CN105220457A - New far infrared cotton fiber that a kind of infant is suitable for and preparation method thereof - Google Patents
New far infrared cotton fiber that a kind of infant is suitable for and preparation method thereof Download PDFInfo
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Abstract
The invention provides applicable new far infrared cotton fiber of a kind of infant and preparation method thereof, concrete operation step is: (1) adds bioprotein enzyme reaction by the silk gum solution obtained after natural silk degumming, take out freeze drying, obtain sericin polypeptide hydrolyzes product; (2) cotton fiber is placed in gaseous nitrogen dioxide environment and lucifuge oxidation is carried out to the primary hydroxyl of cotton fiber, take out vacuum and leave standstill, obtain the cotton fiber be oxidized; (3) sericin polypeptide hydrolyzes product is dissolved in deionization, stirs, add nano-ceramic powder and sodium alginate, stir, obtain the far infrared treatment fluid containing silk gum; (4) cotton fiber of oxidation is placed in the far infrared treatment fluid containing silk gum, dipping vibration, takes out preliminary drying and cures, washing and drying, obtains the far infrared cotton fiber that infant is suitable for.Far infrared cotton fiber prepared by the present invention has excellent far infrared performance, does not affect the performances such as the mechanical strength of cotton fiber, soft pro-skin, moisture absorption be ventilative.
Description
Technical field:
The invention belongs to textile material technical field, be specifically related to applicable far infrared cotton fiber of a kind of infant and preparation method thereof.
Background technology:
Along with safety theory of wearing the clothes progressively is rooted in the hearts of the people, take safety and environmental protection as general requirement, children's garment are also from simple attractive in appearance, durable primary attribute towards emphasizing that the attribute of safe, healthy, comfortable, function and aesthetic feeling changes, novel children's garment product scientific rationality more, the parent being more and more subject to the head of a family and children looks at.And along with the development of science and technology and people are to healthy and safe continuous attention, various functional fiber constantly occurs, process technology is constantly reformed, and functional clothing more and more receives the concern of people, and the functional of clothes is constantly also constantly expanded by systematization and sectionalization range of application.
The main component of human body skin is water, water is ultrared good absorber, ultrared most ability can be carried on the back shallow-layer skin and absorbed, the strenuous exercise of aggravation shallow-layer skin Middle molecule and atom, thus play activated water molecule, activate histocyte, improve microcirculatory effect, strengthen the immunity of people, improve resistance.Prevention and health care is the effective way ensureing people's quality of life and health of human body.The physilogical characteristics that the colony of baby, children has it special, resistivity is poor, very responsive to environment, ensures that the health of environment is clean, more will improve their immunity for this colonial need.Therefore, far-infrared fabric is selected to seem very necessary as the daily health caring clothes of this crowd.
The fragrant body sleeping bag of the disclosed nano-selenium element important far infrared anti-electromagnetic wave teenager anion of Chinese patent CN102090819A (publication date 2011.6.15), this sleeping bag fabric is primarily of compound mixture nano-ceramic powder and cotton, fiber crops, wool, silk, brocade, polypropylene fibre viscose is formed, wherein compound mixture nano-ceramic powder comprises nanometer selenium, the dry body of organic germanium glossy ganoderma edible fungus, honeybee serial nano mixed powder, metallothionein, zinc oxide, magnesia, iron oxide, manganese oxide, silica, titanium dioxide, alundum (Al2O3), di-iron trioxide, medical stone nano powder, tourmaline nano powder, Ag-carried nanometer titanium dioxide antiseptic, sweet osmanthus, peach blossom, apricot flower, yulan magnolia, lilacs etc. are flower naturally, also containing Chinese medicine prescription, give sleeping bag fabric far infrared, anti-electromagnetic wave, anion and there is the performances such as fragrance.The disclosed a kind of chitosan health-care multicomponent knitted stretch underwear fabric of Chinese patent CN102943340A (publication date 2013.2.27), chitin viscose/Modal fibre/far-infrared viscose fiber fiber triblend yarn and spandex is adopted to be interweaved, vortex spinning, obtain having antibacterial, deodorization, stimulate circulation, pro-skin, high moisture-absorbing moisture-keeping, high resilience, degradable, softness next to the skin, smooth comfortable, good etc. without electrostatic, Nantural non-toxic, warmth retention property, be particularly suitable for women, children, old man wear, and various infant-wear.
From above-mentioned prior art, the characteristics such as fabric far infrared can be given by adding functionality ceramic powder or adding functional fiber, but mostly current functional fabric is the functional and comfortableness of simple consideration fabric, do not go from the angle of infant's special physiological feature security and the comfortableness of considering fabric, be therefore necessary to develop the applicable far infrared textile material of a kind of infant.
Summary of the invention:
The technical problem to be solved in the present invention is to provide applicable far infrared cotton fiber of a kind of infant and preparation method thereof, adopt the cotton fiber of primary hydroxy group as main raw material, at surface grafting sericin, nano-ceramic powder and sodium alginate, cotton fiber is made to have excellent far infrared performance, through repeatedly washing, still there is excellent health, and save the mechanical strength of raw cotton fiber, soft pro-skin, the good characteristic that moisture absorption is ventilative, make it the textiles being particularly suitable for making infant, for a long time infrared health is carried out to infant, improve immunity, the generation of prevention body illness.
For solving the problems of the technologies described above, technical scheme of the present invention is:
The far infrared cotton fiber that a kind of infant is suitable for, it is characterized in that, the far infrared cotton fiber that described infant is suitable for is the cotton fiber through sericin and nano ceramics modification, the far infrared cotton fiber that described infant is suitable for comprises top layer and sandwich layer, described top layer comprises sericin, nano-ceramic powder and sodium alginate, and described sandwich layer is cotton fiber.
Preferably, described cotton fiber is the cotton fiber of primary hydroxy group, and the particle diameter of described nano-ceramic powder is 500-800nm.
The preparation method of the far infrared cotton fiber that the present invention also provides a kind of infant to be suitable for, is characterized in that: comprise the following steps:
(1) by adding the bio protease of 0.5-1% in the silk gum solution obtained after natural silk degumming, at 10-20 DEG C, reacting 1-2h, taking out freeze drying, obtaining sericin polypeptide hydrolyzes product;
(2) cotton fiber is placed in gaseous nitrogen dioxide environment and lucifuge oxidation is carried out to the primary hydroxyl of cotton fiber, take out vacuum and leave standstill, obtain the cotton fiber be oxidized;
(3) sericin polypeptide hydrolyzes product prepared by step (1) is dissolved in deionization, stirs, add nano-ceramic powder and sodium alginate, stir, obtain the far infrared treatment fluid containing silk gum;
(4) cotton fiber of oxidation step (2) prepared is placed in the far infrared treatment fluid containing silk gum prepared by step (3), and dipping vibration, takes out preliminary drying and cure, washing and drying, obtaining the far infrared cotton fiber that infant is suitable for.
Preferred as technique scheme, in described step (1), bio protease is papain or serine protease.
Preferred as technique scheme, in described step (1), the pH value of silk gum solution is 8-9.
Preferred as technique scheme, in described step (1), the molecular weight of sericin polypeptide hydrolyzes product is 1200-2000Da.
Preferred as technique scheme, in described step (2), the time of lucifuge oxidation is 30-40min.
Preferred as technique scheme, in described step (3), containing the component in the far infrared treatment fluid of silk gum, by weight, comprising: sericin polypeptide hydrolyzes product 25-35 part, nano-ceramic powder 10-15 part, sodium alginate 20-40 part.
Preferred as technique scheme, in described step (4), the bath raio of dipping vibration is 1:20-30, and the time is 60-90min, and temperature is 50-60 DEG C.
Preferred as technique scheme, in described step (4), the temperature of preliminary drying is 80-90 DEG C, and the time of preliminary drying is 100min, and the temperature of curing is 140-145 DEG C, and the time of curing is 100min.
Compared with prior art, the present invention has following beneficial effect:
(1) raw material of the far infrared cotton fiber that the infant that prepared by the present invention is suitable for is the cotton fiber of primary hydroxyl modification, the main raw material of cotton fiber is cellulose, the cellulose of oxidation has good biocompatibility, biodegradability, environmental friendliness, nontoxic etc., and numerous active group is contained on the cellulosic surface after oxidation, improve the reactivity of cotton fiber, make cotton fiber can be compounded to form new product and intermediate mutually with multiple product, compared with arranging with traditional coating, it is functional will improve greatly, and water-fastness and durability also can significantly improve.Select gaseous nitrogen dioxide gas to be oxidized cotton fiber in the present invention, be swift in response thoroughly, the mechanical strength damage of the oxidized cotton fiber obtained is little, does not have chemical residue.
(2) grafting agent of the far infrared cotton fiber that the infant that prepared by the present invention is suitable for selects sericin, nano-ceramic powder and sodium alginate, the water-soluble macromolecular mass body that can form similar micella of sodium alginate, nano-ceramic powder is wherein coated, combine sericin and sodium alginate with the active group on oxidized cotton fiber surface formation chemical bond, the amino of aldehyde radical on cotton fiber in sericin strand is combined and forms chemical bond, firmly by sericin coating and cotton fiber surface, sodium ion also dissociates away by sodium alginate, be attached to the surface of cotton fiber.Therefore the surface-treated layer of far infrared cotton fiber that prepared by the present invention firmly can be attached to the surface of cotton fiber, forms stabilized zone.
(3) the far infrared cotton fiber that the infant that prepared by the present invention is suitable for improves the anti-wrinkle shrink-proof performance of cotton fiber, give excellent pro-skin performance and ceramic far infrared performance as cotton fiber silk, make cotton fiber on the basis keeping comfortable softness, air-moisture-permeable, pro-skin more, more keep healthy, and green non-pollution, meet all standard of infant textile product.
Detailed description of the invention:
Describe the present invention in detail below in conjunction with specific embodiment, be used for explaining the present invention in this illustrative examples of the present invention and explanation, but not as a limitation of the invention.
Embodiment 1:
(1) by the pH value obtained after natural silk degumming be 8 silk gum solution in add 0.5% papain, react 1h at 10 DEG C, take out freeze drying, obtain the sericin polypeptide hydrolyzes product that molecular weight is 2000Da.
(2) cotton fiber is placed in gaseous nitrogen dioxide environment and lucifuge oxidation 30min is carried out to the primary hydroxyl of cotton fiber, take out vacuum and leave standstill, obtain the cotton fiber be oxidized.
(3) by weight, the sericin polypeptide hydrolyzes product steps of 25 parts (1) prepared is dissolved in the deionization of 40 parts, stirs, adds the nano-ceramic powder of the 500nm of 10 parts and the sodium alginate of 20 parts, stir, obtain the far infrared treatment fluid containing silk gum.
(4) cotton fiber of oxidation step (2) prepared take bath raio as the far infrared treatment fluid containing silk gum that 1:20 is placed in step (3) and prepares, dipping vibration 60min at 50 DEG C, take out, 80 DEG C of preliminary drying 100min and 140 DEG C cure 100min, washing and drying, obtains the far infrared cotton fiber that infant is suitable for.
Embodiment 2:
(1) by the pH value obtained after natural silk degumming be 9 silk gum solution in add 1% serine protease, react 2h at 20 DEG C, take out freeze drying, obtain the sericin polypeptide hydrolyzes product that molecular weight is 1200Da.
(2) cotton fiber is placed in gaseous nitrogen dioxide environment and lucifuge oxidation 40min is carried out to the primary hydroxyl of cotton fiber, take out vacuum and leave standstill, obtain the cotton fiber be oxidized.
(3) by weight, the sericin polypeptide hydrolyzes product steps of 35 parts (1) prepared is dissolved in the deionization of 60 parts, stirs, adds the nano-ceramic powder of the 800nm of 15 parts and the sodium alginate of 40 parts, stir, obtain the far infrared treatment fluid containing silk gum.
(4) cotton fiber of oxidation step (2) prepared take bath raio as the far infrared treatment fluid containing silk gum that 1:30 is placed in step (3) and prepares, dipping vibration 90min at 60 DEG C, take out, 90 DEG C of preliminary drying 100min and 145 DEG C cure 100min, washing and drying, obtains the far infrared cotton fiber that infant is suitable for.
Embodiment 3:
(1) by the pH value obtained after natural silk degumming be 8.5 silk gum solution in add 0.7% papain, react 1.5h at 15 DEG C, take out freeze drying, obtain the sericin polypeptide hydrolyzes product that molecular weight is 1600Da.
(2) cotton fiber is placed in gaseous nitrogen dioxide environment and lucifuge oxidation 35min is carried out to the primary hydroxyl of cotton fiber, take out vacuum and leave standstill, obtain the cotton fiber be oxidized.
(3) by weight, the sericin polypeptide hydrolyzes product steps of 30 parts (1) prepared is dissolved in the deionization of 50 parts, stirs, adds the nano-ceramic powder of the 600nm of 12 parts and the sodium alginate of 30 parts, stir, obtain the far infrared treatment fluid containing silk gum.
(4) cotton fiber of oxidation step (2) prepared take bath raio as the far infrared treatment fluid containing silk gum that 1:25 is placed in step (3) and prepares, dipping vibration 80min at 55 DEG C, take out, 85 DEG C of preliminary drying 100min and 140 DEG C cure 100min, washing and drying, obtains the far infrared cotton fiber that infant is suitable for.
Embodiment 4:
(1) by the pH value obtained after natural silk degumming be 8.2 silk gum solution in add 0.6% serine protease, react 1.2h at 13 DEG C, take out freeze drying, obtain the sericin polypeptide hydrolyzes product that molecular weight is 1500Da.
(2) cotton fiber is placed in gaseous nitrogen dioxide environment and lucifuge oxidation 33min is carried out to the primary hydroxyl of cotton fiber, take out vacuum and leave standstill, obtain the cotton fiber be oxidized.
(3) by weight, the sericin polypeptide hydrolyzes product steps of 27 parts (1) prepared is dissolved in the deionization of 45 parts, stirs, adds the nano-ceramic powder of the 600nm of 12 parts and the sodium alginate of 25 parts, stir, obtain the far infrared treatment fluid containing silk gum.
(4) cotton fiber of oxidation step (2) prepared take bath raio as the far infrared treatment fluid containing silk gum that 1:23 is placed in step (3) and prepares, dipping vibration 70min at 53 DEG C, take out, 84 DEG C of preliminary drying 100min and 142 DEG C cure 100min, washing and drying, obtains the far infrared cotton fiber that infant is suitable for.
Embodiment 5:
(1) by the pH value obtained after natural silk degumming be 8.7 silk gum solution in add 0.8% serine protease, react 1.8h at 17 DEG C, take out freeze drying, obtain the sericin polypeptide hydrolyzes product that molecular weight is 1300Da.
(2) cotton fiber is placed in gaseous nitrogen dioxide environment and lucifuge oxidation 30-40min is carried out to the primary hydroxyl of cotton fiber, take out vacuum and leave standstill, obtain the cotton fiber be oxidized.
(3) by weight, the sericin polypeptide hydrolyzes product steps of 27 parts (1) prepared is dissolved in the deionization of 55 parts, stirs, adds the nano-ceramic powder of the 650nm of 11 parts and the sodium alginate of 35 parts, stir, obtain the far infrared treatment fluid containing silk gum.
(4) cotton fiber of oxidation step (2) prepared take bath raio as the far infrared treatment fluid containing silk gum that 1:30 is placed in step (3) and prepares, dipping vibration 60min at 60 DEG C, take out, 80 DEG C of preliminary drying 100min and 145 DEG C cure 100min, washing and drying, obtains the far infrared cotton fiber that infant is suitable for.
Embodiment 6:
(1) by the pH value obtained after natural silk degumming be 9 silk gum solution in add 1% papain, react 2h at 10 DEG C, take out freeze drying, obtain the sericin polypeptide hydrolyzes product that molecular weight is 1400Da.
(2) cotton fiber is placed in gaseous nitrogen dioxide environment and lucifuge oxidation 40min is carried out to the primary hydroxyl of cotton fiber, take out vacuum and leave standstill, obtain the cotton fiber be oxidized.
(3) by weight, the sericin polypeptide hydrolyzes product steps of 35 parts (1) prepared is dissolved in the deionization of 60 parts, stirs, adds the nano-ceramic powder of the 700nm of 10 parts and the sodium alginate of 40 parts, stir, obtain the far infrared treatment fluid containing silk gum.
(4) cotton fiber of oxidation step (2) prepared take bath raio as the far infrared treatment fluid containing silk gum that 1:30 is placed in step (3) and prepares, dipping vibration 90min at 50 DEG C, take out, 90 DEG C of preliminary drying 100min and 140 DEG C cure 100min, washing and drying, obtains the far infrared cotton fiber that infant is suitable for.
After testing, the result of the mechanical strength of the far infrared cotton fiber that the infant that prepared by embodiment 1-6 is suitable for, far infrared performance, moisture permeability is as follows:
As seen from the above table, the far infrared cotton fiber mechanical strength that infant prepared by the present invention is suitable for, sucting wet air permeability are good, and far infrared transmissivity is high, and wash durability is good, and the fiber after 100 washings still has excellent far infrared transmission performance.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.
Claims (10)
1. the new far infrared cotton fiber that an infant is applicable, it is characterized in that, the far infrared cotton fiber that described infant is suitable for is the cotton fiber through sericin and nano ceramics modification, the far infrared cotton fiber that described infant is suitable for comprises top layer and sandwich layer, described top layer comprises sericin, nano-ceramic powder and sodium alginate, and described sandwich layer is cotton fiber.
2. the new far infrared cotton fiber that a kind of infant according to claim 1 is applicable, it is characterized in that, described cotton fiber is the cotton fiber of primary hydroxy group, and the particle diameter of described nano-ceramic powder is 500-800nm.
3. the preparation method of new far infrared cotton fiber that is suitable for of infant, is characterized in that: comprise the following steps:
(1) by adding the bio protease of 0.5-1% in the silk gum solution obtained after natural silk degumming, at 10-20 DEG C, reacting 1-2h, taking out freeze drying, obtaining sericin polypeptide hydrolyzes product;
(2) cotton fiber is placed in gaseous nitrogen dioxide environment and lucifuge oxidation is carried out to the primary hydroxyl of cotton fiber, take out vacuum and leave standstill, obtain the cotton fiber be oxidized;
(3) sericin polypeptide hydrolyzes product prepared by step (1) is dissolved in deionization, stirs, add nano-ceramic powder and sodium alginate, stir, obtain the far infrared treatment fluid containing silk gum;
(4) cotton fiber of oxidation step (2) prepared is placed in the far infrared treatment fluid containing silk gum prepared by step (3), and dipping vibration, takes out preliminary drying and cure, washing and drying, obtaining the far infrared cotton fiber that infant is suitable for.
4. the preparation method of new far infrared cotton fiber that is suitable for of a kind of infant according to claim 3, it is characterized in that: in described step (1), bio protease is papain or serine protease.
5. the preparation method of new far infrared cotton fiber that is suitable for of a kind of infant according to claim 3, it is characterized in that: in described step (1), the pH value of silk gum solution is 8-9.
6. the preparation method of new far infrared cotton fiber that is suitable for of a kind of infant according to claim 3, it is characterized in that: in described step (1), the molecular weight of sericin polypeptide hydrolyzes product is 1200-2000Da.
7. the preparation method of far infrared cotton fiber that is suitable for of a kind of infant according to claim 3, it is characterized in that: in described step (2), the time of lucifuge oxidation is 30-40min.
8. the preparation method of far infrared cotton fiber that is suitable for of a kind of infant according to claim 3, it is characterized in that: in described step (3), containing the component in the far infrared treatment fluid of silk gum, by weight, comprising: sericin polypeptide hydrolyzes product 25-35 part, nano-ceramic powder 10-15 part, sodium alginate 20-40 part.
9. the preparation method of far infrared cotton fiber that is suitable for of a kind of infant according to claim 3, it is characterized in that: in described step (4), the bath raio of dipping vibration is 1:20-30, and the time is 60-90min, and temperature is 50-60 DEG C.
10. the preparation method of far infrared cotton fiber that is suitable for of a kind of infant according to claim 3, it is characterized in that: in described step (4), the temperature of preliminary drying is 80-90 DEG C, and the time of preliminary drying is 100min, the temperature of curing is 140-145 DEG C, and the time of curing is 100min.
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Cited By (5)
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| CN106758228A (en) * | 2016-11-24 | 2017-05-31 | 江苏爱西施科技服务咨询股份有限公司 | A kind of anti-ultraviolet dressing liquid of raising textile containing modified sericin and preparation method thereof |
| CN107476052A (en) * | 2017-07-25 | 2017-12-15 | 海盐派特普科技有限公司 | A kind of processing method of non-ironing underlinen fabric |
| CN107557905A (en) * | 2017-08-24 | 2018-01-09 | 海盐派特普科技有限公司 | A kind of down jackets anti-static ventilation eider down and preparation method thereof |
| CN107630358A (en) * | 2017-07-25 | 2018-01-26 | 海盐派特普科技有限公司 | A kind of processing technology of western-style clothes Anti-wrinkle fabric |
| CN113584890A (en) * | 2021-06-18 | 2021-11-02 | 吴江市南麻恒兴丝织厂 | Preparation method of anti-wrinkle wool fabric |
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