CN105272150A - Tenmoku glaze procelain - Google Patents

Tenmoku glaze procelain Download PDF

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Publication number
CN105272150A
CN105272150A CN201510658419.0A CN201510658419A CN105272150A CN 105272150 A CN105272150 A CN 105272150A CN 201510658419 A CN201510658419 A CN 201510658419A CN 105272150 A CN105272150 A CN 105272150A
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China
Prior art keywords
parts
glaze
dehua
raw material
china clay
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CN201510658419.0A
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CN105272150B (en
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王小龙
李燕萍
林鸿福
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Beijing Shuangao Tiguan Sports Culture Club Co ltd
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Dehua Heng Yi Ceramic Art Limited-Liability Co
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Abstract

Disclosed tenmoku glaze porcelain comprises china clay and glaze. The glaze is composed of the following raw materials in parts by mass: 15-45 parts of potash feldspar, 10-40 parts of albite, 1-5 parts of aluminium oxide, 1-5 parts of zinc oxide, 1-5 parts of cobalt oxide, 10-50 parts of Dehua kaolin, 1-10 parts of cattle bone powder, and 1-10 parts of straw ash. The china clay is composed of the following raw materials in parts by mass: 20-55 parts of Dehua kaolin, 10-35 parts of dolomite, 5-25 parts of potash feldspar, 5-25 parts of albite, 0-5 parts of aluminium oxide, 0-5 parts of zinc oxide, 0-5 parts of cobalt oxide, 1-15 parts of Dehua mine soil, 1-10 parts of mica, and 5-15 parts of Dehua clay. The employed china clay is brown or black body, the glaze is oil-drop tenmoku glaze, and crystallized piebald points with different sizes are distributed on the glaze surface of the ceramic product prepared by using the glaze and show oil-drop-shaped pattern, and the pattern is extremely attractive.

Description

Temmoku vitreous enamel
Technical field
The present invention relates to ceramic formula technical field, specifically a kind of temmoku vitreous enamel.
Background technology
Temmoku glaze is the black glazed ware device that Japanese takes back from Tianmu Mountains of Zhejiang Province, therefore named.Temmoku glaze is various in style, and famous and precious having oil droplet, the writing brush made of rabbit's hair, sparkling glaze, blackly determine small cup, francolin spot, hawksbill turtle, yellow temmoku etc., is the common name of Song dynasty iron black crystalline glaze.Droplet temmoku glaze face effect has silver color crystalline particle in glaze layer, has microgroove to be flower-shaped in particle.Writing brush made of rabbit's hair temmoku is also known as " writing brush made of rabbit's hair temmoku flower ", " glaze of furry appearance ", " beautiful milli glaze ", and its background color is darker dark purple black, and with foxy milli light, sericate muscle line is filemot coffee color is that background color sets off.Sunlight change of weather order belongs to the superfine product of temmoku glaze, has the solar flare that high temperature burns till under glaze, and solar flare seven glories that can glitter under sunlight and certain temperature condition are swooned.The feature of yohen Tenmoku: naturally appear big and small spot in black glaze in one's mind, round these spot surroundings in addition the colored halation such as red, green, sky blue to glitter under the illumination of different azimuth brilliance.
Temmoku glaze is the famous and precious vitreous enamel of one produced China's Song dynasty, and existing handed down from ancient times oneself is phoenix feathers and unicorn horns, and sunlight change of weather order is then more rare rare, only has three to collect respectively in the huge safety locker in three museums of Japan, within every 7 years, just puts on display once.China not yet finds that yohen Tenmoku porcelain is handed down from ancient times so far, therefore since 19th century, the ceramist of countries in the world falls over each other to have dropped into a large amount of manpower and materials, attempts to copy this name porcelain, but is successfully not yet reported by generally acknowledged the copying of industry.
Summary of the invention
The object of the present invention is to provide a kind of temmoku vitreous enamel of the crystallization piebald point with oil droplet shape.
For achieving the above object, the invention provides following technical scheme:
Temmoku vitreous enamel, comprise china clay and glaze, described glaze is made up of the raw material of following mass parts: potassium felspar sand 15-45 part, albite 10-40 part, aluminum oxide 1-5 part, zinc oxide 1-5 part, cobalt oxide 1-5 part, Dehua kaolin 10-50 part, bovine bone powder 1-10 part, rice-straw ash 1-10 part; Described china clay is made up of the raw material of following mass parts: Dehua kaolin 20-55 part, white clouds soil 10-35 part, potassium felspar sand 5-25 part, albite 5-25 part, aluminum oxide 0-5 part, zinc oxide 0-5 part, cobalt oxide 0-5 part, mine, Dehua soil 1-15 part, mica 1-10 part, Dehua clay 5-15 part.
As the further scheme of the present invention: described glaze is made up of the raw material of following mass parts: potassium felspar sand 30 parts, albite 25 parts, 3 parts, aluminum oxide, 3 parts, zinc oxide, cobalt oxide 3 parts, Dehua kaolin 30 parts, bovine bone powder 5.5 parts, rice-straw ash 5.5 parts; Described china clay is made up of the raw material of following mass parts: 22 parts, Dehua kaolin 38 parts, white clouds soil, potassium felspar sand 15 parts, albite 15 parts, 2.5 parts, aluminum oxide, 2.5 parts, zinc oxide, cobalt oxide 2.5 parts, 8 parts, mine, Dehua soil, 5.5 parts, mica, Dehua clay 10 parts.
As the further scheme of the present invention: the glazing thickness of described glaze on china clay is 0.6-1.5mm.
The making method of described temmoku vitreous enamel, comprises the following steps:
(1) china clay and glaze raw material are processed, comprise the following steps:
1) china clay raw material is processed: by above-mentioned china clay desired raw material, through grinding screening, proportioning, dehydration, old, manual assembly, repaired biscuit and drying obtain porcelain base;
2) glaze raw material is processed: take above-mentioned glaze desired raw material in proportion, enter mill, according to glaze compound: the ratio of the mass ratio=1:0.25-0.34 of water, add water grinding 18-20h, fineness control 250 mesh sieves tail over≤0.1%, obtain glaze water;
(2) glazing: the mode adopting leaching glaze or glaze spraying, makes glaze water adhesion in porcelain base surface, and makes glaze water thickness reach 0.6-1.5mm;
(3) burn till: the porcelain base after glazing being placed in humidity is 0.5-1h under the environment of 80%, reenter klining, first with the ramp to 1050 DEG C of 60-80 DEG C/h, then with the ramp to 1190 DEG C of 40-60 DEG C/h, then with the ramp of 60-80 DEG C/h to 1280-1330 DEG C, insulation 4-6h; Cool to 900 DEG C with the speed of 120-180 DEG C/h again, finally naturally cool to room temperature, obtain temmoku vitreous enamel.
Compared with prior art, the invention has the beneficial effects as follows: the china clay that the present invention adopts is the carcass of brown or black, glaze is droplet temmoku glaze, the ceramic product glaze paint made from this glaze is distributed with crystallization piebald point not of uniform size, these crystallization piebald points present the pattern of oil droplet shape, abnormal exquisite.
Embodiment
Below in conjunction with the embodiment of the present invention, be clearly and completely described the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, temmoku vitreous enamel, comprise china clay and glaze, described glaze is made up of the raw material of following mass parts: potassium felspar sand 15 parts, albite 40 parts, 1 part, aluminum oxide, 5 parts, zinc oxide, cobalt oxide 1 part, Dehua kaolin 50 parts, bovine bone powder 1 part, rice-straw ash 10 parts; Described china clay is made up of the raw material of following mass parts: 35 parts, Dehua kaolin 20 parts, white clouds soil, potassium felspar sand 5 parts, albite 25 parts, 5 parts, zinc oxide, 15 parts, mine, Dehua soil, 1 part, mica, Dehua clay 15 parts.
The making method of described temmoku vitreous enamel, comprises the following steps:
(1) china clay and glaze raw material are processed, comprise the following steps:
1) china clay raw material is processed: by above-mentioned china clay desired raw material, through grinding screening, proportioning, dehydration, old, manual assembly, repaired biscuit and drying obtain porcelain base;
2) glaze raw material is processed: take above-mentioned glaze desired raw material in proportion, enter mill, according to glaze compound: the ratio of the mass ratio=1:0.25 of water, add water grinding 20h, fineness control 250 mesh sieves tail over≤0.1%, obtain glaze water;
(2) glazing: the mode adopting leaching glaze or glaze spraying, makes glaze water adhesion in porcelain base surface, and makes glaze water thickness reach 0.6mm;
(3) burn till: the porcelain base after glazing being placed in humidity is 0.5h under the environment of 80%, reenter klining, first with the ramp to 1050 DEG C of 80 DEG C/h, then with the ramp to 1190 DEG C of 60 DEG C/h, then with the ramp to 1330 DEG C of 80 DEG C/h, insulation 6h; Cool to 900 DEG C with the speed of 180 DEG C/h again, finally naturally cool to room temperature, obtain temmoku vitreous enamel.
Embodiment 2
In the embodiment of the present invention, temmoku vitreous enamel, comprise china clay and glaze, described glaze is made up of the raw material of following mass parts: potassium felspar sand 30 parts, albite 25 parts, 3 parts, aluminum oxide, 3 parts, zinc oxide, cobalt oxide 3 parts, Dehua kaolin 30 parts, bovine bone powder 5.5 parts, rice-straw ash 5.5 parts; Described china clay is made up of the raw material of following mass parts: 22 parts, Dehua kaolin 38 parts, white clouds soil, potassium felspar sand 15 parts, albite 15 parts, 2.5 parts, aluminum oxide, 2.5 parts, zinc oxide, cobalt oxide 2.5 parts, 8 parts, mine, Dehua soil, 5.5 parts, mica, Dehua clay 10 parts.
The making method of described temmoku vitreous enamel, comprises the following steps:
(1) china clay and glaze raw material are processed, comprise the following steps:
1) china clay raw material is processed: by above-mentioned china clay desired raw material, through grinding screening, proportioning, dehydration, old, manual assembly, repaired biscuit and drying obtain porcelain base;
2) glaze raw material is processed: take above-mentioned glaze desired raw material in proportion, enter mill, according to glaze compound: the ratio of the mass ratio=1:03 of water, add water grinding 20h, fineness control 250 mesh sieves tail over≤0.1%, obtain glaze water;
(2) glazing: the mode adopting leaching glaze or glaze spraying, makes glaze water adhesion in porcelain base surface, and makes glaze water thickness reach 1.0mm;
(3) burn till: the porcelain base after glazing being placed in humidity is 0.8h under the environment of 80%, reenter klining, first with the ramp to 1050 DEG C of 70 DEG C/h, then with the ramp to 1190 DEG C of 50 DEG C/h, then with the ramp to 1310 DEG C of 70 DEG C/h, insulation 5h; Cool to 900 DEG C with the speed of 150 DEG C/h again, finally naturally cool to room temperature, obtain temmoku vitreous enamel.
Embodiment 3
In the embodiment of the present invention, temmoku vitreous enamel, comprise china clay and glaze, described glaze is made up of the raw material of following mass parts: potassium felspar sand 45 parts, albite 10 parts, 5 parts, aluminum oxide, 1 part, zinc oxide, cobalt oxide 5 parts, Dehua kaolin 10 parts, bovine bone powder 10 parts, rice-straw ash 1 part; Described china clay is made up of the raw material of following mass parts: 10 parts, Dehua kaolin 55 parts, white clouds soil, potassium felspar sand 25 parts, albite 5 parts, 5 parts, aluminum oxide, cobalt oxide 5 parts, 1 part, mine, Dehua soil, 10 parts, mica, Dehua clay 5 parts.
The making method of described temmoku vitreous enamel, comprises the following steps:
(1) china clay and glaze raw material are processed, comprise the following steps:
1) china clay raw material is processed: by above-mentioned china clay desired raw material, through grinding screening, proportioning, dehydration, old, manual assembly, repaired biscuit and drying obtain porcelain base;
2) glaze raw material is processed: take above-mentioned glaze desired raw material in proportion, enter mill, according to glaze compound: the ratio of the mass ratio=1:0.34 of water, add water grinding 18h, fineness control 250 mesh sieves tail over≤0.1%, obtain glaze water;
(2) glazing: the mode adopting leaching glaze or glaze spraying, makes glaze water adhesion in porcelain base surface, and makes glaze water thickness reach 1.5mm;
(3) burn till: the porcelain base after glazing being placed in humidity is 1h under the environment of 80%, reenter klining, first with the ramp to 1050 DEG C of 60 DEG C/h, then with the ramp to 1190 DEG C of 40 DEG C/h, then with the ramp to 1280 DEG C of 60 DEG C/h, insulation 4h; Cool to 900 DEG C with the speed of 120 DEG C/h again, finally naturally cool to room temperature, obtain temmoku vitreous enamel.
In the raw material adopted in foregoing invention embodiment, Dehua kaolin, mine, Dehua soil, Dehua clay are all from Dehua County, Fujian Province.The carcass of the temmoku vitreous enamel obtained by above-mentioned technique is brown or black, and the glaze paint of carcass surface portion is distributed with crystallization piebald point not of uniform size, these crystallization piebald points present the pattern of oil droplet shape, abnormal exquisite.
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present invention or essential characteristic, the present invention can be realized in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present invention is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the present invention.
In addition, be to be understood that, although this specification sheets is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of specification sheets is only for clarity sake, those skilled in the art should by specification sheets integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.

Claims (3)

1. temmoku vitreous enamel, it is characterized in that, comprise china clay and glaze, described glaze is made up of the raw material of following mass parts: potassium felspar sand 15-45 part, albite 10-40 part, aluminum oxide 1-5 part, zinc oxide 1-5 part, cobalt oxide 1-5 part, Dehua kaolin 10-50 part, bovine bone powder 1-10 part, rice-straw ash 1-10 part; Described china clay is made up of the raw material of following mass parts: Dehua kaolin 20-55 part, white clouds soil 10-35 part, potassium felspar sand 5-25 part, albite 5-25 part, aluminum oxide 0-5 part, zinc oxide 0-5 part, cobalt oxide 0-5 part, mine, Dehua soil 1-15 part, mica 1-10 part, Dehua clay 5-15 part.
2. temmoku vitreous enamel according to claim 1, it is characterized in that, described glaze is made up of the raw material of following mass parts: potassium felspar sand 30 parts, albite 25 parts, 3 parts, aluminum oxide, 3 parts, zinc oxide, cobalt oxide 3 parts, Dehua kaolin 30 parts, bovine bone powder 5.5 parts, rice-straw ash 5.5 parts; Described china clay is made up of the raw material of following mass parts: 22 parts, Dehua kaolin 38 parts, white clouds soil, potassium felspar sand 15 parts, albite 15 parts, 2.5 parts, aluminum oxide, 2.5 parts, zinc oxide, cobalt oxide 2.5 parts, 8 parts, mine, Dehua soil, 5.5 parts, mica, Dehua clay 10 parts.
3. temmoku vitreous enamel according to claim 1, is characterized in that, the glazing thickness of described glaze on china clay is 0.6-1.5mm.
CN201510658419.0A 2015-10-14 2015-10-14 Tenmoku glaze procelain Expired - Fee Related CN105272150B (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106116147A (en) * 2016-06-23 2016-11-16 德化恒瀚艺品有限公司 A kind of oil-spot glaze containing shraff and preparation method thereof
CN107417250A (en) * 2017-06-05 2017-12-01 杨合岭 A kind of Sui's celadon formula and its manufacture craft
CN108840664A (en) * 2018-08-31 2018-11-20 济源市坤彤陶瓷科技开发有限公司 A kind of formula and its manufacture craft of colored porcelain porcelain
CN109052944A (en) * 2018-09-14 2018-12-21 湖南高峰陶瓷制造有限公司 Temmoku glaze and preparation method thereof
CN109369013A (en) * 2018-10-17 2019-02-22 景德镇学院 A kind of celeste glaze and preparation method thereof
CN115259667A (en) * 2022-08-24 2022-11-01 福建省德化意达陶瓷有限公司 Oil-drop temmoku glaze and firing method of oil-drop temmoku glaze ceramic

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105753323B (en) * 2016-03-23 2018-06-01 杨云超 A kind of your porcelain preparation method of emerald green glaze

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005320174A (en) * 2002-05-10 2005-11-17 Ikuyoshi Kojima Process for producing firing-denatured tenmoku tile, firing-denatured tenmoku tile and glaze
CN102070329A (en) * 2009-11-20 2011-05-25 路铠铭 Raw material formula and manufacturing process for temmoku glaze porcelain
CN104496558A (en) * 2014-12-04 2015-04-08 王泽彬 Black oil-drop temmoku glaze
CN104649715A (en) * 2014-12-31 2015-05-27 路今铧 Novel temmoku glazed porcelain and firing method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005320174A (en) * 2002-05-10 2005-11-17 Ikuyoshi Kojima Process for producing firing-denatured tenmoku tile, firing-denatured tenmoku tile and glaze
CN102070329A (en) * 2009-11-20 2011-05-25 路铠铭 Raw material formula and manufacturing process for temmoku glaze porcelain
CN104496558A (en) * 2014-12-04 2015-04-08 王泽彬 Black oil-drop temmoku glaze
CN104649715A (en) * 2014-12-31 2015-05-27 路今铧 Novel temmoku glazed porcelain and firing method thereof

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106116147A (en) * 2016-06-23 2016-11-16 德化恒瀚艺品有限公司 A kind of oil-spot glaze containing shraff and preparation method thereof
CN106116147B (en) * 2016-06-23 2019-02-22 德化恒瀚艺品有限公司 A kind of oil-spot glaze and preparation method thereof containing shraff
CN107417250A (en) * 2017-06-05 2017-12-01 杨合岭 A kind of Sui's celadon formula and its manufacture craft
CN108840664A (en) * 2018-08-31 2018-11-20 济源市坤彤陶瓷科技开发有限公司 A kind of formula and its manufacture craft of colored porcelain porcelain
CN109052944A (en) * 2018-09-14 2018-12-21 湖南高峰陶瓷制造有限公司 Temmoku glaze and preparation method thereof
CN109369013A (en) * 2018-10-17 2019-02-22 景德镇学院 A kind of celeste glaze and preparation method thereof
CN115259667A (en) * 2022-08-24 2022-11-01 福建省德化意达陶瓷有限公司 Oil-drop temmoku glaze and firing method of oil-drop temmoku glaze ceramic

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