CN105326755B - Additive-free mung bean anti-acne maintenance face paper and its Green production method - Google Patents

Abstract

The present invention relates to a kind of additive-free mung bean anti-acne maintenance face paper and its Green production method, belong to cosmetics process technology.Using food-grade or dietotherapeutic raw material mung bean, pearl, pollen pini, lily, white fungus, honeysuckle, dried rose flower, lemon tablet, dried orange peel, it is process meticulously through techniques such as continuous activation, high pressure disintegration, supercritical extracts；Product is without essence, pigment, preservative.Product has good organoleptic quality and clearing heat and detoxicating, antiphlogistic antibacterial effect.It is adapted to the crowd of needs facial care cosmetic needs, and acne（Whelk）Treatment or alleviation skin patient.Process of producing product is pollution-free, and no waste residue, waste vapour and harmful substance produce, and realize green production；The salubrious delicate fragrance of product special flavour, it is safe and non-toxic.It is a kind of new food-grade face paper.Production process of the present invention does not use any chemical reagents, does not add any medicine, does not add any hormone, and safety is without any side effects.

Description

Additive-free mung bean anti-acne maintenance face paper and its Green production method

Technical field

The invention belongs to cosmetics processing technique field, refers in particular to a kind of mung bean anti-acne maintenance face paper and its producer Method.

Background technology

Facial mask is a kind of carrier of skin of face maintenance or cosmetics, is applied or is attached to and keeps certain time on the face, The material that skin health is harmful to when the benefit materials in maintenance or cosmetics are absorbed by the skin, or in epidermis face is adsorbed by facial mask Afterwards, removed it by cleaning or peeling off, reach facial skin quality maintenance or beautification purpose.At present facial mask product species and formulation compared with It is more, such as paste, pulvis, creme, emulsion and using non-woven fabrics, silk, biological fiber material as rely on tearing type hygenic towelette face Film etc..The beauty of facial mask or maintenance principle are exactly to be covered in face's certain time using it, be skin with extraneous air with it is dirty Dye is temporarily isolating, and is improved skin temperature, the pore expansion of skin, is promoted sweat gland secretion and metabolism, make the oxygen content of skin Rise, exclude epidermal cell metabolism product and accumulation oil substances, while the moisture in facial mask and beneficiating ingredient infiltration The cuticula of epidermis, skin become soft, naturally bright flexible.Typically by facial mask be divided into mud cream type, tear-pull, gel-type, Four kinds of forms of hygenic towelette type.Especially wet tissue formula face paper, easy to use, effect is good, easily stored, the deep people to be liked to be beautiful likes, Occupy very big share in cosmetics industry rapidly.It is also deep to be praised highly by manufacturer because storing is convenient, cost of transportation is low, therefore Its consumption figure is very big.The incidence of disease of acne is higher in many facial skin diseases, also known as acne, dark sore, and traditional Chinese medical science ancient times claim face sore, It is dermatology common disease, frequently-occurring disease, it is higher to be particularly in the juvenile onset rate of adolescence, is referred to as " whelk ". According to statistics, have 95% in Adolescent male, women has 85% to suffer from different degrees of acne.If treatment is treated not in time or blindly Maxillofacial disease can be caused more serious, extend the course of disease, or even leave the scar for being difficult to eradicate, it is unhealthful and vivid, it is few to green grass or young crops Year brings psychological shade.Acne is a kind of chronic dermatosis for betiding pilosebaceous follicle, is mainly in Head And Face, neck, shirtfront The abundant position of the sebaceous glands such as back.The main reason for traditional medicine thinks to induce acne is due to overfeeding fatness, sweet, thick and oily so that spleen Accumulate steaming in stomach warm, or lung channel intrinsic heat, outside by ailment said due to cold or exposure, or worry beyond measure, be excited, having the fidgets, penting up of qi and blood it is hot, Or digestive tract function disorder, constipation, appoint rush it is uncomfortable stagnate in face and caused by.Doctor trained in Western medicine thinks acne and male sex hormone in human body Horizontal height, sebum secretion are excessively vigorous, sebaceous gland duct epidermis dyskeratosis blocks hair follicle hole, sebum local accumulation is drained not Freely, bacillus acnes (also referred to as Propionibacterium) infection makes skin of face tissue generation inflammation and the factor such as oedema is relevant.

Patients with acne using drug therapy, reasonable diet conditioning in addition to being lived, and some have the cosmetics of acne-removal function, especially Its facial mask class product has concurrently due to treating maintenance, is easy to use, also deep to be welcome by the people seeking beauty of patients with acne and facial. But it is most at present mitigate or the facial mask products for the treatment of acnes all add dexamethasone, chloramphenicol, metronidazole, A Si The medicines such as woods, clindamycin, erythromycin, chloramphenicol, or even addition hormones, antibiotic；Or addition imidazolidinyl urea, poly- second The additives such as glycol, zinc oxide, propane diols, kaolin.Moreover, nearly all adding preservative, skin is on the one hand set to produce medicine Rely on, long-term use is developed immunity to drugs；Simultaneously also due to skin makes body produce not the taken in excess of medicine or additive Good reaction.

The content of the invention

The present invention provides a kind of additive-free mung bean anti-acne maintenance face paper and its Green production method, and this product is with green Beans, pearl, pollen pini, lily, honeysuckle, dried rose flower, lemon, dried orange peel are primary raw material, do not add any medicine, do not add Any chemical addition agent, i.e., all using food-grade or dietotherapeutic raw material, using activation, high pressure disintegration, supercritical extract, low The techniques such as temperature immersion are process meticulously；Product is free of essence, pigment, preservative, and there is clearing heat and detoxicating, antiphlogistic antibacterial to act on, Product is adapted to each stratum, each age group needs face acnes（Whelk）Treatment or alleviation skin patient, can also meet into The beauty of row skin of face maintenance needs.Process of producing product is pollution-free, and no waste residue, waste vapour and harmful substance produce, and realize green Color produces, and the salubrious delicate fragrance of product special flavour is safe and non-toxic.

The present invention adopts the technical scheme that, is obtained by the raw material and step of following parts by weight：

25~35 parts of mung bean, 3~5 parts of pearl, 2~3 parts of pollen pini, honeysuckle are dry 1~3 part, 2~3 parts of dried rose flower, hundred It is dry 1~2 part to close dry 1~2 part, 1~2 part of lemon tablet, dried orange peel, 0.1~0.5 part of white fungus；

（One）Mung bean continuously activation and crushing

Take when producing ripe mung bean seed screening removal impurity per year, 8~15 DEG C of cold water spray washings are clean, are sent into vortex scalding Groove 3~5s of scalding in 80~90 DEG C of water, first time activation is carried out, then pulled out rapidly aerobic reciprocal in 29~35 DEG C of water of input Vibration immersion 5~9h, carry out second of activation process, frequency of oscillation be 30~80r/min, be passed through into water air capacity be 1~ 3L/h, then circulating water cleaning showers, drain surface moisture, and third time activation is carried out in 40~45 DEG C, 3~5min microwave oscillations Processing, is then freeze-dried to water content 18~25%, be crushed to can all by the active mung bean flour of 60~100 mesh aperture sieves, Aseptic storage, it is standby；

（Two）Mung bean, pollen pini, pearl powder joint high pressure disintegration

Crushing pearl is standby to the pearl powder of 80~100 mesh, then by pearl powder and step（One）The active mung bean of acquisition Powder and pollen pini are well mixed, and adjustment water content mass percent is 24~30%, using screw extruder in pressure 18~ Rotary extrusion under conditions of 20MPa, 102~120 DEG C of temperature, the macromolecular substances in raw material and hard plant material composition is set to exist It is disintegrated under HTHP, is advantageous to the dissolution of active ingredient, extrudate low temperature drying crushes to moisture 6~8% It is 80~100 mesh powders to granularity, aseptic storage is standby；

（Three）White fungus, it is each spend dry, lemon tablet and working of dried orange peel and crush

White fungus, dried lily bulb are handled respectively at 8~15 DEG C of 5~10h of cold water soak rehydrations, are washed out totally, dripping net surface Moisture, activation process is carried out in 40~45 DEG C, 5~8min microwave oscillations, is then freeze-dried to water content 6~8%, lily root flour Being broken to can be all standby by the powder of 60~100 mesh aperture sieves, aseptic storage；White fungus be crushed to can all by 240~ The powder of 500 mesh aperture sieves, aseptic storage are standby；

Dried rose flower, honeysuckle are dry, the dry cleaning removal of impurities of lemon tablet, dried orange peel, and being crushed to can be all by 40~100 mesh aperture The powder of sieve, adds pure water adjustment water content 30~35%, and activation process is carried out in 40~45 DEG C, 5~8min microwave oscillations, Then it is freeze-dried that to water content 6~8%, be crushed to can be all standby by the powder of 60~100 mesh aperture sieves, aseptic storage With；

（Four）Supercritical extract

The material powder prepared by above-mentioned steps is taken, is well mixed, active ingredient extraction is added and guides and supports agent, adjust compound Water content be 28~40%, guide and support agent composition for pure water 96%, 3 ° of light-coloured vinegars 2% of food-grade, the edible alcohol 2% of concentration 30%, then Stir, in 45~60 DEG C, 25~45MPa, 60~120min of time, CO₂19~26L/h of flow carries out CO₂Supercritical fluid Extraction, extract aseptic storage are standby；

（Five）Alternating temperature extracts

By step（Four）Extract remainder taken out from extraction kettle, add the deionized water of 5~15 times of its quality, stirring is equal It is even, 1~3d is impregnated under the conditions of 15~30 DEG C, is then separated, be filtrated to get can whole carrying by 5~10 μm of bore filter films Take liquid, aseptic storage is standby；Dregs after separation are pressed to the deionized water of 4~6 times of its mass ratio addition, stirred, in 40 30~60min is extracted under the conditions of~60 DEG C, 20~40min is extracted under the conditions of 60~90 DEG C, is then separated, be filtrated to get can be whole It is standby by the leaching liquor of 5~10 μm of bore filter films, aseptic storage；

（Six）Allotment, sterilization, dipping

By step（Four）The supercritical extract and step of acquisition（Five）It is well mixed under the leaching liquor cleaning condition of acquisition, White fungus powder is added, continues to stir, then in 130~135 DEG C, 4~9s ultra high temperature short time sterilizations, is cooled to 22~30 DEG C, Obtain the natural mung bean curing fluid of skin of face to deposit in aseptic tank, the natural silk face paper through aseptic process is put into above-mentioned In mung bean curing fluid, 2~6h is impregnated under 25~30 DEG C, aseptic condition, taking-up, smooth, aseptic packaging are in waterproof, airtight Airtight package bag in, as mung bean anti-acne maintenance facial mask paper product.

Product of the present invention not drug containing and chemical addition agent, are all made up of food material, have the peace of food grade products Quan Xing, long-term use have no toxic side effect, and do not produce pharmacological dependence.Additive-free mung bean anti-acne conserves face paper, spreads on during use Face, peel off after 10~25min, washed one's face portion with clear water.It is long-term use of that there is removing dirt, beautification face to skin of face Skin, antiphlogistic antibacterial, mitigate acne, desalinate the effect of whelk scar, while skin of face can be made careful, glossy.

The raw materials used present invention is food-grade or dietotherapeutic with clearing heat and detoxicating anti-inflammatory anti-inflammatory antivirus action Raw material, it is long-term use of without any side effects, it is specific as follows：

Mung bean（Vigna radiata (Linn.) Wilczek.）Belong to pulse family, also known as Semen phaseoli radiati, China existing 2,000 The cultivation history in remaining year, present East Asia various countries are generally planted, and also there is a small amount of plantation in Africa, Europe, the U.S..China is that mung bean is main One of exported country.After testing per 100g mung beans containing 21.6 grams of protein, 0.8 gram of fat, 55.6 grams of carbohydrate, dietary fiber 6.4 grams, 81 milligrams of calcium, 6.5 milligrams of iron, 2.18 milligrams of zinc, 0.95 milligram of vitamin e1.Modern study shows that mung bean contains class The bioactive ingredients such as flavones, tannin, saponin, alkaloid, phytosterol, cumarin, cardiac glycoside.It is green according to clinical trial Beans have anti-allergic effects, have inhibitory action to staphylococcus and some viruses, can be clearing heat and detoxicating；Mung bean has protection liver Dirty, kidney effect.《Kaibao Bencao》Record：" mung bean, it is sweet, tremble with fear, it is nontoxic.Enter the heart, stomach.”《Compendium of Materia Medica》Record：It is " green Beans, though the work(that acne is controlled in detumescence is same as red bean, and the power of thermal detoxification is pressed to cross it.And QI invigorating, thick stomach, qualcomm meridian, no withered people of long term usage Avoid.Surgery controls ulcer, has Neto shield heart to dissipate, and its effect is sayed in pole." and can " solve metal and stone, arsenic, vegetation all poison ".China passes System medical science thinks that mung bean is sweet, cold in nature；Enter the heart, stomach；Play the role of it is clearing heat and detoxicating, relieve summer heat, diuresis, anti-acne.

Dried orange peel：For a variety of mandarin orange classes such as rutaceae citrus reticulata"Chachi” or bowl mandarin orange（Citrus chachiensis Hort.）Fruit Skin, containing hesperidine (Hesperidin), Nobiletin (Nobiletin) and volatile oil.It is acrid flavour, sweet, it is cold in nature, enter spleen, stomach.Tool Have lower gas, adjust in, resolving sputum, relieving alcoholism effect.Cure mainly the full vexed, abdominal distention of feeding desorder, retention of dampness due to stagnation of QI, chest diaphragm, get sick from drinking too much wine it is thirsty Deng disease.Modern medicine study orange peel contains hesperidine and citrin, has anti-inflammatory, anti-allergic effects.

Lemon：The evergreen dungarunga lemon of Rutaceae both citrus（Citrun Limonia Osbeck）Fruit.Lemon is rich Containing citric acid, malic acid, carbohydrate, hesperidine, naringin, vitamin C, vitamin B1, vitamin B2, nicotinic acid, calcium, phosphorus, iron etc. Multiple nutritional components.Lemon is sour, micro-sweet, mild-natured to be slightly cold, enter liver, stomach.With preventing phlegm from forming and stopping coughing, promote the production of body fluid, invigorating the spleen, sharp liver, resist Hardening, Vitamin C, antibiotic and sterilizing, increase immunity and other effects.Mainly treating bronchitis, vitamin C deficiency, polydipsia, appetite are not Shake, receive and the disease such as subtract.Modern medicine, Nutritional studies show that lemon is high alka food, have very strong antioxidation, tool Have and promote the metabolism of body, promote liver and expelling toxin, anti-aging, remove free radical, suppress the effect such as cutaneous pigmentation.

Lily：Edible lily is the underground bulb of lily, rich in starch and protein, fat, alkaloid, calcium, phosphorus, iron etc. Composition and lily saponin, go acyl lily saponin, β-D- glucopyanoside and other functional ingredients.Lily is sweet, slight bitter, cold nature, It is nontoxic, enter the heart, lung channel.With moisten the lung and relieve the cough, replenishing the vital essence and removing heat, clearing away the heart fire and tranquillizing, sharp stool and urine and other effects.Be usually used in chronic cough of deficiency lung, The treatment of the disease such as overstrain cough spitting of blood, pyreticosis waste heat unclear, dysphoria palpitates with fear, insomnia and dreamful sleep.

Pearl powder：Pearl is medicinal in existing more than the 2000 years history of China.The period of Three Kingdoms《Mingyi Bielu》, beam generation《Book on Chinese herbal medicine warp Collection》, the Tang Dynasty《Haiyao Bencao, Oversea Materia Medica》, the Song Dynasty《Kaibao Bencao》, the Ming Dynasty《Compendium of Materia Medica》, the Qing Dynasty《Thunder God drug property cerse》Etc. medical ancient books, All there is clear and definite record to the effect of pearl.《Compendium of Materia Medica》Record " salty sweet nontoxic, the relieving palpitation point mesh of trembling with fear of pearl taste；Pearl applies face, Make us moist good color.--- --- is except face spot, antidiarrheal；Except children's fever (of children) accompanied by fear, pacify soul；Only pass out semen gonorrhoea, solution acne treats poison.... order Gloss is pure white " etc..《Compendium of Materia Medica》In also record, pearl play the role of desalinate freckle, chloasma.Modern medicine study discovery, Containing substantial amounts of trace element in pearl, there are anti-oxidant, enhancing skin activity, heat-clearing toxin expelling, whitening, anti-acne, desalination color spot etc. Effect.《Pharmacopoeia of People's Republic of China》And《Dictionary of medicinal plant》Recording pearl has arresting convulsion of calming the nerves, shade removing, solution taking poison and growing muscle due And other effects.Modern medicine study shows that pearl powder is improving the side such as body immunity, anti-aging, freckle removing and whitening, supplement calcium Face all has the function that uniqueness.

Pollen pini：Pollen pini is the spermatid of pine tree pistil, also known as pine is yellow, is to pick up from China indigenous tree pinaceae plant horse Tail pine（Pinus Massoniana Lamb.）And Chinese pine（Pinus tabulaeformis Carr.）Pure, dry pollen. First pharmacopeia on Chinese history《Sheng Nong's herbal classic》In be just related to the record of " pine yellow ".Ancient medicine writings claim pollen pini " it is sweet, warm, It is nontoxic ", there is " the function such as embellish lung, QI invigorating, wind-dispelling hemostasis, strong Yan Yizhi ".Bright Li Shizhen (1518-1593 A.D.)《Compendium of Materia Medica》：Preserved egg, sweet, warm, It is nontoxic.Embellish lung, QI invigorating, wind-dispelling hemostasis, it can also make wine.Pollen pini is nontoxic, has no side effect, and it does not have the allergy of sensitization Original matter, it will not also cause pollen allergy.China's pre-Qin days ancient books《Zhou Li》" food therapy " recorded has established traditional Chinese medicine The theory of medicine of " preventiveing treatment of disease ", and descendant compile《Dietetic materia medica》, all useful pollen pini cook soup, filling processed, steamed cake, wine brewing Record.Modern medicine independent studies result also demonstrates that pollen pini is nontoxic.

Pollen pini contains whole active nutritional compositions needed for life entity, including multiple proteins, amino acid, mineral Matter, enzyme and coenzyme, nucleic acid, monose, polysaccharide, biotin, cellulose, unrighted acid, flavones, rutin isoreactivity material, always Content is planted up to more than 200, and it is reasonable to arrange in pairs or groups, and can supplement comprehensively, the nutrition needed for balancing human body.Pollen pini contains abundant nutrition And functional component, skin metabolism can be strengthened, increase skin elasticity, delay skin aging, activating cell, remove free radical, block The generation of chloasma, butterfly macules, dermal melanin is eliminated, reduce, remove whelk so that the pure white beauty of skin.

Honeysuckle：Flos Lonicerae(drawing), Caprifoliaceae woodbine honeysuckle and congener dry flower or band The flower just opened, China is originated in, be distributed each province." honeysuckle " one is come from《Compendium of Materia Medica》, because honeysuckle flowers are just opened as white, after Switch to yellow, hence obtain one's name honeysuckle, is described as clearing heat and detoxicating good medicine from ancient times.《Sheng Nong's herbal classic》Carry：" honeysuckle taste cold in nature It is sweet, there is the effect of clearing heat and detoxicating, cool bloodization is become silted up, cure mainly affection of exogenous wind-heat, seasonal febrile diseases from the beginning of, sore serious case of furuncle, red and swollen heat pain, just purulence Blood " etc..《Compendium of Materia Medica》In honeysuckle has been discussed in detail there is the effect of " long term usage is made light of one's life by commiting suicide, promoted longevity ".Honeysuckle property is sweet cold Gas fragrance, clear heat with drugs of sweet flavour and cold nature without injuring one's stomach, fragrance thoroughly up to again can eliminating evil, can dispelling wind-heat, also kind removing summer-heat blood poison, for various heat Venereal disease, such as body heat, dermexanthesis, hair spot, heat toxin sore carbuncle, abscess of throat card.Honeysuckle is cold in nature, sweet, enters lung, the heart, stomach, has The effect of clearing heat and detoxicating, anti-inflammatory anti-inflammatory, qi-restoratives treat wind, cures mainly disease under turgor, warm disease heating, the disease such as heat toxin large carbuncle and tumour.It is right In diseases such as enteritis, measles, pneumonia, epidemic meningitis, septicemia, skin infection, ulcer boils, erysipelas, parotitis, suppurative tonsillitis Disease has certain curative effect.Honeysuckle is just extensive and famous with its medical value since ancient times.

Dried rose flower：Rose originates in China, and cultivation history is long, is a kind of rose family chamiso (Rosa Rugosa), rose hip is edible, rich in Vitamin C, commonly uses what vanilla tea, jam, jelly, fruit juice and bread etc., Yi You Sweden Soup（Nyponsoppa）, hydromel（Rhodomel）.Rose contains Rosa Damascana, and main component is that left-handed perfume is fragrant and mellow, for food With and it is used for cosmetic, petal can cake filling processed, cider, rose in syrup, can be made tea after drying.Rose is warm-natured sweet, micro- Hardship, Return liver, the spleen channel.With promoting the circulation of qi liver soothing and depression relief and blood, analgesic and other effects.It is full vexed to cure mainly chest diaphragm, gastral cavilty, side of body rib, menstruation are not The diseases such as tune, traumatic injury, carbuncle swells.《Food book on Chinese herbal medicine》Calling it, " main sharp lung spleen, beneficial liver and gall, the fragrance of food is sweet and refreshing, makes us refreshing refreshing." long Phase takes, can anti-inflammation and sterilization, dispelling fatigue, improvement constitution, effectively moist skin, removing free radical, elimination pigmentation, U.S. Hold etc..

White fungus：Alias tremella, white ear, mulberry goose, five ancient cooking vessel sesames, the white ears or side handles of a utensil.It is mild-natured, it is sweet, light, it is nontoxic.Return lung, stomach, kidney Through.The foster lung yin of energy, Ji kidney are dry, QI invigorating of refreshing oneself.Promoted the production of body fluid with nourishing, strong smart kidney tonifying, replenishing the vital essence and removing heat moistening lung, nourishing the stomach moisturizing dryheat by clearing the bowels, Tonifying Qi and blood, cardiac stimulant strengthen body, brain refreshing, facial beautification and skin rejuvenation function and other effects.White fungus, which also has, to be alleviated muscular fatigue, prevents radioactivity from damaging The effects such as wound, increase immunity of organisms.There is the tremella polysaccharides and tremella polysaccharide spore contained in white fungus antiulcer, anti-inflammatory to make With.

The present invention provides a kind of with clearing heat and detoxicating, antiphlogistic antibacterial additive-free mung bean anti-acne maintenance face paper, this production Product using mung bean, pearl, pollen pini, lily, honeysuckle, rose, lemon tablet, dried orange peel, white fungus as raw material, do not add any medicine, Additive, i.e., all added meticulously using techniques such as activation, high pressure disintegration, supercritical extracts by food-grade or dietotherapeutic raw material Work forms；Product is without essence, pigment, preservative.Product is adapted to each stratum, each age group needs facial care cosmetic to need Will, and acne（Whelk）Treatment or alleviation skin patient.Process of producing product is pollution-free, no waste residue, waste vapour and has Evil material produces, and realizes green production；The salubrious delicate fragrance of product special flavour, safe and non-toxic, external application surface application, it is a kind of food of new type of safe Grade facial mask.Production process of the present invention does not use any chemical reagents, does not add any medicine, does not add any hormone, has It is the advantages that nontoxic, pollution-free, easy to operate, long-term use of without any side effects.

Embodiment

Embodiment 1

It is to be obtained by the raw material and step of following parts by weight：

25 parts of mung bean, 3 parts of pearl, 2 parts of pollen pini, honeysuckle are dry 1 part, 2 parts of dried rose flower, 1 part of dried lily bulb, lemon tablet 1 Part, dried orange peel are dry 1 part, 0.1 part of white fungus；

（One）Mung bean continuously activation and crushing

Take and remove impurity when producing the screening of ripe mung bean seed per year, 8 DEG C of cold water spray washings are clean, be sent into vortex scalding groove in Scalding 5s in 80 DEG C of water, first time activation is carried out, then pull aerobic reciprocating vibration immersion 9h in 29 DEG C of water of input out rapidly, carry out Second of activation process, frequency of oscillation 30r/min, it is 1L/h that air capacity is passed through into water, then circulating water cleaning showers, drip Dry surface moisture, third time activation process is carried out in 40 DEG C, 5min microwave oscillations, is then freeze-dried to water content 18%, crushes Extremely can be all standby by the active mung bean flour of 60 mesh aperture sieves, aseptic storage；

（Two）Mung bean, pollen pini, pearl powder joint high pressure disintegration

Crushing pearl is standby to the pearl powder of 80 mesh, then by pearl powder and step（One）The active mung bean flour of acquisition and pine Pollen is well mixed, adjustment water content mass percent is 24%, using screw extruder in pressure 18MPa, 102 DEG C of temperature Under the conditions of rotary extrusion, the macromolecular substances in raw material and hard plant material composition is disintegrated at high temperature under high pressure, have Beneficial to the dissolution of active ingredient, extrudate low temperature drying to moisture 6%, it is 80 mesh powders that crushing, which obtains granularity, sterile storage Deposit, it is standby；

（Three）White fungus, it is each spend dry, lemon tablet and working of dried orange peel and crush

White fungus, dried lily bulb are handled respectively at 8 DEG C of cold water soak 10h rehydrations, are washed out totally, dripping net surface moisture, in 40 DEG C, 8min microwave oscillations progress activation process, are then freeze-dried to water content 6%, lily is crushed to can be all by 60 mesh The powder of aperture sieve, aseptic storage are standby；White fungus is crushed to can be all standby by the powder of 240 mesh aperture sieves, aseptic storage With；

Dried rose flower, honeysuckle are dry, the dry cleaning removal of impurities of lemon tablet, dried orange peel, and being crushed to can be all by 40 mesh aperture sieve Powder, adds pure water adjustment water content 30%, carries out activation process in 40 DEG C, 8min microwave oscillations, is then freeze-dried to containing Water 6%, being crushed to can be all standby by the powder of 60 mesh aperture sieves, aseptic storage；

（Four）Supercritical extract

The material powder prepared by above-mentioned steps is taken, is well mixed, active ingredient extraction is added and guides and supports agent, adjust compound Water content is 28%, and it is pure water 96%, 3 ° of light-coloured vinegars 2% of food-grade, the edible alcohol 2% of concentration 30% to guide and support agent composition, is then stirred Uniformly, in 45 DEG C, 25MPa, time 120min, CO₂Flow 19L/h carries out CO₂Supercritical fluid extraction, extract aseptic storage, It is standby；

（Five）Alternating temperature extracts

By step（Four）Extract remainder taken out from extraction kettle, add the deionized water of 5 times of its quality, stir, in 3d is impregnated under the conditions of 15 DEG C, is then separated, be filtrated to get can be all standby by the extract solution of 5 μm of bore filter films, aseptic storage With；Dregs after separation are pressed to the deionized water of 4 times of its mass ratio addition, stirs, 60min is extracted under the conditions of 40 DEG C, Extract 40min under the conditions of 60 DEG C, the leaching liquor of 5 μm of bore filter films, aseptic storage is standby；

（Six）Allotment, sterilization, dipping

By step（Four）The supercritical extract and step of acquisition（Five）It is well mixed under the leaching liquor cleaning condition of acquisition, White fungus powder is added, continues to stir, then in 130 DEG C, 9s ultra high temperature short time sterilizations, is cooled to 22 DEG C, obtains skin of face Natural mung bean curing fluid is deposited in aseptic tank, and the natural silk face paper through aseptic process is put into above-mentioned mung bean curing fluid In, 6h is impregnated under 25 DEG C, aseptic condition, taking-up, smooth, aseptic packaging are in waterproof, air-locked airtight package bag, i.e., Facial mask paper product is conserved for mung bean anti-acne.

Embodiment 2

It is to be obtained by the raw material and step of following parts by weight：

35 parts of mung bean, 5 parts of pearl, 3 parts of pollen pini, honeysuckle are dry 3 parts, 3 parts of dried rose flower, 2 parts of dried lily bulb, lemon tablet 2 Part, dried orange peel are dry 2 parts, 0.5 part of white fungus；

（One）Mung bean continuously activation and crushing

Take when producing ripe mung bean seed screening removal impurity per year, 15 DEG C of cold water spray washings are clean, are sent into vortex scalding groove The scalding 3s in 90 DEG C of water, first time activation is carried out, then pull aerobic reciprocating vibration immersion 5h in 35 DEG C of water of input out rapidly, enter Second of activation process of row, frequency of oscillation 80r/min, it is 3L/h that air capacity is passed through into water, then circulating water cleaning showers, Surface moisture is drained, third time activation process is carried out in 45 DEG C, 3min microwave oscillations, is then freeze-dried to water content 25%, powder Being broken to can be all standby by the active mung bean flour of 100 mesh aperture sieves, aseptic storage；

（Two）Mung bean, pollen pini, pearl powder joint high pressure disintegration

Crushing pearl is standby to the pearl powder of 100 mesh, then by pearl powder and step（One）The active mung bean flour of acquisition and Pollen pini is well mixed, and adjustment water content mass percent is 30%, using screw extruder in 120 DEG C of pressure 20MPa, temperature Under conditions of rotary extrusion, the macromolecular substances in raw material and hard plant material composition is disintegrated at high temperature under high pressure, Be advantageous to the dissolution of active ingredient, extrudate low temperature drying to moisture 8%, it is 100 mesh powders that crushing, which obtains granularity, nothing Bacterium stores, standby；

（Three）White fungus, it is each spend dry, lemon tablet and working of dried orange peel and crush

White fungus, dried lily bulb are handled respectively at 15 DEG C of cold water soak 5h rehydrations, are washed out totally, dripping net surface moisture, in 45 DEG C, 5min microwave oscillations progress activation process, are then freeze-dried to water content 8%, lily is crushed to can be all by 100 The powder of mesh aperture sieve, aseptic storage are standby；White fungus is crushed to can be all by the powder of 500 mesh aperture sieves, aseptic storage, It is standby；

Dried rose flower, honeysuckle are dry, the dry cleaning removal of impurities of lemon tablet, dried orange peel, and being crushed to can be all by 100 mesh aperture sieve Powder, adds pure water adjustment water content 35%, carries out activation process in 45 DEG C, 5min microwave oscillations, is then freeze-dried to containing Water 8%, being crushed to can be all standby by the powder of 100 mesh aperture sieves, aseptic storage；

（Four）Supercritical extract

The material powder prepared by above-mentioned steps is taken, is well mixed, active ingredient extraction is added and guides and supports agent, adjust compound Water content is 40%, and it is pure water 96%, 3 ° of light-coloured vinegars 2% of food-grade, the edible alcohol 2% of concentration 30% to guide and support agent composition, is then stirred Uniformly, in 60 DEG C, 45MPa, time 60min, CO₂Flow 26L/h carries out CO₂Supercritical fluid extraction, extract aseptic storage, It is standby；

（Five）Alternating temperature extracts

By step（Four）Extract remainder taken out from extraction kettle, add the deionized water of 15 times of its quality, stir, in 1d is impregnated under the conditions of 30 DEG C, is then separated, be filtrated to get can be all by the extract solution of 10 μm of bore filter films, aseptic storage, It is standby；Dregs after separation are pressed to the deionized water of 6 times of its mass ratio addition, stirs, is extracted under the conditions of 60 DEG C 30min, extract 20min under the conditions of 90 DEG C, then separate, be filtrated to get can all by the leaching liquor of 10 μm of bore filter films, Aseptic storage, it is standby；

（Six）Allotment, sterilization, dipping

By step（Four）The supercritical extract and step of acquisition（Five）It is well mixed under the leaching liquor cleaning condition of acquisition, White fungus powder is added, continues to stir, then in 135 DEG C, 4s ultra high temperature short time sterilizations, is cooled to 30 DEG C, obtains skin of face Natural mung bean curing fluid is deposited in aseptic tank, and the natural silk face paper through aseptic process is put into above-mentioned mung bean curing fluid In, 2h is impregnated under 30 DEG C, aseptic condition, taking-up, smooth, aseptic packaging are in waterproof, air-locked airtight package bag, i.e., Facial mask paper product is conserved for mung bean anti-acne.

Embodiment 3

It is to be obtained by the raw material and step of following parts by weight：

30 parts of mung bean, 4 parts of pearl, 2.5 parts of pollen pini, honeysuckle are dry 2 parts, 2.5 parts of dried rose flower, 1.5 parts of dried lily bulb, lemon 1.5 parts of lemon piece, dried orange peel are dry 1.5 parts, 0.3 part of white fungus；

（One）Mung bean continuously activation and crushing

Take when producing ripe mung bean seed screening removal impurity per year, 11 DEG C of cold water spray washings are clean, are sent into vortex scalding groove The scalding 4s in 85 DEG C of water, first time activation is carried out, then pull aerobic reciprocating vibration immersion 7h in 32 DEG C of water of input out rapidly, enter Second of activation process of row, frequency of oscillation 55r/min, it is 2L/h that air capacity is passed through into water, then circulating water cleaning showers, Surface moisture is drained, third time activation process is carried out in 42.5 DEG C, 4min microwave oscillations, is then freeze-dried to water content 22%, Being crushed to can be all standby by the active mung bean flour of 80 mesh aperture sieves, aseptic storage；

（Two）Mung bean, pollen pini, pearl powder joint high pressure disintegration

Crushing pearl is standby to the pearl powder of 90 mesh, then by pearl powder and step（One）The active mung bean flour of acquisition and pine Pollen is well mixed, adjustment water content mass percent is 27%, using screw extruder in pressure 19MPa, 111 DEG C of temperature Under the conditions of rotary extrusion, the macromolecular substances in raw material and hard plant material composition is disintegrated at high temperature under high pressure, have Beneficial to the dissolution of active ingredient, extrudate low temperature drying to moisture 7%, it is 90 mesh powders that crushing, which obtains granularity, sterile storage Deposit, it is standby；

（Three）White fungus, it is each spend dry, lemon tablet and working of dried orange peel and crush

White fungus, dried lily bulb are handled respectively at 11 DEG C of cold water soak 8h rehydrations, are washed out totally, dripping net surface moisture, in 42.5 DEG C, 7min microwave oscillations progress activation process, are then freeze-dried to water content 7%, lily is crushed to can be all by 80 The powder of mesh aperture sieve, aseptic storage are standby；White fungus is crushed to can be all by the powder of 380 mesh aperture sieves, aseptic storage, It is standby；

Dried rose flower, honeysuckle are dry, the dry cleaning removal of impurities of lemon tablet, dried orange peel, and being crushed to can be all by 60 mesh aperture sieve Powder, add pure water adjustment water content 33%, in 42.5 DEG C, 7min microwave oscillations carry out activation process, be then freeze-dried to Water content 7%, being crushed to can be all standby by the powder of 80 mesh aperture sieves, aseptic storage；

（Four）Supercritical extract

The material powder prepared by above-mentioned steps is taken, is well mixed, active ingredient extraction is added and guides and supports agent, adjust compound Water content is 34%, and it is pure water 96%, 3 ° of light-coloured vinegars 2% of food-grade, the edible alcohol 2% of concentration 30% to guide and support agent composition, is then stirred Uniformly, in 52 DEG C, 35MPa, time 90min, CO₂Flow 23L/h carries out CO₂Supercritical fluid extraction, extract aseptic storage, It is standby；

（Five）Alternating temperature extracts

By step（Four）Extract remainder taken out from extraction kettle, add the deionized water of 10 times of its quality, stir, in 2d is impregnated under the conditions of 23 DEG C, is then separated, be filtrated to get can be all standby by the extract solution of 8 μm of bore filter films, aseptic storage With；Dregs after separation are pressed to the deionized water of 5 times of its mass ratio addition, stirs, 45min is extracted under the conditions of 50 DEG C, 30min is extracted under the conditions of 75 DEG C, is then separated, be filtrated to get can be all by the leaching liquor of 8 μm of bore filter films, sterile storage Deposit, it is standby；

（Six）Allotment, sterilization, dipping

By step（Four）The supercritical extract and step of acquisition（Five）It is well mixed under the leaching liquor cleaning condition of acquisition, White fungus powder is added, continues to stir, then in 133 DEG C, 6s ultra high temperature short time sterilizations, is cooled to 26 DEG C, obtains skin of face Natural mung bean curing fluid is deposited in aseptic tank, and the natural silk face paper through aseptic process is put into above-mentioned mung bean curing fluid In, 4h is impregnated under 27 DEG C, aseptic condition, taking-up, smooth, aseptic packaging are in waterproof, air-locked airtight package bag, i.e., Facial mask paper product is conserved for mung bean anti-acne.

The present invention works well through crowd's test, as a result such as following table：

The additive-free mung bean anti-acne maintenance face paper using effect test result of table 1

Claims (2)

1. a kind of additive-free mung bean anti-acne maintenance face paper, it is characterised in that obtained by the raw material and step of following parts by weight 's：

25~35 parts of mung bean, 3~5 parts of pearl, 2~3 parts of pollen pini, honeysuckle are dry 1~3 part, 2~3 parts of dried rose flower, dried lily bulb 1~2 part, 1~2 part of lemon tablet, dry 1~2 part of dried orange peel, 0.1~0.5 part of white fungus, natural silk face paper；

（One）Mung bean continuously activation and crushing

Take and remove impurity when producing the screening of ripe mung bean seed per year, 8~15 DEG C of cold water spray washings are clean, be sent into vortex scalding groove in 3~5s of scalding in 80~90 DEG C of water, first time activation is carried out, then pulls aerobic reciprocating vibration in 29~35 DEG C of water of input out rapidly 5~9h to be soaked, carries out second of activation process, frequency of oscillation is 30~80r/min, and it is 1~3L/h that air capacity is passed through into water, Then circulating water cleaning showers, surface moisture is drained, third time activation process is carried out in 40~45 DEG C, 3~5min microwave oscillations, Then it is freeze-dried to water content 18~25%, being crushed to can be sterile all by the active mung bean flour of 60~100 mesh aperture sieves Storage, it is standby；

（Two）Mung bean, pollen pini, pearl powder joint high pressure disintegration

Crushing pearl is standby to the pearl powder of 80~100 mesh, then by pearl powder and step（One）The active mung bean flour of acquisition and Pollen pini is well mixed, and adjustment water content mass percent is 24~30%, using screw extruder in 18~20MPa of pressure, temperature Rotary extrusion under conditions of 102~120 DEG C of degree, make macromolecular substances in raw material and hard plant material composition in HTHP It is lower to be disintegrated, be advantageous to the dissolution of active ingredient, extrudate low temperature drying to moisture 6~8%, crushing obtains granularity and is 80~100 mesh powders, aseptic storage are standby；

（Three）White fungus, it is each spend dry, lemon tablet and working of dried orange peel and crush

White fungus, dried lily bulb are handled respectively at 8~15 DEG C of 5~10h of cold water soak rehydrations, are washed out totally, dripping net surface moisture, Activation process is carried out in 40~45 DEG C, 5~8min microwave oscillations, is then freeze-dried to water content 6~8%, lily is crushed to can It is all standby by the powder of 60~100 mesh aperture sieves, aseptic storage；White fungus is crushed to can be all by 240~500 mesh holes The powder of footpath sieve, aseptic storage are standby；

Dried rose flower, honeysuckle are dry, the dry cleaning removal of impurities of lemon tablet, dried orange peel, and being crushed to can be all by 40~100 mesh aperture sieve Powder, adds pure water adjustment water content 30~35%, carries out activation process in 40~45 DEG C, 5~8min microwave oscillations, then To water content 6~8%, being crushed to can be all standby by the powder of 60~100 mesh aperture sieves, aseptic storage for freeze-drying；

（Four）Supercritical extract

The material powder prepared by above-mentioned steps is taken, is well mixed, active ingredient extraction is added and guides and supports agent, adjustment compound is aqueous Measure as 28~40%, guide and support agent composition be pure water 96%, 3 ° of light-coloured vinegars 2% of food-grade, the edible alcohol 2% of concentration 30%, then stir Uniformly, in 45~60 DEG C, 25~45MPa, 60~120min of time, CO₂19~26L/h of flow carries out CO₂Supercritical fluid extracts Take, extract aseptic storage is standby；

（Five）Alternating temperature extracts

By step（Four）Extract remainder taken out from extraction kettle, add the deionized water of 5~15 times of its quality, stir, in 1~3d is impregnated under the conditions of 15~30 DEG C, then separate, be filtrated to get can all by the extract solution of 5~10 μm of bore filter films, Aseptic storage, it is standby；Dregs after separation are pressed to the deionized water of 4~6 times of its mass ratio addition, stirred, in 40~60 30~60min is extracted under the conditions of DEG C, 20~40min is extracted under the conditions of 60~90 DEG C, then separates, is filtrated to get and can all pass through The leaching liquor of 5~10 μm of bore filter films, aseptic storage are standby；

（Six）Allotment, sterilization, dipping

By step（Four）The supercritical extract and step of acquisition（Five）It is well mixed, adds under the leaching liquor cleaning condition of acquisition White fungus powder, continue to stir, then in 130~135 DEG C, 4~9s ultra high temperature short time sterilizations, be cooled to 22~30 DEG C, obtain The natural mung bean curing fluid of skin of face is deposited in aseptic tank, and the natural silk face paper through aseptic process is put into above-mentioned mung bean In curing fluid, 2~6h is impregnated under 25~30 DEG C, aseptic condition, taking-up, smooth, aseptic packaging are in waterproof, air-locked close In closure pack, as mung bean anti-acne conserves facial mask paper product.

2. a kind of Green production method of additive-free mung bean anti-acne maintenance face paper as claimed in claim 1, its feature exist Then obtained by the raw material and step of following parts by weight：

25~35 parts of mung bean, 3~5 parts of pearl, 2~3 parts of pollen pini, honeysuckle are dry 1~3 part, 2~3 parts of dried rose flower, dried lily bulb 1~2 part, 1~2 part of lemon tablet, dry 1~2 part of dried orange peel, 0.1~0.5 part of white fungus, natural silk face paper；

（One）Mung bean continuously activation and crushing

Take and remove impurity when producing the screening of ripe mung bean seed per year, 8~15 DEG C of cold water spray washings are clean, be sent into vortex scalding groove in 3~5s of scalding in 80~90 DEG C of water, first time activation is carried out, then pulls aerobic reciprocating vibration in 29~35 DEG C of water of input out rapidly 5~9h to be soaked, carries out second of activation process, frequency of oscillation is 30~80r/min, and it is 1~3L/h that air capacity is passed through into water, Then circulating water cleaning showers, surface moisture is drained, third time activation process is carried out in 40~45 DEG C, 3~5min microwave oscillations, Then it is freeze-dried to water content 18~25%, being crushed to can be sterile all by the active mung bean flour of 60~100 mesh aperture sieves Storage, it is standby；

（Two）Mung bean, pollen pini, pearl powder joint high pressure disintegration

Crushing pearl is standby to the pearl powder of 80~100 mesh, then by pearl powder and step（One）The active mung bean flour of acquisition and Pollen pini is well mixed, and adjustment water content mass percent is 24~30%, using screw extruder in 18~20MPa of pressure, temperature Rotary extrusion under conditions of 102~120 DEG C of degree, make macromolecular substances in raw material and hard plant material composition in HTHP It is lower to be disintegrated, be advantageous to the dissolution of active ingredient, extrudate low temperature drying to moisture 6~8%, crushing obtains granularity and is 80~100 mesh powders, aseptic storage are standby；

（Three）White fungus, it is each spend dry, lemon tablet and working of dried orange peel and crush

White fungus, dried lily bulb are handled respectively at 8~15 DEG C of 5~10h of cold water soak rehydrations, are washed out totally, dripping net surface moisture, Activation process is carried out in 40~45 DEG C, 5~8min microwave oscillations, is then freeze-dried to water content 6~8%, lily is crushed to can It is all standby by the powder of 60~100 mesh aperture sieves, aseptic storage；White fungus is crushed to can be all by 240~500 mesh holes The powder of footpath sieve, aseptic storage are standby；

Dried rose flower, honeysuckle are dry, the dry cleaning removal of impurities of lemon tablet, dried orange peel, and being crushed to can be all by 40~100 mesh aperture sieve Powder, adds pure water adjustment water content 30~35%, carries out activation process in 40~45 DEG C, 5~8min microwave oscillations, then To water content 6~8%, being crushed to can be all standby by the powder of 60~100 mesh aperture sieves, aseptic storage for freeze-drying；

（Four）Supercritical extract

The material powder prepared by above-mentioned steps is taken, is well mixed, active ingredient extraction is added and guides and supports agent, adjustment compound is aqueous Measure as 28~40%, guide and support agent composition be pure water 96%, 3 ° of light-coloured vinegars 2% of food-grade, the edible alcohol 2% of concentration 30%, then stir Uniformly, in 45~60 DEG C, 25~45MPa, 60~120min of time, CO₂19~26L/h of flow carries out CO₂Supercritical fluid extracts Take, extract aseptic storage is standby；

（Five）Alternating temperature extracts

By step（Four）Extract remainder taken out from extraction kettle, add the deionized water of 5~15 times of its quality, stir, in 1~3d is impregnated under the conditions of 15~30 DEG C, then separate, be filtrated to get can all by the extract solution of 5~10 μm of bore filter films, Aseptic storage, it is standby；Dregs after separation are pressed to the deionized water of 4~6 times of its mass ratio addition, stirred, in 40~60 30~60min is extracted under the conditions of DEG C, 20~40min is extracted under the conditions of 60~90 DEG C, then separates, is filtrated to get and can all pass through The leaching liquor of 5~10 μm of bore filter films, aseptic storage are standby；

（Six）Allotment, sterilization, dipping

By step（Four）The supercritical extract and step of acquisition（Five）It is well mixed, adds under the leaching liquor cleaning condition of acquisition White fungus powder, continue to stir, then in 130~135 DEG C, 4~9s ultra high temperature short time sterilizations, be cooled to 22~30 DEG C, obtain The natural mung bean curing fluid of skin of face is deposited in aseptic tank, and the natural silk face paper through aseptic process is put into above-mentioned mung bean In curing fluid, 2~6h is impregnated under 25~30 DEG C, aseptic condition, taking-up, smooth, aseptic packaging are in waterproof, air-locked close In closure pack, as mung bean anti-acne conserves facial mask paper product.