CN105326721B - A kind of sheet microcapsules containing pot marigold extract - Google Patents
A kind of sheet microcapsules containing pot marigold extract Download PDFInfo
- Publication number
- CN105326721B CN105326721B CN201510892164.4A CN201510892164A CN105326721B CN 105326721 B CN105326721 B CN 105326721B CN 201510892164 A CN201510892164 A CN 201510892164A CN 105326721 B CN105326721 B CN 105326721B
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- parts
- solution
- mixed
- pot marigold
- marigold extract
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
Abstract
The present invention discloses a kind of sheet microcapsules containing pot marigold extract, belongs to microcapsules technology field；The sheet microcapsules containing pot marigold extract, in parts by weight, including following ingredient：50 ~ 55 parts of sodium alginates, 20 ~ 30 parts of carragheens, 10 ~ 15 parts of hydroxyethyl celluloses, 5 ~ 8 parts of Sodium Hyaluronates, 10 ~ 15 parts of glycerine, 0.1 ~ 0.5 part of pot marigold extract, 0.1 ~ 0.3 part of D＆C Huang 1,0.1 ~ 0.3 part of titanium dioxide, 0.5 ~ 1 part of Phenoxyethanol, 0.1 ~ 0.5 part of Sensiva SC50 and 0.3 ~ 0.5 part of 1,2 ethohexadiol.The present invention has effects that moisturizing oil-control, and while in order to ensure the effect, product stability obtained can also be made good, the present invention is had found only by creative research when selecting raw material of the present invention and formula, the two requirements could be taken into account simultaneously, stablize product property obtained, it is best in quality.
Description
Technical field
The invention belongs to microcapsules technology fields, and in particular to a kind of sheet microcapsules containing pot marigold extract.
Background technology
Consumer increasingly pursues natural and effect of cosmetic personal care's product, and as a daily necessities, not only appearance will
Grace is imbued with attraction and natural imagination, and to stablize with it is powerful.The addition product of plant are added currently on the market, such as
Petal water, petal mile, perfume etc., but genuine plant either produces and preserve many stability in cosmetics
Problem：Such as the cleaning of the plant material in production process, some plants keep insect, worm's ovum etc., are a very big pollutions
The problems such as source, the ingredient during preservation in plant soak out to cause product unstable, and color, which is moved back, to be lost, pollen easy sensitization；
The active ingredient that many plants propose uses also has various stability in cosmetics.
Present microcapsule product is mostly spherical shape, and shape is relatively simple, does not have sheet microcapsules, and sheet is compared to ball
The microcapsules of shape more save space, can make cosmetic base while sheet microcapsules are added to, moreover it is possible to ensure matrix
Additive amount can not be limited.There is no the correlative studys for preparing sheet microcapsules for the prior art, and it is because usually to trace it to its cause
Gel solution can shrink balling-up or irregular gel piece due to surface tension, and microcapsules raw material cannot be made to extend around
Open, and then the microcapsules of slabbing or strip cannot be done, thus there is it is certain the defects of.
Invention content
For deficiencies of the prior art, the technical problems to be solved by the invention are：One kind how is provided to contain
There are the sheet microcapsules of pot marigold extract, break microcapsule product in the prior art and be the conventional understanding of spherical shape, and have
There is the characteristics of stability is good, best in quality, and there is moisturizing oil-control, soothe the skin.
In order to solve the above-mentioned technical problem, the present invention adopts the following technical scheme that：A kind of piece containing pot marigold extract
Shape microcapsules, in parts by weight, including following ingredient：50 ~ 55 parts of sodium alginates, 20 ~ 30 parts of carragheens, 10 ~ 15 parts of ethoxys
Cellulose, 5 ~ 8 parts of Sodium Hyaluronates, 10 ~ 15 parts of glycerine, 0.1 ~ 0.5 part of pot marigold extract, 0.1 ~ 0.3 part of D＆C be No. 1 yellow,
0.1 ~ 0.3 part of titanium dioxide, 0.5 ~ 1 part of Phenoxyethanol, 0.1 ~ 0.5 part of Sensiva SC50 and 0.3 ~ 0.5 part of 1,2 ethohexadiol.
Compared with prior art, the present invention has the advantages that：
1st, the present invention, which using alginate encounters divalent metal salting liquid and can generate the principle of gel, prepares slice-shaped
Capsule, but seaweed acid solution encounters divalent metal salting liquid in the prior art when can balling-up be shunk due to surface tension
Or irregular gel piece, therefore slabbing microcapsules cannot be prepared；For these reasons, the present invention is had found by studying in sea
The preservative or surfactant that the present invention selects are added in Alginic acid solution, the surface tension of colloid can be made reduce, make compounding
Raw material surface tension afterwards be less than salting liquid, these reduce surface tension substance by seaweed acid solution in divalent metal salting liquid
Surface spreading open, while with salting liquid reaction into class disk gel film, these gel film shapes are allowed by the flowing of brine
Shape is made a variation and arrives sheet microcapsules.
2nd, since single alginate is unstable to many substances, easily by alkali, chelating agent, surfactant etc.
Swelling and dissolving, so also having compounded other colloids or high molecular material in raw material of the present invention, pass through the collaboration compatibility of each raw material
Effect, make sheet microcapsules of the present invention base-material for example mile, frost breast, shower cream, in shampoo more stablize, it is well-behaved.
3rd, the collaboration compatibility effect in the present invention between each raw material makes sheet microcapsules of the present invention easy in containing base-material
Soften and become easily to smear, skin sense is more preferable.
4th, the present invention has microcapsules obtained by pot marigold extract and the collaboration compatibility effect of Sodium Hyaluronate
Moisturizing oil-control, the effect of soothing the skin.
5th, while the present invention is in order to ensure the effect, moreover it is possible to make product stability obtained good, it is of the invention logical
Creative research is crossed, finally found that could take into account the two simultaneously will only when selecting raw material of the present invention and formula
It asks, stablizes product property obtained, it is best in quality.
6th, the method for the present invention can realize a large amount of industrial productions of full automation, and without human intervention, flow pollution is few,
Product quality is high, controllability and favorable reproducibility.
Specific embodiment
The present invention is described in further detail with reference to embodiment, in the present embodiment unless otherwise instructed, original used
Material is commercially available.
Sheet microcapsules of the present invention containing pot marigold extract are prepared with the following method：
1）Sodium alginate is configured to the solution that mass concentration is 2% with pure water, carragheen is configured to matter with pure water
A concentration of 1% solution is measured, hydroxyethyl cellulose is configured to the solution that mass concentration is 1% with pure water, by Sodium Hyaluronate
The solution that mass concentration is 1% is configured to pure water；
2）By step 1）After the solution of preparation is heated to 60 DEG C, mixed solution is simultaneously kept the temperature, spare；
3）Glycerine and pot marigold extract are uniformly mixed；
4）D＆C yellow No. 1 and titanium dioxide are milled mixing, and are mixed into step 3）In mixed raw material, stir evenly；
5）Phenoxyethanol, Sensiva SC50 and 1,2 ethohexadiols are mixed to join step 4）In mixed material, obtain
Mixed raw material；
6）By step 5）Mixed raw material adds in step 2）In mixed solution, homogeneous is carried out, and keep the temperature of mixture
It is 60 ~ 70 DEG C to spend, and it is spare to obtain homogeneous object；
7）By step 6）Homogeneous object pump after equal vacuum is exported and is added drop-wise on inclined-plane, and trickling on the inclined-plane has
Mass concentration is 2% calcium chloride solution, obtains the sheet microcapsules containing pot marigold extract.
Embodiment 1：
A kind of sheet microcapsules containing pot marigold extract, component prescription are as shown in table 1 below：
1 component prescription of table
Embodiment 2
A kind of sheet microcapsules containing pot marigold extract, component prescription are as shown in table 2 below：
Sheet microcapsule components formula of the table 2 containing pot marigold extract
The present invention can also allow calcium chloride brine to generate flowing, and colloidal solution dropping point or streamline is avoided to be overlapped, to prepare this
Invention sheet microcapsules.
Finally illustrate, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although applicant
The present invention is described in detail with reference to preferred embodiment, it will be understood by those of ordinary skill in the art that, to the present invention's
Technical solution is modified or replaced equivalently, and without departing from the objective and range of technical solution of the present invention, should all be covered
In scope of the presently claimed invention.
Claims (1)
1. a kind of sheet microcapsules containing pot marigold extract, which is characterized in that in parts by weight, including following ingredient：
50 ~ 55 parts of sodium alginates, 20 ~ 30 parts of carragheens, 10 ~ 15 parts of hydroxyethyl celluloses, 5 ~ 8 parts of Sodium Hyaluronates, 10 ~ 15 parts
Glycerine, 0.1 ~ 0.5 part of pot marigold extract, 0.1 ~ 0.3 part of D＆C are No. 1 yellow, 0.1 ~ 0.3 part of titanium dioxide, 0.5 ~ 1 part of Phenoxyethanol,
0.1 ~ 0.5 part of Sensiva SC50 and 0.3 ~ 0.5 part of 1,2 ethohexadiol；It is prepared with the following method：
1）Sodium alginate is configured to the solution that mass concentration is 2% with pure water, it is dense that carragheen with pure water is configured to quality
The solution for 1% is spent, hydroxyethyl cellulose is configured to the solution that mass concentration is 1% with pure water, by Sodium Hyaluronate with pure
Water purification is configured to the solution that mass concentration is 1%；
2）By step 1）After the solution of preparation is heated to 60 DEG C, mixed solution is simultaneously kept the temperature, spare；
3）Glycerine and pot marigold extract are uniformly mixed；
4）D＆C yellow No. 1 and titanium dioxide are milled mixing, and are mixed into step 3）In mixed raw material, stir evenly；
5）Phenoxyethanol, Sensiva SC50 and 1,2 ethohexadiols are mixed to join step 4）In mixed material, mixed
Raw material；
6）By step 5）Mixed raw material adds in step 2）In mixed solution, homogeneous is carried out, and keeps the temperature of mixture to be
60 ~ 70 DEG C, it is spare to obtain homogeneous object；
7）By step 6）Homogeneous object pump after equal vacuum is exported and is added drop-wise on inclined-plane, and trickling on the inclined-plane has quality
A concentration of 2% calcium chloride solution obtains the sheet microcapsules containing pot marigold extract.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510892164.4A CN105326721B (en) | 2015-11-27 | 2015-11-27 | A kind of sheet microcapsules containing pot marigold extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510892164.4A CN105326721B (en) | 2015-11-27 | 2015-11-27 | A kind of sheet microcapsules containing pot marigold extract |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105326721A CN105326721A (en) | 2016-02-17 |
| CN105326721B true CN105326721B (en) | 2018-07-10 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510892164.4A Active CN105326721B (en) | 2015-11-27 | 2015-11-27 | A kind of sheet microcapsules containing pot marigold extract |
Country Status (1)
| Country | Link |
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| CN (1) | CN105326721B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6391288B1 (en) * | 1999-07-27 | 2002-05-21 | Shiseido Co., Ltd. | Microcapsule and method of making the same |
| CN102100713A (en) * | 2009-12-18 | 2011-06-22 | 中国科学院兰州化学物理研究所 | Method for preparing water-soluble marigold yellow pigment microcapsules |
| CN104490615A (en) * | 2014-12-16 | 2015-04-08 | 重庆小丸科贸有限公司 | Hydrogel microcapsule with pore minimizing efficacy |
-
2015
- 2015-11-27 CN CN201510892164.4A patent/CN105326721B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6391288B1 (en) * | 1999-07-27 | 2002-05-21 | Shiseido Co., Ltd. | Microcapsule and method of making the same |
| CN102100713A (en) * | 2009-12-18 | 2011-06-22 | 中国科学院兰州化学物理研究所 | Method for preparing water-soluble marigold yellow pigment microcapsules |
| CN104490615A (en) * | 2014-12-16 | 2015-04-08 | 重庆小丸科贸有限公司 | Hydrogel microcapsule with pore minimizing efficacy |
Non-Patent Citations (1)
| Title |
|---|
| 锐孔法制备微胶囊技米研究;王显伦;《郑州粮食学院学报》;19951231;第16卷(第4期);第21-26页 * |
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| CN105326721A (en) | 2016-02-17 |
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Address after: 401519 Chongqing Hechuan Industrial Park weir village two Patentee after: Chongqing Xiaowan Biotechnology Co., Ltd. Address before: 401519 Chongqing Hechuan Industrial Park weir village two Patentee before: CHONGQING XIAOWAN TRADE CO., LTD. |