CN105012174A - Chinese herbal toothpaste containing vitamin C and preparation method of Chinese herbal toothpaste - Google Patents
Chinese herbal toothpaste containing vitamin C and preparation method of Chinese herbal toothpaste Download PDFInfo
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Abstract
The invention discloses Chinese herbal toothpaste containing vitamin C and a preparation method of the Chinese herbal toothpaste. The Chinese herbal toothpaste consists of the following ingredients in percentage by weight: 1-2.5% of vitamin C microcapsules, 0.8-2% of Chinese herbal medicine extracts, 25-35% of friction producing material, 15-25% of wetting agents, 0.5-2% of adhesives, 0.8-2.5% of foaming agents, 0.03-0.05% of preservatives, 0.1-0.3% of pH (potential of hydrogen) buffering agents, 0.08-0.15% of sweetening agents, 0.8-2% of essence and the balanced deionized water. The vitamin C is made into the microcapsules; the circumstance that the vitamin C is in contact with air, is oxidized and then fails can be avoided effectively; Chinese herbal medicinal ingredients are added into the toothpaste; conventional effects such as sterilization, inflammation diminishing and tooth cleaning of the toothpaste can be achieved while oral ulcers are prevented and treated; the Chinese herbal medicinal ingredients and the vitamin C are simultaneously added into the toothpaste, the vitamin C has a synergistic interaction effect on the Chinese herbal medicinal ingredients, and thus the effect of the Chinese herbal medicinal ingredients can be achieved sufficiently.
Description
Technical field
The invention belongs to field of toothpaste, be specifically related to a kind of containing ascorbic Chinese herbal toothpaste and preparation method thereof.
Background technology
Toothpaste is dental care products required in the middle of people's daily life, and its basic function is cleaning teeth, fresh breath.In recent years; due to the change of people's living habit and consumption idea; more requirement is proposed to toothpaste; the various toothpaste with health care commercially emerges in large numbers; especially Chinese herb medicine toothpaste occupies the huge market share; Chinese herbal toothpaste has suppression oral cavity noxious bacteria, fresh breath, takes care of one's teeth, prevents and treats the health cares such as oral disease; at present; adopt the toothpaste containing Chinese herbal medicine to carry out preventing and treating and treat gingivitis to have been widely recognized, it has the features such as safe, simple to operate, easy to carry.
Vitamin C is slightly acid, is ingested in body as micronutrient, and dissolve in body, digest, the impact of its Acidity of Aikalinity on human body is very little, so excessively need not take notice of its Acidity of Aikalinity.Vitamin C helps consolidates cell tissue, contributes to the synthesis of collagen protein, and the strong skeleton of energy and tooth, also can prevent gingival hemorrhage, long-term taking is harmless and useful to tooth, gingiva.As can be seen here, vitamin C plays vital effect to the mankind.Toothpaste belongs to the articles for daily use of people's routine, cleaning for oral cavity, utilizes toothpaste to reach to utilize ascorbic object, economical and practical simple again.
The research joined in toothpaste by Chinese herbal medicine is at present many, also there is Chinese invention patent (publication number is CN 102935037 A) " a kind of toothpaste containing vitamin C " to be disclosed in toothpaste and with the addition of vitamin C, but vitamin C is oxidizable in atmosphere, especially mouth of pipe ingress of air place, although it is many to add ascorbic amount, but what really play a role is few, therefore, there is the problem that utilization rate is low.
Summary of the invention
For present situation, the invention provides a kind of containing ascorbic Chinese herbal toothpaste and preparation method thereof, in toothpaste, add vitamin C, and vitamin C is made the form of microcapsule, obtained toothpaste can the various oral disease of effectively preventing.
To achieve these goals, the invention provides following technical scheme:
A kind of containing ascorbic Chinese herbal toothpaste, by weight percentage, composed of the following components: vitamin C microcapsule 1 ~ 2.5%, Chinese herbal medicine extract 0.8 ~ 2%, abrasivus 25 ~ 35%, wetting agent 15 ~ 25%, binding agent 0.5 ~ 2%, foaming agent 0.8 ~ 2.5%, antiseptic 0.03 ~ 0.05%, pH value buffer agent 0.1 ~ 0.3%, sweeting agent 0.08 ~ 0.15%, essence 0.8 ~ 2%, all the other are deionized water;
Described vitamin C microcapsule is made up of capsule material 50 ~ 70% and core 30 ~ 50%; Described capsule material by the hydroxypropyl cellulose of 95%, the vitamin E of 2% and 3% tea polyphenols form, described core is vitamin C;
Described Chinese herbal medicine extract, according to listed as parts by weight, is made up of following raw material: Dens Equi look for 10 ~ 20 parts, Flos Chrysanthemi Indici 15 ~ 20 parts, Radix Notoginseng 20 ~ 30 parts, Caulis Bambusae In Taenia 5 ~ 10 parts, the Rhizoma Pinelliae 6 ~ 12 parts;
The preparation method of described vitamin C microcapsule is:
(1) hydroxypropyl cellulose, vitamin E and tea polyphenols are dissolved in the hot water of 60 ~ 75 DEG C, are cooled to 30 ~ 35 DEG C after stirring and dissolving, the consumption of hot water is 3 ~ 4 times of hydroxypropyl cellulose, vitamin E and tea polyphenols gross weight;
(2) add vitamin C in the mixture obtained to step (1), embed, stir 20 ~ 30min to mix homogeneously;
(3) use cutter emulsification pretreatment, then use homogenizer homogenizing, form the nanoscale emulsion of uniform particle diameter;
(4) be placed in hot bath heating and thermal insulation stirring reaction again in the emulsion obtained to step (3), then through atomizer pelletize, be prepared into vitamin C microcapsule;
The preparation method of described Chinese medicine extract is: looked for by raw material Dens Equi, Flos Chrysanthemi Indici, Radix Notoginseng, Caulis Bambusae In Taenia, the Rhizoma Pinelliae be proportionally mixed to get mixture, adding relative to the determining alcohol of 2 ~ 4 times, mixture is the ethanol of 75 ~ 85%, heating and refluxing extraction 2 ~ 4 times, each reflux, extract, 1 ~ 2 hour, merge extractive liquid, concentrating under reduced pressure, obtains concentrated extracting solution; Drying, obtains and gets dry extract, and pulverizes and is screened into 100 ~ 200 object powder.
Aforementioned containing in ascorbic Chinese herbal toothpaste, described abrasivus is one or more mixing in calcium carbonate, Alumina hydrate, silicon dioxide, calcium hydrogen phosphate, aluminium hydroxide, thermoplastic resin.
Aforementioned containing in ascorbic Chinese herbal toothpaste, one or more mixing in the Polyethylene Glycol that described wetting agent is propylene glycol, sorbitol, glycerol, molecular weight are 400-600, xylitol.Aforementioned containing in ascorbic Chinese herbal toothpaste, described binding agent is one or more mixing in xanthan gum, extra large bath acid sodium, hydroxyethyl-cellulose, guar gum, carboxymethyl cellulose, carrageenan.
Aforementioned containing in ascorbic Chinese herbal toothpaste, described foaming agent is one or more mixing in sodium lauryl sulphate, phenolic group sodium glutamate, N-sodium lauroyl sarcosine, methyl cocoa ester group sodium taurocholate.
Aforementioned containing in ascorbic Chinese herbal toothpaste, described antiseptic is sodium benzoate.
Aforementioned containing in ascorbic Chinese herbal toothpaste, pH value buffer agent is one or both mixing in potassium dihydrogen phosphate, sodium dihydrogen phosphate.
It is aforementioned containing in ascorbic Chinese herbal toothpaste, described sweeting agent is one or more mixing in sucrose, cyclamate, glucide, dipeptide sodium.
Aforementioned containing in ascorbic Chinese herbal toothpaste, described essence is one or more mixing in peppermint, Borneolum Syntheticum, winter wood oil, lemon sesame oil, orange oil, citrus seed oil, Oleum Caryophylli, Oleum Cinnamomi, Oleum Anisi Stellati, Oleum Menthae Rotundifoliae.
The aforementioned preparation method containing ascorbic Chinese herbal toothpaste, comprises the following steps:
The first step, prepares described Chinese medicine ingredients powder;
Second step, the vitamin C microcapsule described in preparation;
3rd step, described Chinese medicine ingredients powder, wetting agent and antiseptic are mixed in described ratio and puts into the deionized water solution that deionized water for stirring makes, add binding agent, abrasivus, foaming agent mixing subsequently in proportion, send into three-in-one vacuum Manufacturing medicine extract machine, high-speed stirred is milled 25 ~ 40 minutes, vacuum outgas, add essence, correctives and pH value buffer agent subsequently to stir again and mill 10 ~ 25 minutes, finally add vitamin C microcapsule and stir mixing in 10 ~ 15 minutes, obtain lotion of toothpaste, by sterile filling, packaging.
The invention has the beneficial effects as follows:
1, vitamin C is joined in toothpaste, the generation of the effective preventing canker sore of life-time service.In order to avoid vitamin C meets air oxidation, be made into the form of microcapsule, effectively solve this problem.
2, also with the addition of Chinese medicine ingredients in toothpaste simultaneously, while there is prevention and therapy oral ulcer, also there is effect of toothpaste routine: sterilization, antiinflammatory, cleaning teeth, vitamin C joins in toothpaste simultaneously, Chinese medicine ingredients is had to the effect of Synergistic, what Chinese medicine effect was played is more abundant.
Detailed description of the invention
The experimental technique used in following embodiment if no special instructions, is conventional method.
Material used in following embodiment, reagent etc., if no special instructions, all can obtain from commercial channels.
Embodiment 1
A kind of containing ascorbic Chinese herbal toothpaste, by weight percentage, composed of the following components: vitamin C microcapsule 1%, Chinese herbal medicine extract 2%, abrasivus (calcium carbonate) 25%, wetting agent (propylene glycol) 25%, binding agent (xanthan gum) 0.5%, foaming agent (sodium lauryl sulphate, phenolic group sodium glutamate with arbitrarily than mixing) 2.5%, antiseptic (sodium benzoate) 0.03%, pH value buffer agent (potassium dihydrogen phosphate) 0.1%, sweeting agent (sucrose) 0.08%, essence (Oleum Caryophylli and peppermint with arbitrarily than mixing) 2%, all the other are deionized water,
Described vitamin C microcapsule is made up of capsule material 50% and core 50%; Described capsule material by the hydroxypropyl cellulose of 95%, the vitamin E of 2% and 3% tea polyphenols form, described core is vitamin C;
Described Chinese herbal medicine extract, according to listed as parts by weight, is made up of following raw material: Dens Equi look for 10 parts, Flos Chrysanthemi Indici 20 parts, Radix Notoginseng 20 parts, Caulis Bambusae In Taenia 5 parts, the Rhizoma Pinelliae 12 parts;
The preparation method of described vitamin C microcapsule is:
(1) hydroxypropyl cellulose, vitamin E and tea polyphenols are dissolved in the hot water of 60 DEG C, are cooled to 30 DEG C after stirring and dissolving, the consumption of hot water is 3 times of hydroxypropyl cellulose, vitamin E and tea polyphenols gross weight;
(2) add vitamin C in the mixture obtained to step (1), embed, stir 20min to mix homogeneously;
(3) use cutter emulsification pretreatment, then use homogenizer homogenizing, form the nanoscale emulsion of uniform particle diameter;
(4) be placed in hot bath heating and thermal insulation stirring reaction again in the emulsion obtained to step (3), then through atomizer pelletize, be prepared into vitamin C microcapsule;
The preparation method of described Chinese medicine extract is: looked for by raw material Dens Equi, Flos Chrysanthemi Indici, Radix Notoginseng, Caulis Bambusae In Taenia, the Rhizoma Pinelliae be proportionally mixed to get mixture, adding relative to the determining alcohol of 2 times, mixture is the ethanol of 7%, heating and refluxing extraction 2 times, each reflux, extract, 2 hours, merge extractive liquid, concentrating under reduced pressure, obtains concentrated extracting solution; Drying, obtains and gets dry extract, and pulverizes and is screened into 100 object powder.
The aforementioned preparation method containing ascorbic Chinese herbal toothpaste, comprises the following steps:
The first step, prepares described Chinese medicine ingredients powder;
Second step, the vitamin C microcapsule described in preparation;
3rd step, described Chinese medicine ingredients powder, wetting agent and antiseptic are mixed in described ratio and puts into the deionized water solution that deionized water for stirring makes, add binding agent, abrasivus, foaming agent mixing subsequently in proportion, send into three-in-one vacuum Manufacturing medicine extract machine, high-speed stirred is milled 25 minutes, vacuum outgas, add essence, correctives and pH value buffer agent subsequently to stir again and mill 25 minutes, finally add vitamin C microcapsule and stir mixing in 10 minutes, obtain lotion of toothpaste, by sterile filling, packaging.
Embodiment 2
A kind of containing ascorbic Chinese herbal toothpaste, by weight percentage, consist of the following composition: vitamin C microcapsule 1.5%, Chinese herbal medicine extract 1%, abrasivus (Alumina hydrate and silicon dioxide with arbitrarily than mixing) 30%, wetting agent (sorbitol and glycerol with arbitrarily than mixing) 20%, binding agent (extra large bath acid sodium) 1%, foaming agent (phenolic group sodium glutamate) 1%, antiseptic (sodium benzoate) 0.04%, pH value buffer agent (sodium dihydrogen phosphate) 0.2%, sweeting agent (cyclamate) 0.1%, essence (Borneolum Syntheticum, winter wood oil, lemon sesame oil with arbitrarily than mixing) 1%, all the other are deionized water,
Described vitamin C microcapsule is made up of capsule material 60% and core 40%; Described capsule material by the hydroxypropyl cellulose of 95%, the vitamin E of 2% and 3% tea polyphenols form, described core is vitamin C;
Described Chinese herbal medicine extract, according to listed as parts by weight, is made up of following raw material: Dens Equi look for 15 parts, Flos Chrysanthemi Indici 18 parts, Radix Notoginseng 25 parts, Caulis Bambusae In Taenia 8 parts, the Rhizoma Pinelliae 10 parts;
The preparation method of described vitamin C microcapsule is:
(1) hydroxypropyl cellulose, vitamin E and tea polyphenols are dissolved in the hot water of 65 DEG C, are cooled to 30 DEG C after stirring and dissolving, the consumption of hot water is 4 times of hydroxypropyl cellulose, vitamin E and tea polyphenols gross weight;
(2) add vitamin C in the mixture obtained to step (1), embed, stir 25min to mix homogeneously;
(3) use cutter emulsification pretreatment, then use homogenizer homogenizing, form the nanoscale emulsion of uniform particle diameter;
(4) be placed in hot bath heating and thermal insulation stirring reaction again in the emulsion obtained to step (3), then through atomizer pelletize, be prepared into vitamin C microcapsule;
The preparation method of described Chinese medicine extract is: looked for by raw material Dens Equi, Flos Chrysanthemi Indici, Radix Notoginseng, Caulis Bambusae In Taenia, the Rhizoma Pinelliae be proportionally mixed to get mixture, adding relative to the determining alcohol of 3 times, mixture is the ethanol of 80%, heating and refluxing extraction 3 times, each reflux, extract, 1.5 hours, merge extractive liquid, concentrating under reduced pressure, obtains concentrated extracting solution; Drying, obtains and gets dry extract, and pulverizes and is screened into 150 object powder.
The aforementioned preparation method containing ascorbic Chinese herbal toothpaste, comprises the following steps:
The first step, prepares described Chinese medicine ingredients powder;
Second step, the vitamin C microcapsule described in preparation;
3rd step, described Chinese medicine ingredients powder, wetting agent and antiseptic are mixed in described ratio and puts into the deionized water solution that deionized water for stirring makes, add binding agent, abrasivus, foaming agent mixing subsequently in proportion, send into three-in-one vacuum Manufacturing medicine extract machine, high-speed stirred is milled 30 minutes, vacuum outgas, add essence, correctives and pH value buffer agent subsequently to stir again and mill 15 minutes, finally add vitamin C microcapsule and stir mixing in 10 minutes, obtain lotion of toothpaste, by sterile filling, packaging.
Embodiment 3
A kind of containing ascorbic Chinese herbal toothpaste, by weight percentage, consist of the following composition: vitamin C microcapsule 2%, Chinese herbal medicine extract 1.5%, abrasivus (calcium hydrogen phosphate and aluminium hydroxide with arbitrarily than mixing) 30%, wetting agent (molecular weight is the Polyethylene Glycol of 400-600) 20%, binding agent (guar gum and carboxymethyl cellulose with arbitrarily than mixing) 1.5%, foaming agent (N-sodium lauroyl sarcosine) 2%, antiseptic (sodium benzoate) 0.04%, pH value buffer agent (potassium dihydrogen phosphate and sodium dihydrogen phosphate with arbitrarily than mixing) 0.2%, sweeting agent (glucide) 0.12%, essence (lemon sesame oil, orange oil and citrus seed oil are with arbitrarily than mixing) 1.5%, all the other are deionized water,
Described vitamin C microcapsule is made up of capsule material 65% and core 35%; Described capsule material by the hydroxypropyl cellulose of 95%, the vitamin E of 2% and 3% tea polyphenols form, described core is vitamin C;
Described Chinese herbal medicine extract, according to listed as parts by weight, is made up of following raw material: Dens Equi look for 18 parts, Flos Chrysanthemi Indici 18 parts, Radix Notoginseng 23 parts, Caulis Bambusae In Taenia 6 parts, the Rhizoma Pinelliae 8 parts;
The preparation method of described vitamin C microcapsule is:
(1) hydroxypropyl cellulose, vitamin E and tea polyphenols are dissolved in the hot water of 70 DEG C, are cooled to 35 DEG C after stirring and dissolving, the consumption of hot water is 3 times of hydroxypropyl cellulose, vitamin E and tea polyphenols gross weight;
(2) add vitamin C in the mixture obtained to step (1), embed, stir 30min to mix homogeneously;
(3) use cutter emulsification pretreatment, then use homogenizer homogenizing, form the nanoscale emulsion of uniform particle diameter;
(4) be placed in hot bath heating and thermal insulation stirring reaction again in the emulsion obtained to step (3), then through atomizer pelletize, be prepared into vitamin C microcapsule;
The preparation method of described Chinese medicine extract is: looked for by raw material Dens Equi, Flos Chrysanthemi Indici, Radix Notoginseng, Caulis Bambusae In Taenia, the Rhizoma Pinelliae be proportionally mixed to get mixture, adding relative to the determining alcohol of 3 times, mixture is the ethanol of 80%, heating and refluxing extraction 3 times, each reflux, extract, 2 hours, merge extractive liquid, concentrating under reduced pressure, obtains concentrated extracting solution; Drying, obtains and gets dry extract, and pulverizes and is screened into 100 object powder.
The aforementioned preparation method containing ascorbic Chinese herbal toothpaste, comprises the following steps:
The first step, prepares described Chinese medicine ingredients powder;
Second step, the vitamin C microcapsule described in preparation;
3rd step, described Chinese medicine ingredients powder, wetting agent and antiseptic are mixed in described ratio and puts into the deionized water solution that deionized water for stirring makes, add binding agent, abrasivus, foaming agent mixing subsequently in proportion, send into three-in-one vacuum Manufacturing medicine extract machine, high-speed stirred is milled 35 minutes, vacuum outgas, add essence, correctives and pH value buffer agent subsequently to stir again and mill 20 minutes, finally add vitamin C microcapsule and stir mixing in 15 minutes, obtain lotion of toothpaste, by sterile filling, packaging.
Embodiment 4
A kind of containing ascorbic Chinese herbal toothpaste, by weight percentage, consist of the following composition: vitamin C microcapsule 2.5%, Chinese herbal medicine extract 0.8%, abrasivus (thermoplastic resin) 35%, wetting agent (xylitol) 15%, binding agent (carrageenan) 2%, foaming agent (methyl cocoa ester group sodium taurocholate) 0.8%, antiseptic (sodium benzoate) 0.05%, pH value buffer agent (sodium dihydrogen phosphate) 0.3%, sweeting agent (dipeptide sodium) 0.15%, essence (Oleum Menthae Rotundifoliae) 0.8%, all the other are deionized water;
Described vitamin C microcapsule is made up of capsule material 70% and core 30%; Described capsule material by the hydroxypropyl cellulose of 95%, the vitamin E of 2% and 3% tea polyphenols form, described core is vitamin C;
Described Chinese herbal medicine extract, according to listed as parts by weight, is made up of following raw material: Dens Equi look for 20 parts, Flos Chrysanthemi Indici 15 parts, Radix Notoginseng 30 parts, Caulis Bambusae In Taenia 5 parts, the Rhizoma Pinelliae 12 parts;
The preparation method of described vitamin C microcapsule is:
(1) hydroxypropyl cellulose, vitamin E and tea polyphenols are dissolved in the hot water of 75 DEG C, are cooled to 35 DEG C after stirring and dissolving, the consumption of hot water is 4 times of hydroxypropyl cellulose, vitamin E and tea polyphenols gross weight;
(2) add vitamin C in the mixture obtained to step (1), embed, stir 30min to mix homogeneously;
(3) use cutter emulsification pretreatment, then use homogenizer homogenizing, form the nanoscale emulsion of uniform particle diameter;
(4) be placed in hot bath heating and thermal insulation stirring reaction again in the emulsion obtained to step (3), then through atomizer pelletize, be prepared into vitamin C microcapsule;
The preparation method of described Chinese medicine extract is: looked for by raw material Dens Equi, Flos Chrysanthemi Indici, Radix Notoginseng, Caulis Bambusae In Taenia, the Rhizoma Pinelliae be proportionally mixed to get mixture, adding relative to the determining alcohol of 4 times, mixture is the ethanol of 75%, heating and refluxing extraction 4 times, each reflux, extract, 1 hour, merge extractive liquid, concentrating under reduced pressure, obtains concentrated extracting solution; Drying, obtains and gets dry extract, and pulverizes and is screened into 200 object powder.
The aforementioned preparation method containing ascorbic Chinese herbal toothpaste, comprises the following steps:
The first step, prepares described Chinese medicine ingredients powder;
Second step, the vitamin C microcapsule described in preparation;
3rd step, described Chinese medicine ingredients powder, wetting agent and antiseptic are mixed in described ratio and puts into the deionized water solution that deionized water for stirring makes, add binding agent, abrasivus, foaming agent mixing subsequently in proportion, send into three-in-one vacuum Manufacturing medicine extract machine, high-speed stirred is milled 40 minutes, vacuum outgas, add essence, correctives and pH value buffer agent subsequently to stir again and mill 25 minutes, finally add vitamin C microcapsule and stir mixing in 15 minutes, obtain lotion of toothpaste, by sterile filling, packaging.
Toothpaste the present invention obtained carries out clinical effectiveness test, and concrete outcome is shown in the table 1 that clinical observation is added up.
The clinical observation statistical table of table 1 toothpaste of the present invention
| Disease | Number (individual) | Effective (individual) | Effectively (individual) | Effective percentage (%) |
| Oral ulcer | 38 | 29 | 6 | 92.1 |
| Gingival hemorrhage | 42 | 34 | 5 | 92.9 |
| Periodontitis | 31 | 19 | 7 | 83.8 |
| Gingivitis | 38 | 26 | 8 | 89.9 |
| Tooth macula lutea | 20 | 12 | 5 | 85.0 |
| Dental caries | 28 | 15 | 8 | 82.1 |
Toothpaste of the present invention, every day uses sooner or later, when using at every turn, after Tooth paste brush is gone out foam, include about 1 minute at mouth, can the generation of effective preventing canker sore, for the people of oral ulcer, the time of pain lasts can be reduced, for the people of oral ulcer of often showing effect, use after 2 ~ 3 months, sickness rate obviously reduces, use above person half a year, oral ulcer of almost no longer showing effect.
The present invention, while having above-mentioned effect, also has sterilization, antiinflammatory, the effect such as reducing swelling and alleviating pain, tooth-whitening, also can the symptom such as effectively preventing gingival hemorrhage, gingivitis, periodontitis, gingival swelling and pain, can also the generation of caries prevention.
Claims (10)
1. one kind contains ascorbic Chinese herbal toothpaste, it is characterized in that, by weight percentage, consist of the following composition: vitamin C microcapsule 1 ~ 2.5%, Chinese herbal medicine extract 0.8 ~ 2%, abrasivus 25 ~ 35%, wetting agent 15 ~ 25%, binding agent 0.5 ~ 2%, foaming agent 0.8 ~ 2.5%, antiseptic 0.03 ~ 0.05%, pH value buffer agent 0.1 ~ 0.3%, sweeting agent 0.08 ~ 0.15%, essence 0.8 ~ 2%, all the other are deionized water;
Described vitamin C microcapsule is made up of capsule material 50 ~ 70% and core 30 ~ 50%; Described capsule material by the hydroxypropyl cellulose of 95%, the vitamin E of 2% and 3% tea polyphenols form, described core is vitamin C;
Described Chinese herbal medicine extract, according to listed as parts by weight, is made up of following raw material: Dens Equi look for 10 ~ 20 parts, Flos Chrysanthemi Indici 15 ~ 20 parts, Radix Notoginseng 20 ~ 30 parts, Caulis Bambusae In Taenia 5 ~ 10 parts, the Rhizoma Pinelliae 6 ~ 12 parts;
The preparation method of described vitamin C microcapsule is:
(1) hydroxypropyl cellulose, vitamin E and tea polyphenols are dissolved in the hot water of 60 ~ 75 DEG C, are cooled to 30 ~ 35 DEG C after stirring and dissolving, the consumption of hot water is 3 ~ 4 times of hydroxypropyl cellulose, vitamin E and tea polyphenols gross weight;
(2) add vitamin C in the mixture obtained to step (1), embed, stir 20 ~ 30min to mix homogeneously;
(3) use cutter emulsification pretreatment, then use homogenizer homogenizing, form the nanoscale emulsion of uniform particle diameter;
(4) be placed in hot bath heating and thermal insulation stirring reaction again in the emulsion obtained to step (3), then through atomizer pelletize, be prepared into vitamin C microcapsule;
The preparation method of described Chinese medicine extract is: looked for by raw material Dens Equi, Flos Chrysanthemi Indici, Radix Notoginseng, Caulis Bambusae In Taenia, the Rhizoma Pinelliae be proportionally mixed to get mixture, adding relative to the determining alcohol of 2 ~ 4 times, mixture is the ethanol of 75 ~ 85%, heating and refluxing extraction 2 ~ 4 times, each reflux, extract, 1 ~ 2 hour, merge extractive liquid, concentrating under reduced pressure, obtains concentrated extracting solution; Drying, obtains and gets dry extract, and pulverizes and is screened into 100 ~ 200 object powder.
2. one according to claim 1 contains ascorbic Chinese herbal toothpaste, it is characterized in that, described abrasivus is one or more mixing in calcium carbonate, Alumina hydrate, silicon dioxide, calcium hydrogen phosphate, aluminium hydroxide, thermoplastic resin.
3. one according to claim 1 contains ascorbic Chinese herbal toothpaste, it is characterized in that, one or more mixing in the Polyethylene Glycol that described wetting agent is propylene glycol, sorbitol, glycerol, molecular weight are 400-600, xylitol.
4. one according to claim 1 contains ascorbic Chinese herbal toothpaste, it is characterized in that, described binding agent is one or more mixing in xanthan gum, extra large bath acid sodium, hydroxyethyl-cellulose, guar gum, carboxymethyl cellulose, carrageenan.
5. one according to claim 1 contains ascorbic Chinese herbal toothpaste; it is characterized in that, described foaming agent is one or more mixing in sodium lauryl sulphate, phenolic group sodium glutamate, N-sodium lauroyl sarcosine, methyl cocoa ester group sodium taurocholate.
6. one according to claim 1 contains ascorbic Chinese herbal toothpaste, it is characterized in that, described antiseptic is sodium benzoate.
7. one according to claim 1 contains ascorbic Chinese herbal toothpaste, it is characterized in that, pH value buffer agent is one or both mixing in potassium dihydrogen phosphate, sodium dihydrogen phosphate.
8. one according to claim 1 contains ascorbic Chinese herbal toothpaste, it is characterized in that, described sweeting agent is one or more mixing in sucrose, cyclamate, glucide, dipeptide sodium.
9. one according to claim 1 contains ascorbic Chinese herbal toothpaste, it is characterized in that, described essence is one or more mixing in peppermint, Borneolum Syntheticum, winter wood oil, lemon sesame oil, orange oil, citrus seed oil, Oleum Caryophylli, Oleum Cinnamomi, Oleum Anisi Stellati, Oleum Menthae Rotundifoliae.
10. the preparation method containing ascorbic Chinese herbal toothpaste according to claim 1 ~ 9 any one, is characterized in that, comprise the following steps:
The first step, prepares described Chinese medicine ingredients powder;
Second step, the vitamin C microcapsule described in preparation;
3rd step, described Chinese medicine ingredients powder, wetting agent and antiseptic are mixed in described ratio and puts into the deionized water solution that deionized water for stirring makes, add binding agent, abrasivus, foaming agent mixing subsequently in proportion, send into three-in-one vacuum Manufacturing medicine extract machine, high-speed stirred is milled 25 ~ 40 minutes, vacuum outgas, add essence, correctives and pH value buffer agent subsequently to stir again and mill 10 ~ 25 minutes, finally add vitamin C microcapsule and stir mixing in 10 ~ 15 minutes, obtain lotion of toothpaste, by sterile filling, packaging.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107095827A (en) * | 2017-06-30 | 2017-08-29 | 合肥卓畅农业科技有限公司 | One kind is antibacterial to remove stain Chinese medicinal toothpaste and preparation method thereof |
| CN108904410A (en) * | 2018-08-27 | 2018-11-30 | 广州市盛龙口腔清洁用品有限公司 | A kind of friction-type toothpaste and preparation method thereof |
| CN112294837A (en) * | 2020-11-17 | 2021-02-02 | 广州三三医药生物科技有限公司 | Arginine, taurine and glutamine capsule and preparation method thereof |
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2015
- 2015-07-10 CN CN201510403774.3A patent/CN105012174A/en active Pending
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| 中华人民共和国***: "《化妆品卫生规范》", 31 January 2007 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107095827A (en) * | 2017-06-30 | 2017-08-29 | 合肥卓畅农业科技有限公司 | One kind is antibacterial to remove stain Chinese medicinal toothpaste and preparation method thereof |
| CN108904410A (en) * | 2018-08-27 | 2018-11-30 | 广州市盛龙口腔清洁用品有限公司 | A kind of friction-type toothpaste and preparation method thereof |
| CN112294837A (en) * | 2020-11-17 | 2021-02-02 | 广州三三医药生物科技有限公司 | Arginine, taurine and glutamine capsule and preparation method thereof |
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Application publication date: 20151104 |