CN105043933B - A kind of high parameter fracturing fluid property test evaluation device - Google Patents
A kind of high parameter fracturing fluid property test evaluation device Download PDFInfo
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Abstract
The invention discloses a kind of high parameter fracturing fluid property test evaluation devices, including liquid CO2Pump note unit, aqueous fracturing fluid base fluid pump note unit, foaming agent pump note unit, CO2The liquid passage inlet of foam maker in the outlet connection foaming of pump note unit and heating unit；The fluid path import of the outlet connection foam maker of aqueous fracturing fluid base fluid pump note unit；Foaming agent pump note unit is separately connected CO by a diversion three-way2The export pipeline of pump note unit and aqueous fracturing fluid base fluid pump note unit；Foaming and the outlet of heating unit connect rheology and friction test unit, heat exchange test cell, leak-off and core damage test cell by Three branched pipe road and valve；The test cell that exchanges heat connects rheology and friction test unit, leak-off and core damage test cell by two branch lines and valve；Rheology and friction test unit are connect with leak-off and core damage test cell.
Description
Technical field
The present invention relates to the experimental provisions that fracturing fluid property in oil-gas field development geology transformation process is tested.
Background technology
With the fast development of national economy, the consumption of energy-consuming level especially petroleum resources is also quick year by year
Increase.2014,3.08 hundred million tons of China's whole year net importation oil, dependence on foreign countries for oil reached 59.5%；Imported gas amount
For 590 billion cubic meters, increase by 11.5% on a year-on-year basis, external dependence degree rises to 32.2%, and the situation risen year by year is presented.
The explored oil-remaining recoverable reserves per capita in China are only that the world is averaged 1/10th of reserves, and wherein Low Permeability Oil/gas is remote
Scape stock number accounts for the 49% and 42.8% of national total resources respectively.Low Permeability Oil/gas proportion in following China's oil and gas production
To persistently it increase.Hypotonic-special low permeability oil field has porosity low, the feature of permeability difference.This geologic feature determines
The difficulty and expense of its oil-gas exploration and exploitation are huge, it is necessary to could obtain the economic exploitation valence using advanced volume increase production technique
It is worth and realizes and is produced in increasing the storage.Therefore implement fracture technology exactly solve to face during China's oil and gas development at this stage it is tired
Difficult one of most effective means.Hydraulic fracturing technology application starts from nineteen forty-seven earliest, has carried out experiment in Texas, USA
Research, and effect of increasing production is achieved, later with the gradual progress of technology, achieve prodigious development.Hydraulic fracturing is mainly
In discharge capacity injection well by ground high pressure pump group by high-viscous liquid to substantially exceed formation absorption ability, immediately near shaft bottom
High pressure is formed, this pressure forms crack after the tensile strength of crustal stress and rock near more than shaft bottom on stratum；Continue to inject
Load fluid with proppant, crack extend forward and fill out with proppant, and crack closure is on proppant after closing well, in well
The sand packed fracture with certain geometric dimension and high flow conductivity is formed near bottom in stratum, oil/gas well is made to reach increasing yield and injection
Purpose.In recent years, external to be widely used in hydraulic fracturing technology in the exploitation of low-permeability oil gas field, and play significant
Effect.According to statistics, the 25%~30% of american petroleum reserves is to reach the economic exploitation condition by fracturing yield increasing.This technology
The oil gas field of original industrial value is set not become the oil gas field with certain production capacity, meaning is considerably beyond a well
Increasing yield and injection effect.In general, after fracturing, the individual well daily output is 3~5 times higher than before pressure break for oil/gas well.Oil simultaneously
Gas well yield can also carry out refracturing before being once decremented to pressure break.
Fracturing fluid is the liquid with certain viscosity that fracturing reform is applied in the process, and fracturing fluid is as a kind of in construction
Carrier conveying proppant enters pipeline, is delivered to stratum, then gos deep into crack, prevents the closure of fissure channel after pressure, extension from splitting
Slit width degree and generation simultaneously support long crack, and then form high flow conductivity channel, meanwhile, fracturing fluid can be viscous from height in the earth formation
Degree is restored to low viscosity and finally realizes the row of returning after driving a well.In addition during formation breakdown the compatibility of fracturing fluid quality, meeting
Play the role of to entire pressing crack construction success or not critical.
By the development of over half a century, fracturing fluid by single pure plant colloid system till now include foam
Fracturing fluid, CO2The present situation of many body systems such as base fracturing fluid, oil base fracturing fluid, clean fracturing fluid, but still for the detection of its performance
There are several problems to be solved, are mainly manifested in：There is presently no can simulate foam fracturing fluid under the conditions of practice of construction
Rheological behavior, heat transfer characteristic, leak-off and core damage performance and the visual bubble shape of foam fracturing fluid, size and flow pattern are surveyed
The Multifunctional comprehensive type experimental system of examination.
Invention content
The object of the present invention is to provide under a kind of achievable model engineering construction working condition high parameter (>=30MPa, >=
100 DEG C) fracturing fluid property test experimental provision.Wherein, fracturing fluid includes aqueous fracturing fluid, water-base foam fracturing fluid, dry method
Fracturing fluid liquid etc.；Performance includes rheological behavior, friction loss characteristic, heat transfer characteristic, filtration characteristics and core damage performance, foam fracturing
The visualization bubble shape and flow pattern of liquid.
In order to reach object above, the present invention, which adopts the following technical scheme that, to be achieved.
A kind of test evaluation device of high parameter fracturing fluid property, which is characterized in that including liquid CO2Pump note unit, water
Base fracturing fluid base fluid pump note unit, foaming agent pump note unit, foaming and heating unit, heat exchange test cell, rheology and frictional resistance are surveyed
Try unit, leak-off and core damage test cell, the CO2Foam occurs in the outlet connection foaming of pump note unit and heating unit
The liquid passage inlet of device；The fluid path import of the outlet connection foam maker of the aqueous fracturing fluid base fluid pump note unit；Described
Infusion pump note unit is separately connected CO by a diversion three-way2The outlet of pump note unit and aqueous fracturing fluid base fluid pump note unit
Pipeline；The foaming and the outlet of heating unit connect rheology and friction test unit, heat exchange by Three branched pipe road and valve
Test cell, leak-off and core damage test cell；The heat exchange test cell connects rheology by two branch lines and valve
And friction test unit, leak-off and core damage test cell；The rheology and friction test unit and leak-off and core damage
Test cell connects.
In said program, the CO2Pump note unit includes liquid CO2Storage tank, by pipeline successively with shut-off valve, quality
Flowmeter and liquid CO2Liquid passage inlet after high pressure series connection of pumps again with foam maker is connected；It is sent out in high-pressure plunger pump and foam
Between raw device CO is connected on pipeline2Buffer container, pipeline winds heating tape after buffer.
The aqueous fracturing fluid base fluid pump note unit：Solution pool by pipeline successively with shut-off valve, gear pump, y type mistakes
It is connected again with the fluid path import of foam maker after filter, flowmeter, high-pressure plunger pump and check-valves series connection；In high-pressure plunger pump
Buffer container is connected on pipeline between foam maker.
Foaming agent pump note unit includes water pot, water pot by pipeline successively with shut-off valve, y type filters, quality stream
Gauge, plunger type metering pump, high pressure piston container and check-valves series connection after again by diversion three-way respectively with water-based fracturing liquid-based
Liquid pump notes unit, CO2The intermediate conduit connection of pump note unit.
The fracturing fluid foaming and heating unit are made of foam maker and heater, and foam maker outlet connection adds
Hot device.
The heat exchange test cell includes vertical heat exchange sleeve, and shell-side passes through coolant circulation pump, buffer container, flowmeter
Circulation loop is formed, pipe side outlet is separately connected rheology and friction test unit by threeway.
The rheology and friction test unit include buffer container, by pipeline successively with high-pressure gas-liquid mixing pump, flow
Meter, heat exchanger, rheometer test section connect to form circulation loop；High pressure form container is connected in circulation loop bypass.
Compared with prior art, it is an advantage of the invention that：
1、CO2Pump note unit, aqueous fracturing fluid base fluid pump note unit and foaming agent pump note unit are respectively provided with closed loop flow control
Processing procedure sequence inputs required flow value on remote control panel, is transmitted on the frequency converter of pump, makes flow needed for pump output.When
When the flow of flowmeter detection fluctuates, frequency converter output is automatically adjusted by controlling program, to make stability of flow.
2, high-pressure plunger pump discharge installs pressure control program, when system pressure is more than setting pressure, program feedback letter
Number, realize pump trip, it is ensured that the safety of system and personnel.
3, low temperature liquid CO2Storage tank is directly connected to CO by mass flowmenter2High-pressure plunger pump.CO2Square tube after pump note unit
Road winds heating tape, heating low temperature liquid CO2, prevent from meeting water freezing.
4, rheology and friction test unit, using closed circuit, when fracturing fluid is full of circuit, startup high-pressure gas-liquid mixes defeated
Pump, to which aerated fluid is in closed circuit internal circulation flow.
5, the visual bypass of 50MPa in friction test unit pipe is set, the bubble of high pressure is recorded using High-speed Photography Technology
The flow pattern of foam structural form and aerated fluid.
6, core damage test cell tests its dynamic filtration characteristic using closed circuit, circulation shear foam fracturing fluid,
And circulation shear part and the rheology and public high-pressure gas-liquid mixing pump of friction test unit, high-pressure buffering pot and flowmeter.
Description of the drawings
Below in conjunction with the accompanying drawings and specific implementation mode the present invention is described in further detail.
Fig. 1 is the overall structure diagram of apparatus of the present invention.
In figure：V01. solution pool；V02. water pot；V03. liquid CO2Storage tank；P01. gear pump；P02. high-pressure plunger pump；
P03. plunger type metering pump；P04.CO2High-pressure plunger pump；E01. flowmeter；E02. electro connecting pressure gauge；Y01, Y02.y type mistake
Filter；V04-V06. buffer container；E13. heating tape；E12. foam maker；E14. heater；E15. heat exchange sleeve；V07.
Buffer container；V08. high-pressure buffer vessel；V09. high pressure visable container；E16. low temperature thermostat bath；E17. heat exchanger；P06. it cools down
Recycle water dispenser；P07. high-pressure gas-liquid mixing pump；E09-E11. Rosemount differential pressure transmitter；E03. quiet leak-off core holding unit；
E04. leak-off core holding unit is moved；E05. gas-liquid separator；E06. gas-liquid separator；E07. electronic balance；E08-F. soap-film stream
Gauge；E08-G. glass tube flowmeter；V11. simulated formation water pot；V12. simulative oilcan；V13. coal oilcan；V14. piston holds
Device；P09. constant-flux pump；P10. high pressure constant flow pump；P11. hand-operating pressure pump；V10. nitrogen cylinder；V17. beaker；V15. gas buffer
Tank；V16. liquid reserve tank；V18. cleaning solution pond；V19. intermediate receptacle, B01, B02 counterbalance valve
Specific implementation mode
Referring to Fig.1, the test evaluation device of a kind of high parameter fracturing fluid property for hydrocarbon reservoirs transformation, by following
Ten units are constituted：
(1)CO2Pump note unit
Liquid CO2The outlets storage tank V03 are sequentially connected shut-off valve, mass flowmenter E01-FIC301, liquid CO2High-pressure plunger
P04 is pumped, the liquid CO flowed out through plunger pump2One into the foam maker E12 in fracturing fluid foaming and heating unit enters
Mouthful, wherein in CO2The outlet installation electro connecting pressure gauge and safety valve of high-pressure plunger pump P04, pipeline is logical after plunger pump P04
The outlet of a threeway connection foaming agent pump note unit is crossed, and CO is installed on this pipeline2Buffer container and laying heating tape；Matter
It measures flowmeter E01 and high-pressure plunger pump P04 and one closed-loop control system is formed by program, the moment controls the output of high-pressure pump, dimension
Hold output flow stabilization.
(2) aqueous fracturing fluid base fluid pump note unit
Including solution pool V01, gear pump P01, high-pressure plunger pump P02, flowmeter E01-FIC101 etc..Solution pool V01 goes out
Mouth pipe is connect with gear pump P01, and forms circulation loop, realizes preparation and the stirring shear treatment of fracturing fluid base fluid, mixing pump
Outlet connection y type filters, flowmeter and high-pressure plunger pump P02, the fracturing fluid flowed out through plunger pump enter fracturing fluid foaming and
Another entrance of foam maker E12 in heating unit.Pipeline passes through a threeway connection blistering after plunger pump P02
The outlet of agent pump note unit；Flowmeter E01 and high-pressure plunger pump P02 forms a closed-loop control system, moment control by program
The output of high-pressure pump maintains output flow to stablize.
(3) foaming agent pump note unit
Closed loop is formed including water pot V02, the y type filters for connecting water pot, mass flowmenter E01-FIC201 and flowmeter
The plunger type metering pump P03 of control, the piston container V14 for connecting plunger type metering pump, are separately connected finally by diversion three-way
CO2The outlet conduit of pump note unit and conventional fracturing fluid base fluid pump note unit, wherein intermediate receptacle V19 is for giving piston container
V14 liquid filling bodies, installation check-valves and small buffer container V05 on same pipeline.
(4) foaming and heating unit
Including foam maker E12, foam maker outlet is divided into two-way, all the way by heater E14 by a threeway
Heat exchange sleeve E15 in connection heat exchange test cell；Another way pipeline connects rheology and friction test unit, filter by branched pipe
Mistake and core damage test cell and the counterbalance valve B02 of experimental system outlet, wherein temperature measuring point is installed in the outlets heater E14,
Closed-loop control system is formed with heater, heating power is controlled, keeps output fluid temperature constant.
(5) exchange heat test cell
Including vertical heat exchange sleeve E15, coolant circulation pump P06, buffer container V03 and flowmeter E01-FRI406, vertically
The shell-side of heat exchange sleeve E15 forms circulation loop by coolant circulation pump P06, buffer container and flowmeter, realizes heat exchange sleeve
The heat exchange of interior fracturing fluid hot fluid and cold fluid in shell-side.Vertical heat exchange test casing E15 is vertically changed using reverse-flow
Thermal sleeve, the mode of double-wall heat exchange realize the cooling down to fracturing fluid using countercurrent flow of the cooling water in endless tube.Pipe
Side outlet is separately connected rheology and friction test unit and experimental bench discharge knockout drum by threeway.
(6) rheology and friction test unit
Including high-pressure gas-liquid mixing pump P07, high-pressure buffer vessel V08, flowmeter E01-FRI505, high pressure visable container
V09, low temperature thermostat bath E16, heat exchanger E17, Rosemount differential pressure transmitter E09, E10, E11 and distribution three pipes connected in parallel
The horizontal rheology test section of diameter (4mm, 6mm and 8mm).In the unit in one entrance of rheometer test pipeline section and heat exchange test cell
The pipe side of vertical heat exchange test casing E15 is connected by a high pressure electric gate；The unit forms the circuit of a closure, opens
Dynamic high-pressure gas-liquid mixing pump can be realized in horizontal rheology test section, it can be achieved that fracturing fluid circulation shear in the closed circuit
The switching of different tube diameters.When high-pressure foam fracturing fluid flows through the high pressure visable container of bypass, high-speed camera instrument records high pressure bubble
The fluidised form and foaming structure of foam fracturing fluid.In addition the dynamic leak-off test in the unit and leak-off and core damage test cell is public
A set of circulation shear；High-pressure gas-liquid mixing pump P07 and flowmeter E01-FRI505 forms a closed-loop control system by program, when
The output of control high-pressure gas-liquid mixing pump P07 is carved, output flow is maintained to stablize.
(7) leak-off and core damage test cell
Including static filtration core holding unit E03, dynamic filtration core holding unit E04, constant-flux pump P09, high pressure constant flow pump
P10, with P10 form closed circuit 3 piston container V14, by counterbalance valve B02 with static state and dynamic core holding unit it is homogeneous
Gas-liquid separator E05 even, separator lower part outlet the liquid stream that goes out enter to be placed on beaker V17 and gas-liquid on electronic balance E07
Mass flowmenter E01-FRI606 and E01-FRI607, the flowmeter for 2 different ranges that separator upper outlet is connected go out
Mouth connection gas buffer tank V15, the nitrogen cylinder V10 being connected with static filtration core holding unit, add ring pressure to core holding unit
Hand-operating pressure pump P11, the glass tube flowmeter E08-G for the measurement gas being connected with static filtration core holding unit one end and measurement
The soap film flowmeter E08-F of liquid, the simulated formation water pot V11 being connected with constant-flux pump and simulative oilcan V12 and high voltage and constant current
Pump the connected coal oilcan V13 of P10.The unit can realize the test of sound state filtration characteristics, core permeability test and core damage
Test.The dynamic filtration core holding unit E04 of the unit and rheology and buffer container V08, the high-pressure gas-liquid of friction test unit
Mixing pump P07 and flowmeter E01-FRI505 form closed circuit, are used for the dynamic filtration characteristic of mini-frac liquid.
(8) cleaning systems unit
Including cleaning solution pond, the centrifugal water pump being connected with solution pool；Main wash aqueous fracturing fluid branch all the way,
Heat exchange test cell and leak-off and core damage unit are then flowed through, is finally discharged from system outlet；Another way main wash follows
Ring shears part, is then discharged from system outlet.
(9) experimental system exports
Including counterbalance valve B01, gas-liquid separator E06, the gas buffer tank V15 being connected with gas-liquid separator upper airways
The liquid reserve tank V16 being connected with gas-liquid separator lower part fluid path.
Experimental system design pressure 50MPa, 200 DEG C of design temperature highest.
The operation principle of Fig. 1 devices is as follows：
1) solution pool V01 is added in each ingredient of aqueous fracturing fluid, starts the stirring motor on solution pool, prepare water-based fracturing
Liquid-based liquid；Solution pool V01 outlet at bottom pipe is connect with gear pump P02, forms circulation loop, starts stirring motor and tooth before testing
Wheel pump P02 realizes the abundant shearing to fracturing fluid in solution pool and stirring, opens shut-off valve later, fracturing fluid is carried by gear pump
The hydraulic head of confession flows through y type filters and flowmeter, is finally pumped to high-pressure plunger pump P02, realizes to conventional water-based fracturing
The pressurized treatment of liquid, later high pressure fracture liquid stream enter a liquid inlet of foam maker.It is high to ensure that output flow is stablized
Hydraulic plunger pump outlet installation buffer container.Setting in experiment about high-pressure plunger pump discharge is inputted in distal end, and control is passed through
Program controls the output of frequency converter, then so that pump output flow is stablized by closed loop control process.
Pump fluid injection state CO2When, it is first turned on storage tank valve, ensures that entire experimental system outlet is unimpeded, utilizes low temperature liquid
CO2The pump head of pipeline and high-pressure plunger pump P04 is cooled down, after 3-5 minutes cooling, opens high-pressure plunger pump P04, distal end
Liquid CO needed for setting2Flow utilizes the closed loop control process for the mass flowmenter E01-FIC301 compositions installed with pump discharge
Maintain flow constant；When needing aqueous fracturing fluid and liquid CO in experiment2When mixing, start CO2On the pipeline of pump note unit rear
Heating tape, to low temperature liquid CO2It is preheated, is preheated to 0 DEG C or more, avoid meeting water freezing.
Since the foaming agent/tackifier viscosity having is higher, note cannot directly be pumped using plunger pump, therefore utilize high pressure piston
Container is fetched water by high-pressure plunger pump to push foaming agent/tackifier of the piston other side to enter high-pressure system.It is first in experiment
First intermediate receptacle V19 is given to fill foaming agent/tackifier, intermediate receptacle is accessed by foaming agent/tackifier pressure using the nitrogen of high pressure
Enter high pressure piston container；Then foaming agent/thickening agent flux needed for the setting of remote control panel, clicks and starts, plunger type meter
Foaming agent/tackifier are pumped into the aqueous fracturing fluid or liquid CO of high pressure by pump priming by amount pump P03 in certain proportion2System
System.Equally, pump output flow is made to stablize by the closed loop control process between plunger type metering pump P03 and flowmeter.
When preparing high pressure fracture liquid, three of the above fracturing fluid additive usually according to a certain percentage, and then is arranged corresponding
Flow mixed, into foam maker E12 and heater E14, then entered with required flow velocity and temperature corresponding
Test system.
2) when the fracturing fluid of parameter needed for flows through heat exchange sleeve E15, coolant circulation pump P06, the coolant circulation pump for being are opened
The temperature of fluid is exported, the capture program moment records corresponding temperature value and flow value, and pressure break is calculated using multiple wall heat transfer theory
The corresponding coefficient of heat transfer of liquid.
3) it is gentle to the pipeline of the test cell first when the fracturing fluid of parameter needed for flows through rheology and friction test unit
Container V08 filling liquids are rushed, when buffer container V08 reaches required pressure, by the control program of setting, realize termination of pumping, generation automatically
Table filling liquid is completed；The valve outside the unit is closed, fracturing fluid is in the closed loop of the unit, and required pressure then is arranged in distal end
It splits the flow value of liquid and starts high-pressure gas-liquid mixing pump P07, equally, high-pressure gas-liquid mixing pump P07 and flowmeter E01-FIC505
Closed loop control system is formed, stability of flow is maintained；It is surveyed by way of changing flow and caliber (4mm, 6mm and 8mm)
Try the fracturing fluid rheology under different shear rate and friction loss characteristic.It is recorded in high pressure visable container V09 and is steeped by high-speed camera instrument
The structure of foam flow pattern corresponding with its.
4) fracturing fluid of parameter needed for flows through leak-off and core damage test cell, when static filtration characteristic need to be tested,
The fracturing fluid to come first from pressure break liquid pump note unit carries out filling liquid to piston container V14, and fracturing fluid is closed after the completion of filling liquid
Pump note unit, starts high pressure constant flow pump, to high pressure piston container V14 pump note kerosene, pushes piston, and then fracturing fluid is pushed to pass through
Static filtration core holding unit E03, the static filtration characteristic of mini-frac liquid；When the dynamic filtration characteristic for needing mini-frac liquid
When, the equally buffer container V08 to rheology and friction test unit and high-pressure gas-liquid mixing pump P07 filling liquids close rheometer test
Valve on Duan Sangen different tube diameters, after the completion of filling liquid, setting flow starts high-pressure gas-liquid mixing pump P07, and fracturing fluid is with certain
Shear rate flow through the rock core end face of dynamic filtration core holding unit E04, the dynamic filtration characteristic of mini-frac liquid.Work as test
After the filtration characteristics of complete fracturing fluid, rock core is placed in static filtration core holding unit E03, utilizes nitrogen mini-frac liquid pair
The injury characteristic of rock core.
Using the branch line at heater rear, above each fracturing fluid characteristic test unit may be implemented individually to test,
Integration test can be achieved.
Claims (5)
1. a kind of high parameter fracturing fluid property test evaluation device, which is characterized in that including liquid CO2Pump note unit, water-based fracturing
Liquid-based liquid pump note unit, foaming agent pump note unit, foaming and heating unit, heat exchange test cell, rheology and friction test unit,
Leak-off and core damage test cell, the liquid CO2Foam maker in the outlet connection foaming of pump note unit and heating unit
Liquid passage inlet；The fluid path import of the outlet connection foam maker of the aqueous fracturing fluid base fluid pump note unit；The blistering
Agent pump note unit is separately connected liquid CO by a diversion three-way2Pump note unit and aqueous fracturing fluid base fluid pump note going out for unit
Mouth pipeline；The foaming and the outlet of heating unit connect rheology and friction test unit by Three branched pipe road and valve, change
Thermal test unit, leak-off and core damage test cell；The heat exchange test cell passes through two branch lines and valve connection flow
Change and friction test unit, leak-off and core damage test cell；The rheology and friction test unit are hindered with leak-off and rock core
Evil test cell connection；
The heat exchange test cell includes vertical heat exchange sleeve, and shell-side passes through coolant circulation pump, cooling water buffer container, flow
Meter forms circulation loop, and pipe side outlet is separately connected the export pipeline of rheology and friction test unit and device by threeway；
The rheology and friction test unit include buffer container, by pipeline successively with high-pressure gas-liquid mixing pump, gas-liquid flow
Meter, heat exchanger, rheometer test section connect to form circulation loop；High pressure form container is connected in circulation loop bypass.
2. high parameter fracturing fluid property test evaluation device as described in claim 1, which is characterized in that the liquid CO2Pump
It includes liquid CO to note unit2Storage tank, by pipeline successively with CO2High-pressure stop valve, CO2Mass flowmenter and liquid CO2High-pressure column
It is connected again with the liquid passage inlet of foam maker after plug series connection of pumps；In liquid CO2It is managed between high-pressure plunger pump and foam maker
Liquid CO is connected on road2Buffer container, liquid CO2Pipeline winds heating tape after buffer container.
3. high parameter fracturing fluid property test evaluation device as described in claim 1, which is characterized in that the water-based fracturing
Liquid-based liquid pump notes unit：Solution pool by pipeline successively with aqueous fracturing fluid base fluid shut-off valve, gear pump, the first y type filters,
Liquid inventory meter, aqueous fracturing fluid base fluid high-pressure plunger pump and first check-valve series connection after again with the fluid path import of foam maker
It is connected；Aqueous fracturing fluid base fluid buffering is connected on pipeline between aqueous fracturing fluid base fluid high-pressure plunger pump and foam maker to hold
Device.
4. high parameter fracturing fluid property test evaluation device as described in claim 1, which is characterized in that the foaming agent pump note
Unit includes water pot, water pot by pipeline successively with foaming agent shut-off valve, the 2nd y type filters, foaming agent mass flowmenter, column
It is pumped and is noted with aqueous fracturing fluid base fluid respectively by diversion three-way after plug metering pump, high pressure piston container and second check-valve series connection
Unit outlet conduit and liquid CO2The outlet conduit connection of pump note unit.
5. high parameter fracturing fluid property test evaluation device as described in claim 1, which is characterized in that the foaming and heating
Unit is made of foam maker and heater, foam maker outlet connection heater.
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Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4848461A (en) * | 1988-06-24 | 1989-07-18 | Halliburton Company | Method of evaluating fracturing fluid performance in subsurface fracturing operations |
| US5271675A (en) * | 1992-10-22 | 1993-12-21 | Gas Research Institute | System for characterizing pressure, movement, temperature and flow pattern of fluids |
| CN201546718U (en) * | 2009-11-04 | 2010-08-11 | 湖北创联石油科技有限公司 | High-pressure high-temperature dynamic fluid loss instrument |
| CN201802396U (en) * | 2010-05-10 | 2011-04-20 | 湖北创联石油科技有限公司 | High-temperature salt-resistant double-core dynamic filter press |
| CN102766450A (en) * | 2012-08-15 | 2012-11-07 | 中国石油大学(华东) | Nitrogen foam fracturing fluid for coal bed methane and preparation method of nitrogen foam fracturing fluid |
| CN102914494A (en) * | 2012-11-03 | 2013-02-06 | 中国石油大学(华东) | Device for measuring dynamic leak-off of foam fracturing fluid and working method thereof |
| CN103808636A (en) * | 2012-11-13 | 2014-05-21 | 张红梅 | Method for testing static leaking-off property of fracturing fluid |
| CN103969160A (en) * | 2014-04-23 | 2014-08-06 | 伊向艺 | High-temperature high-pressure foam liquid dynamic filtration evaluation system and method |
| CN104007043A (en) * | 2014-03-27 | 2014-08-27 | 中国华能集团清洁能源技术研究院有限公司 | Large multifunctional fracturing fluid experiment system |
| CN104034630A (en) * | 2014-06-17 | 2014-09-10 | 西安交通大学 | Fracturing liquid performance experimental system for geological transformation of oil and gas reservoir |
| CN104502552A (en) * | 2015-01-22 | 2015-04-08 | 中国石油大学(华东) | High-temperature and high-pressure foam static filter tester and application thereof |
| CN104568699A (en) * | 2014-12-29 | 2015-04-29 | 中国石油大学(华东) | Method for measuring filtration coefficient of supercritical carbon dioxide fracturing fluid |
| CN204405491U (en) * | 2015-02-15 | 2015-06-17 | 陕西延长石油(集团)有限责任公司研究院 | A kind of CO 2dry method fracturing liquid dynamic filtration device for evaluating performance |
-
2015
- 2015-07-27 CN CN201510447789.XA patent/CN105043933B/en not_active Expired - Fee Related
Patent Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4848461A (en) * | 1988-06-24 | 1989-07-18 | Halliburton Company | Method of evaluating fracturing fluid performance in subsurface fracturing operations |
| US5271675A (en) * | 1992-10-22 | 1993-12-21 | Gas Research Institute | System for characterizing pressure, movement, temperature and flow pattern of fluids |
| CN201546718U (en) * | 2009-11-04 | 2010-08-11 | 湖北创联石油科技有限公司 | High-pressure high-temperature dynamic fluid loss instrument |
| CN201802396U (en) * | 2010-05-10 | 2011-04-20 | 湖北创联石油科技有限公司 | High-temperature salt-resistant double-core dynamic filter press |
| CN102766450A (en) * | 2012-08-15 | 2012-11-07 | 中国石油大学(华东) | Nitrogen foam fracturing fluid for coal bed methane and preparation method of nitrogen foam fracturing fluid |
| CN102914494A (en) * | 2012-11-03 | 2013-02-06 | 中国石油大学(华东) | Device for measuring dynamic leak-off of foam fracturing fluid and working method thereof |
| CN103808636A (en) * | 2012-11-13 | 2014-05-21 | 张红梅 | Method for testing static leaking-off property of fracturing fluid |
| CN104007043A (en) * | 2014-03-27 | 2014-08-27 | 中国华能集团清洁能源技术研究院有限公司 | Large multifunctional fracturing fluid experiment system |
| CN103969160A (en) * | 2014-04-23 | 2014-08-06 | 伊向艺 | High-temperature high-pressure foam liquid dynamic filtration evaluation system and method |
| CN104034630A (en) * | 2014-06-17 | 2014-09-10 | 西安交通大学 | Fracturing liquid performance experimental system for geological transformation of oil and gas reservoir |
| CN104568699A (en) * | 2014-12-29 | 2015-04-29 | 中国石油大学(华东) | Method for measuring filtration coefficient of supercritical carbon dioxide fracturing fluid |
| CN104502552A (en) * | 2015-01-22 | 2015-04-08 | 中国石油大学(华东) | High-temperature and high-pressure foam static filter tester and application thereof |
| CN204405491U (en) * | 2015-02-15 | 2015-06-17 | 陕西延长石油(集团)有限责任公司研究院 | A kind of CO 2dry method fracturing liquid dynamic filtration device for evaluating performance |
Non-Patent Citations (3)
| Title |
|---|
| CO2泡沫压裂液两相流流动特性的试验研究;王树众 等;《西安交通大学学报》;20030930;第37卷(第9期);第975-978页 * |
| 二氧化碳泡沫压裂液性能研究;孙长健 等;《精细石油化工进展》;20090331;第10卷(第3期);第12-15页 * |
| 氮气泡沫压裂液流变特性试验;段百齐 等;《石油钻采工艺》;20050831;第27卷(第4期);第71-74页 * |
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