CN105077272A - Preparation method of dendrobium plasmogen oral liquid - Google Patents
Preparation method of dendrobium plasmogen oral liquid Download PDFInfo
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- CN105077272A CN105077272A CN201510422475.4A CN201510422475A CN105077272A CN 105077272 A CN105077272 A CN 105077272A CN 201510422475 A CN201510422475 A CN 201510422475A CN 105077272 A CN105077272 A CN 105077272A
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- dendrobium
- stem
- noble dendrobium
- magma
- plasmogen
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- 239000007788 liquid Substances 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 241001523681 Dendrobium Species 0.000 title abstract description 18
- 239000000341 volatile oil Substances 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 244000276331 Citrus maxima Species 0.000 claims abstract description 15
- 235000001759 Citrus maxima Nutrition 0.000 claims abstract description 15
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 11
- 239000012535 impurity Substances 0.000 claims abstract description 8
- 235000011194 food seasoning agent Nutrition 0.000 claims abstract description 5
- 238000009835 boiling Methods 0.000 claims abstract description 4
- 240000004638 Dendrobium nobile Species 0.000 claims description 56
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 21
- 241000026010 Dendrobium candidum Species 0.000 claims description 13
- 239000002131 composite material Substances 0.000 claims description 9
- 239000000706 filtrate Substances 0.000 claims description 7
- 206010033546 Pallor Diseases 0.000 claims description 6
- 241000581835 Monodora junodii Species 0.000 claims description 5
- 238000005352 clarification Methods 0.000 claims description 5
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 4
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 4
- 230000000844 anti-bacterial effect Effects 0.000 claims description 4
- 230000009514 concussion Effects 0.000 claims description 4
- 235000011090 malic acid Nutrition 0.000 claims description 4
- 239000001630 malic acid Substances 0.000 claims description 4
- 108010059892 Cellulase Proteins 0.000 claims description 3
- 238000010009 beating Methods 0.000 claims description 3
- 229940106157 cellulase Drugs 0.000 claims description 3
- 238000005119 centrifugation Methods 0.000 claims description 3
- 108010025790 chlorophyllase Proteins 0.000 claims description 3
- 230000009849 deactivation Effects 0.000 claims description 3
- 238000004945 emulsification Methods 0.000 claims description 3
- 239000012528 membrane Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 230000008569 process Effects 0.000 claims description 3
- 238000009849 vacuum degassing Methods 0.000 claims description 3
- 239000002569 water oil cream Substances 0.000 claims description 3
- 239000000796 flavoring agent Substances 0.000 abstract description 3
- 235000019634 flavors Nutrition 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 abstract 3
- 238000001914 filtration Methods 0.000 abstract 2
- 238000004537 pulping Methods 0.000 abstract 2
- 102000004190 Enzymes Human genes 0.000 abstract 1
- 108090000790 Enzymes Proteins 0.000 abstract 1
- 229930002875 chlorophyll Natural products 0.000 abstract 1
- 235000019804 chlorophyll Nutrition 0.000 abstract 1
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 235000012055 fruits and vegetables Nutrition 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- 238000004321 preservation Methods 0.000 description 4
- 239000003814 drug Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 230000001408 fungistatic effect Effects 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 241000233855 Orchidaceae Species 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000004320 controlled atmosphere Methods 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 230000035784 germination Effects 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000000241 respiratory effect Effects 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 206010021143 Hypoxia Diseases 0.000 description 1
- 240000005319 Sedum acre Species 0.000 description 1
- 235000014327 Sedum acre Nutrition 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000010433 feldspar Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 230000029058 respiratory gaseous exchange Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Medicines Containing Plant Substances (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention relates to a preparation method of dendrobium plasmogen oral liquid. The preparation method comprises the following steps: (1) selecting fresh dendrobium branches, removing earth and impurities, rinsing the fresh dendrobium branches without the earth or the impurities with clean water, and airing the rinsed dendrobium branches; (2) processing the treated dendrobium branches with hot water for 4-5 minutes under the condition of boiling water of 100 DEG C, so that chlorophyll enzymes are completely inactivated, after the dendrobium branches are processed with the hot water, rapidly cooling the hot dendrobium branches, and draining water; (3) protecting color, mixing the fresh dendrobium and a saline solution according to the weight ratio of the fresh dendrobium to the saline solution being 1:10 so as to obtain a mixture, conveying the mixture into a pulping machine, and pulping the mixture for 10 minutes to obtain dendrobium plasmogen; and (4) filtering the dendrobium plasmogen by using a double-layer gauze to obtain filter residues, subsequently filtering the filter residues, performing color protection on the filtered filter residues, and seasoning the filter residues after the color protection to obtain the dendrobium plasmogen oral liquid. In order to achieve a better bacteriostasis effect and conceal foreign flavor to obtain delicate fragrant mouth feel, pummelo pericarp essential oil according to the concentration of 0.2-0.3 [mu] g/ml is added to the dendrobium plasmogen, and the dendrobium plasmogen and the pummelo pericarp essential oil are vibrated for 20 minutes through microwaves, so that the pummelo pericarp essential oil is uniformly distributed in the plasmogen. The essential oil can conceal primary foreign flavor of dendrobium, so that excellent mouth feel of the oral liquid can be guaranteed.
Description
Technical field:
The invention belongs to technical field of preservation of fresh, relate to stem of noble dendrobium oral liquid, especially a kind of preparation method of stem of noble dendrobium magma oral liquid.
Background technology:
The Chinese medicine stem of noble dendrobium is the orchid family (Orchidaceae) Dendrobium (DendrobiumSw.) herbaceos perennial, about there are 500 genus in the whole world, kind more than 15000, nearly 76 kinds of China, wherein has 33 kinds to be purchased using the former plant as the commodity stem of noble dendrobium.The most common kind is the celestial grass 2 kinds of HERBA DENDROBII-whorlleaf stonecrop herb and dendrobium candidum-the first.The seed of dendrobium candidum is minimum, without endosperm, not containing the nutritional labeling that can supply growth of seedling, therefore, natural propagation rate is extremely low.Add artificial exhaustive exploitation and the destruction of ecological environment, its wild resource is endangered, and within 1987, State Council is classified as National Wild Conservative Plants.At present, artificial cultivation dendrobium candidum has obtained certain achievement, effectively ensure that the demand of market to the stem of noble dendrobium, decreases the exhaustive exploitation to wild resource simultaneously, protect wild resource.According to the preliminary statistics, the existing dendrobium candidum cultivated area of China is about 267km2, and produce fresh treaty 1,000,000 kg per year, practitioner about 400,000 people, the output value 5,000,000,000 yuan, wherein Zhejiang accounts for more than 50%, and plantation area is mainly 10 provinces, cities and regions such as Yunnan, Guangxi, Zhejiang, Fujian.Raising along with people's living standard and the understanding to health, the demand of market to the stem of noble dendrobium increases day by day, present dendrobium candidum market mainly in Zhejiang, Shanghai, Hongkong and Macro, south east asia, in addition, western developed country carries out long-term import to the stem of noble dendrobium of China.In the last few years, universal along with TCM Culture, the Chinese medicine stem of noble dendrobium such as also to start to Beijing at the North City expansion, and consumption figure constantly increases, visible, the wide market of the stem of noble dendrobium.The stem of noble dendrobium because of its higher medical value and health-care efficacy, can reach at home 1000 yuan per jin, for local farmers provides economic benefit, facilitate the fast development of stem of noble dendrobium industry.
Controlled atmosphere technology refers to a kind of preservation technique because of storage period and shelf life of usually extending food such as gas componant by adjusting and control in storage environment and ratio and control temperature, humidity and ethene etc.Adopt rear fruits and vegetables and still carry out respiration, constantly consume the nutriment of self, the nutritional labeling of fruits and vegetables, quality, local flavor etc. are changed, affects the edibility of fruits and vegetables.Controlled atmosphere technology effectively can be suppressed fruits and vegetables respiratory intensity by the environment manufacturing hypoxia-hypercapania, be postponed the appearance of respiratory climacteric, thus extends the storage time of fruits and vegetables.
The stem of noble dendrobium is that the traditional rare Chinese medicine of China has higher medical value and health care, dark liking, especially based on the fresh goods stem of noble dendrobium by consumers in general.Fresh goods stem of noble dendrobium normal temperature is placed easy dehydration, germination, is rotted, and research fresh goods stem of noble dendrobium preservation technique can effectively solve the quality problem occurred in stem of noble dendrobium storage.In the storage period of the downward feldspar dry measure used in former times of prerequisite of guarantee stem of noble dendrobium quality, avoid causing precious resources to waste.The research of stem of noble dendrobium preservation technique, the problem such as effective solve dendrobe fresh product dehydration, germination, rot, pulls stem of noble dendrobium industry restructuring optimization and upgrading, for agricultural product volume increase, farmer richness escort.
Summary of the invention:
The object of the invention is to overcome the deficiencies in the prior art part, provide that a kind of mouthfeel is good, the stem of noble dendrobium magma oral liquid of long shelf-life and preparation method thereof.
In order to realize above object, the technical solution adopted in the present invention is as follows:
A preparation method for stem of noble dendrobium magma oral liquid, step is as follows:
(1) select fresh stem of noble dendrobium branch, removing earth and impurity, dry after clear water rinsing;
(2), under 100 DEG C of boiling water conditions, by the stem of noble dendrobium branch blanching 4-5min after process, make chlorophyllase complete deactivation, cool rapidly after blanching, drain away the water;
(3) configure the saline solution colour protecting liquid of 1wt% ~ 2wt%, mixed by the fresh stem of noble dendrobium with the ratio of saline solution according to weight ratio 1:10, send into beater and pull an oar, the time is 10min, obtains stem of noble dendrobium magma;
(4) use double gauze to filter to obtain filter residue to stem of noble dendrobium magma;
(5) in filter residue, add saline solution colour protecting liquid according to 1:2 ratio and carry out secondary making beating;
(6) the stem of noble dendrobium magma after (4) liquid of being pulled an oar by secondary filter with step mixes, and joins in stem of noble dendrobium magma, enzymolysis 2h under 50 DEG C of water bath condition according to the ratio of weight ratio cellulase 1.5%, pectase 2.0%;
(7) after enzymolysis completes, filtrate is mixed fresh juice PH and is adjusted to 4.0-5.0 and carries out secondary and protect look, antibacterial, seasoning by the malic acid of the green apple inspissated juice and 1-2wt% that add 5%-10%, adopt centrifugal separator to be separated filtrate, centrifuge speed controls at 5000r/min, centrifugation time 20min;
Centrifugal complete after, under the pressure of 1-2Mpa, multi-pipeline bundle type micro-hole filter membrane filters to use aperture to be 0.2-1.0 μm, removes large molecular impurity, obtains the dendrobium candidum composite fresh juice of clarification;
(9) use homogenizer to carry out homogeneous, homogenizer Stress control is at 2 ~ 5MPa; Dendrobium candidum composite fresh juice vacuum degassing machine after homogeneous carries out degassed; Obtain stem of noble dendrobium magma oral liquid.
And after (8) step obtains the dendrobium candidum composite fresh juice of clarification, add Essential Oil From Citrus Grandis Peel according to the concentration of 0.2 μ g/ml-0.3 μ g/ml, microwave concussion 20min, makes Essential Oil From Citrus Grandis Peel be evenly distributed in magma; WMH-1 type pulsed oil-water emulsion device is adopted to carry out emulsification to adding the fresh juice of the Essential Oil From Citrus Grandis Peel stem of noble dendrobium.
Advantage of the present invention and good effect as follows:
The present invention obtains delicate fragrance mouthfeel for reaching good fungistatic effect and covering assorted taste, in stem of noble dendrobium magma, adds Essential Oil From Citrus Grandis Peel according to the concentration of 0.2 μ g/ml-0.3 μ g/ml, and microwave concussion 20min, makes Essential Oil From Citrus Grandis Peel be evenly distributed in magma.The assorted taste that the stem of noble dendrobium covered of essential oil is original, can ensure the best mouthfeel of oral liquid.
The present invention is after enzymolysis completes, and filtrate is mixed fresh juice PH and is adjusted to 4.0-5.0 and carries out secondary and protect look, more antibacterial seasoning by the malic acid of the green apple inspissated juice and 1-2wt% that add 5%-10%, can ensure the mouthfeel of stem of noble dendrobium oral liquid.
Detailed description of the invention:
Below by specific embodiment, the invention will be further described, and following examples are descriptive, is not determinate, can not limit protection scope of the present invention with this.
A preparation method for stem of noble dendrobium magma oral liquid, step is as follows:
(1) select fresh stem of noble dendrobium branch, removing earth and impurity, dry after clear water rinsing.
(2), under 100 DEG C of boiling water conditions, by the stem of noble dendrobium branch blanching 4-5min after process, make chlorophyllase complete deactivation, cool rapidly after blanching, drain away the water.
(3) configure the saline solution colour protecting liquid of 1wt% ~ 2wt%, mixed by the fresh stem of noble dendrobium with the ratio of saline solution according to weight ratio 1:10, send into beater and pull an oar, the time is 10min, obtains stem of noble dendrobium magma.
(4) use double gauze to filter to obtain filter residue to stem of noble dendrobium magma.
(5) in filter residue, add saline solution colour protecting liquid according to 1:2 ratio and carry out secondary making beating.
(6) the stem of noble dendrobium magma after (4) liquid of being pulled an oar by secondary filter with step mixes, and joins in stem of noble dendrobium magma, enzymolysis 2h under 50 DEG C of water bath condition according to the ratio of weight ratio cellulase 1.5%, pectase 2.0%.
(7) after enzymolysis completes, filtrate is mixed fresh juice PH and is adjusted to 4.0-5.0 and carries out secondary and protect look, antibacterial, seasoning by the malic acid of the green apple inspissated juice and 1-2wt% that add 5%-10%, adopt centrifugal separator to be separated filtrate, centrifuge speed controls at 5000r/min, centrifugation time 20min.
Centrifugal complete after, under the pressure of 1-2Mpa, multi-pipeline bundle type micro-hole filter membrane filters to use aperture to be 0.2-1.0 μm, removes large molecular impurity, obtains the dendrobium candidum composite fresh juice of clarification.
(9) to mix taste for reaching good fungistatic effect and covering dendrobium candidum composite fresh juice, obtain delicate fragrance mouthfeel, in stem of noble dendrobium magma, add Essential Oil From Citrus Grandis Peel according to the concentration of 0.2 μ g/ml-0.3 μ g/ml, microwave concussion 20min, makes Essential Oil From Citrus Grandis Peel be evenly distributed in magma.
(10) adopting WMH-1 type pulsed oil-water emulsion device to carry out emulsification to adding the fresh juice of the Essential Oil From Citrus Grandis Peel stem of noble dendrobium, making that Essential Oil From Citrus Grandis Peel is molten to be scattered in magma, reach best fungistatic effect, obtain stem of noble dendrobium magma oral liquid.
(11) use homogenizer to carry out homogeneous, homogenizer Stress control is at 2 ~ 5MPa.
(12) the dendrobium candidum composite fresh juice vacuum degassing machine after homogeneous carries out degassed.
(13) brown bottle carries out filling, ultra high temperature short time sterilization, packed products after inspection.
The green apple inspissated juice that the present invention uses is commercially available prod, does not need special restriction.
Claims (2)
1. a preparation method for stem of noble dendrobium magma oral liquid, is characterized in that: step is as follows:
(1) select fresh stem of noble dendrobium branch, removing earth and impurity, dry after clear water rinsing;
(2), under 100 DEG C of boiling water conditions, by the stem of noble dendrobium branch blanching 4-5min after process, make chlorophyllase complete deactivation, cool rapidly after blanching, drain away the water;
(3) configure the saline solution colour protecting liquid of 1wt% ~ 2wt%, mixed by the fresh stem of noble dendrobium with the ratio of saline solution according to weight ratio 1:10, send into beater and pull an oar, the time is 10min, obtains stem of noble dendrobium magma;
(4) use double gauze to filter to obtain filter residue to stem of noble dendrobium magma;
(5) in filter residue, add saline solution colour protecting liquid according to 1:2 ratio and carry out secondary making beating;
(6) the stem of noble dendrobium magma after (4) liquid of being pulled an oar by secondary filter with step mixes, and joins in stem of noble dendrobium magma, enzymolysis 2h under 50 DEG C of water bath condition according to the ratio of weight ratio cellulase 1.5%, pectase 2.0%;
(7) after enzymolysis completes, filtrate is mixed fresh juice PH and is adjusted to 4.0-5.0 and carries out secondary and protect look, antibacterial, seasoning by the malic acid of the green apple inspissated juice and 1-2wt% that add 5%-10%, adopt centrifugal separator to be separated filtrate, centrifuge speed controls at 5000r/min, centrifugation time 20min;
Centrifugal complete after, under the pressure of 1-2Mpa, multi-pipeline bundle type micro-hole filter membrane filters to use aperture to be 0.2-1.0 μm, removes large molecular impurity, obtains the dendrobium candidum composite fresh juice of clarification;
(9) use homogenizer to carry out homogeneous, homogenizer Stress control is at 2 ~ 5MPa; Dendrobium candidum composite fresh juice vacuum degassing machine after homogeneous carries out degassed; Obtain stem of noble dendrobium magma oral liquid.
2. the preparation method of stem of noble dendrobium magma oral liquid according to claim 1, it is characterized in that: after (8) step obtains the dendrobium candidum composite fresh juice of clarification, Essential Oil From Citrus Grandis Peel is added according to the concentration of 0.2 μ g/ml-0.3 μ g/ml, microwave concussion 20min, makes Essential Oil From Citrus Grandis Peel be evenly distributed in magma; WMH-1 type pulsed oil-water emulsion device is adopted to carry out emulsification to adding the fresh juice of the Essential Oil From Citrus Grandis Peel stem of noble dendrobium.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105901219A (en) * | 2016-04-20 | 2016-08-31 | 安徽舒绿茶业有限公司 | Dendrobe ginger tea and preparation method for same |
CN108478711A (en) * | 2018-05-23 | 2018-09-04 | 云南农业大学 | A kind of dendrobium candidum nutrition liquid preparing process |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103099285A (en) * | 2013-01-18 | 2013-05-15 | 六安同济生生物科技有限公司 | Preparation method of dendrobium huoshanense composite fresh juice and oral liquid thereof |
CN103300450A (en) * | 2013-06-14 | 2013-09-18 | 浙江大学 | Preparation method of raw dendrobium officinale pulp beverage |
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2015
- 2015-07-16 CN CN201510422475.4A patent/CN105077272A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103099285A (en) * | 2013-01-18 | 2013-05-15 | 六安同济生生物科技有限公司 | Preparation method of dendrobium huoshanense composite fresh juice and oral liquid thereof |
CN103300450A (en) * | 2013-06-14 | 2013-09-18 | 浙江大学 | Preparation method of raw dendrobium officinale pulp beverage |
Non-Patent Citations (1)
Title |
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郝鹏飞等: "《天然药物化学》", 31 July 2014, 中国农业大学出版社 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105901219A (en) * | 2016-04-20 | 2016-08-31 | 安徽舒绿茶业有限公司 | Dendrobe ginger tea and preparation method for same |
CN108478711A (en) * | 2018-05-23 | 2018-09-04 | 云南农业大学 | A kind of dendrobium candidum nutrition liquid preparing process |
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Inventor after: Shao Nan Inventor after: Li Xihong Inventor after: Li Limei Inventor after: Hao Meimei Inventor before: Li Xihong Inventor before: Huo Yuxia Inventor before: Hao Meimei Inventor before: Liu Jia Inventor before: Liu Xia |
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Application publication date: 20151125 |