CN105168056A - Shower gel including folium artemisiae argyi - Google Patents
Shower gel including folium artemisiae argyi Download PDFInfo
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- CN105168056A CN105168056A CN201510613618.XA CN201510613618A CN105168056A CN 105168056 A CN105168056 A CN 105168056A CN 201510613618 A CN201510613618 A CN 201510613618A CN 105168056 A CN105168056 A CN 105168056A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The invention discloses shower gel including folium artemisiae argyi. The shower gel is prepared from, by weight, 0.1-10 parts of folium artemisiae argyi extract, 1-10 parts of lauryl amphoteric sodium acetate, 2-15 parts of AES, 0.1-1 part of EDTA-4Na, 1-10 parts of glycine betaine, 1-3 parts of cocamidopropyl dimethylamine oxide, 0.1-5 parts of sodium chloride, 0.1-1 part of citric acid, 0.1-1 part of folium artemisiae argyi essence and 100 parts of deionized water. The shower gel including the folium artemisiae argyi has the effects of carrying out cleaning, restraining bacteria, improving the immunocompetence of females, relieving menstrual period symptoms and the like.
Description
Technical field
The present invention relates to health care daily necessities chemical field.More particularly, the present invention relates to a kind of Folium Artemisiae Argyi bath gel.
Background technology
Folium Artemisiae Argyi, as traditional Chinese medical science good medicine, has blood of regulating the flow of vital energy, by effects such as cold-damp, antiabortive, antibacterial, antiviral, hemostasis and anticoagulation, increase immunocompetence, antipyretic calmness, clinically, Folium Artemisiae Argyi is widely used in treating gynaecopathia, respiratory tract disease.Because of the multiple effectiveness that it has, Folium Artemisiae Argyi is widely used in bath product, and the compatibilities such as many and Ramulus Mori, the Radix Angelicae Dahuricae, Rhizoma Alpiniae Officinarum, Radix Puerariae, Herba Menthae work effects such as preventing and treating dermatosis, deodorization, relieve muscle spasms, improving water flood.
Along with the raising of people's living standard, a lot of "smart" products result in the poverty of movement of human organism, body constitution is deteriorated, especially women, operating pressure, stay up late, long-term sitting, endocrine disturbance, cause the gynaecopathias such as female menstrual disorder, abdominal pain in menstruation, menses blackout, the functions such as general bath product is, skin moistening clean for skin, deodorization carry out researching and developing and selling, but but rarely have symptoms such as can alleviating female menstrual period imbalance stomachache, improve the bath gel product of female body immunity.Further, female menstrual period resistance is poor, easily causes courses of infection, and skin is responsive, and a lot of bath gel product has certain chemical stimulation, can not well for consumer.
Summary of the invention
An object of the present invention is to solve at least the problems referred to above, and the advantage will illustrated at least is below provided.
A further object of the invention is to provide a kind of Folium Artemisiae Argyi bath gel, has clean, antibacterial, raising women immunocompetence, alleviates the effects such as menstrual symptoms.
A further object of the invention is that raising is a kind of by adding Folium Artemisiae Argyi bath gel prepared by Fructus Litchi ferment extracting solution of the present invention, and life-time service can improve the gynaecopathias such as consumer's menoxenia.
In order to realize according to these objects of the present invention and other advantage, provide a kind of Folium Artemisiae Argyi bath gel, comprise the following raw material with parts by weight: Folium Artemisiae Argyi extract 0.1-10 part, lauryl both sexes sodium acetate 1-10 part, AES2-15 part, EDTA-4Na0.1-1 part, betanin 1-10 part, cocamidopropyl propyl amide amine oxide 1-3 part, sodium chloride 0.1-5 part, citric acid 0.1-1 part, Folium Artemisiae Argyi essence 0.1-1 part and deionized water 100 parts.
Preferably, described Folium Artemisiae Argyi bath gel, comprises the following raw material with parts by weight: Folium Artemisiae Argyi extract 6 parts, lauryl both sexes sodium acetate 4 parts, AES6 part, EDTA-4Na0.5 part, betanin 4 parts, cocamidopropyl propyl amide amine oxide 2 parts, 2 parts, sodium chloride, citric acid 0.5 part, 0.2 part, Folium Artemisiae Argyi essence and deionized water 100 parts.
Present invention also offers a kind of technical scheme:
A preparation method for Folium Artemisiae Argyi bath gel, comprises the following steps:
Step one, the deionized water of above-mentioned weight portion is heated to 65-70 DEG C inserts in reactor, then the Folium Artemisiae Argyi extract of above-mentioned weight portion is added in reactor, stir 10-15min with the rotating speed of 20-25r/min;
Step 2, the AES then adding above-mentioned weight portion, lauryl both sexes sodium acetate and EDTA-4Na, stir 30-40min with the rotating speed of 15r/min;
Step 3, the cocamidopropyl propyl amide amine oxide adding above-mentioned weight portion again and betanin, stir 15-20min with the rotating speed of 25r/min;
Step 4, add the sodium chloride of above-mentioned weight portion, stir 10-20min with the rotating speed of 10r/min again, be cooled to rapidly less than 45 DEG C, add citric acid and the Folium Artemisiae Argyi essence of above-mentioned weight portion, stir 20-30min with the rotating speed of 35-40r/min again, after 180 mesh filter screens filter, obtain first product bath gel.
Preferably, the preparation method of described Folium Artemisiae Argyi bath gel, the preparation method of described Folium Artemisiae Argyi extract is as follows:
A1, fresh Folium Artemisiae Argyi is placed in 80 DEG C of hot water soaks 8-10min, take out Folium Artemisiae Argyi, obtain first liquid, for subsequent use,
A2, again that described Folium Artemisiae Argyi is broken, the volume fraction adding its 5 times of weight is the alcoholic solution of 70%, heating and refluxing extraction 2 times, and the extracting solution merging 2 times obtains second liquid, and the filtering residue merging 2 times obtains the first filtering residue, for subsequent use;
A3, by the first filtering residue by its quality inoculation bacillus subtilis of the 0.3% and Lactococcus of 0.1%, in room temperature bottom fermentation 15-20 days, add ethyl acetate by 3 of its weight times after sterilizing and soak, backflow is collected, and obtains the 3rd liquid;
A4, by concentrated after first liquid, second liquid and the 3rd liquid mixing and spraying dry, pulverize and sieve 200 orders afterwards, obtain described Folium Artemisiae Argyi extract.
Preferably, the preparation method of described Folium Artemisiae Argyi bath gel, adds the Fructus Litchi ferment extracting solution of 3-4 weight portion after being also included in step one, stir 30min with the rotating speed of 35r/min, wherein, the preparation method of described Fructus Litchi ferment is as follows:
S1, get 32-42 weight portion Exocarpium Litchi and 5-8 weight portion Semen Litchi pulverizes rear mistake 40 mesh sieve, mixing respectively, add the Sucus Zingberis of 12-15 weight portion and the parched rice-bran of 10-12 weight portion, the first mixture is obtained after mixing, for subsequent use, described Sucus Zingberis is Rhizoma Zingiberis Recens and pure water according to mass ratio is to obtain at 1: 30, described parched rice-bran be Testa oryzae at 100-120 DEG C in rotary frying pan parch 15-20min obtain;
S2, fermenter inner surface will spray the nano-silver water solution that mass fraction is 0.02%, described first mixture is added after 30min, add the rice wine wine with dregs of 5-8 weight portion and the Fructus Jujubae of 3-5 weight portion again, the second mixture is obtained after mixing, probiotic bacteria is inoculated by the 0.2%-0.4% of described second mixture weight, airtight described fermenter, ferments and obtains the first tunning in 3-5 days;
Described probiotic bacteria is to form at 1.2: 1 by bacillus subtilis and bacillus bifidus according to mass ratio, and described Fructus Jujubae is that after fresh Chinese dates enucleation, fragmentation obtains;
S3, by broken after 3-5 weight portion Herba Leonuri, 2-3 weight portion Fructus Solani melongenae root, 2-3 weight portion Caulis Spatholobi, the 1 weight portion Radix Astragali, 1 weight portion Rhizoma Chuanxiong, 1.5 weight portion Radix Bupleuri, 0.5 weight portion Fructus Forsythiae, 1.8 weight portion Radix rosae multifloraes and the mixing of 2 weight portion Radix Schefflerae Arboricolae (Caulis et Folium Schefflerae Arboricolae)s, add 100 parts by weight of purified water, be placed in infusion 1h under slow fire, filter to obtain the first filtrate and the second filtering residue, for subsequent use;
S4, add the second filtering residue from charging aperture, airtight described charging aperture after mixing with the first tunning, continue fermentation 2 days the second tunning;
S5, by the germinated brown rice plasm of 2-4 weight portion Plumula Nelumbinis, 0.5 weight portion Herba Schizonepetae, 1 weight portion spirulina and 5 weight portions mixing after grind, add from charging aperture, airtight after mixing with the second tunning, continue fermentation after 4-5 days the 3rd tunning, the sprout brown rice of described germinated brown rice plasm to be fructus zizaniae caduciflorae be raw material is that 1: 3 defibrination obtains with removing pure water according to mass ratio;
S6, the 3rd tunning to be cooled after microwave sterilizating, filter 100 mesh sieves, obtain Fructus Litchi ferment extracting solution.
Preferably, the preparation method of described Folium Artemisiae Argyi bath gel, also comprises:
Step 5, described first product bath gel is placed in hydrostatic column, at interval of 24h with the rotational speed hydrostatic column 10min of 5r/min, takes out after 7-10 days, after 240 mesh filter screens filter Folium Artemisiae Argyi bath gel; Wherein,
Described hydrostatic column is the bamboo making that inner hollow diameter reaches more than 20cm, its closed at both ends, bamboo sidewall offers charging aperture, and hinged sealing cover body is set, described hydrostatic column two ends connect a rotating shaft respectively, and removably connected by rotating shaft and bracing frame, described rotating shaft connects motor and rotates to control described hydrostatic column.
Preferably, the preparation method of described Folium Artemisiae Argyi bath gel, described fermenter comprises:
Stack shell, it is cylindrical, and described stack shell is the lower seal of the bamboo making that internal diameter is greater than 30cm, described stack shell;
Bung, it is hinged on the top of described stack shell, described bung is provided with charging aperture, it extends to form the underfeed of falling funnel-form pipe to described fermenter bottom, funnelform top feed pipe is extended to form to described fermenter top, the upper articulation of described top feed pipe is with lid, and described lid, top feed pipe, underfeed pipe and bung all adopt nano silver material to make.
Preferably, the preparation method of described Folium Artemisiae Argyi bath gel, in described step 3, the powder obtained add 1.5 weight portion Sargassum powder, 2.5 weight portion Margarita powder and described first concentrating filter liquor drying after the cocamidopropyl propyl amide amine oxide adding above-mentioned weight portion and betanin after.
The present invention at least comprises following beneficial effect:
1) Folium Artemisiae Argyi extract is inhibited to Common Pathogenic dermatophytes in vitro, can suppress the growth of pyogenic baeceria completely, can also prevent and treat the symptoms such as few abdomen cold type of pain, coldness and unbalance in meridians, skin pruritus; The clean skin ability of AES (polyoxyethylenated alcohol sodium sulfate) is strong, and gentleness can not damage skin; Betanin has the ability of good penetrability, bactericidal antiphlogistic, scale removal of removing contamination; Folium Artemisiae Argyi bath gel life-time service of the present invention, has effect of glabrous skin, bactericidal antiphlogistic, alleviation female menstrual period pain.
2) the present invention prepares the method for Folium Artemisiae Argyi bath gel simply, is added by substep, and with different rotating speeds mixing material, the Folium Artemisiae Argyi bath gel obtained, the compatibility is good, homogeneous, and between each material, effect concertedness is good.
3) first product bath gel takes out after quiet mixed 7-10 days by the present invention in bamboo hydrostatic column, give the fragrance that Folium Artemisiae Argyi bath gel bamboo is fresh and clean, the more important thing is, improve the antiphlogistic antibacterial of Folium Artemisiae Argyi bath gel, alleviate the effect of pain in menstrual period, be particularly suitable for women and use.
4) by adding Fructus Litchi ferment extracting solution of the present invention, can while making full use of resource twice laid, Folium Artemisiae Argyi bath gel is made to have raising body immunity, improve female menstrual period malaise symptoms and menoxenia, life-time service can nurse one's health skin and endocrine from outside to inside, thus makes consumer radiant, full of vigor.
Wherein, Exocarpium Litchi has regulates the flow of vital energy, pain relieving, promotes the production of body fluid, beneficial blood, separates tired effect, and Semen Litchi can promoting QI to circulate and dispersing the agglomeration of the pathogens; Parched rice-bran is rich in various nutrient and biological active substances, and the microorganism be fermented obviously can increase the content of each nutrient in Fructus Litchi ferment extracting solution after utilizing; Rice wine wine with dregs can be introduced yeast and carry out culture propagation, and the meter Xiang itself had and aroma can give the abnormal smells from the patient of mediation Exocarpium Litchi and Semen Litchi, Folium Artemisiae Argyi bath gel is had and makes skin fragrance, ruddy effect; Fructus Jujubae has mends weak breath, effect of invigorating blood circulation, for symptoms such as joint aches, physical weakness, menoxenias.Herba Leonuri, Fructus Solani melongenae root, Caulis Spatholobi, the Radix Astragali, Rhizoma Chuanxiong, Radix Bupleuri, Fructus Forsythiae, Radix rosae multiflorae and Radix Schefflerae Arboricolae (Caulis et Folium Schefflerae Arboricolae) compatibility, have inducing diuresis to remove edema, relaxing muscles and tendons to promote blood circulation, nourishing blood for regulating menstruation, heat clearing away solution tired, antibacterial, improve the effects such as immunologic function, antithrombotic, promoting the circulation of QI to relieve pain, the effect of menoxenia, abdominal pain in menstruation can be treated.Plumula Nelumbinis clearing away heart-fire for tranquillization, Herba Schizonepetae heat-clearing and toxic substances removing, spirulina enhancing immunity, germinated brown rice plasm provides anthocyanidin and γ-aminobutyric acid, can improve the bullet humidity of skin, slow down the aging of epidermis cell, strengthens skin immunization power; Bacillus subtilis and bacillus bifidus are as probiotic bacteria, and making with Exocarpium Litchi and Semen Litchi etc. is that major ingredient can fully improve its effect at interior raw material after fermentation, improves the compatibility of Fructus Litchi ferment extracting solution in Folium Artemisiae Argyi bath gel simultaneously.
5) the present invention adopts fermenter to carry out the sweat of Fructus Litchi ferment extracting solution, miscellaneous bacteria can be stopped infect, the fermentation simultaneously using bamboo to carry out Fructus Litchi ferment extracting solution for stack shell is standby, the natural scents of abundant purification, mediation Fructus Litchi ferment extracting solution, the effects such as antibacterial, the heat clearing away also making bamboo itself have incorporate in Fructus Litchi ferment extracting solution, further increase the antiphlogistic antibacterial effect of bath gel of the present invention.
6) Sargassum powder has moisturizing, increases skin deflation and elasticity wrinkle removing effect, and Margarita powder significantly can strengthen reparation and the regeneration function of damaged skin tissue together with Sargassum powder and Fructus Litchi enzyme liquid, makes the smooth delicacy of the skin of consumer, bright and clean as jade; The powder obtained after described first concentrating filter liquor drying is that in literary composition, the lixiviate of each Chinese medicine ingredients material obtains, though without fermentation process, has effect of certain antibacterial, pain relieving, regulating menstruation and enhancing immunity.
7) Folium Artemisiae Argyi extract of the present invention contain by after alcohol extraction by after solid constituent inoculation fermentation again with ethyl acetate extract composition, compare the method for direct alcohol extraction, more can extract the effective efficiency factor in Folium Artemisiae Argyi, promote the function that Folium Artemisiae Argyi itself has, improve the utilization rate of Folium Artemisiae Argyi.
Part is embodied by explanation below by other advantage of the present invention, target and feature, part also will by research and practice of the present invention by those skilled in the art is understood.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, can implement according to this with reference to description word to make those skilled in the art.
Embodiment 1:
A kind of Folium Artemisiae Argyi bath gel, comprises the following raw material with parts by weight: Folium Artemisiae Argyi extract 0.1 part, lauryl both sexes sodium acetate 1 part, AES2 part, EDTA-4Na0.1 part, betanin 1 part, cocamidopropyl propyl amide amine oxide 1 part, 0.1 part, sodium chloride, citric acid 0.1 part, 0.1 part, Folium Artemisiae Argyi essence and deionized water 100 parts.Wherein, AES is surfactant.
A preparation method for Folium Artemisiae Argyi bath gel, comprises the following steps:
Step one, the deionized water of above-mentioned weight portion is heated to 65 DEG C inserts in reactor, then the Folium Artemisiae Argyi extract of above-mentioned weight portion is added in reactor, stir 10min with the rotating speed of 20r/min;
Step 2, the AES then adding above-mentioned weight portion, lauryl both sexes sodium acetate and EDTA-4Na, stir 30min with the rotating speed of 15r/min;
Step 3, the cocamidopropyl propyl amide amine oxide adding above-mentioned weight portion again and betanin, stir 15min with the rotating speed of 25r/min;
Step 4, add the sodium chloride of above-mentioned weight portion, stir 10min with the rotating speed of 10r/min again, be cooled to rapidly less than 45 DEG C, add citric acid and the Folium Artemisiae Argyi essence of above-mentioned weight portion, stir 20min with the rotating speed of 35r/min again, after 180 mesh filter screens filter, obtain first product bath gel.
Embodiment 2:
A kind of Folium Artemisiae Argyi bath gel, comprises the following raw material with parts by weight: Folium Artemisiae Argyi extract 6 parts, lauryl both sexes sodium acetate 4 parts, AES6 part, EDTA-4Na0.5 part, betanin 4 parts, cocamidopropyl propyl amide amine oxide 2 parts, 2 parts, sodium chloride, citric acid 0.5 part, 0.2 part, Folium Artemisiae Argyi essence and deionized water 100 parts.
A preparation method for Folium Artemisiae Argyi bath gel, comprises the following steps:
Step one, the deionized water of above-mentioned weight portion is heated to 68 DEG C inserts in reactor, then the Folium Artemisiae Argyi extract of above-mentioned weight portion is added in reactor, stir 13min with the rotating speed of 22r/min;
Step 2, the AES then adding above-mentioned weight portion, lauryl both sexes sodium acetate and EDTA-4Na, stir 35min with the rotating speed of 15r/min;
Step 3, the cocamidopropyl propyl amide amine oxide adding above-mentioned weight portion again and betanin, stir 18min with the rotating speed of 25r/min;
Step 4, add the sodium chloride of above-mentioned weight portion, stir 15min with the rotating speed of 10r/min again, be cooled to rapidly less than 45 DEG C, add citric acid and the Folium Artemisiae Argyi essence of above-mentioned weight portion, stir 25min with the rotating speed of 38r/min again, after 180 mesh filter screens filter, obtain first product bath gel.
Embodiment 3:
A kind of Folium Artemisiae Argyi bath gel, comprises the following raw material with parts by weight: Folium Artemisiae Argyi extract 10 parts, lauryl both sexes sodium acetate 10 parts, AES15 part, EDTA-4Na1 part, betanin 10 parts, cocamidopropyl propyl amide amine oxide 3 parts, 5 parts, sodium chloride, citric acid 1 part, 1 part, Folium Artemisiae Argyi essence and deionized water 100 parts.
A preparation method for Folium Artemisiae Argyi bath gel, comprises the following steps:
Step one, the deionized water of above-mentioned weight portion is heated to 70 DEG C inserts in reactor, then the Folium Artemisiae Argyi extract of above-mentioned weight portion is added in reactor, stir 15min with the rotating speed of 25r/min;
Step 2, the AES then adding above-mentioned weight portion, lauryl both sexes sodium acetate and EDTA-4Na, stir 40min with the rotating speed of 15r/min;
Step 3, the cocamidopropyl propyl amide amine oxide adding above-mentioned weight portion again and betanin, stir 20min with the rotating speed of 25r/min;
Step 4, add the sodium chloride of above-mentioned weight portion, stir 20min with the rotating speed of 10r/min again, be cooled to rapidly less than 45 DEG C, add citric acid and the Folium Artemisiae Argyi essence of above-mentioned weight portion, stir 30min with the rotating speed of 40r/min again, after 180 mesh filter screens filter, obtain first product bath gel.
Embodiment 4:
On the basis of embodiment 2, the preparation method of described Folium Artemisiae Argyi bath gel, the preparation method of described Folium Artemisiae Argyi extract is as follows:
A1, fresh Folium Artemisiae Argyi is placed in 80 DEG C of hot water soaks 8-10min, take out Folium Artemisiae Argyi, obtain first liquid, for subsequent use,
A2, again that described Folium Artemisiae Argyi is broken, the volume fraction adding its 5 times of weight is the alcoholic solution of 70%, heating and refluxing extraction 2 times, and the extracting solution merging 2 times obtains second liquid, and the filtering residue merging 2 times obtains the first filtering residue, for subsequent use;
A3, by the first filtering residue by its quality inoculation bacillus subtilis of the 0.3% and Lactococcus of 0.1%, in room temperature bottom fermentation 15-20 days, add ethyl acetate by 3 of its weight times after sterilizing and soak, backflow is collected, and obtains the 3rd liquid;
A4, by concentrated after first liquid, second liquid and the 3rd liquid mixing and spraying dry, pulverize and sieve 200 orders afterwards, obtain described Folium Artemisiae Argyi extract.
Embodiment 5:
On the basis of embodiment 2, the preparation method of described Folium Artemisiae Argyi bath gel, adds the Fructus Litchi ferment extracting solution of 3-4 weight portion after being also included in step one, stir 30min with the rotating speed of 35r/min, wherein, the preparation method of described Fructus Litchi ferment is as follows:
S1, get 32-42 weight portion Exocarpium Litchi and 5-8 weight portion Semen Litchi pulverizes rear mistake 40 mesh sieve, mixing respectively, add the Sucus Zingberis of 12-15 weight portion and the parched rice-bran of 10-12 weight portion, the first mixture is obtained after mixing, for subsequent use, described Sucus Zingberis is Rhizoma Zingiberis Recens and pure water according to mass ratio is to obtain at 1: 30, described parched rice-bran be Testa oryzae at 100-120 DEG C in rotary frying pan parch 15-20min obtain;
S2, fermenter inner surface will spray the nano-silver water solution that mass fraction is 0.02%, described first mixture is added after 30min, add the rice wine wine with dregs of 5-8 weight portion and the Fructus Jujubae of 3-5 weight portion again, the second mixture is obtained after mixing, probiotic bacteria is inoculated by the 0.2%-0.4% of described second mixture weight, airtight described fermenter, ferments and obtains the first tunning in 3-5 days;
Described probiotic bacteria is to form at 1.2: 1 by bacillus subtilis and bacillus bifidus according to mass ratio, and described Fructus Jujubae is that after fresh Chinese dates enucleation, fragmentation obtains;
S3, by broken after 3-5 weight portion Herba Leonuri, 2-3 weight portion Fructus Solani melongenae root, 2-3 weight portion Caulis Spatholobi, the 1 weight portion Radix Astragali, 1 weight portion Rhizoma Chuanxiong, 1.5 weight portion Radix Bupleuri, 0.5 weight portion Fructus Forsythiae, 1.8 weight portion Radix rosae multifloraes and the mixing of 2 weight portion Radix Schefflerae Arboricolae (Caulis et Folium Schefflerae Arboricolae)s, add 100 parts by weight of purified water, be placed in infusion 1h under slow fire, filter to obtain the first filtrate and the second filtering residue, for subsequent use;
S4, add the second filtering residue from charging aperture, airtight described charging aperture after mixing with the first tunning, continue fermentation 2 days the second tunning;
S5, by the germinated brown rice plasm of 2-4 weight portion Plumula Nelumbinis, 0.5 weight portion Herba Schizonepetae, 1 weight portion spirulina and 5 weight portions mixing after grind, add from charging aperture, airtight after mixing with the second tunning, continue fermentation after 4-5 days the 3rd tunning, the sprout brown rice of described germinated brown rice plasm to be fructus zizaniae caduciflorae be raw material is that 1: 3 defibrination obtains with removing pure water according to mass ratio;
S6, the 3rd tunning to be cooled after microwave sterilizating, filter 100 mesh sieves, obtain Fructus Litchi ferment extracting solution.
Wherein, the preparation method of described Folium Artemisiae Argyi bath gel, described fermenter comprises:
Stack shell, it is cylindrical, and described stack shell is the lower seal of the bamboo making that internal diameter is greater than 30cm, described stack shell;
Bung, it is hinged on the top of described stack shell, described bung is provided with charging aperture, it extends to form the underfeed of falling funnel-form pipe to described fermenter bottom, funnelform top feed pipe is extended to form to described fermenter top, the upper articulation of described top feed pipe is with lid, and described lid, top feed pipe, underfeed pipe and bung all adopt nano silver material to make.
Embodiment 6:
On the basis of embodiment 2, the preparation method of described Folium Artemisiae Argyi bath gel, also comprises:
Step 5, described first product bath gel is placed in hydrostatic column, at interval of 24h with the rotational speed hydrostatic column 10min of 5r/min, takes out after 7-10 days, after 240 mesh filter screens filter Folium Artemisiae Argyi bath gel; Wherein,
Described hydrostatic column is the bamboo making that inner hollow diameter reaches more than 20cm, its closed at both ends, bamboo sidewall offers charging aperture, and hinged sealing cover body is set, described hydrostatic column two ends connect a rotating shaft respectively, and removably connected by rotating shaft and bracing frame, described rotating shaft connects motor and rotates to control described hydrostatic column.
Embodiment 7:
On the basis of embodiment 5, the preparation method of described Folium Artemisiae Argyi bath gel, in described step 3, the powder obtained add 1.5 weight portion Sargassum powder, 2.5 weight portion Margarita powder and described first concentrating filter liquor drying after the cocamidopropyl propyl amide amine oxide adding above-mentioned weight portion and betanin after.
Comparative example 1:
A kind of Folium Artemisiae Argyi bath gel, comprises the following raw material with parts by weight: Folium Artemisiae Argyi extract 6 parts, lauryl both sexes sodium acetate 4 parts, AES6 part, EDTA-4Na0.5 part, betanin 4 parts, cocamidopropyl propyl amide amine oxide 2 parts, 2 parts, sodium chloride, citric acid 0.5 part, 0.2 part, Folium Artemisiae Argyi essence and deionized water 100 parts.
A kind of preparation method of Folium Artemisiae Argyi bath gel, the deionized water of above-mentioned weight portion is heated to 68 DEG C inserts in reactor, again the Folium Artemisiae Argyi extract of above-mentioned weight portion, AES, lauryl both sexes sodium acetate, EDTA-4Na, cocamidopropyl propyl amide amine oxide, betanin and sodium chloride are added in reactor, Heat preservation 80min after stirring, be cooled to rapidly less than 45 DEG C, add citric acid and the Folium Artemisiae Argyi essence of above-mentioned weight portion, stir 25min with the rotating speed of 38r/min again, after 180 mesh filter screens filter, obtain first product bath gel.
The women that Folium Artemisiae Argyi bath gel of the present invention is not limited to suffer from dysmenorrhea and menoxenia symptom uses, but in order to effect of the present invention is described, applicant of the present invention provides comparative experiments as follows:
By comparative example 1, embodiment 2, embodiment 4-6 make first product bath gel or Folium Artemisiae Argyi bath gel respectively to have long-term dysmenorrhea experience, menoxenia 100 women carry out the test of 2 months by a definite date, 5 months respectively in table 1 and table 2.
Table 1 uses the application form after 2 months
Table 2 uses the application form after 5 months
From table 1 and table 2, the Folium Artemisiae Argyi bath gel product of embodiment 5 and embodiment 6, for the women having dysmenorrhea, menoxenia, have remarkable result, but permanence operation is better.
Although embodiment of the present invention are open as above, but it is not restricted to listed in description and embodiment utilization, it can be applied to various applicable the field of the invention completely, for those skilled in the art, can easily realize other amendment, therefore do not deviating under the general concept that claim and equivalency range limit, the present invention is not limited to specific details and illustrates here and the embodiment described.
Claims (8)
1. a Folium Artemisiae Argyi bath gel, it is characterized in that, comprise the following raw material with parts by weight: Folium Artemisiae Argyi extract 0.1-10 part, lauryl both sexes sodium acetate 1-10 part, AES2-15 part, EDTA-4Na0.1-1 part, betanin 1-10 part, cocamidopropyl propyl amide amine oxide 1-3 part, sodium chloride 0.1-5 part, citric acid 0.1-1 part, Folium Artemisiae Argyi essence 0.1-1 part and deionized water 100 parts.
2. Folium Artemisiae Argyi bath gel as claimed in claim 1, it is characterized in that, comprise the following raw material with parts by weight: Folium Artemisiae Argyi extract 6 parts, lauryl both sexes sodium acetate 4 parts, AES6 part, EDTA-4Na0.5 part, betanin 4 parts, cocamidopropyl propyl amide amine oxide 2 parts, 2 parts, sodium chloride, citric acid 0.5 part, 0.2 part, Folium Artemisiae Argyi essence and deionized water 100 parts.
3. a preparation method for Folium Artemisiae Argyi bath gel as claimed in claim 1 or 2, is characterized in that, comprise the following steps:
Step one, the deionized water of above-mentioned weight portion is heated to 65-70 DEG C inserts in reactor, then the Folium Artemisiae Argyi extract of above-mentioned weight portion is added in reactor, stir 10-15min with the rotating speed of 20-25r/min;
Step 2, the AES then adding above-mentioned weight portion, lauryl both sexes sodium acetate and EDTA-4Na, stir 30-40min with the rotating speed of 15r/min;
Step 3, the cocamidopropyl propyl amide amine oxide adding above-mentioned weight portion again and betanin, stir 15-20min with the rotating speed of 25r/min;
Step 4, add the sodium chloride of above-mentioned weight portion, stir 10-20min with the rotating speed of 10r/min again, be cooled to rapidly less than 45 DEG C, add citric acid and the Folium Artemisiae Argyi essence of above-mentioned weight portion, stir 20-30min with the rotating speed of 35-40r/min again, after 180 mesh filter screens filter, obtain first product bath gel.
4. the preparation method of Folium Artemisiae Argyi bath gel as claimed in claim 3, it is characterized in that, the preparation method of described Folium Artemisiae Argyi extract is as follows:
A1, fresh Folium Artemisiae Argyi is placed in 80 DEG C of hot water soaks 8-10min, take out Folium Artemisiae Argyi, obtain first liquid, for subsequent use,
A2, again that described Folium Artemisiae Argyi is broken, the volume fraction adding its 5 times of weight is the alcoholic solution of 70%, heating and refluxing extraction 2 times, and the extracting solution merging 2 times obtains second liquid, and the filtering residue merging 2 times obtains the first filtering residue, for subsequent use;
A3, by the first filtering residue by its quality inoculation bacillus subtilis of the 0.3% and Lactococcus of 0.1%, in room temperature bottom fermentation 15-20 days, add ethyl acetate by 3 of its weight times after sterilizing and soak, backflow is collected, and obtains the 3rd liquid;
A4, by concentrated after first liquid, second liquid and the 3rd liquid mixing and spraying dry, pulverize and sieve 200 orders afterwards, obtain described Folium Artemisiae Argyi extract.
5. the preparation method of Folium Artemisiae Argyi bath gel as claimed in claim 3, is characterized in that, adds the Fructus Litchi ferment extracting solution of 3-4 weight portion after being also included in step one, and stir 30min with the rotating speed of 35r/min, wherein, the preparation method of described Fructus Litchi ferment is as follows:
S1, get 32-42 weight portion Exocarpium Litchi and 5-8 weight portion Semen Litchi pulverizes rear mistake 40 mesh sieve, mixing respectively, add the Sucus Zingberis of 12-15 weight portion and the parched rice-bran of 10-12 weight portion, the first mixture is obtained after mixing, for subsequent use, described Sucus Zingberis is Rhizoma Zingiberis Recens and pure water according to mass ratio is to obtain at 1: 30, described parched rice-bran be Testa oryzae at 100-120 DEG C in rotary frying pan parch 15-20min obtain;
S2, fermenter inner surface will spray the nano-silver water solution that mass fraction is 0.02%, described first mixture is added after 30min, add the rice wine wine with dregs of 5-8 weight portion and the Fructus Jujubae of 3-5 weight portion again, the second mixture is obtained after mixing, probiotic bacteria is inoculated by the 0.2%-0.4% of described second mixture weight, airtight described fermenter, ferments and obtains the first tunning in 3-5 days;
Described probiotic bacteria is to form at 1.2: 1 by bacillus subtilis and bacillus bifidus according to mass ratio, and described Fructus Jujubae is that after fresh Chinese dates enucleation, fragmentation obtains;
S3, by broken after 3-5 weight portion Herba Leonuri, 2-3 weight portion Fructus Solani melongenae root, 2-3 weight portion Caulis Spatholobi, the 1 weight portion Radix Astragali, 1 weight portion Rhizoma Chuanxiong, 1.5 weight portion Radix Bupleuri, 0.5 weight portion Fructus Forsythiae, 1.8 weight portion Radix rosae multifloraes and the mixing of 2 weight portion Radix Schefflerae Arboricolae (Caulis et Folium Schefflerae Arboricolae)s, add 100 parts by weight of purified water, be placed in infusion 1h under slow fire, filter to obtain the first filtrate and the second filtering residue, for subsequent use;
S4, add the second filtering residue from charging aperture, airtight described charging aperture after mixing with the first tunning, continue fermentation 2 days the second tunning;
S5, by the germinated brown rice plasm of 2-4 weight portion Plumula Nelumbinis, 0.5 weight portion Herba Schizonepetae, 1 weight portion spirulina and 5 weight portions mixing after grind, add from charging aperture, airtight after mixing with the second tunning, continue fermentation after 4-5 days the 3rd tunning, the sprout brown rice of described germinated brown rice plasm to be fructus zizaniae caduciflorae be raw material is that 1: 3 defibrination obtains with removing pure water according to mass ratio;
S6, the 3rd tunning to be cooled after microwave sterilizating, filter 100 mesh sieves, obtain Fructus Litchi ferment extracting solution.
6. the preparation method of Folium Artemisiae Argyi bath gel as claimed in claim 3, is characterized in that, also comprise:
Step 5, described first product bath gel is placed in hydrostatic column, at interval of 24h with the rotational speed hydrostatic column 10min of 5r/min, takes out after 7-10 days, after 240 mesh filter screens filter Folium Artemisiae Argyi bath gel; Wherein,
Described hydrostatic column is the bamboo making that inner hollow diameter reaches more than 20cm, its closed at both ends, bamboo sidewall offers charging aperture, and hinged sealing cover body is set, described hydrostatic column two ends connect a rotating shaft respectively, and removably connected by rotating shaft and bracing frame, described rotating shaft connects motor and rotates to control described hydrostatic column.
7. the preparation method of Folium Artemisiae Argyi bath gel as claimed in claim 5, it is characterized in that, described fermenter comprises:
Stack shell, it is cylindrical, and described stack shell is the lower seal of the bamboo making that internal diameter is greater than 30cm, described stack shell;
Bung, it is hinged on the top of described stack shell, described bung is provided with charging aperture, it extends to form the underfeed of falling funnel-form pipe to described fermenter bottom, funnelform top feed pipe is extended to form to described fermenter top, the upper articulation of described top feed pipe is with lid, and described lid, top feed pipe, underfeed pipe and bung all adopt nano silver material to make.
8. the preparation method of Folium Artemisiae Argyi bath gel as claimed in claim 7, it is characterized in that, in described step 3, the powder obtained add 1.5 weight portion Sargassum powder, 2.5 weight portion Margarita powder and described first concentrating filter liquor drying after the cocamidopropyl propyl amide amine oxide adding above-mentioned weight portion and betanin after.
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Application publication date: 20151223 |