CN105056556B - A kind of concentration device for material liquid and its feed liquid evaporator - Google Patents
A kind of concentration device for material liquid and its feed liquid evaporator Download PDFInfo
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- CN105056556B CN105056556B CN201510565984.2A CN201510565984A CN105056556B CN 105056556 B CN105056556 B CN 105056556B CN 201510565984 A CN201510565984 A CN 201510565984A CN 105056556 B CN105056556 B CN 105056556B
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Abstract
The present invention provides a kind of liquid vaporising device and its feed liquid evaporator for using, including heater, the vaporization chamber and for making the vaporization chamber produce the vavuum pump of subnormal ambient heated for feed liquid;Have between the heater and the vaporization chamber and feed liquid is delivered to the first pipeline of the vaporization chamber and so that feed liquid is back to the second pipeline of the heater from the vaporization chamber from the heater;One end that first pipeline connects the vaporization chamber is the spiral section for making feed liquid be vortexed in the evaporator inside sidewalls shape.Spiral section is set on the first pipeline so that the vortex of downward spiral motion can be formed on the wall of vaporization chamber side by the feed liquid that vaporization chamber is entered into after spiral section, increased the evaporation specific surface area into the feed liquid of vaporization chamber, improve evaporation efficiency.
Description
Technical field
The present invention relates to concentration of liquid medicine technical field, more particularly to a kind of concentration device for material liquid and its feed liquid evaporator.
Background technology
In technical fields such as pharmacy, chemical industry, for the purification for realizing active principle is concentrated, concentration device for material liquid need to be typically used
Carry out concentration purification processes.Liquid medicine concentration device is typically heated using heater to low concentration feed liquid, using filming technology
Foams mix body is produced in the heater and foams mix body is transported in vaporization chamber by pipeline, caused under condition of negative pressure
Liquid rapid evaporation.
In existing production equipment, turned on by shorter straight-through pipeline between heater and vaporization chamber, what filming was produced
Foams mix body enters directly into evaporator and quickly drops into base of evaporator and is back to heat exchanger, it is impossible to which effective increase is steamed
Fermentation product, reduces evaporation efficiency, increases energy resource consumption.
The content of the invention
To improve the thickening efficiency of existing concentration device for material liquid, energy ezpenditure being reduced, the invention provides a kind of feed liquid
Evaporator;Separately present invention also offers a kind of concentration device for material liquid using foregoing feed liquid evaporator.
The present invention provides a kind of feed liquid evaporator, including heater, the vaporization chamber and described for making heated for feed liquid
Vaporization chamber produces the vavuum pump of subnormal ambient;Have between the heater and the vaporization chamber and feed liquid is conveyed from the heater
To the vaporization chamber the first pipeline and cause that feed liquid is back to the second pipeline of the heater from the vaporization chamber;Described
One end that one pipeline connects the vaporization chamber is the spiral section for making feed liquid that vortex is formed in the evaporator inside sidewalls.
Spiral section is set on the first pipeline so that can be in vaporization chamber by the feed liquid that vaporization chamber is entered into after spiral section
The vortex of downward spiral motion is formed on the wall of side, the evaporation specific surface area into the feed liquid of vaporization chamber is increased, evaporation is improve
Efficiency.
Optionally, first pipeline and the heater connection end are straightway;The straightway and the spiral section
Seal and conduct.
Straightway is set on the first pipeline, facilitates the connection of spiral section and heater.
Optionally, the rectangular cross-section of first pipeline.
Optionally, second pipeline also has the assisted circulation device for promoting feed solution flow.
Assisted circulation device is set, feed liquid filming in the heater can be preferably realized, the flow velocity of feed liquid is also improved,
While increase forms swirling helical quantity, the circulation rate of feed liquid is increased;The solute patch in feed liquid can be also reduced simultaneously
Invest the problem of heater side wall and carbonization effect feed liquid color and quality.
Optionally, the feed liquid evaporator also has foam separator;The foam separator is installed on the vaporization chamber
Upside.
Set foam separator, can make in vaporization chamber produce bubble collapse formed feed liquid liquid be back to vaporization chamber,
Prevent from entering into the service efficiency that follow-up equipment improves feed liquid.
Present invention also offers a kind of concentration device for material liquid, with the foregoing feed liquid evaporator of at least one-level.
Optionally, the concentration device for material liquid has two-stage or the multistage feed liquid evaporator;Feed liquid described in previous stage is steamed
Send out the heating intake line conducting of the vaporization chamber of device and the heater of feed liquid evaporator described in rear stage.
Concentration device for material liquid sets feed liquid evaporator more than two-stage or two-stage, can fully use previous stage vaporization chamber feed liquid
The steam for producing is evaporated as rear stage heat source, reduces the heat input of whole concentration device for material liquid, and then reduce energy
Consumption.
Optionally, the concentration device for material liquid also has stirring evaporator;The stirring evaporator has agitator and institute
State the stirring vaporization chamber of agitator circulation conducting and for making the stirring vaporization chamber produce the second vavuum pump of subnormal ambient;Institute
Agitator is stated with feed liquid base of evaporator conducting described in afterbody.
Set stirring evaporator, by mobility it is poor, can not be by the feed liquid agitation cycle of feed liquid evaporator evaporation solvent
Flowing, in the subnormal ambient evaporation of stirring vaporization chamber, can further improve the concentrating degree of feed liquid, adapt to some particular/special requirements.
Optionally, the concentration device for material liquid also includes cooling component;The material of the cooling component and afterbody
The vaporization chamber of liquid evaporator is turned on and/or turned on the stirring vaporization chamber.
Heat recovery during feed liquid is evaporated itself or feed liquid agitator by cooling component is set, heat dissipation is reduced, energy is improved
Thermal pollution is decreased while the utilization ratio of source and other pollute.
Optionally, the cooling component includes the first cooler, the second cooler and the first gas-liquid separator;Described first
The vaporization chamber of the feed liquid evaporator of cooler and afterbody is turned on and/or turned on the stirring vaporization chamber;Institute
The first cooler and second cooler is stated to be turned on by first gas-liquid separator.
Brief description of the drawings
Fig. 1 is concentration device for material liquid schematic diagram of the present invention
Fig. 2 is A-A faces schematic diagram in Fig. 1.
Specific embodiment
To make those skilled in the art be better understood from technical scheme, below in conjunction with the accompanying drawings and specific embodiment
The present invention is described in further detail.
Concentration device for material liquid in the present invention, low concentration feed liquid is collectively promoted by the collective effect of heating and negative-pressure vacuum
The evaporation of middle solvent, realizes the concentration purification of feed liquid.
Fig. 1 is concentration device for material liquid schematic diagram of the present invention, and it has feed liquid evaporator and is steamed with feed liquid as can be seen from Figure
The cooling component that hair device is connected in series.Wherein feed liquid evaporator realizes the concentration purification of feed liquid, and cooling component realizes follow-up heat
Recycling (cooling component be not to realize feed liquid concentrating function).
Specifically, feed liquid evaporator includes heater 1, vaporization chamber 2 and vaporization chamber 2 is produced the vacuum of subnormal ambient
Pump.Heater 1 is used to be heated to being poured in feed liquid therein, improves the temperature of feed liquid, and cause that solvent is waved by heating
Send out the solution expansion filming around the bubbles entrain for producing.Vaporization chamber 2 is a sealed shell of tank structure, and volume is larger, in vavuum pump
Under suction function, vaporization chamber 2 forms the subnormal ambient of subatmospheric pressure;The gentle pass for being pressed into inverse ratio of volatilization according to liquid
System, evaporation of the subnormal ambient beneficial to feed liquid.
Between heater 1 and vaporization chamber 2 have two connecting pipelines, respectively positioned at upside, for by feed liquid from
Heater 1 be transported to the first pipeline 3 of vaporization chamber 2 and positioned at downside, make vaporization chamber 2 in feed liquid be back to the of heater 1
Two pipelines 4.Feed liquid is circulated and solvent flashing, solute concentration between heater 1, the first pipeline 3, the pipeline 4 of vaporization chamber 2 and second
Gradually increase.
The pipeline of traditional feed liquid evaporator, connection heater 1 and vaporization chamber 2 is shorter straight line pipeline, and filming is produced
Foam material liquid be rapidly introduced into vaporization chamber 2 by shorter straight line pipeline and hurtle down under gravity, be deposited on steaming
The hair bottom of room 2.So, feed liquid do not have enough surface areas evaporated in subnormal ambient, it is necessary to circulation time more long and compared with
Many heat consumptions can be only achieved certain concentration value.
To improve the evaporation efficiency of feed liquid, evaporation efficiency can be improved by increasing the method for the specific surface area that feed liquid is evaporated.
Therefore, the end of the first pipeline 3, that is, the part of the conducting vaporization chamber 2 of the first pipeline 3 are set to spiral section 31 by the present invention.
Using this structure, the gas-liquid mixed feed liquid that filming is produced from heater 1 generates rotation in spiral section 31, in spiral section 31
End be cut into the inside of vaporization chamber 2, the vortex of rotation is formed along the surface of vaporization chamber 2, rather than the direct of such as traditional structure
The mode of falling falls, and improves the specific surface area of feed liquid evaporation, that is, improves the disengagement area of unit volume feed liquid, increases
The evaporation rate of feed liquid.
Fig. 2 be Fig. 1 in A-A faces schematic diagram, the horizontal cross-section of its coupling part for having intercepted the pipeline 3 of vaporization chamber 2 and first,
Can be seen that the spiral section 31 of the first pipeline 3 in figure is end and the tangent semicircle of side wall of vaporization chamber 2.It is contemplated that end coils extend
Direction is not completely tangent both representatives with the plane tangent of vaporization chamber 2, and the extension of spiral section 31 can be tangent under ideal conditions
In the side wall of vaporization chamber 2, and the spiral section 31 of other positions can not be tangential on vaporization chamber 2.It should be noted that spiral section in Fig. 2
31 is a kind of special circumstances for semicircle, or other angles or characteristic spiral section 31.
It is also seen that vaporization chamber 2 can be led for the vaporization chamber 2 that section is circle, that is, whole vaporization chamber 2 from Fig. 2
Body (excluding two ends connection, hermetic unit) can be cylindrical structure;Certainly, its section is alternatively the polygonized structure of other evaginations,
And the formation of without prejudice to swirling helical;However, it is contemplated that under the premise of identical sectional area and volume, other polygonized structure phases
Evaporation efficiency for the vaporization chamber 2 of cylindrical structure wants smaller.
Separately it is noted that heater of the invention 1 can be using the steam heating used in conventional art or high-pressure water heating
The modes such as heating, the electrical heating that can be also used using other field, as long as realizing improving feed temperature and filming.But consider
Using high-temperature steam or high-pressure water heating mode of heating can be relatively stable maintain heating-up temperature, reduce heating process in temperature wave
The dynamic influence to feed liquid, preferably steam heating or high-pressure water heating mode of heating.Additionally, considering that it can from the structure of heater 1
Think tube heater 1, or baffle heater 1, but it should ensure in heater 1 can preferable filming, prevent because
The space of heater 1 it is smaller and make bubble quick crashing, reduce filming efficiency.
From amechanical angle analysis, it is vortexed to be formed, the feed liquid entered into vaporization chamber 2 from the spiral section 31 of the first pipeline 3 should
It is the bigger the better when with certain speed, and speed;And only may can not cause that feed liquid speed is enough by spiral section 31
Greatly.
To increase the speed that circulates of feed liquid, the present invention is provided with the power-assisted for promoting feed solution flow in the second pipeline 4
EGR 5, by the effect of assisted circulation device 5, while increasing the filming efficiency and cycle rate of feed liquid, also improves
Into the feed liquid speed of vaporization chamber 2 so that the spiral quantity of formation increases, and improves evaporation specific surface area.Separately it is contemplated that due to helping
The impetus of power EGR 5 increased the flowing of feed liquid, can also prevent the attaching viscosity on the heat exchange wall of heater 1 larger
Feed liquid solute and reduce heat exchange efficiency and prevent the solute from influenceing concentrate face in the heat exchange wall side high temperature cabonization of heater 1
Color, quality.Assisted circulation device 5 can be relatively conventional centrifugal pump, axial-flow pump or mixed-flow pump.Certainly, can also be not provided with helping
Power EGR 5, the flow circuit of feed liquid is promoted only with heater 1 plus the effect of thermogenetic filming.
It is also contemplated that be under negative pressure state because the first pipeline 3 and vaporization chamber 2 are turned on, from the gas of the outflow of heater 1
Liquid mixed liquor is capable of achieving solvent evaporation in the first pipeline 3.To increase the evaporation rate in the first pipeline 3, can be by first
Pipeline 3 is set to rectangle pipeline, increases the area in gas-liquid separation face;Certainly, for example traditional circular pipe in other kinds of section
Also evaporation of the foregoing feed liquid in the first pipeline can be realized, but evaporation effect may be not so good as rectangle pipeline.
The settable multistage foregoing feed liquid evaporator of concentration device for material liquid in the present invention.Multistage feed liquid evaporator string
Connection connection, realizes the concentration step by step of feed liquid, makes full use of heat;Certainly, can also be steamed only with one-level feed liquid according to the actual requirements
Hair device.Concentration device for material liquid in Fig. 1 is exactly to employ two-stage feed liquid evaporator.Concentration device for material liquid in Fig. 1 is employed
Water is used as feed liquid medium, wherein the feed liquid evaporator positioned at front side is the first evaporator, it is the positioned at the feed liquid evaporator of rear side
Two evaporators, the heating intake line conducting of the heater 1 of the feed liquid evaporator of vaporization chamber 2 and second of the first feed liquid evaporator,
Namely from the first feed liquid evaporator exclude steam as the second feed liquid evaporator thermal source, through the second feed liquid evaporator plus
Hot device 1 is transferred to the feed liquid being located in the second feed liquid evaporator.Certainly, job requirement can not be reached in first order vaporization chamber heat
When, can also introduce extraneous steam to rear stage heater.
The feed liquid of the second feed liquid evaporator is obtained by the first feed liquid evaporator evaporation partial solvent.It is to steam the first feed liquid
The feed liquid for sending out device transfers to the second feed liquid evaporator, and the two sets connecting pipeline in bottom section, and control is provided with connecting pipeline
The valve whether system turns on.Additionally, also there is compensator and delivery pump and corresponding valve in the first feed liquid evaporator front end, use
In the low concentration feed liquid of storage preamble production process production, and level condition and concentration situation according to the first feed liquid evaporator to
First feed liquid evaporator pumps new feed liquid.Above valve can use magnetic valve, by the opening and closing of each magnetic valve of Collaborative Control,
Realize the conveying of various concentrations feed liquid.Pipeline is also seen that the assisted circulation device 5 in each feed liquid evaporator from Fig. 1
Can be used as the power source to rear stage evaporator conveying feed liquid.
Fig. 1 not show but the core of concentration device for material liquid of the invention, also by its supporting thermal source supply line
Show.Corresponding steam supply pipe road directly provides saturated vapor, return duct to the heater 1 in the first feed liquid evaporator
Flow back residual steam and condensate on road;The high-temperature steam excluded by the top of vaporization chamber 2 in the first feed liquid evaporator supplies to pass by the road
The import of heater 1 of the second feed liquid evaporator is transported to the feed liquid heating in the second feed liquid evaporator, and is returned by return line
It flow to the return line of thermal source supply line.Additionally, being provided with steam trap dress in steam supply pipe road and return line
Put, be automatically drained out steam condensate and on-condensible gas in firing equipment and pipeline.
Foregoing concentration device for material liquid employs water as feed liquid solvent, therefore can directly by previous stage vaporization chamber
2 steam is conducted to rear stage heater 1.As used other media such as ethanol, ketone as solvent, to realize this class solvent
Recycling, reduce pollution, then connection method can not set described above, but the completely self-contained thermal source supply line of setting
With feed liquid pipeline, it is impossible to realize the intersection connection of the two, also cannot be using the steam of previous stage generation as rear stage heater
Thermal source, the valve in corresponding previous stage vaporization chamber 2 and rear stage heater connecting pipeline need close.
Simultaneously, it is also noted that because part feed liquid can be expanded to foam in previous stage vaporization chamber 2, containing big in foam
The feed liquid solute of amount, the heater 1 for being directly conducted to rear stage feed liquid evaporator by pipeline can cause a large amount of of active principle
Waste.Therefore, such as Fig. 1, foam separator 6 is additionally provided with the upside of previous stage vaporization chamber 2, will be taken using foam separator 6
Bubble collapse with active principle is into feed liquid liquid and feed liquid liquid is back to vaporization chamber 2, and only causes that steam passes through pipeline
It is transferred to the heater 1 of rear stage.As a kind of possible situation, such as technological parameter or feed liquid characteristic will not in vaporization chamber 2 shape
Into a large amount of foams, foam separator 6 can be also not provided with.
The core to concentration device for material liquid is analyzed above, and the concentration device for material liquid in accompanying drawing 1 employs multistage material
Liquid evaporator, it should be noted that according to application demand, one-level feed liquid evaporator also can be only set.
For some fields, although feed concentration is very high, but still its use requirement can not be met (such as in Chinese herbal medicine industry
Common Chinese medicinal granule or Crataegi pill etc.), it is necessary to further concentration.And due to dense, using foregoing feed liquid evaporator
Can not filming, feed solution flow it is also very poor.Therefore, concentration device for material liquid of the invention is also provided with for this applicable cases
Stirring evaporator 8.
There is stirring evaporator 8 agitator 81 and agitator 81 to circulate the stirring volatilization room 82 of conducting and for making stirring
Volatilization room 82 produces the vavuum pump of subnormal ambient.Vavuum pump can be using the vavuum pump that above feed liquid evaporator is used, or list
The vavuum pump for solely setting.
Stirring evaporator 8 is connected by pipeline with the feed liquid evaporator of afterbody.Reached in afterbody feed liquid evaporator
After being delivered to the agitator 81 of stirring evaporator 8 to certain density feed liquid, stirred using agitator 81 and be delivered to stirring and waved
Hair room 82, the solvent evaporation in realizing feed liquid under subnormal ambient;After feed concentration in entirely stirring evaporator 8 is up to standard, just
Concentration feed liquid up to standard can be discharged.To improve the stirring feed solution flow efficiency of evaporator 8, corresponding pressurization can be also set in pipeline
Pump.
Certainly, as without the demand for further concentrating feed liquid, can also be not provided with stirring evaporator 8, be evaporated only with feed liquid
Device.
To realize the recycling of energy, the concentration device for material liquid in Fig. 1 is also provided with cooling down component 7.Using stirring
In the case of evaporator 8, cooling component 7 may be provided at stirring volatilization room 82 and the evaporation of afterbody feed liquid of stirring evaporator 8
The exhaust ports of vaporization chamber 2 of device, the heat that will be stirred in the steam that evaporator 8 and feed liquid afterbody feed liquid evaporator are excluded is returned
Receive;Relative to cooling component 7, stirring evaporator 8 and afterbody feed liquid evaporator are preferably and are set up in parallel.Such as it is not provided with stirring
Evaporator 8, can will directly cool down the exhaust ports that component 7 is arranged on the vaporization chamber 2 of afterbody feed liquid evaporator.It is dense from evaporating
The functional perspective of contracting considers that cooling component 7 is not the essential element for realizing this function, and such as whole enrichment facility is finally outside
The heat of discharge seldom, can also be not provided with cooling down component 7.
Cooling component 7 can be only only has one-level cooler, may also set up two grades or multistage cooler.Cooling in Fig. 1
Component 7 uses secondary coolers, including the first cooler 71, the second cooler 72, the first gas-liquid separator 73, the second gas-liquid point
From the gas-liquid separator 75 of device 74 and the 3rd.First gas-liquid separator 73 will cool down product through the first cooler 71 and the second cooler 72
Raw condensation water collection discharge, the second cooler 72 is sent to by the gas that the first cooler 71 is not cooled down;3rd gas-liquid point
The upside of the second cooler 72 is arranged on from device 75, will be discharged by the on-condensible gas of the second cooler 72;Second gas-liquid separator
74 by the condensation water collection discharged from the vaporization chamber 2 of afterbody feed liquid evaporator and are sent to the row of the first gas-liquid separator 73
Go out.Certainly, the second gas-liquid separator 74, the 3rd gas-liquid separator 75 can be also not provided with, the first gas-liquid separator 73 is directly used
Separate aqueous vapor.
Cooler in cooling component 7 can use water-cooling pattern, can also use other high-performance coolant refrigeration modes.It is special
It is not directed to using the concentration device for material liquid of ethanol equal solvent, cooling component 7 is preferably with high-performance coolant refrigeration, raising ethanol
Organic efficiency.It is contemplated that such as using ethanol as solvent, then should be direct per the vaporization chamber of one-level feed liquid evaporator
The follow-up cooling component 7 of connection.
In an embodiment of the present invention, using above-described all parts make a kind of general structure as described in Figure 1
Concentration device for material liquid, needing to realize at the pipeline that special time conducting, special time disconnect there is provided magnetic valve, in
The work of control machine Collaborative Control each magnetic valve.Feed liquid starts through balancing after latter hour of the first feed liquid evaporator is delivered in implantation
Continuously output meets the concentration feed liquid of technological requirement concentration.In the case where other process conditions are constant, this feed liquid
Enrichment facility performance is 1.5 times of original equipment, and energy consumption is only the 25% of original equipment.
The concentration device for material liquid in the embodiment of the present invention and its feed liquid evaporator are described in detail above.Herein should
Principle of the invention and implementation method are set forth with specific case, the explanation of above example is only intended to help and manages
Core concept of the invention is solved, without departing from the principles of the present invention, can also some improvement and modification be carried out to the present invention,
These are improved and modification also falls within the scope of the present invention.
Claims (4)
1. a kind of concentration device for material liquid, it is characterised in that:With at least one-level feed liquid evaporator, the feed liquid evaporator, including
Heater (1), vaporization chamber (2) for feed liquid heating and the vavuum pump for making the vaporization chamber (2) generation subnormal ambient;Institute
State to have between heater (1) and the vaporization chamber (2) and feed liquid is delivered to the of the vaporization chamber (2) from the heater (1)
One pipeline (3) and cause that feed liquid is back to second pipeline (4) of the heater (1) from the vaporization chamber (2);Its feature exists
In:First pipeline (3) connects one end of the vaporization chamber (2) to make feed liquid be formed in the vaporization chamber (2) inside sidewalls
The spiral section (31) of vortex;First pipeline (3) is straightway (32) with the heater (1) connection end;The straightway
(32) sealed and conducted with the spiral section (31);The rectangular cross-section of first pipeline (3);
Second pipeline (4) also has the assisted circulation device (5) for promoting feed solution flow;Also there is foam separator
(6);The foam separator (6) is installed on the upside of the vaporization chamber (2);
The concentration device for material liquid also has stirring evaporator (8);Stirring evaporator (8) is with agitator (81) and institute
State stirring volatilization room (82) of agitator (81) circulation conducting and for making stirring volatilization room (82) produce subnormal ambient
Vavuum pump;The agitator (81) turns on vaporization chamber (2) bottom of feed liquid evaporator described in afterbody.
2. concentration device for material liquid according to claim 1, it is characterised in that:With two-stage or the multistage feed liquid evaporation
Device;The vaporization chamber (2) of feed liquid evaporator described in previous stage and the heater (1) of feed liquid evaporator described in rear stage
Heating intake line conducting.
3. the concentration device for material liquid according to any one of claim 1 or 2, it is characterised in that:Also include cooling component (7);
Cooling component (7) is waved with the vaporization chamber (2) conducting of the feed liquid evaporator of afterbody and/or with the stirring
Hair room (82) conducting.
4. concentration device for material liquid according to claim 3, it is characterised in that:Cooling component (7) includes the first cooling
Device (71), the second cooler (72) and the first gas-liquid separator (73);First cooler (71) and afterbody it is described
The vaporization chamber (2) of feed liquid evaporator is turned on and/or turned on stirring volatilization room (82);First cooler (71)
Turned on by first gas-liquid separator (73) with second cooler (72).
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Effective date of registration: 20230628 Address after: No. 985, Baihe Road, High tech Zone, Bozhou City, Anhui Province 236000 Patentee after: Anhui Huili Equipment Technology Co.,Ltd. Address before: Jiajiu Road, Kalun Industrial Park, Jiutai Economic Development Zone, Changchun City, Jilin Province, 130507 Patentee before: JILIN HUILI MODERN LIGHT INDUSTRIAL EQUIPMENT Co.,Ltd. |
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