CN105125443B - Facial mask with tremella as main raw material and preparation method thereof - Google Patents

Facial mask with tremella as main raw material and preparation method thereof Download PDF

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Publication number
CN105125443B
CN105125443B CN201510589173.6A CN201510589173A CN105125443B CN 105125443 B CN105125443 B CN 105125443B CN 201510589173 A CN201510589173 A CN 201510589173A CN 105125443 B CN105125443 B CN 105125443B
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parts
powder
white fungus
facial mask
glue
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CN105125443A (en
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不公告发明人
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Zhongshan Deshang Weiye Biotechnology Co ltd
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Zhongshan Deshang Weiye Biotechnology Co ltd
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Abstract

The invention provides a mask taking tremella as a main raw material, which comprises the following components in parts by weight: 50-60 parts of fresh tremella; 2-8 parts of carboxymethyl cellulose; 2-8 parts of carrageenan; 3-9 parts of sodium alginate; 6-9 parts of chitosan; 0.1-0.2 part of gypsum; 4-8 parts of coix seed powder; 0.1-0.3 part of preservative; 0.4-1 part of 3D printing glue; the preservative is selected from one of methyl paraben, propyl paraben or phenoxyethanol. The raw materials used by the mask are all cosmetic allowable additives, and are basically edible raw materials, so that the mask has no stimulation to skin, the white fungus filter residue and the white fungus filtrate have whitening and moisturizing effects, and the whitening and moisturizing effects are achieved by combining the coix seed powder.

Description

It is a kind of using white fungus as facial mask of primary raw material and preparation method thereof
Technical field
The invention belongs to cosmetic field, and in particular to a kind of using white fungus as the skin care item of primary raw material and its preparation side Method.
Background technology
Tremella Tremellaceae Tremella, it is a fructification for Basidiomycota fungi white fungus.White fungus is rich in natural plant glue Matter, its nutritional ingredient include protein, fat, carbohydrate, crude fibre, ash content and iron, calcium, phosphorus, carrotene, dimension life Plain B1, B2 and C etc., long-term use have the effect of Yin-nourishing and Qi-supplementing, the hat being described as in bacterium.White fungus is just realized before China more than 100 years Artificial cultivation, has been widely used in food materials, tonic and cosmetics.
Various tremella face masks, such as tremella face mask disclosed in patent CN101073551A on current market be present, It is coated onto on the face using white fungus and fresh milk as main nutrient composition, during use, is not the finished product of film forming;Patent CN102988272A is proposed Tremella face mask be made up of NMF, thickener, nutritional agents and water, and the mixture of paste.
These facial mask majorities refer to the addition of dried tremella extract in facial mask liquid, simply using white fungus as an effect Agent uses, and really makes not having substantially for carrier with white fungus, because white fungus is a kind of fungi, fiber content is fewer, does not allow Easy film forming, if white fungus is cooked film forming, it is necessary to film forming agent is added in white fungus, it is done so that film out, shaky, Toughness is bad, and fragile rotten, and practicality is bad.
The content of the invention
For weak point existing for this area, it is an object of the invention to provide a kind of raw material is simple, definite ingredients, work( Effect is notable, the flexible solid tremella face mask of good toughness of feasible process.
It is another object of the present invention to propose the preparation method of the facial mask.
Realize that above-mentioned purpose technical scheme of the present invention is:
A kind of facial mask using white fungus as primary raw material, include the composition of following parts by weight:Fresh white fungus 50-60 parts;Carboxylic first Base cellulose 2-8 parts;Carragheen 2-8 parts;Sodium alginate 3-9 parts;Chitosan 6-9 parts;Gypsum 0.1-0.2 parts;Lotus-seed-heart powder 4-8 Part;Preservative 0.1-0.3 parts;3D printing glue 0.4-1 parts;Described preservative be selected from methyl hydroxybenzoate, propylben or One kind in Phenoxyethanol.
In the facial mask composition that the application proposes, adlay is the fruit of grass Job's tears (Coix lacryma-jobi L.) It is real, rich in protein, can softening skin cutin, make skin smooth, eliminate pigment spot, Glycerin can be reached for a long time by drinking The effect of.In the present invention, the adlay Powder Particle Size of use is less than 100 mesh (i.e. below 0.15mm powder).
Described facial mask preferably, includes the composition of following parts by weight:Fresh 50 parts of white fungus;4 parts of carboxymethyl cellulose;Card Draw 4 parts of glue;6 parts of sodium alginate;8 parts of chitosan;0.15 part of gypsum;5 parts of lotus-seed-heart powder;0.2 part of preservative;3D printing glue 0.6 Part.
Wherein described 3D printing glue is resinae, acrylic compounds, one kind in silicone.
Wherein, the face-like film that the facial mask is molded for 3D printing, thickness 0.65mm.
The method for preparing facial mask proposed by the present invention, including step:
(1) go the removal of impurity to clean up in fresh white fungus, be then placed in high-speed grinder and be ground to 60 mesh, then Filtered with less than 60 mesh filter screens, by white fungus filter residue heating, drying after filtering, be used to make Essence after filtrate sterilizing;
(2) by step (1) dry after white fungus filter residue with pulverizer crush with 100 eye mesh screens after, then with carboxymethyl cellulose Element, carragheen, sodium alginate, chitosan, gypsum, lotus-seed-heart powder, preservative (above-mentioned material fineness is respectively less than 100 mesh) are mixed It is abundant to close stirring, as the body of powder in 3D printing;
(3) modeled using the 3D modeling software of Auto CAD softwares for facial mask, be divided into m layers to cut the threedimensional model built up Face, m are 4-8 integer, and cross section information is stored in computer;
(4) raw material is added to the print cartridge of 3D printer, one of them is glue print cartridge, and another is the print cartridge of powder, The spray volume for adjusting two print cartridges controls the thickness of 3D printing powder bed and glue layer, first prints one layer of powder every time, then beat One layer of glue is printed, prints m layers altogether, facial mask is printed as type;
(5) excessive powder is washed with water in the facial mask of system in (4), then white fungus film is put into 110- in pressure steam sterilizer 130 DEG C of autoclaving 20-40 minutes;
(6) tremella face mask to have sterilized is loaded into packaging bag, pours into the Essence made of white fungus filtrate, encapsulation.
Specifically, in the step (1), go the removal of impurity to clean up in fresh white fungus, 10 are added by 50-60 parts by weight Parts by weight water, then it is ground, filters.
Wherein, the equipment for carrying out 3D printing is photocuring printer.
In step (4), include the computer that is connected with 3D printer of 3D printer using equipment, designed in computer Need to prepare the three-dimensional stereo model of tremella face mask, and slicing delamination has been carried out to the three-dimensional stereo model of the facial mask and obtained often The shaping information of one layer of powder layer and glue layer, 3D printing are printed according to every layer of shaping information.
Wherein, in the step (4), the spray volume volume ratio that the print cartridge of 3D printing glue print cartridge and powder is each is 4-5: 6-7。
Preferably, each spray volume volume of the print cartridge of the 3D printing glue print cartridge and powder be respectively 4.5mL and 6.75mL。
Wherein, in the step (4), one layer of powder is first printed every time, then prints one layer of glue, prints 5 layers altogether, wherein Three-layer powder, two layers of glue.
Wherein, in the step (4), one layer of powder has often been printed, printer automatically turns on uviol lamp 10s, accelerates glue Solidification.
In step (5), the pressure of pressure steam sterilizer can be 0.1-0.2Mpa (gauge pressure).
The beneficial effects of the present invention are:
Raw materials used facial mask of the present invention is that cosmetics allow additive, and is substantially the raw material of food grade, to skin Skin is non-stimulated, and white fungus filter residue and white fungus filtrate inherently have the effect of skin whitening, moisturizing, and with reference to lotus-seed-heart powder, collaboration reaches whitening and moistening skin The effect of;
The present invention makes the powder suitable for 3D printing, the preparation technology flow of facial mask is simple, behaviour by rational formula Facilitate.
Brief description of the drawings
Fig. 1 is flow chart prepared by facial mask of the present invention.
Embodiment
Illustrate the present invention below by most preferred embodiment.Those skilled in the art institute it should be understood that, embodiment is only used for Illustrate rather than for limiting the scope of the present invention.
In embodiment, 3D printer is the logical SLA photocuring printers in west, and printing glue is Kraft spy K-3820.
In embodiment, unless otherwise instructed, means used are the conventional means in this area.
Embodiment 1:
Raw material (gram) is weighed by following weight;
Fresh 50 parts of white fungus;4 parts of carboxymethyl cellulose;4 parts of carragheen;6 parts of sodium alginate;8 parts of chitosan;Gypsum 0.15 Part;5 parts of lotus-seed-heart powder;0.2 part of preservative methyl hydroxybenzoate;0.6 part of 3D printing glue.
Preparation method is following (flow is shown in Fig. 1):
(1) 50 parts of the fresh white fungus that the removal of impurity cleans up will be gone to add 10 parts of water (adding water to be more abundant in order to grind) to put Enter in high-speed grinder and be ground, then the strainer filtering with 60 mesh, white fungus filter residue heating, drying, filtrate sterilization are gone out after filtering It is used to make Essence after bacterium.
(2) by step (1) dry after white fungus filter residue with pulverizer crush with 100 eye mesh screens after, then with carboxymethyl cellulose Element, carragheen, sodium alginate, chitosan, gypsum, lotus-seed-heart powder, preservative (above-mentioned material fineness is respectively less than 100 mesh); Mix fully, as the powder in 3D printing.
(3) modeled using Auto CAD3D modeling softwares for the facial mask of printing, be divided into 5 layers to cut the threedimensional model built up Face, and cross section information is stored in computer.
(4) raw material is added into the print cartridge of 3D printer, one of print cartridge adds 3D printing glue, another addition Powder, print cartridge spray volume is adjusted, each spray volume 4.5mL of 3D printing glue, powder spray volume is 6.75mL, every so as to control The thickness of layer glue is 0.1mm, and the thickness of every layer of powder is that (area of facial mask is 45000mm to 0.15mm2, glue spray volume= 45000mm2× 0.1mm=4.5mL, powder spray volume=45000mm2× 0.15mm=6.75mL).
(5) use equipment to include the computer that 3D printer is connected with 3D printer, required system is designed with computer The three-dimensional stereo model of standby tremella face mask, and slicing delamination has been carried out to the three-dimensional stereo model of the facial mask and has obtained each layer of powder The shaping information of body layer and glue layer, 3D printing is then carried out, 3D printing is printed according to every layer of shaping information, makes glue Alternately sprayed with powder, often printed one layer of powder, printer automatically turns on uviol lamp 10s, accelerates glue curing.Uviol lamp closes Close, final tremella face mask is printed as type.
(6) excessive powder is washed with water in the facial mask of system in (5), then white fungus film is put into 121 in pressure steam sterilizer DEG C, 0.1034MPa autoclavings 20 minutes.
(7) tremella face mask to have sterilized is loaded into packaging bag, pours into the Essence that 30g makes of white fungus filtrate, encapsulated.
Embodiment 2
Raw material (gram) is weighed by following weight
Fresh 55 parts of white fungus;Carboxymethyl cellulose 2;2 parts of carragheen;3 parts of sodium alginate;6 parts of chitosan;0.1 part of gypsum; 4 parts of lotus-seed-heart powder;0.1 part of preservative;0.4 part of 3D printing glue.
Preparation method is the same as embodiment 1.
Test example 1 tests the stability of tremella face mask of the present invention
Embodiments of the invention 1 and the sealing of the facial mask of embodiment 2 were placed in environment 40 DEG C of relative humidity, 85% environment after 30 days, Carry out physical and chemical index test (standard:QB/T2872-2007), facial mask globality is detected:Facial mask does not rot, without other Peculiar smell, thickness=0.65 ± 0.05mm and toughness >=200g/cm (method of testings:Extension test, tester are carried out using tensiometer The sub- concerted effort NTTONIC 7760 of device Japan), therefore facial mask is moderately good, the shelf-life of facial mask converts do shady and cool in the case where sealing state Its shelf-life of dry place is no less than 3 years.
Embodiment above is only that the preferred embodiment of the present invention is described, and not the scope of the present invention is entered Row limits, on the premise of design spirit of the present invention is not departed from, technical side of this area ordinary skill technical staff to the present invention The all variations and modifications that case is made, it all should fall into the protection domain of claims of the present invention determination.

Claims (3)

1. a kind of preparation method using white fungus as the facial mask of primary raw material, the facial mask is composed of the following components in parts by weight:Newly Fresh white fungus 50-60 parts;Carboxymethyl cellulose 2-8 parts;Carragheen 2-8 parts;Sodium alginate 3-9 parts;Chitosan 6-9 parts;Gypsum 0.1-0.2 parts;Lotus-seed-heart powder 4-8 parts;Preservative 0.1-0.3 parts;3D printing glue 0.4-1 parts;Described preservative is selected from Ni Bo One kind in tortoise beetle ester, propylben or Phenoxyethanol;The face-like film that the facial mask is molded for 3D printing, thickness 0.6- 0.7mm, the equipment for carrying out 3D printing are photocuring printer;
The preparation method of the facial mask comprises the following steps:
(1) go the removal of impurity to clean up in white fungus, be ground to 60 mesh, then filtered with 60 mesh filter screens, filter white fungus after filtering Slag heating, drying, it is used to make Essence after filtrate sterilizing;
(2) after white fungus filter residue is crushed with 100 eye mesh screens with pulverizer after step (1) is dried, then it is respectively less than with material fineness Carboxymethyl cellulose, carragheen, sodium alginate, chitosan, gypsum, lotus-seed-heart powder, the preservative of 100 mesh mix abundant, work For the body of powder in 3D printing;
(3) modeled using the 3D modeling software of Auto CAD softwares for facial mask, the threedimensional model built up be divided into 5 layer cross sections, And cross section information is stored in computer;
(4) raw material is added to the print cartridge of 3D printer, one of them is glue print cartridge, and another is the print cartridge of powder, regulation The spray volume of print cartridge controls the thickness of 3D printing powder bed and glue layer, and facial mask is printed as type;3D printing glue print cartridge and The each spray volume volume of powder print cartridge is respectively 4.5mL and 6.75mL, first prints one layer of powder every time, then print one layer of glue Water, 5 layers, wherein three-layer powder, two layers of glue being printed altogether, often having printed one layer of powder, printer automatically turns on uviol lamp 10s, accelerate glue curing;
(5) excessive powder is washed with water in the facial mask of system in (4), then white fungus film is put into 110-130 in pressure steam sterilizer DEG C autoclaving 20-40 minutes;
(6) tremella face mask to have sterilized is loaded into packaging bag, pours into the Essence made of white fungus filtrate, encapsulation.
2. preparation method according to claim 1, it is characterised in that the facial mask is composed of the following components in parts by weight: Fresh 50 parts of white fungus;4 parts of carboxymethyl cellulose;4 parts of carragheen;6 parts of sodium alginate;8 parts of chitosan;0.15 part of gypsum;Adlay 5 parts of powder;0.2 part of preservative;0.6 part of 3D printing glue.
3. preparation method according to claim 1, it is characterised in that in the step (1), fresh white fungus is gone to clean Matter cleans up, and adds 10 parts by weight water by 50-60 parts by weight, is then ground, filters.
CN201510589173.6A 2015-09-16 2015-09-16 Facial mask with tremella as main raw material and preparation method thereof Active CN105125443B (en)

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CN109010224A (en) * 2018-11-07 2018-12-18 通江县裕德源润耳生物科技有限公司 A kind of production method of the organic section of wooden tremella face mask

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CN101530382A (en) * 2009-04-20 2009-09-16 尚治国 Tremella gel mask and preparation method thereof
KR101342925B1 (en) * 2013-03-13 2013-12-18 (주)에이엘미디어 Beauty treatment pack and manufacturing method
CN104721061B (en) * 2015-02-10 2017-08-29 广州赛莱拉干细胞科技股份有限公司 A kind of preparation method of 3D facial masks and its 3D facial masks of preparation

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