CN105038397A - Ultrasonic cleaning resistant mirror ink for mobile phone lens - Google Patents
Ultrasonic cleaning resistant mirror ink for mobile phone lens Download PDFInfo
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- CN105038397A CN105038397A CN201510402329.5A CN201510402329A CN105038397A CN 105038397 A CN105038397 A CN 105038397A CN 201510402329 A CN201510402329 A CN 201510402329A CN 105038397 A CN105038397 A CN 105038397A
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Abstract
The invention discloses ultrasonic cleaning resistant mirror ink for a mobile phone lens. The ultrasonic cleaning resistant mirror ink is prepared from the following raw materials in percentage by weight: 20-30% of ketone-formaldehyde resin, 5-10% of amino resin, 3-5% of cellulose acetate butyrate, 45-55% of mirror silver paste, 0.5-35 of an amino adhesion accelerant, 3-5% of auxiliary materials and 5-10% of a diluent. The ultrasonic cleaning resistant mirror ink for the mobile phone lens disclosed by the invention is good in adhesion, not liable to drop, excellent in ultrasonic cleaning resistance and low in price.
Description
Technical field
The present invention relates to ink with mirror effect technical field, particularly relate to a kind of mobile-phone lens ink with mirror effect of resistance to ultrasonic cleaning.
Background technology
In the global IT application epoch, along with being showing improvement or progress day by day of science and technology and improving constantly of standard of living, the electronic product such as mobile phone, notebook computer is growing and universal, in this process, various countries' electronic enterprise is all constantly devoted to the continuous research and development of these electronic products from function to outward appearance and improvement, to occupying more market.
Current mobile-phone lens is installed on the top of the display screen of mobile phone, and is fixed by shell; Described mobile-phone lens adopts transparent glass to make usually, comprises display space and Printing Zone; The transparent setting in described display space, display screen is revealed in described display space; Described Printing Zone is generally frame, and described frame needs printing-ink, for hiding the position that mobile-phone lens engages with shell, display screen, makes mobile phone have better outward appearance; Meanwhile, certain in Printing Zone position needs to stamp the significant pattern that brand LOGO etc. represents certain enterprise.
These patterns are generally the back side being imprinted on glass by silk screen printing, see pattern by the front of glass, the printing of these patterns, most employing ink with mirror effect.The mobile-phone lens ink with mirror effect now commercially used, after finishing printing during ultrasonic cleaning, because the sticking power of ink is bad, easily comes off.
Summary of the invention
Based on the technical problem that background technology exists, the present invention proposes a kind of mobile-phone lens ink with mirror effect of resistance to ultrasonic cleaning, sticking power is good, difficult drop-off, and wherein resistance to ultrasonic cleaning performance is particularly excellent, and cheap.
The mobile-phone lens ink with mirror effect of a kind of resistance to ultrasonic cleaning that the present invention proposes, its raw materials by weight comprises: aldehyde ketone resin 20-30%, aminoresin 5-10%, cellulose acetate butyrate 3-5%, mirror-like silver slurry 45-55%, amino adhesion promoter 0.5-3%, supplies 3-5%, thinner 5-10%.
In embodiment, the weight percent of aldehyde ketone resin can be 20%, 21%, 22%, 23%, 24%, 25%, 26%, 27%, 28%, 29%, 30%, the weight percent of aminoresin can be 5%, 5.2%, 6%, 6.4%, 7%, 7.6%, 8%, 8.8%, 9%, 9.5%, 10%, the weight percent of cellulose acetate butyrate can be 3%, 3.2%, 3.4%, 3.6%, 3.8%, 4%, 4.2%, 4.4%, 4.6%, 4.8%, 5%, the weight percent of mirror-like silver slurry can be 45%, 46%, 47%, 48%, 49%, 50%, 51%, 52%, 53%, 54%, 55%, the weight percent of amino adhesion promoter can be 0.5%, 0.8%, 1%, 1.2%, 1.5%, 1.7%, 2%, 2.3%, 2.5%, 2.8%, 3%, the weight percent of supplies can be 3%, 3.2%, 3.4%, 3.6%, 3.8%, 4%, 4.2%, 4.4%, 4.6%, 4.8%, 5%, the weight percent of thinner can be 5%, 5.2%, 6%, 6.4%, 7%, 7.6%, 8%, 8.8%, 9%, 9.5%, 10%.
Preferably, supplies comprise by weight: siccative 20-30 part, antioxidant 10-15 part, defoamer 6-9 part, tensio-active agent 7-10 part, dispersion agent 5-8 part, flow agent 10-15 part, slipping agent 5-10 part.
In embodiment, the weight part of siccative can be 20 parts, 21 parts, 22 parts, 23 parts, 24 parts, 25 parts, 26 parts, 27 parts, 28 parts, 29 parts, 30 parts, the weight part of antioxidant can be 10 parts, 10.2 parts, 11 parts, 11.4 parts, 12 parts, 12.6 parts, 13 parts, 13.8 parts, 14 parts, 14.5 parts, 15 parts, the weight part of defoamer can be 6 parts, 6.2 part, 6.6 part, 7 parts, 7.4 part, 7.8 part, 8 parts, 8.5 part, 9 parts, the weight part of tensio-active agent can be 7 parts, 7.4 part, 7.8 part, 8 parts, 8.2 part, 8.6 part, 9 parts, 9.3 part, 9.7 part, 10 parts, the weight part of dispersion agent can be 5 parts, 5.2 part, 5.6 part, 6 parts, 6.4 part, 6.8 part, 7 parts, 7.3 part, 7.7 part, 8 parts, the weight part of flow agent can be 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts, the weight part of slipping agent can be 5 parts, 5.2 part, 5.6 part, 6 parts, 6.4 part, 6.8 part, 7 parts, 7.3 part, 7.7 part, 8 parts, 8.2 part, 8.6 part, 9 parts, 9.3 part, 9.7 part, 10 parts.
Preferably, siccative is one or more compositions in cobalt naphthenate, manganese naphthenate, manganese linoleate, zirconium caprylate.
Preferably, antioxidant comprises by weight: Resorcinol 5-8 part, BHT 3-4 part, tertiarybutylhydroquinone 1-2 part.
In embodiment, the weight part of Resorcinol can be 5 parts, 5.2 parts, 5.6 parts, 6 parts, 6.4 parts, 6.8 parts, 7 parts, 7.3 parts, 7.7 parts, 8 parts, 2, the weight part of 6-di-tert-butyl methyl phenol can be 3 parts, 3.1 parts, 3.2 parts, 3.3 parts, 3.4 parts, 3.5 parts, 3.6 parts, 3.7 parts, 3.8 parts, 3.9 parts, 4 parts, and the weight part of tertiarybutylhydroquinone can be 1 part, 1.1 parts, 1.2 parts, 1.3 parts, 1.4 parts, 1.5 parts, 1.6 parts, 1.7 parts, 1.8 parts, 1.9 parts, 2 parts.
Preferably, defoamer comprises by weight: polyoxyethylene polyoxypropylene tetramethylolmethane ether 10-15 part, GPES type defoamer 8-10 part, stearic acid 3-6 part.
In embodiment, the weight part of polyoxyethylene polyoxypropylene tetramethylolmethane ether can be 10 parts, 10.2 parts, 11 parts, 11.4 parts, 12 parts, 12.6 parts, 13 parts, 13.8 parts, 14 parts, 14.5 parts, 15 parts, the weight part of GPES type defoamer can be 8 parts, 8.2 parts, 8.4 parts, 8.6 parts, 8.8 parts, 9 parts, 9.2 parts, 9.4 parts, 9.6 parts, 9.8 parts, 10 parts, and stearic weight part can be 3 parts, 3.2 parts, 3.6 parts, 4 parts, 4.4 parts, 4.8 parts, 5 parts, 5.3 parts, 5.7 parts, 6 parts.
Preferably, tensio-active agent is fatty acid methyl ester ethoxylate sodium sulfonate.
Preferably, slipping agent is cocoanut fatty acid diethanolamide or amine hydroxybenzene.
Preferably, thinner is one or more compositions in acetone, dehydrated alcohol, propyl carbinol, N-BUTYL ACETATE, methylethylketone.
Preferably, the weight ratio of siccative, antioxidant, flow agent, slipping agent is 23-27:12-13:12-13:6-8.
Preferably, the weight ratio of aldehyde ketone resin, aminoresin, mirror-like silver slurry, thinner is 22-28:7-8:48-52:7-8.5.
Preparation method of the present invention is: add in thinner by aldehyde ketone resin and aminoresin, be warming up to 50-80 DEG C, add again mirror-like silver slurry stir after, then add amino adhesion promoter, cellulose acetate butyrate and supplies carry out stirring at low speed evenly after, cross the mobile-phone lens ink with mirror effect that 250-300 mesh sieve obtains resistance to ultrasonic cleaning.
The present invention adopts aldehyde ketone resin, aminoresin, cellulose acetate butyrate and mirror-like silver to starch and cooperatively interacts, improve the consistency of mirror-like silver slurry and resin, above-mentioned raw materials is made to form entirety, significantly improve sticking power of the present invention, thus improve the performance of water boiling resistance of the present invention and resistance to ultrasonic cleaning; Cellulose acetate butyrate also can be used as flow agent, impels ink of the present invention smooth in drying and forming-film process, smooth, even with the flow agent components matching in supplies; Siccative adopts cobalt naphthenate, manganese naphthenate, manganese linoleate, zirconium caprylate, the cross-linking density of aldehyde ketone resin, aminoresin can be promoted, thus improve sticking power further, antioxidant adopts Resorcinol, 2, one or more in 6-di-tert-butyl methyl phenol, tertiarybutylhydroquinone, substantially increase antioxidant property of the present invention, thus mirror-like silver can be protected to starch, prevent the present invention from occurring returning the black phenomenon of thick hair in printing process; Defoamer, tensio-active agent and dispersion agent coordinate, and improve the homogeneity of each material dispersion of the present invention, extend quality guaranteed period of the present invention and work-ing life.In sum, sticking power of the present invention is good, difficult drop-off, and wherein resistance to ultrasonic cleaning performance is particularly excellent, and cheap.
Embodiment
Below, by specific embodiment, technical scheme of the present invention is described in detail.
Embodiment 1
The mobile-phone lens ink with mirror effect of a kind of resistance to ultrasonic cleaning that the present invention proposes, its raw materials by weight comprises: aldehyde ketone resin 20%, aminoresin 10%, cellulose acetate butyrate 3%, mirror-like silver slurry 55%, amino adhesion promoter 0.5%, supplies 5%, acetone 6.8%, amounts to 100%.
Supplies comprise by weight: cobalt naphthenate 20 parts, antioxidant 15 parts, defoamer 6 parts, fatty acid methyl ester ethoxylate sodium sulfonate 10 parts, dispersion agent 5 parts, flow agent 15 parts, cocoanut fatty acid diethanolamide 5 parts.
Wherein, antioxidant comprises by weight: Resorcinol 5 parts, BHT 4 parts, tertiarybutylhydroquinone 1 part.
Embodiment 2
The mobile-phone lens ink with mirror effect of a kind of resistance to ultrasonic cleaning that the present invention proposes, its raw materials by weight comprises: aldehyde ketone resin 30%, aminoresin 5%, cellulose acetate butyrate 5%, mirror-like silver slurry 45%, amino adhesion promoter 3%, supplies 3%, methylethylketone 9%, amounts to 100%.
Supplies comprise by weight: manganese naphthenate 30 parts, antioxidant 10 parts, defoamer 9 parts, fatty acid methyl ester ethoxylate sodium sulfonate 7 parts, dispersion agent 8 parts, flow agent 10 parts, amine hydroxybenzene 10 parts.
Wherein, defoamer comprises by weight: 10 parts, polyoxyethylene polyoxypropylene tetramethylolmethane ether, GPES type defoamer 10 parts, stearic acid 3 parts.
Embodiment 3
The mobile-phone lens ink with mirror effect of a kind of resistance to ultrasonic cleaning that the present invention proposes, its raw materials by weight comprises: aldehyde ketone resin 22%, aminoresin 8%, cellulose acetate butyrate 3.5%, mirror-like silver slurry 52%, amino adhesion promoter 1.5%, supplies 4.5%, propyl carbinol 8.5%, amounts to 100%.
Supplies comprise by weight: manganese linoleate 23 parts, antioxidant 13 parts, defoamer 7 parts, fatty acid methyl ester ethoxylate sodium sulfonate 9 parts, dispersion agent 6 parts, flow agent 13 parts, amine hydroxybenzene 6 parts.
Wherein, antioxidant comprises by weight: Resorcinol 8 parts, BHT 3 parts, tertiarybutylhydroquinone 2 parts.
Embodiment 4
The mobile-phone lens ink with mirror effect of a kind of resistance to ultrasonic cleaning that the present invention proposes, its raw materials by weight comprises: aldehyde ketone resin 28%, aminoresin 7%, cellulose acetate butyrate 4.5%, mirror-like silver slurry 48%, amino adhesion promoter 2%, supplies 3.5%, N-BUTYL ACETATE 7%, amounts to 100%.
Supplies comprise by weight: zirconium caprylate 27 parts, antioxidant 12 parts, defoamer 8 parts, fatty acid methyl ester ethoxylate sodium sulfonate 8 parts, dispersion agent 7 parts, flow agent 12 parts, cocoanut fatty acid diethanolamide 8 parts.
Wherein, defoamer comprises by weight: 15 parts, polyoxyethylene polyoxypropylene tetramethylolmethane ether, GPES type defoamer 8 parts, stearic acid 6 parts.
Embodiment 5
The mobile-phone lens ink with mirror effect of a kind of resistance to ultrasonic cleaning that the present invention proposes, its raw materials by weight comprises: aldehyde ketone resin 25%, aminoresin 7.5%, cellulose acetate butyrate 4%, mirror-like silver slurry 50%, amino adhesion promoter 1.8%, supplies 4%, thinner 7.7%, amounts to 100%.
Supplies comprise by weight: siccative 25 parts, antioxidant 12.5 parts, defoamer 7.8 parts, fatty acid methyl ester ethoxylate sodium sulfonate 8.9 parts, dispersion agent 6.7 parts, flow agent 12.3 parts, amine hydroxybenzene 6.8 parts; Thinner is the composition of acetone and methylethylketone.
Wherein, siccative is the composition of cobalt naphthenate and zirconium caprylate; Antioxidant comprises by weight: Resorcinol 6 parts, BHT 3.4 parts, tertiarybutylhydroquinone 1.2 parts; Defoamer comprises by weight: 13 parts, polyoxyethylene polyoxypropylene tetramethylolmethane ether, GPES type defoamer 9 parts, stearic acid 5 parts.
Performance test is carried out to the present invention: the mobile-phone lens ink with mirror effect of the resistance to ultrasonic cleaning that embodiment 5 is obtained and regular handset eyeglass ink with mirror effect by 300 order silk screen printings on mobile-phone lens, carry out ultrasonic cleaning, before and after its ultrasonic cleaning, detected result is as follows:
As seen from the above table: the present invention has excellent resistance to ultrasonic cleaning performance relative to prior art.
The above; be only the present invention's preferably embodiment; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (10)
1. the mobile-phone lens ink with mirror effect of a resistance to ultrasonic cleaning, it is characterized in that, its raw materials by weight comprises: aldehyde ketone resin 20-30%, aminoresin 5-10%, cellulose acetate butyrate 3-5%, mirror-like silver slurry 45-55%, amino adhesion promoter 0.5-3%, supplies 3-5%, thinner 5-10%.
2. the mobile-phone lens ink with mirror effect of resistance to ultrasonic cleaning according to claim 1, it is characterized in that, supplies comprise by weight: siccative 20-30 part, antioxidant 10-15 part, defoamer 6-9 part, tensio-active agent 7-10 part, dispersion agent 5-8 part, flow agent 10-15 part, slipping agent 5-10 part.
3. the mobile-phone lens ink with mirror effect of resistance to ultrasonic cleaning according to claim 2, is characterized in that, siccative is one or more compositions in cobalt naphthenate, manganese naphthenate, manganese linoleate, zirconium caprylate.
4. the mobile-phone lens ink with mirror effect of resistance to ultrasonic cleaning according to Claims 2 or 3, it is characterized in that, antioxidant comprises by weight: Resorcinol 5-8 part, BHT 3-4 part, tertiarybutylhydroquinone 1-2 part.
5. the mobile-phone lens ink with mirror effect of resistance to ultrasonic cleaning according to any one of claim 2-4, it is characterized in that, defoamer comprises by weight: polyoxyethylene polyoxypropylene tetramethylolmethane ether 10-15 part, GPES type defoamer 8-10 part, stearic acid 3-6 part.
6. the mobile-phone lens ink with mirror effect of resistance to ultrasonic cleaning according to any one of claim 2-5, is characterized in that, tensio-active agent is fatty acid methyl ester ethoxylate sodium sulfonate.
7. the mobile-phone lens ink with mirror effect of resistance to ultrasonic cleaning according to any one of claim 2-6, is characterized in that, slipping agent is cocoanut fatty acid diethanolamide or amine hydroxybenzene.
8. the mobile-phone lens ink with mirror effect of resistance to ultrasonic cleaning according to any one of claim 1-7, is characterized in that, thinner is one or more compositions in acetone, dehydrated alcohol, propyl carbinol, N-BUTYL ACETATE, methylethylketone.
9. the mobile-phone lens ink with mirror effect of resistance to ultrasonic cleaning according to any one of claim 1-8, is characterized in that, the weight ratio of siccative, antioxidant, flow agent, slipping agent is 23-27:12-13:12-13:6-8.
10. the mobile-phone lens ink with mirror effect of resistance to ultrasonic cleaning according to any one of claim 1-9, is characterized in that, the weight ratio of aldehyde ketone resin, aminoresin, mirror-like silver slurry, thinner is 22-28:7-8:48-52:7-8.5.
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| CN201510402329.5A CN105038397A (en) | 2015-07-08 | 2015-07-08 | Ultrasonic cleaning resistant mirror ink for mobile phone lens |
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| CN201510402329.5A CN105038397A (en) | 2015-07-08 | 2015-07-08 | Ultrasonic cleaning resistant mirror ink for mobile phone lens |
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| CN105419479A (en) * | 2015-12-21 | 2016-03-23 | 王景泉 | Superbright aluminum paste printing ink for PC printing and preparation method thereof |
| CN105957800A (en) * | 2016-05-09 | 2016-09-21 | 浙江海洋大学 | Substrate surface treatment process |
| CN110104327A (en) * | 2019-05-06 | 2019-08-09 | 青岛市贤俊龙彩印有限公司 | A kind of mirror-like silver packing box and its processing technology |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105419479A (en) * | 2015-12-21 | 2016-03-23 | 王景泉 | Superbright aluminum paste printing ink for PC printing and preparation method thereof |
| CN105957800A (en) * | 2016-05-09 | 2016-09-21 | 浙江海洋大学 | Substrate surface treatment process |
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| CN110104327A (en) * | 2019-05-06 | 2019-08-09 | 青岛市贤俊龙彩印有限公司 | A kind of mirror-like silver packing box and its processing technology |
| CN110104327B (en) * | 2019-05-06 | 2020-06-19 | 青岛市贤俊龙彩印有限公司 | Mirror silver packaging box and processing technology thereof |
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