CN105293493A - Sulfur catcher used in carbon disulfide production - Google Patents
Sulfur catcher used in carbon disulfide production Download PDFInfo
- Publication number
- CN105293493A CN105293493A CN201510813196.0A CN201510813196A CN105293493A CN 105293493 A CN105293493 A CN 105293493A CN 201510813196 A CN201510813196 A CN 201510813196A CN 105293493 A CN105293493 A CN 105293493A
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- Prior art keywords
- plate
- broken gas
- gas plate
- chamber
- usedly
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- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 title claims abstract description 52
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title claims abstract description 19
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 19
- 229910052717 sulfur Inorganic materials 0.000 title abstract 4
- 239000011593 sulfur Substances 0.000 title abstract 4
- 238000009833 condensation Methods 0.000 claims abstract description 31
- 230000005494 condensation Effects 0.000 claims abstract description 31
- 239000002893 slag Substances 0.000 claims abstract description 5
- 239000005864 Sulphur Substances 0.000 claims description 15
- 230000008676 import Effects 0.000 claims description 5
- 238000007373 indentation Methods 0.000 claims description 3
- 239000011229 interlayer Substances 0.000 claims description 3
- 239000012535 impurity Substances 0.000 abstract description 7
- 238000006477 desulfuration reaction Methods 0.000 abstract description 5
- 230000023556 desulfurization Effects 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 3
- 239000003795 chemical substances by application Substances 0.000 abstract description 2
- 238000005192 partition Methods 0.000 abstract 3
- 230000003009 desulfurizing effect Effects 0.000 abstract 1
- 230000001404 mediated effect Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
Landscapes
- Carbon And Carbon Compounds (AREA)
- Refinement Of Pig-Iron, Manufacture Of Cast Iron, And Steel Manufacture Other Than In Revolving Furnaces (AREA)
Abstract
The invention discloses a sulfur catcher used in carbon disulfide production. The sulfur catcher includes a container shaped condensation cavity (20) composed of a trough shell (26), the condensation cavity (20) is provided with an air inlet (21), an air outlet (25) and a slag outlet (22), the condensation cavity (20) is internally provided with at least one partition plate (31) that separates the condensation cavity (20) into more than two condensation chambers, the height of the partition plate (31) upper edge is lower than the inner cavity height of the condensation cavity (20), each condensation chamber is internally provided with at least one gas breaking plate (32) disposed at the upper part of the condensation cavity (20), the height of the gas breaking plate (32) lower edge is lower than the upper edge of the partition plate (31), and the gas breaking plate (32) lower edge is jagged. Compared with the prior art, the sulfur catcher provided by the invention segments the carbon disulfide gas injected into the condensation cavity into fine bubbles through the jagged lower edge of the gas breaking plate (32), so that carbon disulfide gas can better contact a desulfurizing agent, and the desulfurization and impurity removal effects are greatly improved.
Description
Technical field
The present invention relates to a kind of molten sulphur device, usedly in a kind of carbon disulphide production specifically catch sulphur device.
Background technology
In carbon disulphide production, particularly in semicoke formula carbon disulphide production, dithiocarbonic anhydride is vaporized state after generating, and is wherein mingled with more impurity, mainly excessive sulphur, needs to be removed by these impurity be mingled with wherein further, just can become finished product.
Mainly remove impurity by condensing mode at present.The import of carbon disulfide gas from condenser inputs by the condenser used at present, and the other end is sent.Due to the reasons in structure of condenser, impurity desulfurization ability is weak, and effect is bad.The usual employing operational version that is together in series by multiple condenser solves, and causes the increase of the too fat to move of production unit and production cost.
Summary of the invention
The object of this invention is to provide and usedly in the effective carbon disulphide production of a kind of impurity desulfurization catch sulphur device.
The object of the invention is to be realized by following structure: comprise a container-like condensation chamber (20) be made up of channel-shaped housing (26), this condensation chamber (20) is provided with inlet mouth (21), air outlet (25) and slag notch (22), it is characterized in that being provided with at least one piece of dividing plate (31) in condensation chamber (20) is separated into plural condensing chamber by condensation chamber (20), the height of dividing plate (31) top is lower than condensation chamber (20) cavity heights, at least one piece of broken gas plate (32) is provided with in each condensing chamber, this broken gas plate (32) is arranged at condensation chamber (20) top, the following height of broken gas plate (32) is lower than the top of dividing plate (31), and broken gas plate (32) goes up indentation below.
As improvement, overflow port (23) is preferably provided with in the condensing chamber that above-mentioned dividing plate (31) is divided into, this overflow port (23) is preferably provided with adjustable plate (24), to adjust, the height of overflow port (23) position.
Further again, above-mentioned housing (26) is preferably the interlayer being provided with thermal medium chamber (12), this thermal medium chamber (12) is provided with heat transferring medium import (11) and heat transferring medium outlet (13), can make to keep relative temperature constant state in condensation chamber (20) by filling heat-conductive medium middle in this thermal medium chamber (12), as temperature is too high, lower the temperature, temperature is too low, heats.
Again further, above-mentioned broken gas plate (32) is preferably the adjustable plate shape of height, to regulate the height that broken gas plate (32) is following as required.
Again further, above-mentioned each condensing chamber preferably arranges the broken gas plate (32) of more than two pieces, and the broken gas plate (32) of more than two pieces is from front to back in following step arrangement from low to high.
Compared with prior art, the carbon disulfide gas injecting condensation chamber is divided into tiny bubble by the present invention goes up indentation below limit by broken gas plate, make carbon disulfide gas better with desulfurization agent, thus impurity desulfurization effect improves greatly.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the invention will be further described.
Fig. 1 is the structural representation of the embodiment of the present invention 1.
Fig. 2 is the structural representation of the broken gas plate of the embodiment of the present invention 1.
Fig. 3 is the structural representation of the broken gas plate of the embodiment of the present invention 2.
Fig. 4 is the structural representation of the embodiment of the present invention 3.
Shown in figure: 11 is heat transferring medium import, 12 is thermal medium chamber, and 13 is heat transferring medium outlet, and 20 is condensation chamber, and 21 is inlet mouth, and 22 is slag notch, and 23 is overflow port, and 24 is adjustable plate, and 25 is air outlet, and 26 is housing, and 31 is dividing plate, and 32 is broken gas plate.
Embodiment
Embodiment 1: with reference to Fig. 1, Fig. 2, for the structural representation of the embodiment of the present invention 1, the container-like condensation chamber 20 be made up of channel-shaped housing 26 by one, this condensation chamber 20 is provided with inlet mouth 21, air outlet 25 and slag notch 22, housing 26 is for being provided with the interlayer in thermal medium chamber 12, this thermal medium chamber 12 is provided with heat transferring medium import 11 and heat transferring medium outlet 13, by filling heat-conductive medium in this thermal medium chamber 12, heat-conducting medium can be thermal oil or steam, can make to keep relative temperature constant state in condensation chamber 20, as temperature is too high, lower the temperature, temperature is too low, heats, be provided with two pieces of dividing plates 31 in each condensation chamber 20 and condensation chamber 20 is separated into 3 condensing chambers, the height of dividing plate 31 top is lower than condensation chamber 20 cavity heights, one block of broken gas plate 32 is provided with in each condensing chamber, broken gas plate 32 is the adjustable plate shape of height, be arranged at condensation chamber 20 top, the following height of broken gas plate 32 is lower than the top of dividing plate 31, and broken gas plate 32 is upper in sharp spination below, overflow port 23 is provided with in the condensing chamber be divided into by dividing plate 31, overflow port 23 is provided with adjustable plate 24, with adjustment, the height of overflow port 23 position.
Embodiment 2: with reference to Fig. 3, be the structural representation of the embodiment of the present invention 2, compared with embodiment 1, the difference of the present embodiment is: described broken gas plate 32 is upper in square spination below.
Embodiment 3: with reference to Fig. 4, for the structural representation of the embodiment of the present invention 2, compared with embodiment 1 or 2, the difference of the present embodiment is: each condensing chamber all arranges the broken gas plate 32 of more than two pieces, wherein two condensing chambers at inlet mouth 21 and place, air outlet 25 all arrange two blocks of broken gas plates 32,3 blocks of broken gas plates 32 are set in the condensing chamber mediated, and described broken gas plate 32 is arranged in following step from low to high all from front to back in each condensing chamber.
Below be only the preferred embodiment of the present invention, it should be pointed out that above-mentioned preferred implementation should not be considered as limitation of the present invention, protection scope of the present invention should be as the criterion with claim limited range.For those skilled in the art, without departing from the spirit and scope of the present invention, some improvements and modifications can also be made and also should be considered as protection scope of the present invention.
Claims (10)
1. usedly in a carbon disulphide production catch sulphur device, comprise a container-like condensation chamber (20) be made up of channel-shaped housing (26), this condensation chamber (20) is provided with inlet mouth (21), air outlet (25) and slag notch (22), it is characterized in that: be provided with at least one piece of dividing plate (31) in condensation chamber (20) and condensation chamber (20) is separated into plural condensing chamber, the height of dividing plate (31) top is lower than condensation chamber (20) cavity heights, at least one piece of broken gas plate (32) is provided with in each condensing chamber, this broken gas plate (32) is arranged at condensation chamber (20) top, the following height of broken gas plate (32) is lower than the top of dividing plate (31), and broken gas plate (32) goes up indentation below.
2. usedly in carbon disulphide production according to claim 1 catch sulphur device, it is characterized in that: in the condensing chamber that described dividing plate (31) is divided into, be provided with overflow port (23).
3. usedly in carbon disulphide production according to claim 2 catch sulphur device, it is characterized in that: described this overflow port (23) is provided with adjustable plate (24).
4. usedly in the carbon disulphide production according to claim 1,2 or 3 catch sulphur device, it is characterized in that: described housing (26) is for being provided with the interlayer of thermal medium chamber (12), and this thermal medium chamber (12) is provided with heat transferring medium import (11) and heat transferring medium outlet (13).
5. usedly in the carbon disulphide production according to claim 1,2 or 3 catch sulphur device, it is characterized in that: described broken gas plate (32) is the adjustable plate shape of height.
6. usedly in carbon disulphide production according to claim 4 catch sulphur device, it is characterized in that: described broken gas plate (32) is the adjustable plate shape of height.
7. usedly in the carbon disulphide production according to claim 1,2 or 3 catch sulphur device, it is characterized in that: the broken gas plate (32) being provided with more than two pieces in described each condensing chamber, and the broken gas plate (32) of more than two pieces is from front to back in following step arrangement from low to high.
8. usedly in carbon disulphide production according to claim 4 catch sulphur device, it is characterized in that: the broken gas plate (32) being provided with more than two pieces in described each condensing chamber, and the broken gas plate (32) of more than two pieces is from front to back in following step arrangement from low to high.
9. usedly in carbon disulphide production according to claim 5 catch sulphur device, it is characterized in that: the broken gas plate (32) being provided with more than two pieces in described each condensing chamber, and the broken gas plate (32) of more than two pieces is from front to back in following step arrangement from low to high.
10. usedly in carbon disulphide production according to claim 6 catch sulphur device, it is characterized in that: the broken gas plate (32) being provided with more than two pieces in described each condensing chamber, and the broken gas plate (32) of more than two pieces is from front to back in following step arrangement from low to high.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510813196.0A CN105293493B (en) | 2015-11-20 | 2015-11-20 | Sulphur device is caught used in carbon disulphide production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510813196.0A CN105293493B (en) | 2015-11-20 | 2015-11-20 | Sulphur device is caught used in carbon disulphide production |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105293493A true CN105293493A (en) | 2016-02-03 |
| CN105293493B CN105293493B (en) | 2017-10-17 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510813196.0A Active CN105293493B (en) | 2015-11-20 | 2015-11-20 | Sulphur device is caught used in carbon disulphide production |
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| Country | Link |
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| CN (1) | CN105293493B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107117615A (en) * | 2016-12-06 | 2017-09-01 | 张贯彪 | The retracting device of gaseous sulfur in carbon disulphide production |
| CN107117614A (en) * | 2016-12-06 | 2017-09-01 | 张贯彪 | Anti-leak environmental protection plus sulphur device in carbon disulphide production |
| CN108939803A (en) * | 2018-08-29 | 2018-12-07 | 阳城县绿色科技研发中心 | Gaseous state carbon disulfide desulfurizer |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4406872A (en) * | 1981-05-28 | 1983-09-27 | Diamond West Energy Corporation | Desulfurization of delayed petroleum coke |
| CN2330640Y (en) * | 1997-12-27 | 1999-07-28 | 李清水 | Vapor-free desulfurizing reaction furnace for producing carbon bisulfide |
| CN201308807Y (en) * | 2008-12-01 | 2009-09-16 | 李怀毅 | Retracting device of carbon disulfide in carbon disulfide tail gas in semi-coking method production |
| CN203964550U (en) * | 2014-06-16 | 2014-11-26 | 成都丽雅纤维股份有限公司 | In carbon disulfide preparation process, from hydrogen sulfide tail gas, reclaim the device of carbon disulfide |
| CN205115058U (en) * | 2015-11-20 | 2016-03-30 | 张贯彪 | Used sulphur ware of catching in carbon disulfide production |
-
2015
- 2015-11-20 CN CN201510813196.0A patent/CN105293493B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4406872A (en) * | 1981-05-28 | 1983-09-27 | Diamond West Energy Corporation | Desulfurization of delayed petroleum coke |
| CN2330640Y (en) * | 1997-12-27 | 1999-07-28 | 李清水 | Vapor-free desulfurizing reaction furnace for producing carbon bisulfide |
| CN201308807Y (en) * | 2008-12-01 | 2009-09-16 | 李怀毅 | Retracting device of carbon disulfide in carbon disulfide tail gas in semi-coking method production |
| CN203964550U (en) * | 2014-06-16 | 2014-11-26 | 成都丽雅纤维股份有限公司 | In carbon disulfide preparation process, from hydrogen sulfide tail gas, reclaim the device of carbon disulfide |
| CN205115058U (en) * | 2015-11-20 | 2016-03-30 | 张贯彪 | Used sulphur ware of catching in carbon disulfide production |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107117615A (en) * | 2016-12-06 | 2017-09-01 | 张贯彪 | The retracting device of gaseous sulfur in carbon disulphide production |
| CN107117614A (en) * | 2016-12-06 | 2017-09-01 | 张贯彪 | Anti-leak environmental protection plus sulphur device in carbon disulphide production |
| CN107117614B (en) * | 2016-12-06 | 2023-08-04 | 濮阳天泓实业有限公司 | Leak-proof environment-friendly vulcanizing device in carbon disulfide production |
| CN108939803A (en) * | 2018-08-29 | 2018-12-07 | 阳城县绿色科技研发中心 | Gaseous state carbon disulfide desulfurizer |
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| Publication number | Publication date |
|---|---|
| CN105293493B (en) | 2017-10-17 |
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Effective date of registration: 20181130 Address after: 457000 Puxian Industrial Park, fan County Industrial Agglomeration Area, Puyang, Henan Patentee after: Puyang Tianhong Industry Co., Ltd. Address before: 833400 Quxinhua Transfer of Office Building of Tianshan Street No.8 Party and Government Service Center, Alashankou City, Bortala Mongolian Autonomous Prefecture, Xinjiang Uygur Autonomous Region Patentee before: Zhang Guanbiao |