CN105267122A - Natural moisturizing and pore shrinking gel and preparation method thereof - Google Patents
Natural moisturizing and pore shrinking gel and preparation method thereof Download PDFInfo
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- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
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Abstract
The invention discloses natural moisturizing and pore shrinking gel. The natural moisturizing and pore shrinking gel comprises witch hazel extract, gallnut extract, apple seed extract, green tea extract, bletilla striata extract, rosemary extract, azone, sodium hyaluronate, Carbomer 941, triethanolamine, sodium alginate and ice crystal formation agent. Compared with the prior art, the natural moisturizing and pore shrinking gel has the advantages that the gel is light green, appropriate in viscosity, good in stability, fragrant, refreshing in texture and capable of keeping the moisture of the skin, relieving wrinkles, improving roughness, shrinking pores and promoting skin cell regeneration.
Description
Technical field
The present invention relates to a kind of gel and preparation method thereof, particularly a kind of natural moisture preserving pore refining gel and preparation method thereof.
Background technology
Skin is one of organ of wanting of our body weight for humans, and it protects our health as one natural cover for defense.Healthy skin is undoubtedly that everyone wants to have, and it directly concerns " face value ", concerns the direct impression of person to person's contacts, affects our physical and mental health.
Corse sweat pore is at the masculinity femininity of each ages skin problem common with it.Its Crack cause can be divided into following several:
1, the vigorous obstruction caused of dirt obstruction-fat secretion makes skin metabolism not smooth, cannot come off as scheduled, cause pore to expand.
2, squeeze small pox overstimulation-excessive compression pimples, acne, once hurt corium, pore just can be made to become thick.This phenomenon occurs more at adolescence.Be coated with irritating cosmetics and medicine frost can make obstruction become serious, pore also can be increasing.
3, oil suction excessively-use oil-Absorbing Sheets and deep cleansing mask, but excessive oil suction can the normal secretions of disorderly oils and fats, and a lot of deep layer cleaning product is first by pore support greatly, could go deep into pore by oil content and dirtyly to bring out.
4, smoke-when you enjoy puff away smug time, medicated cigarette but allows your vasoconstriction, and blood circulation slows down, and nutrient successfully cannot send to Skin Cell, and report for work all ahead of time so dry, aging, face's lines naturally droop, and pore support is large.
5, the dyskeratosis of follicular keratosis-hair follicle and the sebaceous gland mouth of pipe, due to inharmonious, the factor such as hormone secretion, seasonal variations of rule of life, cause cutin can not homergy, the cutin of hair follicle and sebaceous gland mouth of pipe overheap, pore is made to become coarse, easy blocking, thus cause corse sweat pore.
6, aging, the atrophy of skin aging, atrophy-skin histology, the aging of skin is inevitable, has usually arrived certain age bracket, and skin pore just there will be lax, and blood circulation can be not smooth gradually yet, and skin metabolism starts slack-off.Meanwhile, skin lacks flexibility, and skin collagen starts slack and undisciplined, is not enough to support pore around, makes pore occur oval thick state.Therefore, corse sweat pore is usually the easiest at some dynamic stricture of vaginas, as seen near crows-feet, corners of the mouth stricture of vagina, decree stricture of vagina etc.
7, xerosis cutis, hydropenia-xerosis cutis, hydropenia, the cell around pore also can hydropenia shrink, and simultaneously cutin also there will be drying, coarse, and pore will be more obvious.
Repair corse sweat pore problem, protection skin is except carrying out exfoliation, control oil, deep layer cleaning work, and also need the moisturizing accomplishing skin, most important is pore refining.There being the natural plant extracts of pore refining effect to be dissolved in the middle of skin care item, it is the Development Trend of modern skin protection science and technology.For the modern pursuing high-quality life, using containing the moisturizing pore refining gel of natural component extract is an excellent selection.
Summary of the invention
The object of the present invention is to provide one can soft cutin and deep layer cleaning pore hair follicle, improve the problems such as coarse, the hydropenia of skin, promote Skin Cell regeneration, make the skin of corse sweat pore return fine and smooth a kind of natural moisture preserving pore refining gel and preparation method thereof.
A kind of natural moisture preserving pore refining gel of the present invention, wherein includes the material of following consumption:
In a kind of natural moisture preserving pore refining gel described above, preferably, Radix Hamamelidis Mollis extracting solution 1-2ml, Chinese nutgall 1-2ml, Apple Seeds extracting solution 1-2ml, green tea extractive liquor 1-2ml, Rhizoma Bletillae extraction solution 1-2ml, Herba Rosmarini Officinalis extracting solution 1-2ml.
In a kind of natural moisture preserving pore refining gel described above, described Radix Hamamelidis Mollis extracting solution prepares by the following method: take Radix Hamamelidis Mollis appropriate, soak 0.25-0.75 hour, be heated to 90-100 DEG C, decoct extraction three times: the water adding Radix Hamamelidis Mollis weight 30-50 times amount for the first time, extract 0.5-2h, four layers of filtered through gauze; Second time adds the water of filtering residue weight 25-45 times amount, extracts 0.5-1.5h, four layers of filtered through gauze; Third time adds the water of filtering residue weight 20-40 times amount, and extract 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, and filtrate is concentrated into 6-10 times of Radix Hamamelidis Mollis weight, while hot sucking filtration and get final product.
In a kind of natural moisture preserving pore refining gel described above, described Chinese nutgall is prepared by the following method: take Galla Chinensis appropriate, be ground into coarse powder, add water and be heated to 90-100 DEG C, decoct extraction three times: the water adding Galla Chinensis weight 12-18 times amount for the first time, extract 0.5-2h, four layers of filtered through gauze; Second time adds the water of filtering residue weight 8-12 times amount, extracts 0.5-1.5h, four layers of filtered through gauze; Third time adds the water of filtering residue weight 5-10 times amount, and extract 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, and filtrate is concentrated into 5-8 times of Galla Chinensis weight, while hot sucking filtration and get final product.
In a kind of natural moisture preserving pore refining gel described above, described Apple Seeds extracting solution prepares by the following method: take Apple Seeds and be ground into coarse powder, soak 0.25-0.75 hour, be heated to 90-100 DEG C, decoct extraction three times: the water adding Apple Seeds weight 35-45 times amount for the first time, extract 0.5-2h, four layers of filtered through gauze; Second time adds the water of filtering residue weight 30-38 times amount, extracts 0.5-1.5h, four layers of filtered through gauze; Third time adds the water of filtering residue weight 28-35 times amount, and extract 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, and filtrate is concentrated into 6-10 times of Apple Seeds weight, while hot sucking filtration and get final product.
In a kind of natural moisture preserving pore refining gel described above, described green tea extractive liquor prepares by the following method: take green tea appropriate, soak 0.25-0.75 hour, be heated to 90-100 DEG C, decoct extraction three times: first time is with the water of green tea weight 30-50 times amount, extract 0.5-2h, four layers of filtered through gauze; Second time adds the water of filtering residue weight 25-45 times amount, extracts 0.5-1.5h, four layers of filtered through gauze; Third time adds the water of filtering residue weight 20-40 times amount, and extract 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, and filtrate is concentrated into 6-10 times of green tea weight, while hot sucking filtration and get final product.
In a kind of natural moisture preserving pore refining gel described above, described Rhizoma Bletillae extraction solution prepares by the following method: take the Pseudobulbus Bletillae (Rhizoma Bletillae) appropriate, be ground into coarse powder, soak 0.25-0.75 hour, be heated to 90-100 DEG C, decoct extraction three times: the water that first time adds Pseudobulbus Bletillae (Rhizoma Bletillae) weight 12-18 times amount, extract 0.5-2h, four layers of filtered through gauze; Second time adds the water of filtering residue weight 8-12 times amount, extracts 0.5-1.5h, four layers of filtered through gauze; Third time adds the water of filtering residue weight 5-8 times amount, and extract 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, and filtrate is concentrated into 5-8 times of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, while hot sucking filtration and get final product.
In a kind of natural moisture preserving pore refining gel described above, described Herba Rosmarini Officinalis extracting solution prepares by the following method: take Herba Rosmarini Officinalis appropriate, soak 0.25-0.75 hour, be heated to 90-100 DEG C, decoct extraction three times: the water adding Herba Rosmarini Officinalis weight 30-50 times amount for the first time, extract 0.5-2h, four layers of filtered through gauze; Second time adds the water of filtering residue weight 25-45 times amount, extracts 0.5-1.5h, four layers of filtered through gauze; Third time adds the water of filtering residue weight 20-35 times amount, and extract 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, and filtrate is concentrated into 6-10 times of Herba Rosmarini Officinalis weight, while hot sucking filtration and get final product.
The preparation method of a kind of natural moisture preserving pore refining gel of the present invention, comprises the following steps:
A) taking sodium alginate 0.5-2g, add 20-40ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, is substrate 1;
B) take carbomer 0.1-2g, add 25-45ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, drips 30% triethanolamine solution 0.05-1ml, is uniformly mixed, and is substrate 2;
C) taking ice crystal forming agent 0.5-2g with beaker, add 30-50ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, is substrate 3;
D) Radix Hamamelidis Mollis extracting solution 0.5-3ml, Chinese nutgall 0.5-3ml, Apple Seeds extracting solution 0.5-3ml, green tea extractive liquor 0.5-3ml, Rhizoma Bletillae extraction solution 0.5-3ml, Herba Rosmarini Officinalis extracting solution 0.5-3ml mix homogeneously is got as solution 1;
E) by substrate 1, substrate 2, substrate 3 Homogeneous phase mixing, add in solution 1, Homogeneous phase mixing; In mixture, add azone 0.5-2ml again, 1% sodium hyaluronate solution 1-4ml, 2% ethyl hydroxybenzoate alcoholic solution 0.05-2ml, 2% potassium sorbate solution 0.05-2ml, stir, Homogeneous phase mixing, obtains natural moisture preserving pore refining gel.
30% triethanolamine solution described in the present invention, 1% sodium hyaluronate solution, 2% ethyl hydroxybenzoate alcoholic solution, 2% potassium sorbate solution all can be buied or prepared before use from market, wherein 30% triethanolamine solution is volumetric concentration, other are weight concentration, and ethyl hydroxybenzoate alcoholic solution can be the alcoholic solution of ethyl hydroxybenzoate or the propylene glycol, glycerin solution etc. of ethyl hydroxybenzoate.In the present invention, carbomer is Carbopol 941, and ice crystal forming agent is ice crystal forming agent AVC.
Certainly can add essence in product of the present invention better to improve product odour, its consumption can at 0.05-0.5ml as added mix homogeneously in step (e).
Various compositions in the present invention are as follows:
Radix Hamamelidis Mollis includes multiple tannin matter such as Ellagtannin and Hamamlitannin can regulate sebum secretion, Hydrolyzed Protein and Milk Protein.Promote lymph blood circulation, eye bladder and black eye in morning can be overcome specially.The effect of have calmness, pacifying, is improved effect to be full of cracks, sunburn, acne.Effectively can help the regeneration capacity at skin night.Remove eye pouch, loosen and relax and have very excellent effect to what oiliness skin or the skin of allergy.Releive, restrain, antibacterial, antidotal effect, because there being the significant curative effect of convergence control oil, sterilization, for children in adolescence or the more serious skin of fuel-displaced situation, be only selection.
Galla Chinensis is containing a large amount of tannic acid, and tannic acid has protein and solidifies and precipitation.After the ulcer contact tannic acid of skin, mucosa, namely its tissue protein is solidified, and forms one deck tunicle, thus plays astriction.
Apple Seeds extract can directly supplement from natural plant (Fructus Mali pumilae) gonadal hormone, plant (Fructus Mali pumilae) hormone, and causes the sex hormones secretion of human body self; Promote skin scar reparation, promote collagen protein and the keratin normal growth of skin area.
Green tea contributes to slow down aging, prevention and therapy radiation injury.The tea polyphenols contributing to beauty and skin care in green tea has very strong non-oxidizability and physiologically active, is the scavenger of human free radical, has blocking-up lipid peroxidation, the effect of scavenging capacity enzyme.Tea polyphenols and oxidation product thereof have the ability absorbing radioactive substance strontium 90 and Co 60 murder by poisoning.Tea polyphenols is water-soluble substances, washes one's face can remove the greasy of face with it, and convergence pore, has sterilization, sterilizing, resisting age of skin, and the ultraviolet radiation in minimizing daylight is to effects such as the damages of skin.
The rich viscosity of the Pseudobulbus Bletillae (Rhizoma Bletillae), containing Pseudobulbus Bletillae (Rhizoma Bletillae) colloid, i.e. bletilla mannan, there is the functions such as convergence, hemostasis, delay skin aging, moisturizing, to preventing and treat skin chilblain and chapping, blood circulation promoting, improve skin-nourishing situation and prevent wrinkle etc. to have obvious curative effects, can Glycerin, beauty treatment speckle removing, make skin as smooth as jade, and without side reaction and toxicity." property of medicine opinion " points out that Radix Chloranthi Serrati " is controlled Shao-bleb on face, made us flesh and slide.”
Antioxidant content in Herba Rosmarini Officinalis is mainly the compositions such as carnosic acid, carnosol, rosmanol, ursolic acid, rosmarinic acid.Herba Rosmarini Officinalis is the famous plant having convergence effect, can help our clean hair follicle and deep skin, and pore can be allowed more tiny, thus allow skin seem finer and smoother more smooth.In addition, Herba Rosmarini Officinalis non-oxidizability, also certain effect is served to delaying senility.Herba Rosmarini Officinalis also has tranquillizing and allaying excitement, refreshment effect.
Hyaluronate sodium has another name called hyaluronic acid sodium, hyaluronic acid sodium, is a kind of acid mucopolysaccharide.Hyaluronic acid extracts from the special materials such as the umbilical cord of buphthalmos, cockscomb, people, recently also has from some antibacterial as extracted actinomycetes.Hyaluronate sodium itself is one of formation of human body skin, is the widest a kind of acid mucopolysaccharide of people's distribution in vivo, is present in the substrate of connective tissue, has good moisture-keeping function.Containing a large amount of carboxyls and hydroxyl in hyaluronan molecule, formed in molecule in aqueous and intermolecular hydrogen bond, this makes it have powerful water retention, can in conjunction with self water of more than 400 times, be the best material of the occurring in nature moisture retention that finds at present, be called as desirable nature moisturizing factor.The pure hyaluronic acid aqueous solution of 2% can keep 98% moisture securely.
Sodium alginate has another name called sodium alginate, seaweed gel, Algin, alginate, is by the natural polysaccharide carbohydrate extracted in Thallus Laminariae (Thallus Eckloniae).Japanese calls the food being rich in sodium alginate " life prolonging food ", and American is then called " marvellous food additive ".Sodium alginate has natural moisture preserving effect, is a kind of thickening agent of good performance.
Carbomer is cross-linked with acrylic acid the acrylic acid crosslinked resin obtained with tetramethylolmethane etc., and in skin care item, Chang Zuowei hydrophilic thickening agent, stabilising emulsifier, suspending agent, gel, have good transparency, is widely used in emulsion, cream frost, gel.
Triethanolamine is used as emulsifying agent, wetting agent, humidizer, thickening agent, PH poising agent in cosmetics (comprising skin washing, eye glue, moisturizing, shampoo etc.).Triethanolamine is the most frequently used nertralizer containing acid high-molecular gels such as carbomers, and triethanolamine, by neutralizing with carboxyls such as carbomers, forms stable macromolecular structure, reaches the effect of thickening and moisturizing.
Ice crystal forming agent is without the need to heating, without the need to neutralization, acidproof, directly add slightly to stir after water sparkling and crystal-clear cautious gel, finished product has the dermal sensation be as cheerful as a lark, and makes product absorb sooner, low viscosity.
Ethyl hydroxybenzoate is used as bacteriostatic preservative, is widely used in liquid preparation and semi-solid preparation, also can be used for the anticorrosion of food and cosmetics.
Potassium sorbate is the antisepsis antistaling agent of the highly effective and safe of international food and agricultural organization and Health Organisation recommendations, is widely used in the industries such as food, beverage, Nicotiana tabacum L., pesticide, cosmetics.
Through the Radix Hamamelidis Mollis selected by experimental verification the present invention, Galla Chinensis, Apple Seeds, green tea, the Pseudobulbus Bletillae (Rhizoma Bletillae), Herba Rosmarini Officinalis, its plant extraction elite all has pore refining effect in various degree, can maintenance corse sweat pore skin from inside to outside, in moisturizing, clean, reparation, antioxidation etc., have good synergy simultaneously.Special interpolation azone-a kind of all has obvious transdermal to help the material of the effect of oozing to oleophylic, hydrophilic medicament and active component, keratodermatitis and lipid can be made to interact, reduce the phase inversion temperature of active substance to lipid in horny layer gap, add mobility, medicine or the active additive diffusional resistance in horny layer is reduced, therefore play and very strong shortly ooze effect, the effective ingredient in gel can be made fully to be absorbed by skin.
Gel made by the present invention is light gray green, is the color of natural component itself, and viscosity is suitable for, evenly fine and smooth, and stretchability is good, cool and comfortable, good stability, fragrant.Water-soluable gel skin care item contain comparatively juicy, have moisturizing, clearly act on, be applicable to oily skin.And oily skin is just the skin properties of the group of people at high risk of corse sweat pore problem.This gel can be used as facial film, long be conducive to it with the contact skin time and imitate composition and fully absorbed by skin.Its natural component can soft cutin and deep layer cleaning pore hair follicle, improves the problems such as coarse, the hydropenia of skin, promotes Skin Cell regeneration to make the skin of corse sweat pore return exquisiteness.Simple and elegant fragrant atmosphere, more allows people enjoy the enjoyment of skin protection to the full.
Detailed description of the invention
Following embodiment further illustrates using as the explaination to the technology of the present invention content for content of the present invention; but flesh and blood of the present invention is not limited in described in following embodiment, those of ordinary skill in the art can and should know any simple change based on connotation of the present invention or replace all should belong to protection domain of the presently claimed invention.
Being prepared as follows of each extracting solution:
The preparation of 1 Radix Hamamelidis Mollis extracting solution:
Take Radix Hamamelidis Mollis appropriate, soak 0.4 hour, be heated to 100 DEG C, decoct extraction three times: the water that first time adds Radix Hamamelidis Mollis weight 40 times amount, extract 1h, four layers of filtered through gauze; Filter the water adding filtering residue weight 30 times amount in gained filtering residue again to first time, extract 1h, four layers of filtered through gauze; Filter the water adding filtering residue weight 25 times amount in gained filtering residue again to second time, extract 1h, four layers of filtered through gauze.Filtering residue discards.Merge three filtrates, filtrate is concentrated into 6 times of Radix Hamamelidis Mollis weight, while hot sucking filtration and get final product.
The preparation of 2 Chinese nutgall:
Take Galla Chinensis appropriate, after pulverization process, add water and be heated to 100 DEG C, decoct extraction three times: the water that first time adds Galla Chinensis weight 15 times amount, extract 1h, four layers of filtered through gauze; Filter the water adding filtering residue weight 10 times amount in gained filtering residue again to first time, extract 1h, four layers of filtered through gauze; Filter the water adding filtering residue weight 8 times amount in gained filtering residue again to second time, extract 1h, four layers of filtered through gauze.Filtering residue discards.Merge three filtrates, filtrate is concentrated into 5 times of Galla Chinensis weight, while hot sucking filtration and get final product.
The preparation of 3 Apple Seeds extracting solution:
Take Apple Seeds appropriate, soak 0.4 hour, be heated to 100 DEG C, decoct extraction three times: the water that first time adds Apple Seeds weight 40 times amount, extract 1h, four layers of filtered through gauze; Filter the water adding filtering residue weight 35 times amount in gained filtering residue again to first time, extract 1h, four layers of filtered through gauze; Filter the water adding filtering residue weight 30 times amount in gained filtering residue again to second time, extract 1h, four layers of filtered through gauze.Filtering residue discards.Merge three filtrates, filtrate is concentrated into 6 times of Apple Seeds weight, while hot sucking filtration and get final product.
The preparation of liquid got by 4 green tea:
Take green tea appropriate, soak 0.4 hour, be heated to 100 DEG C, decoct extraction three times: first time, with the water of green tea weight 35 times amount, extracts 1h, four layers of filtered through gauze; Filter the water adding filtering residue weight 30 times amount in gained filtering residue again to first time, extract 1h, four layers of filtered through gauze; Filter the water adding filtering residue weight 25 times amount in gained filtering residue again to second time, extract 1h, four layers of filtered through gauze.Filtering residue discards.Merge three filtrates, filtrate is concentrated into 6 times of green tea weight, while hot sucking filtration and get final product.
The preparation of 5 Rhizoma Bletillae extraction solution:
Take the Pseudobulbus Bletillae (Rhizoma Bletillae) appropriate, be ground into coarse powder, soak 0.4 hour, be heated to 100 DEG C, decoct extraction three times: the water that first time adds Pseudobulbus Bletillae (Rhizoma Bletillae) weight 16 times amount, extract 1h, four layers of filtered through gauze; Filter the water adding filtering residue weight 12 times amount in gained filtering residue again to first time, extract 1h, four layers of filtered through gauze; Filter the water adding filtering residue weight 8 times amount in gained filtering residue again to second time, extract 1h, four layers of filtered through gauze.Filtering residue discards.Merge three filtrates, filtrate is concentrated into 5 times of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, while hot sucking filtration and get final product.
The preparation of 6 Herba Rosmarini Officinalis extracting solution:
Take Herba Rosmarini Officinalis appropriate, soak 0.4 hour, be heated to 100 DEG C, decoct extraction three times: the water that first time adds Herba Rosmarini Officinalis weight 45 times amount, extract 1h, four layers of filtered through gauze; Filter the water adding filtering residue weight 35 times amount in gained filtering residue again to first time, extract 1h, four layers of filtered through gauze; Filter the water adding filtering residue weight 30 times amount in gained filtering residue again to second time, extract 1h, four layers of filtered through gauze.Filtering residue discards.Merge three filtrates, filtrate is concentrated into 6 times of Herba Rosmarini Officinalis weight, while hot sucking filtration and get final product.
Embodiment 1
The preparation of natural moisture preserving pore refining gel:
A) taking sodium alginate 1g with beaker, add 30ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, is substrate 1;
B) take carbomer 1g with beaker, add 40ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, drips 30% triethanolamine solution 0.3ml, is uniformly mixed, and is substrate 2;
C) taking ice crystal forming agent 0.8g with beaker, add 40ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, is substrate 3;
D) Radix Hamamelidis Mollis extracting solution 1.5ml, Chinese nutgall 1.5ml, Apple Seeds extracting solution 1.5ml, green tea extractive liquor 1.5ml, Rhizoma Bletillae extraction solution 1.5ml, Herba Rosmarini Officinalis extracting solution 1.5ml mix homogeneously is got as solution 1;
E) by substrate 1,2,3 Homogeneous phase mixing, solution 1 is added, Homogeneous phase mixing; In mixture, add azone 0.5ml again, 1% sodium hyaluronate solution 3ml, 2% ethyl hydroxybenzoate alcoholic solution 0.3ml, 2% potassium sorbate solution 0.2ml, stir, Homogeneous phase mixing; Finally add essence 0.05ml, mixing and stirring, obtain natural moisture preserving pore refining gel.
Embodiment 2
The preparation of natural moisture preserving pore refining gel:
A) taking sodium alginate 0.8g with beaker, add 28ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, is substrate 1;
B) take carbomer 1.2g with beaker, add 45ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, drips 30% triethanolamine solution 0.5ml, is uniformly mixed, and is substrate 2;
C) taking ice crystal forming agent 1.2g with beaker, add 50ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, is substrate 3;
D) Radix Hamamelidis Mollis extracting solution 1.8ml, Chinese nutgall 1.8ml, Apple Seeds extracting solution 1.8ml, green tea extractive liquor 1.8ml, Rhizoma Bletillae extraction solution 1.8ml, Herba Rosmarini Officinalis extracting solution 1.8ml mix homogeneously is got as solution 1;
E) by substrate 1,2,3 Homogeneous phase mixing, solution 1 is added, Homogeneous phase mixing; In mixture, add azone 0.8ml again, 1% sodium hyaluronate solution 2.8ml, 2% ethyl hydroxybenzoate alcoholic solution 0.2ml, 2% potassium sorbate solution 0.3ml, stir, Homogeneous phase mixing; Finally add essence 0.05ml, mixing and stirring, obtain natural moisture preserving pore refining gel.
Embodiment 3
The preparation of natural moisture preserving pore refining gel:
A) taking sodium alginate 0.8g with beaker, add 30ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, is substrate 1;
B) take carbomer 1.2g with beaker, add 45ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, drips 30% triethanolamine solution 0.5ml, is uniformly mixed, and is substrate 2;
C) taking ice crystal forming agent 1.2g with beaker, add 48ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, is substrate 3;
D) Radix Hamamelidis Mollis extracting solution 1.5ml, Chinese nutgall 1.5ml, Apple Seeds extracting solution 1.5ml, green tea extractive liquor 1.5ml, Rhizoma Bletillae extraction solution 1.5ml, Herba Rosmarini Officinalis extracting solution 1.5ml mix homogeneously is got as solution 1;
E) by substrate 1,2,3 Homogeneous phase mixing, solution 1 is added, Homogeneous phase mixing; In mixture, add azone 0.5ml again, 1% sodium hyaluronate solution 2.5ml, 2% ethyl hydroxybenzoate alcoholic solution 0.2ml, 2% potassium sorbate solution 0.3ml, stir, Homogeneous phase mixing; Finally add essence 0.05ml, mixing and stirring, obtain natural moisture preserving pore refining gel.
Test example 1
The physical and chemical index of embodiment 1-3 products obtained therefrom is as follows:
1 character
This product is light gray green, and viscosity is suitable for, evenly fine and smooth, and stretchability is good, cool and comfortable, good stability, fragrant.
2pH value checks
Dip a small amount of gel with the PH reagent paper of moistening, pH is 6-7.
3 caloric tests
Gel is packaged in transparence cosmetic bottle, observes without lamination in the refrigerator cold-storages about a week of 4 DEG C.24h in the calorstat of 55 DEG C, gel is without layering, the phenomenon such as spoiled.
4 centrifugal tests
Be packaged in by gel in tool plug test tube, the centrifugal 20min of 3000r/min, without lamination.
5 irritation tests, anaphylaxis are tested
White mice back cuts off hair, smears the gel prepared by embodiment 1-3 respectively in cutting plucked position, and is not coated with position and compares, and result does not have zest and anaphylaxis.
Example product 1 gram is applied in volunteer (15-45 year, 100 people) gesture and facial expression, observes, all do not occur rubescent, dermexanthesis, foaming phenomena after spending 30 minutes.
6 room temperatures place experiment
Gel made for embodiment 1-3 is placed in bottle for cosmetics, and room temperature leaves standstill investigation 6 months, without lamination, with after feel unchanged, abnormal smells from the patient is unchanged.
7 pore refining effects
Choose volunteer (15-45 year, 100 people), be applied to volunteer on the face with obtained gel, after crossing 20min, rinse out with water.Generally feel that skin slip is comfortable with rear volunteers, feel is better, without greasy feeling.Skin moisturization is better, washes rear without pruritus phenomenon.Through the continuous use of month, pore obviously shrank to some extent, and water is tender can people.
Test example 2
Pore refining effect experimental
Choose 150 15-45 year age bracket people as object on probation, be divided into arbitrarily three groups, apply face with moisturizing pore refining gel prepared by embodiment 1-3 respectively, every day sooner or later each once, a 15-20 minute, service time is one month.Wherein embodiment 1, in 50 examples, man 22 example, female 28 example; Embodiment 2, in 50 examples, man 26 example, female 24 example; Embodiment 3, in 50 examples, man 25 example, female 25 example.The thick degree of selected masculinity femininity skin pore is different.
Effect standard: effective, pore significantly diminishes; Effectively, pore restrains oneself.Invalid, pore is still thick.The results are shown in Table 1:
Table 1 pore refining experimental result
| Effective (people) | Effectively (people) | Invalid (people) | Total effective rate (%) | |
| Embodiment 1 | 40 | 5 | 5 | 90 |
| Embodiment 2 | 38 | 6 | 6 | 88 |
| Embodiment 3 | 37 | 6 | 7 | 86 |
Test example 3
Moisturizing pore refining gel resultant effect is investigated:
Below utilize effect feeling to come the moisturizing pore refining gel that Evaluation operation example produces on probation.Adopt public-opinion poll point system, choose 150 15-45 year age bracket people as object on probation, be divided into arbitrarily three groups, be applied on the face with moisturizing pore refining gel prepared by embodiment 1-3 respectively, wash off with clear water after 25min.Every day early, evening, respectively once a 15-20 minute, service time was 1 month.Every result of use total score is 5 points: 5 be divided into best result, represents better, very satisfaction; 4 are divided into very well; 3 are divided into and can accept; Less than 3 points is bad, can not accept.Be below every average, the results are shown in Table 2:
Table 2 resultant effect is investigated
In sum, this moisturizing pore refining gel is evenly fine and smooth, fragrant, spatter property, moisture retention, alimentary good, has pore refining effect.
Claims (8)
1. a natural moisture preserving pore refining gel, is characterized in that: the material including following consumption:
2. a kind of natural moisture preserving pore refining gel according to claim 1, it is characterized in that: described Radix Hamamelidis Mollis extracting solution prepares by the following method: take Radix Hamamelidis Mollis appropriate, soak 0.25-0.75 hour, be heated to 90-100 DEG C, decoct extraction three times: the water adding Radix Hamamelidis Mollis weight 30-50 times amount for the first time, extract 0.5-2h, four layers of filtered through gauze; Second time adds the water of filtering residue weight 25-45 times amount, extracts 0.5-1.5h, four layers of filtered through gauze; Third time adds the water of filtering residue weight 20-40 times amount, and extract 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, and filtrate is concentrated into 6-10 times of Radix Hamamelidis Mollis weight, while hot sucking filtration and get final product.
3. a kind of natural moisture preserving pore refining gel according to claim 1, it is characterized in that: described Chinese nutgall is prepared by the following method: take Galla Chinensis appropriate, be ground into coarse powder, add water and be heated to 90-100 DEG C, decoct extraction three times: the water adding Galla Chinensis weight 12-18 times amount for the first time, extract 0.5-2h, four layers of filtered through gauze; Second time adds the water of filtering residue weight 8-12 times amount, extracts 0.5-1.5h, four layers of filtered through gauze; Third time adds the water of filtering residue weight 5-10 times amount, and extract 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, and filtrate is concentrated into 5-8 times of Galla Chinensis weight, while hot sucking filtration and get final product.
4. a kind of natural moisture preserving pore refining gel according to claim 1, it is characterized in that: described Apple Seeds extracting solution prepares by the following method: take Apple Seeds and be ground into coarse powder, soak 0.25-0.75 hour, be heated to 90-100 DEG C, decoct extraction three times: the water adding Apple Seeds weight 35-45 times amount for the first time, extract 0.5-2h, four layers of filtered through gauze; Second time adds the water of filtering residue weight 30-38 times amount, extracts 0.5-1.5h, four layers of filtered through gauze; Third time adds the water of filtering residue weight 28-35 times amount, and extract 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, and filtrate is concentrated into 6-10 times of Apple Seeds weight, while hot sucking filtration and get final product.
5. a kind of natural moisture preserving pore refining gel according to claim 1, it is characterized in that: described green tea extractive liquor prepares by the following method: take green tea appropriate, soak 0.25-0.75 hour, be heated to 90-100 DEG C, decoct extraction three times: first time is with the water of green tea weight 30-50 times amount, extract 0.5-2h, four layers of filtered through gauze; Second time adds the water of filtering residue weight 25-45 times amount, extracts 0.5-1.5h, four layers of filtered through gauze; Third time adds the water of filtering residue weight 20-40 times amount, and extract 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, and filtrate is concentrated into 6-10 times of green tea weight, while hot sucking filtration and get final product.
6. a kind of natural moisture preserving pore refining gel according to claim 1, it is characterized in that: described Rhizoma Bletillae extraction solution prepares by the following method: take the Pseudobulbus Bletillae (Rhizoma Bletillae) appropriate, be ground into coarse powder, soak 0.25-0.75 hour, be heated to 90-100 DEG C, decoct extraction three times: the water that first time adds Pseudobulbus Bletillae (Rhizoma Bletillae) weight 12-18 times amount, extract 0.5-2h, four layers of filtered through gauze; Second time adds the water of filtering residue weight 8-12 times amount, extracts 0.5-1.5h, four layers of filtered through gauze; Third time adds the water of filtering residue weight 5-8 times amount, and extract 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, and filtrate is concentrated into 5-8 times of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, while hot sucking filtration and get final product.
7. a kind of natural moisture preserving pore refining gel according to claim 1, it is characterized in that: described Herba Rosmarini Officinalis extracting solution prepares by the following method: take Herba Rosmarini Officinalis appropriate, soak 0.25-0.75 hour, be heated to 90-100 DEG C, decoct extraction three times: the water adding Herba Rosmarini Officinalis weight 30-50 times amount for the first time, extract 0.5-2h, four layers of filtered through gauze; Second time adds the water of filtering residue weight 25-45 times amount, extracts 0.5-1.5h, four layers of filtered through gauze; Third time adds the water of filtering residue weight 20-35 times amount, and extract 0.5-1.5h, four layers of filtered through gauze, filtering residue discards, and merges three filtrates, and filtrate is concentrated into 6-10 times of Herba Rosmarini Officinalis weight, while hot sucking filtration and get final product.
8. the preparation method of a kind of natural moisture preserving pore refining gel described in any one of claim 1-7, comprises the following steps:
A) taking sodium alginate 0.5-2g, add 20-40ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, is substrate 1;
B) take Carbopol 941 0.1-2g, add 25-45ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, drips 30% triethanolamine solution 0.05-1ml, is uniformly mixed, and is substrate 2;
C) taking ice crystal forming agent AVC0.5-2g with beaker, add 30-50ml distilled water, the transparent sparkling and crystal-clear state of naturally swelling formation, is substrate 3;
D) Radix Hamamelidis Mollis extracting solution 0.5-3ml, Chinese nutgall 0.5-3ml, Apple Seeds extracting solution 0.5-3ml, green tea extractive liquor 0.5-3ml, Rhizoma Bletillae extraction solution 0.5-3ml, Herba Rosmarini Officinalis extracting solution 0.5-3ml mix homogeneously is got as solution 1;
E) by substrate 1, substrate 2, substrate 3 Homogeneous phase mixing, add in solution 1, Homogeneous phase mixing; In mixture, add azone 0.5-2ml again, 1% sodium hyaluronate solution 1-4ml, 2% ethyl hydroxybenzoate alcoholic solution 0.05-2ml, 2% potassium sorbate solution 0.05-2ml, stir, Homogeneous phase mixing, obtains natural moisture preserving pore refining gel.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106691976A (en) * | 2017-03-03 | 2017-05-24 | 北京华奥光程化妆品有限公司 | Plant extract capable of controlling oil and shrinking pores and preparation method and application of plant extract |
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| CN104546808A (en) * | 2015-01-29 | 2015-04-29 | 珠海国佳新材股份有限公司 | Gel patch and preparation method thereof |
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| CN101502483A (en) * | 2009-03-14 | 2009-08-12 | 刘希山 | Skin-tendering element with moisture-keeping efficacy |
| CN101697956A (en) * | 2009-10-19 | 2010-04-28 | 海南京润珍珠生物技术股份有限公司 | Anti-acne jelly with pearl hydrolyzate liposome |
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| CN106691976A (en) * | 2017-03-03 | 2017-05-24 | 北京华奥光程化妆品有限公司 | Plant extract capable of controlling oil and shrinking pores and preparation method and application of plant extract |
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Effective date of registration: 20200810 Address after: 510000, Guangdong province Guangzhou Baiyun District People and town show Sheng Road, written by A188 Patentee after: Guangzhou Meiya Cosmetics Co.,Ltd. Address before: 241000 No. 22 West Wenchang Road, Wuhu higher education zone, Anhui Patentee before: WANNAN MEDICAL College |