CN105213203A - A kind of preparation method of microcapsule-type moisturizing eye cream - Google Patents
A kind of preparation method of microcapsule-type moisturizing eye cream Download PDFInfo
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- CN105213203A CN105213203A CN201510721537.1A CN201510721537A CN105213203A CN 105213203 A CN105213203 A CN 105213203A CN 201510721537 A CN201510721537 A CN 201510721537A CN 105213203 A CN105213203 A CN 105213203A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
The present invention discloses a kind of preparation method of microcapsule-type moisturizing eye cream, with potassium alginate, sodium hydroxyethyl cellulose, hyaluronic acid, mink oil, squalane, lecithin, Jojoba wax, glycerol, batilol, serine, Maninot esculenta crantz. porous-starch, bupleurumol extract, Semen Coicis ethanol extract, Radix Paeoniae Alba ethanol extract, Dendrobium nobile ethanol extract, coenzyme Q10 and polysorbate60 are raw material, first prepare capsule wall solution A and capsule-core mixture B, by first dispersed with stirring homogenizing again after A and B mixing, obtain homogenizing fluid C, homogenizing fluid C is instilled in calcium chloride solution, wash after filtration, obtain described moisturizing eye cream.The microcapsule-type moisturizing eye cream that the present invention obtains can make to be adsorbed on active component in Maninot esculenta crantz. porous-starch in use and oils and fats slowly evenly discharges, and can not discharge in a large number the short time and bring too much nutrition and oil content to skin, and then can not cause the generation of fat granule, and the present invention also has the feature of good penetrability.
Description
Technical field
The invention belongs to microcapsule technology field, be specifically related to a kind of preparation method of microcapsule-type moisturizing eye cream.
Background technology
Eye skin is the thinnest skin of human body, is again activity position the most frequently simultaneously, but also is pull the maximum place of skin number of times in making up, and is very easy to grow wrinkle.The FAQs of eye has following several: black eye, eye pouch, edema, microgroove, dry stricture of vagina, crows-feet, fat granule, eyes lack expression etc., and these eye problems, once occur, are easy to make people seem aged without god.Eye cream is one of skin type product, and it can moisten eye part skin, alleviates the generation of wrinkle, microgroove, effectively prevents the generation of black eye, eye pouch problem, totally plays the effect alleviating eye part skin aging.Based on above-mentioned effect of eye cream, the personage that more and more likes to be beautiful using eye cream as one of daily indispensable skin care item.
If but the eye cream used is improper, also can bring certain harmful effect to eye skin.As most higher containing lubricant component in existing eye cream, contained neutraceutical active ingredients discharges too fast and is not easily absorbed, these oils and fatss or nutritional labeling are deposited on eye part skin, be easy to the generation causing fat granule for a long time in the past, fat granule, once produce elimination in the very difficult short time, can not be despised on the impact that eye part skin causes; If but the eye cream using quality comparatively frivolous, the moist degree of eye cream can be made again to decline, do not reach good maintenance effect.Moreover; the active substance adopted in existing eye cream is most not through certain protection, and directly contacts with external environment, along with the prolongation of time; these active substances be easy to be oxidized by the external world, photodissociation and lose the activity that should possess, and then cause product failure.
Summary of the invention
For prior art above shortcomings, technical problem to be solved by this invention is: the preparation method how providing a kind of microcapsule-type moisturizing eye cream, the product Middle nutrition active component making the method obtained evenly can discharge in use and be easy to absorb, have nourish effective, can not cause that fat granule produces, active substance is not easily by feature that external environment is destroyed.
In order to solve the problems of the technologies described above, the present invention adopts following technical scheme: a kind of preparation method of microcapsule-type moisturizing eye cream, comprises the steps:
1) material of following weight portion is taken: 55 ~ 60 parts of potassium alginates, 12 ~ 18 parts of sodium hydroxyethyl cellulose, 4 ~ 8 parts of hyaluronic acids, 16 ~ 22 parts of mink oils, 6 ~ 14 parts of squalanes, 4 ~ 8 parts of lecithin, 6 ~ 8 parts of Jojoba waxes, 10 ~ 12 parts of glycerol, 6 ~ 10 parts of batilols, 2 ~ 4 parts of serines, 8 ~ 10 parts of Maninot esculenta crantz. porous-starchs, 2 ~ 4 parts of bupleurumol extracts, 3 ~ 4 parts of Semen Coicis ethanol extract, 2 ~ 3 parts of Radix Paeoniae Alba ethanol extract, 1.5 ~ 2 parts of Dendrobium nobile ethanol extract, 1 ~ 4 part of coenzyme Q10 and 3 ~ 8 parts of polysorbate60s,
2) add in deionized water by the potassium alginate taken, sodium hydroxyethyl cellulose and hyaluronic acid, at 60 ~ 75 DEG C, Ultrasonic Heating dissolves 3 ~ 5min, obtains capsule wall solution A; Wherein, the deionized water volume added is 45 ~ 50 times of potassium alginate, sodium hydroxyethyl cellulose and hyaluronic acid gross mass; Ultrasonic power is 350 ~ 400W;
3) mink oil, squalane, lecithin, Jojoba wax, glycerol, batilol, serine, Maninot esculenta crantz. porous-starch, bupleurumol extract, Semen Coicis ethanol extract, Radix Paeoniae Alba ethanol extract, Dendrobium nobile ethanol extract, coenzyme Q10 and the surfactant mix homogeneously that will take, under 60 ~ 80 DEG C of water bath condition, stir 0.5 ~ 1h, obtain capsule-core mixture B; The mixing speed of wherein said stirring is 200 ~ 250r/min;
4) mixed by capsule wall solution A and capsule-core mixture B, after blender dispersion 15 ~ 20min, homogenizing 3 ~ 8min, obtains homogenizing fluid C; Wherein, the rotating speed of described blender is 250 ~ 320r/min, and the homogenization pressure of described homogenizing is 40 ~ 50MPa;
5) homogenizing fluid C is heated to 80 ~ 85 DEG C, using glue head dropper homogenizing fluid C to be slowly added dropwise to mass concentration is in the calcium chloride solution of 3% ~ 6%;
6) calcium chloride solution after step 5) instillation homogenizing fluid C is filtered, discard filtrate, collect oversize;
7) to the oversize deionized water wash 2 ~ 3 times that step 6) is collected, the moisturizing eye cream of described microcapsule-type is obtained.
Compared to existing technology, the present invention has following beneficial effect:
1, the present invention adopts Maninot esculenta crantz. porous-starch, lubricant component in core materials and active component are adsorbed, and then the microcapsule-type moisturizing eye cream making the method obtain can make to be adsorbed on active component in Maninot esculenta crantz. porous-starch in use and oils and fats slowly evenly discharges, and can not discharge in a large number the short time and bring too much nutrition and oil content to skin, and then the generation of fat granule can not be caused.
2, in order to strengthen the permeability of the microcapsule-type moisturizing eye cream that the inventive method obtains, the present invention is special by a large amount of experimental studies, choose mink oil, squalane, Jojoba wax, batilol is as core materials, and the collaborative compatibility relationship that further study between a few person, final discovery is when using " 16 ~ 22 parts of mink oils, 6 ~ 14 parts of squalanes, 6 ~ 8 parts of Jojoba waxes and 6 ~ 10 parts of batilols " time, the moist degree of this product can either be ensured, again can not be too greasy, and what is more important is when this several material plays collaborative compatibility effect with this ratio, the permeability of this product can be strengthened, and then enable skin fully absorb nutritional labeling, import respond well.
3, the present invention adopts microcapsule technology, neutraceutical active ingredients embedding is got up, makes this product in use, can not the impact that in external environment, light, heat, oxygen etc. are too much be subject to, effectively ensure that the activity of active substance is not destroyed, the effect extending product keeps the phase.
4, the present invention adopts active skull cap components as nutrient, and this several natural materials is carried out composite, them are made farthest to play collaborative compatibility effect, the preparation method of giving microcapsule-type moisturizing eye cream of the present invention with moisturizing, eliminate bubble eye, alleviate black-eyed associating effect, and Dendrobium nobile ethanol extract also has good antioxidation, effectively stop light, ultraviolet to the damage of skin.
5, cyst wall hydrogel material of the present invention brings certain water moisture feeling to this product, and hyaluronic interpolation further increases the performance of keeping humidity of product, make this product in use, it is easier that eye part skin is pushed open, only need massage gently with finger and get final product uniform application, use convenient, the overnutrition at this position will be made to cause fat granule because product is deposited in a certain position of eye part skin.
6, shape of product of the present invention is regular, cyst wall has uniform thickness, and has uniform intensity, can retain the perfect shape of microcapsule and not be destroyed, the problem that capsule-core is revealed can not be caused, can not be damaged during effectively ensureing product stock, transport, shelf life.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, in the present embodiment if no special instructions, raw materials used be commercially available.
Described bupleurumol extract, Semen Coicis ethanol extract, Radix Paeoniae Alba ethanol extract, Dendrobium nobile ethanol extract are after the ethanol water of employing 60% carries out alcohol extraction to Radix Bupleuri, Semen Coicis, the Radix Paeoniae Alba and Dendrobium nobile respectively, successively the extract that obtains of decompression recycling ethanol, lyophilization.
Embodiment 1:
The present embodiment microcapsule-type moisturizing eye cream is a kind of microcapsule of nucleocapsid structure, and cyst material is: 55 parts of potassium alginates, 12 parts of sodium hydroxyethyl cellulose and 4 parts of hyaluronic acids; Core materials is: 16 parts of mink oils, 6 parts of squalanes, 4 parts of lecithin, 6 parts of Jojoba waxes, 10 parts of glycerol, 6 parts of batilols, 2 parts of serines, 8 parts of Maninot esculenta crantz. porous-starchs, 2 parts of bupleurumol extracts, 3 parts of Semen Coicis ethanol extract, 2 parts of Radix Paeoniae Alba ethanol extract, 1.5 parts of Dendrobium nobile ethanol extract, 1 part of coenzyme Q10 and 3 parts of polysorbate60s.
Adopt and prepare with the following method and obtain:
1) material of above-mentioned weight portion is taken;
2) add in deionized water by the potassium alginate taken, sodium hydroxyethyl cellulose and hyaluronic acid, at 60 DEG C, Ultrasonic Heating dissolves 3min, obtains capsule wall solution A; Wherein, the deionized water volume added is 45 times of potassium alginate, sodium hydroxyethyl cellulose and hyaluronic acid gross mass; Ultrasonic power is 350W;
3) mink oil, squalane, lecithin, Jojoba wax, glycerol, batilol, serine, Maninot esculenta crantz. porous-starch, bupleurumol extract, Semen Coicis ethanol extract, Radix Paeoniae Alba ethanol extract, Dendrobium nobile ethanol extract, coenzyme Q10 and the surfactant mix homogeneously that will take, under 60 DEG C of water bath condition, stir 0.5h, obtain capsule-core mixture B; The mixing speed of wherein said stirring is 200r/min;
4) mixed by capsule wall solution A and capsule-core mixture B, after blender dispersion 15min, homogenizing 3min, obtains homogenizing fluid C; Wherein, the rotating speed of described blender is 250r/min, and the homogenization pressure of described homogenizing is 40MPa;
5) homogenizing fluid C is heated to 80 DEG C, using glue head dropper homogenizing fluid C to be slowly added dropwise to mass concentration is in the calcium chloride solution of 3%;
6) calcium chloride solution after step 5) instillation homogenizing fluid C is filtered, discard filtrate, collect oversize;
7) to the oversize deionized water wash 2 ~ 3 times that step 6) is collected, the moisturizing eye cream of described microcapsule-type is obtained.
Embodiment 2:
The present embodiment microcapsule-type moisturizing eye cream is a kind of microcapsule of nucleocapsid structure, and cyst material is: 60 parts of potassium alginates, 18 parts of sodium hydroxyethyl cellulose and 8 parts of hyaluronic acids; Core materials is: 22 parts of mink oils, 14 parts of squalanes, 8 parts of lecithin, 8 parts of Jojoba waxes, 12 parts of glycerol, 10 parts of batilols, 4 parts of serines, 10 parts of Maninot esculenta crantz. porous-starchs, 4 parts of bupleurumol extracts, 4 parts of Semen Coicis ethanol extract, 3 parts of Radix Paeoniae Alba ethanol extract, 2 parts of Dendrobium nobile ethanol extract, 4 parts of coenzyme Q10s and 8 parts of polysorbate60s.
Adopt and prepare with the following method and obtain:
1) material of above-mentioned weight portion is taken;
2) add in deionized water by the potassium alginate taken, sodium hydroxyethyl cellulose and hyaluronic acid, at 75 DEG C, Ultrasonic Heating dissolves 5min, obtains capsule wall solution A; Wherein, the deionized water volume added is 50 times of potassium alginate, sodium hydroxyethyl cellulose and hyaluronic acid gross mass; Ultrasonic power is 400W;
3) mink oil, squalane, lecithin, Jojoba wax, glycerol, batilol, serine, Maninot esculenta crantz. porous-starch, bupleurumol extract, Semen Coicis ethanol extract, Radix Paeoniae Alba ethanol extract, Dendrobium nobile ethanol extract, coenzyme Q10 and the surfactant mix homogeneously that will take, under 80 DEG C of water bath condition, stir 1h, obtain capsule-core mixture B; The mixing speed of wherein said stirring is 250r/min;
4) mixed by capsule wall solution A and capsule-core mixture B, after blender dispersion 20min, homogenizing 8min, obtains homogenizing fluid C; Wherein, the rotating speed of described blender is 320r/min, and the homogenization pressure of described homogenizing is 50MPa;
5) homogenizing fluid C is heated to 85 DEG C, using glue head dropper homogenizing fluid C to be slowly added dropwise to mass concentration is in the calcium chloride solution of 6%;
6) calcium chloride solution after step 5) instillation homogenizing fluid C is filtered, discard filtrate, collect oversize;
7) to the oversize deionized water wash 2 ~ 3 times that step 6) is collected, the moisturizing eye cream of described microcapsule-type is obtained.
Embodiment 3:
The present embodiment microcapsule-type moisturizing eye cream is a kind of microcapsule of nucleocapsid structure, and cyst material is: 58 parts of potassium alginates, 16 parts of sodium hydroxyethyl cellulose and 6 parts of hyaluronic acids; Core materials is: 20 parts of mink oils, 10 parts of squalanes, 6 parts of lecithin, 8 parts of Jojoba waxes, 12 parts of glycerol, 8 parts of batilols, 4 parts of serines, 10 parts of Maninot esculenta crantz. porous-starchs, 4 parts of bupleurumol extracts, 4 parts of Semen Coicis ethanol extract, 2 parts of Radix Paeoniae Alba ethanol extract, 1.5 parts of Dendrobium nobile ethanol extract, 3 parts of coenzyme Q10s and 6 parts of polysorbate60s.
Adopt and prepare with the following method and obtain:
1) material of above-mentioned weight portion is taken;
2) add in deionized water by the potassium alginate taken, sodium hydroxyethyl cellulose and hyaluronic acid, at 75 DEG C, Ultrasonic Heating dissolves 5min, obtains capsule wall solution A; Wherein, the deionized water volume added is 50 times of potassium alginate, sodium hydroxyethyl cellulose and hyaluronic acid gross mass; Ultrasonic power is 400W;
3) mink oil, squalane, lecithin, Jojoba wax, glycerol, batilol, serine, Maninot esculenta crantz. porous-starch, bupleurumol extract, Semen Coicis ethanol extract, Radix Paeoniae Alba ethanol extract, Dendrobium nobile ethanol extract, coenzyme Q10 and the surfactant mix homogeneously that will take, under 70 DEG C of water bath condition, stir 1h, obtain capsule-core mixture B; The mixing speed of wherein said stirring is 230r/min;
4) mixed by capsule wall solution A and capsule-core mixture B, after blender dispersion 18min, homogenizing 5min, obtains homogenizing fluid C; Wherein, the rotating speed of described blender is 300r/min, and the homogenization pressure of described homogenizing is 45MPa;
5) homogenizing fluid C is heated to 80 ~ 85 DEG C, using glue head dropper homogenizing fluid C to be slowly added dropwise to mass concentration is in the calcium chloride solution of 6%;
6) calcium chloride solution after step 5) instillation homogenizing fluid C is filtered, discard filtrate, collect oversize;
7) to the oversize deionized water wash 2 ~ 3 times that step 6) is collected, the moisturizing eye cream of described microcapsule-type is obtained.
The present invention adopts Maninot esculenta crantz. porous-starch, lubricant component in core materials and active component are adsorbed, and then the microcapsule-type moisturizing eye cream making the present invention obtain in use, can make to be adsorbed on active component in Maninot esculenta crantz. porous-starch and oils and fats slowly evenly discharges, and can not discharge in a large number the short time and bring too much nutrition and oil content to skin, and then the generation of fat granule can not be caused.
In order to strengthen the permeability of the microcapsule-type moisturizing eye cream that the present invention obtains, the present invention is special by a large amount of experimental studies, choose mink oil, squalane, Jojoba wax, batilol is as core materials, and the collaborative compatibility relationship that further study between three, final discovery is when using " 16 ~ 22 parts of mink oils, 6 ~ 14 parts of squalanes, 6 ~ 8 parts of Jojoba waxes and 6 ~ 10 parts of batilols " time, the moist degree of this product can either be ensured, again can not be too greasy, and what is more important is when this several material plays collaborative compatibility effect with this ratio, the permeability of this product can be strengthened, and then enable skin fully absorb nutritional labeling, import respond well.
What finally illustrate is, above embodiment is only in order to illustrate technical scheme of the present invention and unrestricted, although applicant's reference preferred embodiment is to invention has been detailed description, those of ordinary skill in the art is to be understood that, technical scheme of the present invention is modified or equivalent replacement, and do not depart from the aim of technical solution of the present invention and scope, all should be encompassed in the middle of right of the present invention.
Claims (5)
1. a preparation method for microcapsule-type moisturizing eye cream, is characterized in that, comprises the steps:
1) material of following weight portion is taken: 55 ~ 60 parts of potassium alginates, 12 ~ 18 parts of sodium hydroxyethyl cellulose, 4 ~ 8 parts of hyaluronic acids, 16 ~ 22 parts of mink oils, 6 ~ 14 parts of squalanes, 4 ~ 8 parts of lecithin, 6 ~ 8 parts of Jojoba waxes, 10 ~ 12 parts of glycerol, 6 ~ 10 parts of batilols, 2 ~ 4 parts of serines, 8 ~ 10 parts of Maninot esculenta crantz. porous-starchs, 2 ~ 4 parts of bupleurumol extracts, 3 ~ 4 parts of Semen Coicis ethanol extract, 2 ~ 3 parts of Radix Paeoniae Alba ethanol extract, 1.5 ~ 2 parts of Dendrobium nobile ethanol extract, 1 ~ 4 part of coenzyme Q10 and 3 ~ 8 parts of polysorbate60s,
2) add in deionized water by the potassium alginate taken, sodium hydroxyethyl cellulose and hyaluronic acid, at 60 ~ 75 DEG C, Ultrasonic Heating dissolves 3 ~ 5min, obtains capsule wall solution A; Wherein, the deionized water volume added is 45 ~ 50 times of potassium alginate, sodium hydroxyethyl cellulose and hyaluronic acid gross mass; Ultrasonic power is 350 ~ 400W;
3) mink oil, squalane, lecithin, Jojoba wax, glycerol, batilol, serine, Maninot esculenta crantz. porous-starch, bupleurumol extract, Semen Coicis ethanol extract, Radix Paeoniae Alba ethanol extract, Dendrobium nobile ethanol extract, coenzyme Q10 and the surfactant mix homogeneously that will take, under 60 ~ 80 DEG C of water bath condition, stir 0.5 ~ 1h, obtain capsule-core mixture B; The mixing speed of wherein said stirring is 200 ~ 250r/min;
4) mixed by capsule wall solution A and capsule-core mixture B, after blender dispersion 15 ~ 20min, homogenizing 3 ~ 8min, obtains homogenizing fluid C; Wherein, the rotating speed of described blender is 250 ~ 320r/min, and the homogenization pressure of described homogenizing is 40 ~ 50MPa;
5) homogenizing fluid C is heated to 80 ~ 85 DEG C, using glue head dropper homogenizing fluid C to be slowly added dropwise to mass concentration is in the calcium chloride solution of 3% ~ 6%;
6) calcium chloride solution after step 5) instillation homogenizing fluid C is filtered, discard filtrate, collect oversize;
7) to the oversize deionized water wash 2 ~ 3 times that step 6) is collected, the moisturizing eye cream of described microcapsule-type is obtained.
2. the preparation method of microcapsule-type moisturizing eye cream according to claim 1, is characterized in that, step 2) described in ultrasonic power be 400W.
3. the preparation method of microcapsule-type moisturizing eye cream according to claim 1, it is characterized in that, mixing speed described in step 3) is 230r/min.
4. the preparation method of microcapsule-type moisturizing eye cream according to claim 1, is characterized in that, with after blender dispersion 18min in step 4), and homogenizing 5min.
5. the preparation method of microcapsule-type moisturizing eye cream according to claim 1, it is characterized in that, the rotating speed of blender described in step 4) is 300r/min, and the homogenization pressure of described homogenizing is 45MPa.
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| CN201510721537.1A CN105213203A (en) | 2015-10-30 | 2015-10-30 | A kind of preparation method of microcapsule-type moisturizing eye cream |
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| CN201510721537.1A CN105213203A (en) | 2015-10-30 | 2015-10-30 | A kind of preparation method of microcapsule-type moisturizing eye cream |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107714614A (en) * | 2017-11-21 | 2018-02-23 | 常州市蓝勖化工有限公司 | A kind of preparation method of anti-wrinkle eye cream |
| CN111296839A (en) * | 2020-03-25 | 2020-06-19 | 华熙生物科技股份有限公司 | Health-care water ball for improving osteoarthritis, preparation method and application thereof |
| WO2023037900A1 (en) * | 2021-09-10 | 2023-03-16 | 株式会社 資生堂 | Capsuled cosmetic material |
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| CN103202469A (en) * | 2013-03-28 | 2013-07-17 | 吉林大学 | Egg yolk lecithin microcapsules and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107714614A (en) * | 2017-11-21 | 2018-02-23 | 常州市蓝勖化工有限公司 | A kind of preparation method of anti-wrinkle eye cream |
| CN111296839A (en) * | 2020-03-25 | 2020-06-19 | 华熙生物科技股份有限公司 | Health-care water ball for improving osteoarthritis, preparation method and application thereof |
| WO2023037900A1 (en) * | 2021-09-10 | 2023-03-16 | 株式会社 資生堂 | Capsuled cosmetic material |
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Application publication date: 20160106 |