CN105067401B - A kind of device and operating method for quickly reclaiming transparent native mesopore solution - Google Patents

A kind of device and operating method for quickly reclaiming transparent native mesopore solution Download PDF

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Publication number
CN105067401B
CN105067401B CN201510443325.1A CN201510443325A CN105067401B CN 105067401 B CN105067401 B CN 105067401B CN 201510443325 A CN201510443325 A CN 201510443325A CN 105067401 B CN105067401 B CN 105067401B
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transparent
thick
solution
walled vessel
conduit
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CN105067401A (en
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齐昌广
刘干斌
王艳
邓岳保
范高飞
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Ningbo University
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Ningbo University
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  • Investigation Of Foundation Soil And Reinforcement Of Foundation Soil By Compacting Or Drainage (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

The present invention relates to a kind of device and operating method for quickly reclaiming transparent native mesopore solution, the device is by thick-walled vessel, sealing ring, stress disk, what conduit and pore solution container formed, thick-walled vessel is transparent, larger interior confined pressure can be born, outer confined pressure and vertical load, sealing ring is connected with stress disk close and firm, after thick-walled vessel is pressed into, can be with closing contact on the inside of thick-walled vessel, simultaneously can under vertical pressure along thick-walled vessel Slideslip, overfall is opened up in stress disk, overfall is directly connected with conduit, the other end of conduit is deep into pore solution container, the pore solution in transparent soil for accommodating recovery, the present invention also provides the measure for reclaiming solid particle in transparent soil indirectly while transparent native mesopore solution is reclaimed.In addition, the present invention also disclosed a kind of operating method for quickly reclaiming transparent native mesopore solution.

Description

A kind of device and operating method for quickly reclaiming transparent native mesopore solution
Technical field
It is more particularly to a kind of using low viscous the present invention relates to a kind of operating method for quickly reclaiming transparent native mesopore solution The recovery technology and operating method for the transparent native mesopore solution that the mixing liquid of stickiness is formulated.
Background technology
Due to the non-transparency of traditional soil body, it is impossible to the deformation of Continuous Observation to inside soil body arbitrfary point, but With transparent native appearance and its application in Geotechnical Engineering physical simulation experiment so that observe the soil deformation and soil of inside Internal portion structures are deformed into possibility.Transparent soil is the pore solution group to be matched by transparent solid particle and refractive index Into the composition transparent native solid particle and pore solution used that current academic documents are recorded are as shown in Figure 1.It is transparent soil by with To study the mechanism problem in some Geotechnical Engineerings, such as seepage flow, shallow foundation and deep foundation.Afterwards, in order to study the transparent soil body- Interaction between works, the system of the transparent native internal modification of a non-intrusive measurement is developed again.Therefore, transparent soil is in work Irreplaceable effect has been played in the research of journey mechanism.
In transparent native application experiment, what is be most difficult to is how to configure transparent preferably transparent soil, its process for preparation It is general relatively slow.From figure 5 it can be seen that the transparent native pore solution of preparation used is by 2 kinds of changes (in addition to family 3) Learn what is be formulated with oil according to certain mass ratio or volume ratio, chemistry is generally individually smaller than the density of water body with the density of oil. In Vehicles Collected from Market, 1/10th of the price deficiency Unit Weight pore solution price of the solid particle of Unit Weight, thus it is transparent The preparation price of soil is the price decision by pore solution, in addition, transparent soil is disposable, does not possess nonexpondable spy Property, therefore currently used transparent native cost remains high.If it is possible to the transparent soil after experiment is recycled again In pore solution will reduce it is transparent soil experiment cost.However, at present during transparent native experiment, also without one kind The equipment or method of the transparent native mesopore solution of effective recycling.
Therefore, need badly at present and seek one kind and can reduce experimental cost, and can recycles transparent native mesopore solution Rapid recovery device or method seem particularly significant.
The content of the invention
The purpose of the present invention is exactly to overcome drawbacks described above, there is provided a kind of device for quickly reclaiming transparent native mesopore solution and Operating method.
A kind of device for quickly reclaiming transparent native mesopore solution, including:Thick-walled vessel, sealing ring, stress disk, conduit and Pore solution container;Thick-walled vessel is transparent, and sealing ring is connected with stress disk close and firm, is pressed into after thick-walled vessel and thickness Wall container inside is in closing contact, can under vertical pressure along thick-walled vessel Slideslip;Overfall is opened up in stress disk, is overflowed Mouth is directly connected with conduit, and the other end of conduit is deep into pore solution container.
A kind of operating method for quickly reclaiming transparent native mesopore solution, comprises the following steps:
Step 1: loosening the transparent soil prepared in transparent soil container, loose condition (of surface) is at;
Step 2: the transparent soil of loose condition (of surface) is poured into thick-walled vessel, and pour into the distilled water of same volume;
Step 3: using the mixture of the transparent soil of mini-sized blender stirring and distilled water, make the pore solution in transparent soil Suspend and rise, distilled water and transparent native solid particle sink;
Step 4: connecting stress disk and the sealing ring with overfall, overfall connects conduit, and is inserted into and fills In transparent native thick-walled vessel;
Step 5: after stress disk contacts with pore solution surface, apply vertical pressure, pore solution then passes through overfall Progressively it is transferred in pore solution container with conduit;
Step 6: stop applying vertical pressure after stress disk just contact distillation water;
Step 7: being separated using the way of distillation to pore solution, the recovery of transparent native mesopore solution is completed.
As preferred, in step 1:Pore solution in transparent soil is mixed by two kinds of different oil bodies of refractive index , a kind of refractive index of oil body is more than the refractive index of solid particle, and the refractive index of another oil body is less than the refraction of solid particle Rate, the density of each liquid is less than the density of distilled water, and is not mixed with distilled water.
As preferred, in step 5:Vertical pressure can be applied by machinery, can also manual control application.
The beneficial effects of the invention are as follows:
The present invention separates to the transparent soil configured in current experiment after use, by the transparent native of configuration Raw material extract respectively so that transparent native raw material have obtained recycling, largely avoided waste of material, save Experimental cost.
The present invention also indirectly separates the solid particle in transparent soil while being reclaimed to transparent native mesopore solution Go out, it is also can obtain recycling, further avoid waste of material, save experimental cost.
The pore solution reclaimed using the present invention can be made directly as next transparent soil model, without weighing again The pore solution that new configuration refractive index matches, saves and prepares the transparent native time.
The pore solution that can be reclaimed to the present invention carries out separated, and each mixing liquid in pore solution is divided one by one Separate out, you can the system for new pore solution is matched somebody with somebody, it can also be used to the needs of other experiments so that experiment material obtains again With make full use of.
Brief description of the drawings
Fig. 1 is the device for quickly reclaiming transparent native mesopore solution;
Fig. 2 is the Section A-A schematic diagram in Fig. 1;
Fig. 3 is the connection sectional detail drawing of sealing ring and stress disk;
Fig. 4 is the separation schematic diagram of transparent native solid particle and pore solution.
Fig. 5 is transparent native composition schematic diagram.
Description of reference numerals:1- thick-walled vessels;2- solid particles;3- distilled water;4- pore solutions;5- sealing rings;6- by Power disk;7- vertical pressures;8- overfalls;9- conduits;10- pore solution containers;The transparent soil containers of 11-;12- mini-sized blenders.
Embodiment
The present invention is described further with reference to the accompanying drawings and examples.Although the present invention will enter with reference to preferred embodiment Row description, it should be understood that being not offered as limiting the invention in the embodiment.It can be included on the contrary, the present invention will cover Alternative, modified and the equivalent in the scope of the present invention that appended claims limits.
Reference picture 1, a kind of device for quickly reclaiming transparent native mesopore solution 4 is by thick-walled vessel 1, sealing ring 5, stress What disk 6, conduit 9 and pore solution container 10 formed.Diameter=200mm, height=400mm, wall thickness are made using lucite =20mm half opening thick-walled vessel 1, external diameter=10mm is made using lucite, internal diameter=8mm, length=700mm are led Pipe 9, conduit 9 is inserted into the overfall 8 at the middle part of stress disk 6, making diameter=100mm, height=200mm, wall thickness= 10mm half opening pore solution container 10.
Reference picture 2 and Fig. 3, diameter=150mm, thickness=10mm stress disk 6 being made, the edge of stress disk 6 is concave, It is convenient that tight jail is connected with sealing ring 5, while the overfall 8 that aperture is 5mm is opened up among stress disk 6, in addition, using rubber material Material makes centerline diameter=160mm, annulus thickness=10mm annular seal ring 5, and sealing ring 5 is enclosed in stress disk 6.
Reference picture 4, it is the saturating of length × width × height × thickness=200mm × 200mm × 200mm × 10mm by the size having been used up The transparent soil of height=100mm in bright soil container 11 is poured into the thick-walled vessel 1 of opening, and adds 1L distilled water 3, is used Mini-sized blender 12 is stirred to the mixture of transparent soil and distilled water 3, and whipping process by progressively accelerating slowly, until transparent soil In pore solution 4 and solid particle 2 separate, pore solution 4 rise to top, solid particle 2 and distilled water 3 sink down into bottom Portions, then the stress disk 6 made, sealing ring 5 and conduit 9 are connected as a single entity, are inserted into thick-walled vessel 1, conduit 9 it is another One end is inserted into pore solution container 10, applies vertical pressure 7 on stress disk 6, when stress disk 6 touches pore solution 4 Liquid level when, pore solution 4 is progressively moved on in pore solution container 10 along overfall 8 and conduit 9, when stress disk 6 just connects When contacting the liquid level of distilled water 3, stop applying vertical pressure 7, and extract stress disk 6, with dropper remaining in the hole in conduit 9 Gap solution 4 is siphoned away, and is put into pore solution container 10, and finally pore solution container 10 is placed in distillation case pore solution 4 In each mixing liquid progressively separated, the quick recovery of transparent native mesopore solution 4 is completed, in addition, by thick-walled vessel 1 In distilled water 3 outwell, remaining solid particle 2 is placed in drying chamber and dried, completes the recovery of solid particle 2.

Claims (2)

  1. A kind of 1. operating method for quickly reclaiming transparent native mesopore solution, it is characterised in that including:Thick-walled vessel (1), sealing Enclose (5), stress disk (6), conduit (9) and pore solution container (10);Thick-walled vessel (1) is transparent, sealing ring (5) and stress Disk (6) close and firm connects, and is pressed into thick-walled vessel (1) afterwards with being in closing contact on the inside of thick-walled vessel (1), can be in vertical pressure It is lower along thick-walled vessel (1) interior Slideslip;Overfall (8) is opened up in stress disk (6), overfall (8) is directly connected with conduit (9), The other end of conduit (9) is deep into pore solution container (10);Comprise the following steps:
    Step 1: loosening the transparent soil prepared in transparent soil container (11), loose condition (of surface) is at;In transparent soil Pore solution (4) is mixed by two kinds of different oil bodies of refractive index, and a kind of refractive index of oil body is more than solid particle (2) Refractive index, the refractive index of another oil body is less than the refractive index of solid particle (2), and the density of each liquid is less than distilled water (3) Density, and do not mixed with distilled water (3);
    Step 2: the transparent soil of loose condition (of surface) is poured into thick-walled vessel (1), and pour into the distilled water (3) of same volume;
    Step 3: using the mixture of the transparent soil of mini-sized blender (12) stirring and distilled water (3), make the hole in transparent soil molten Liquid (4), which suspends, to be risen, and distilled water (3) and transparent native solid particle (2) sink;
    Step 4: connecting the stress disk (6) and sealing ring (5) with overfall, overfall connects conduit (9), and inserts It is interior to transparent native thick-walled vessel (1) is filled;
    Step 5: after stress disk (6) contacts with pore solution (4) surface, apply vertical pressure, pore solution (4) then passes through Overfall (8) and conduit (9) are progressively transferred in pore solution container (10);
    Step 6: stop applying vertical pressure behind stress disk (6) just contact distillation water (3);
    Step 7: being separated using the way of distillation to pore solution (4), the recovery of transparent native mesopore solution (4) is completed.
  2. 2. the operating method according to claim 1 for quickly reclaiming transparent native mesopore solution, it is characterised in that step 5 In:Vertical pressure can be applied by machinery, can also manual control application.
CN201510443325.1A 2015-07-24 2015-07-24 A kind of device and operating method for quickly reclaiming transparent native mesopore solution Active CN105067401B (en)

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CN110538506B (en) * 2019-09-25 2023-10-13 浙江海洋大学 Transparent soil pore liquid recovery device and recovery method
CN112196526A (en) * 2020-10-29 2021-01-08 西南石油大学 Transparent soil seepage model with oil-water interface and preparation method thereof

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US9207152B2 (en) * 2009-06-25 2015-12-08 Hitachi High-Technologies Corporation Pretreatment apparatus and mass analyzing apparatus equipped with the same
JP4621802B1 (en) * 2010-02-09 2011-01-26 株式会社ワールドケミカル Self-priming solid-liquid separator
CN202778681U (en) * 2012-04-27 2013-03-13 河南新大新材料股份有限公司 Micro powder automatic siphon size grading device
CN204882182U (en) * 2015-07-24 2015-12-16 宁波大学 Retrieve pore solution's in transparent soil device fast

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CN1765522A (en) * 2005-10-21 2006-05-03 南京大学 Method for treating leak oil polluted quartz beach sand

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