CN105017756A - Composite terrace material for municipal road and preparation method of composite terrace material - Google Patents
Composite terrace material for municipal road and preparation method of composite terrace material Download PDFInfo
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- CN105017756A CN105017756A CN201510508796.6A CN201510508796A CN105017756A CN 105017756 A CN105017756 A CN 105017756A CN 201510508796 A CN201510508796 A CN 201510508796A CN 105017756 A CN105017756 A CN 105017756A
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Abstract
The invention discloses a composite terrace material for a municipal road and a preparation method of the composite terrace material. The composite terrace material for the municipal road comprises, by weight, 30-40 parts of organosilicon modified polyurethane, 15-25 parts of bisphenol F type epoxy resin, 4-10 parts of fluorocarbon resin, 3-6 parts of nitrogen-bearing phenolic resin, 4-6 parts of montmorillonite powder, 2-4 parts of magnesium oxide, 3-7 parts of dioctyl phthalate, 3-6 parts of tridecyl isononoate and 4-8 parts of oleic acid diethanolamide. The preparation method of the composite terrace material comprises the processes of smashing, stirring, mixing and the like of the components, the prepared composite terrace material has the performance of good mechanical strength, and can be used as materials of municipal engineering such as roads, and the strength and comfort of the materials of the roads are improved.
Description
Technical field
The invention belongs to public works field, relate to a kind of town road composite terrace material and preparation method thereof.
Background technology
What conventional town road ground, industrial ground design often used is: concrete floor, cement mortar surface, epoxy ground, abrasion-resistant ground, terrazzo floor etc., through using the investigation after 1-3 to upper ground surface, all occur in various degree play dirt, dusting, the phenomenon that comes off, to such an extent as to affect the normal use on ground.Occur that the major cause of these problems is: the problem in work-ing life of construction quality and product itself.Referring to of epoxide terrace technology covers painting epoxypaint on the cement level ground of having solidified, and covers and is coated with thickness at about 1-5mm, forms an airtight organism protective layer.Because epoxy resin is organism; so this protective layer has the good chemical property such as surperficial water tolerance, oil-proofness, resistance to acids and bases, salt fog resistance; and it is smooth seamless, easy to clean; be the terrace material longer that modern industry widely uses, be widely used in medicine, food (sterile production) and the industry such as electronics, chemical industry (anti-electrostatic).Composite terrace material kind for town road is less, and the performance of only floor material is also not enough to meet and uses.
Summary of the invention
The technical problem solved: the earth material kind that town road uses is more, wherein floor material obtains and promotes widely in town road, floor material for town road needs to possess higher ultimate compression strength and folding strength, the object of the invention is open a kind of town road composite terrace material and preparation method thereof, improve the ultimate compression strength of floor material, folding strength and tensile strength.
Technical scheme: for the problems referred to above, the invention discloses a kind of town road composite terrace material and preparation method thereof, and described town road composite terrace material comprises the composition of following weight parts:
Organic silicon modified polyurethane 30-40 part,
Bisphenol f type epoxy resin 15-25 part,
Fluorocarbon resin 4-10 part,
Nitrogen-containing Phenolic Resins 3-6 part,
Montmorillonite powder 4-6 part,
Magnesium oxide 2-4 part,
Dioctyl phthalate (DOP) 3-7 part,
Tridecyl alcohol different pelargonate 3-6 part,
Lauric acid amide of ethanol 4-8 part.
Preferably, described a kind of town road composite terrace material, comprises the composition of following weight parts:
Organic silicon modified polyurethane 32-38 part,
Bisphenol f type epoxy resin 17-23 part,
Fluorocarbon resin 6-9 part,
Nitrogen-containing Phenolic Resins 4-5 part,
Montmorillonite powder 5-6 part,
Magnesium oxide 3-4 part,
Dioctyl phthalate (DOP) 4-6 part,
Tridecyl alcohol different pelargonate 4-5 part,
Lauric acid amide of ethanol 5-7 part.
The preparation method of described a kind of town road composite terrace material, comprises the following steps:
Step 1: montmorillonite powder and magnesium oxide are pulverized in pulverizer, is crushed to montmorillonite powder and magnesium oxide is 200 order-500 object powder;
Step 2: by weight respectively by the montmorillonite powder 4-6 part after organic silicon modified polyurethane 30-40 part, bisphenol f type epoxy resin 15-25 part, fluorocarbon resin 4-10 part, Nitrogen-containing Phenolic Resins 3-6 part, pulverizing, magnesium oxide 2-4 part, above-mentioned composition is stirred, raised temperature is 110-120 DEG C, stirs 15-30min;
Step 3: add dioctyl phthalate (DOP) 3-7 part, tridecyl alcohol different pelargonate 3-6 part, lauric acid amide of ethanol 4-8 part again in the material of step 2, temperature is reduced to 80-90 DEG C, then stirs 10-20min;
Step 4: after the material naturally cooling of step 3 is town road composite terrace material.
Preferably, the preparation method of described a kind of town road composite terrace material, in described step 2, raised temperature is 115 DEG C, stirs 20min.
Preferably, the preparation method of described a kind of town road composite terrace material, reduces to 85 DEG C by temperature in described step 3, then stirs 15min.
Preferably, the preparation method of described a kind of town road composite terrace material, is crushed to montmorillonite powder in described step 1 and magnesium oxide is 300 order-400 object powder.
Beneficial effect: town road composite terrace material of the present invention effectively raises the ultimate compression strength of composite terrace material, folding strength and tensile strength, improve the defect of conventional town road composite terrace material, improve its wearing quality, the resinous principle added and inorganic components have all played larger function to its performance of raising, and the floor material of preparation is applicable in the fields such as the road of public works.
Embodiment
Embodiment 1
Step 1: montmorillonite powder and magnesium oxide are pulverized in pulverizer, is crushed to montmorillonite powder and magnesium oxide is 500 object powder; Step 2: by weight respectively by montmorillonite powder 6 parts, 4 parts, the magnesium oxide after organic silicon modified polyurethane 30 parts, bisphenol f type epoxy resin 25 parts, fluorocarbon resin 4 parts, Nitrogen-containing Phenolic Resins 3 parts, pulverizing, above-mentioned composition is stirred, raised temperature is 110 DEG C, stirs 30min; Step 3: add dioctyl phthalate (DOP) 7 parts, the different pelargonate of tridecyl alcohol 3 parts, lauric acid amide of ethanol 8 parts again in the material of step 2, temperature is reduced to 90 DEG C, then stir 10min; Step 4: after the material naturally cooling of step 3 is town road composite terrace material.
Embodiment 2
Step 1: montmorillonite powder and magnesium oxide are pulverized in pulverizer, is crushed to montmorillonite powder and magnesium oxide is 200 object powder; Step 2: by weight respectively by montmorillonite powder 4 parts, 2 parts, the magnesium oxide after organic silicon modified polyurethane 40 parts, bisphenol f type epoxy resin 15 parts, fluorocarbon resin 10 parts, Nitrogen-containing Phenolic Resins 6 parts, pulverizing, above-mentioned composition is stirred, raised temperature is 120 DEG C, stirs 15min; Step 3: add dioctyl phthalate (DOP) 3 parts, the different pelargonate of tridecyl alcohol 6 parts, lauric acid amide of ethanol 4 parts again in the material of step 2, temperature is reduced to 80 DEG C, then stir 20min; Step 4: after the material naturally cooling of step 3 is town road composite terrace material.
Embodiment 3
Step 1: montmorillonite powder and magnesium oxide are pulverized in pulverizer, is crushed to montmorillonite powder and magnesium oxide is 400 object powder; Step 2: by weight respectively by montmorillonite powder 5 parts, 3 parts, the magnesium oxide after organic silicon modified polyurethane 32 parts, bisphenol f type epoxy resin 17 parts, fluorocarbon resin 9 parts, Nitrogen-containing Phenolic Resins 5 parts, pulverizing, above-mentioned composition is stirred, raised temperature is 110 DEG C, stirs 30min; Step 3: add dioctyl phthalate (DOP) 6 parts, the different pelargonate of tridecyl alcohol 4 parts, lauric acid amide of ethanol 5 parts again in the material of step 2, temperature is reduced to 90 DEG C, then stir 10min; Step 4: after the material naturally cooling of step 3 is town road composite terrace material.
Embodiment 4
Step 1: montmorillonite powder and magnesium oxide are pulverized in pulverizer, is crushed to montmorillonite powder and magnesium oxide is 300 object powder; Step 2: by weight respectively by montmorillonite powder 6 parts, 4 parts, the magnesium oxide after organic silicon modified polyurethane 38 parts, bisphenol f type epoxy resin 23 parts, fluorocarbon resin 6 parts, Nitrogen-containing Phenolic Resins 4 parts, pulverizing, above-mentioned composition is stirred, raised temperature is 120 DEG C, stirs 15min; Step 3: add dioctyl phthalate (DOP) 4 parts, the different pelargonate of tridecyl alcohol 5 parts, lauric acid amide of ethanol 7 parts again in the material of step 2, temperature is reduced to 80 DEG C, then stir 20min; Step 4: after the material naturally cooling of step 3 is town road composite terrace material.
Embodiment 5
Step 1: montmorillonite powder and magnesium oxide are pulverized in pulverizer, is crushed to montmorillonite powder and magnesium oxide is 300 object powder; Step 2: by weight respectively by montmorillonite powder 6 parts, 3 parts, the magnesium oxide after organic silicon modified polyurethane 30 parts, bisphenol f type epoxy resin 20 parts, fluorocarbon resin 8 parts, Nitrogen-containing Phenolic Resins 4 parts, pulverizing, above-mentioned composition is stirred, raised temperature is 115 DEG C, stirs 20min; Step 3: add dioctyl phthalate (DOP) 5 parts, the different pelargonate of tridecyl alcohol 4 parts, lauric acid amide of ethanol 6 parts again in the material of step 2, temperature is reduced to 85 DEG C, then stir 15min; Step 4: after the material naturally cooling of step 3 is town road composite terrace material.
Comparative example 1
Step 1: montmorillonite powder and magnesium oxide are pulverized in pulverizer, is crushed to montmorillonite powder and magnesium oxide is 200 object powder; Step 2: by weight respectively by montmorillonite powder 4 parts, 2 parts, the magnesium oxide after organic silicon modified polyurethane 40 parts, Nitrogen-containing Phenolic Resins 6 parts, pulverizing, stirred by above-mentioned composition, raised temperature is 120 DEG C, stirs 15min; Step 3: add dioctyl phthalate (DOP) 3 parts, the different pelargonate of tridecyl alcohol 6 parts, lauric acid amide of ethanol 4 parts again in the material of step 2, temperature is reduced to 80 DEG C, then stir 20min; Step 4: after the material naturally cooling of step 3 is town road composite terrace material.
Comparative example 2
Step 1: montmorillonite powder and magnesium oxide are pulverized in pulverizer, is crushed to montmorillonite powder and magnesium oxide is 200 object powder; Step 2: by weight respectively by montmorillonite powder 4 parts, 2 parts, the magnesium oxide after organic silicon modified polyurethane 40 parts, bisphenol f type epoxy resin 15 parts, fluorocarbon resin 10 parts, pulverizing, stirred by above-mentioned composition, raised temperature is 120 DEG C, stirs 15min; Step 3: add dioctyl phthalate (DOP) 3 parts, the different pelargonate of tridecyl alcohol 6 parts, lauric acid amide of ethanol 4 parts again in the material of step 2, temperature is reduced to 80 DEG C, then stir 20min; Step 4: after the material naturally cooling of step 3 is town road composite terrace material.
Comparative example 3
Step 1: montmorillonite powder and magnesium oxide are pulverized in pulverizer, is crushed to montmorillonite powder and magnesium oxide is 200 object powder; Step 2: by weight respectively by montmorillonite powder 4 parts, 2 parts, the magnesium oxide after organic silicon modified polyurethane 40 parts, bisphenol f type epoxy resin 15 parts, fluorocarbon resin 10 parts, Nitrogen-containing Phenolic Resins 6 parts, pulverizing, above-mentioned composition is stirred, raised temperature is 120 DEG C, stirs 15min; Step 3: add dioctyl phthalate (DOP) 3 parts again in the material of step 2, temperature is reduced to 80 DEG C, then stir 20min; Step 4: after the material naturally cooling of step 3 is town road composite terrace material.
After preparing town road composite terrace material, measure its ultimate compression strength, folding strength and tensile strength, the performance of the composite terrace material of embodiment 1 to 5 is as follows:
| Ultimate compression strength (MPa) | Folding strength (MPa) | Tensile strength (MPa) | |
| Embodiment 1 | 13.4 | 5.6 | 11.1 |
| Embodiment 2 | 13.2 | 5.5 | 11.3 |
| Embodiment 3 | 14.5 | 7.1 | 13.6 |
| Embodiment 4 | 14.1 | 6.7 | 13.8 |
| Embodiment 5 | 16.4 | 7.8 | 15.5 |
Lacked some key ingredients in floor material of the present invention in comparative example 1 to 4 respectively, after removing, its performance is as follows:
| Ultimate compression strength (MPa) | Folding strength (MPa) | Tensile strength (MPa) | |
| Comparative example 1 | 10.3 | 4.5 | 9.7 |
| Comparative example 2 | 9.5 | 3.9 | 8.6 |
| Comparative example 3 | 10.6 | 4.7 | 9.3 |
Claims (6)
1. a town road composite terrace material, is characterized in that, described town road composite terrace material comprises the composition of following weight parts:
Organic silicon modified polyurethane 30-40 part,
Bisphenol f type epoxy resin 15-25 part,
Fluorocarbon resin 4-10 part,
Nitrogen-containing Phenolic Resins 3-6 part,
Montmorillonite powder 4-6 part,
Magnesium oxide 2-4 part,
Dioctyl phthalate (DOP) 3-7 part,
Tridecyl alcohol different pelargonate 3-6 part,
Lauric acid amide of ethanol 4-8 part.
2. a kind of town road composite terrace material according to claim 1, is characterized in that, described town road composite terrace material comprises the composition of following weight parts:
Organic silicon modified polyurethane 32-38 part,
Bisphenol f type epoxy resin 17-23 part,
Fluorocarbon resin 6-9 part,
Nitrogen-containing Phenolic Resins 4-5 part,
Montmorillonite powder 5-6 part,
Magnesium oxide 3-4 part,
Dioctyl phthalate (DOP) 4-6 part,
Tridecyl alcohol different pelargonate 4-5 part,
Lauric acid amide of ethanol 5-7 part.
3. the preparation method of a kind of town road composite terrace material according to claim 1, it is characterized in that, described preparation method comprises the following steps:
Step 1: montmorillonite powder and magnesium oxide are pulverized in pulverizer, is crushed to montmorillonite powder and magnesium oxide is 200 order-500 object powder;
Step 2: by weight respectively by the montmorillonite powder 4-6 part after organic silicon modified polyurethane 30-40 part, bisphenol f type epoxy resin 15-25 part, fluorocarbon resin 4-10 part, Nitrogen-containing Phenolic Resins 3-6 part, pulverizing, magnesium oxide 2-4 part, above-mentioned composition is stirred, raised temperature is 110-120 DEG C, stirs 15-30min;
Step 3: add dioctyl phthalate (DOP) 3-7 part, tridecyl alcohol different pelargonate 3-6 part, lauric acid amide of ethanol 4-8 part again in the material of step 2, temperature is reduced to 80-90 DEG C, then stirs 10-20min;
Step 4: after the material naturally cooling of step 3 is town road composite terrace material.
4. the preparation method of a kind of town road composite terrace material according to claim 3, is characterized in that, in described step 2, raised temperature is 115 DEG C, stirs 20min.
5. the preparation method of a kind of town road composite terrace material according to claim 3, is characterized in that, in described step 3, temperature is reduced to 85 DEG C, then stir 15min.
6. the preparation method of a kind of town road composite terrace material according to claim 3, is characterized in that, is crushed to montmorillonite powder and magnesium oxide is 300 order-400 object powder in described step 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510508796.6A CN105017756A (en) | 2015-08-19 | 2015-08-19 | Composite terrace material for municipal road and preparation method of composite terrace material |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510508796.6A CN105017756A (en) | 2015-08-19 | 2015-08-19 | Composite terrace material for municipal road and preparation method of composite terrace material |
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| CN105017756A true CN105017756A (en) | 2015-11-04 |
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| CN201510508796.6A Pending CN105017756A (en) | 2015-08-19 | 2015-08-19 | Composite terrace material for municipal road and preparation method of composite terrace material |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105482442A (en) * | 2015-12-31 | 2016-04-13 | 广东生益科技股份有限公司 | Halogen-free resin composition and cover film prepared from the same |
| CN107903611A (en) * | 2017-11-26 | 2018-04-13 | 长沙秋点兵信息科技有限公司 | Composite terrace material for municipal roads and preparation method thereof |
| CN107936526A (en) * | 2017-11-26 | 2018-04-20 | 长沙秋点兵信息科技有限公司 | Composite terrace material for municipal roads and preparation method thereof |
Citations (2)
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| CN101654583A (en) * | 2009-09-24 | 2010-02-24 | 北京红狮漆业有限公司 | Compound epoxy flooring coating and preparation method thereof |
| CN102898613A (en) * | 2012-11-09 | 2013-01-30 | 陕西邦希化工有限公司 | Method for preparing water-soluble organosilicone modified polyurethane resin |
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2015
- 2015-08-19 CN CN201510508796.6A patent/CN105017756A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101654583A (en) * | 2009-09-24 | 2010-02-24 | 北京红狮漆业有限公司 | Compound epoxy flooring coating and preparation method thereof |
| CN102898613A (en) * | 2012-11-09 | 2013-01-30 | 陕西邦希化工有限公司 | Method for preparing water-soluble organosilicone modified polyurethane resin |
Non-Patent Citations (2)
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| 胡玉明 等: "《固化剂》", 31 January 2001 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105482442A (en) * | 2015-12-31 | 2016-04-13 | 广东生益科技股份有限公司 | Halogen-free resin composition and cover film prepared from the same |
| CN107903611A (en) * | 2017-11-26 | 2018-04-13 | 长沙秋点兵信息科技有限公司 | Composite terrace material for municipal roads and preparation method thereof |
| CN107936526A (en) * | 2017-11-26 | 2018-04-20 | 长沙秋点兵信息科技有限公司 | Composite terrace material for municipal roads and preparation method thereof |
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Application publication date: 20151104 |
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