 正安县黔蕊茶业有限公司 A kind of processing technique of green tea beverage
CN107047859A (en) * 2017-03-17 2017-08-18 遵义茗香康源茶饮发展科技有限公司 A kind of preparation method of Traditional Chinese medicine tea drink
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CN110839725A (en) * 2019-12-28 2020-02-28 许昌学院 Clinacanthus nutans functional tea beverage formula and preparation method
CN111329983A (en) * 2020-03-13 2020-06-26 广东瑞博制药有限公司 Traditional Chinese medicine composition containing clinacanthus nutans and preparation method thereof
CN111329983B (en) * 2020-03-13 2022-02-15 广东瑞博制药有限公司 Traditional Chinese medicine composition containing clinacanthus nutans and preparation method thereof
CN112006194A (en) * 2020-09-14 2020-12-01 五指山通盛生物科技有限公司 Clinacanthus nutans beverage and preparation method thereof
IT202100011798A1 (en) * 2021-05-07 2022-11-07 Ngn Healthcare New Generation Nutraceuticals S R L PROCESS TO INCREASE THE INTESTINAL BIOACCESSIBILITY OF POLYPHENOLS IN A LYOPHILISATE OF A VEGETABLE MATRIX WITH HIGH POLYPHENOL CONTENT
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