CN105000253B - Antistatic paper and plastics compound bag and preparation method thereof - Google Patents
Antistatic paper and plastics compound bag and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of antistatic paper and plastics compound bag and preparation method thereof, the paper and plastics compound bag includes plastic layer and paper layer, and the plastic layer is located on the surface of the paper layer;Wherein, the plastic layer includes polyvinyl chloride, polyethylene, alkyl quaternary ammonium salts, polyphenylene sulfide, sodium alkyl sulfonate, glycollic amide, cyclohexanone, tin indium oxide, glycerine, lactose, butylene phthalate and odium stearate.The antistatic paper and plastics compound bag has excellent antistatic property, and preparation method is simple and easy to do, with low cost.
Description
Technical field
Field is manufactured the present invention relates to paper plastic bag, in particular it relates to a kind of antistatic paper and plastics compound bag and preparation method thereof.
Background technology
Paper plastic bag has been widely applied in daily life as a kind of easily storing apparatus, for shipping
Small ancestor's bulk powder shape material, is a kind of packaging material being in daily use at present.Paper plastic bag is a kind of compound paper bag, including paper layer
And plastic layer.
At present, the plastic layer of paper plastic bag is typically to be made up of polypropylene or polyethylene, and the paper plastic bag that this material is made exists
Surface can take electrostatic when using, and these electrostatic can attract the dust in air, paper plastic bag surface is covered by dust, when people's
When hand touches paper plastic bag surface, the sense of touch of electric shock is might have, the normal of paper plastic bag has been had a strong impact on and has used.
The content of the invention
For above-mentioned prior art, it is an object of the invention to provide a kind of antistatic paper and plastics compound bag, the antistatic paper
Complex pocket has excellent antistatic property, and preparation method is simple and easy to do, with low cost.
To achieve these goals, the invention provides a kind of antistatic paper and plastics compound bag, the antistatic paper-plastic stick
Bag includes plastic layer and paper layer, and the plastic layer is located on the surface of the paper layer;
Wherein, the plastic layer includes polyvinyl chloride, polyethylene, alkyl quaternary ammonium salts, polyphenylene sulfide, sodium alkyl sulfonate, second
Alkylolamides, cyclohexanone, tin indium oxide, glycerine, lactose, butylene phthalate and odium stearate.
Present invention also offers a kind of preparation method of antistatic paper and plastics compound bag, the preparation method includes:
(1) by polyvinyl chloride, polyethylene, alkyl quaternary ammonium salts, polyphenylene sulfide, sodium alkyl sulfonate, glycollic amide, cyclohexanone,
Film is made in extrusion molding after tin indium oxide, glycerine, lactose, butylene phthalate and odium stearate mixing;
(2) film is heated and is coated on the surface of paper layer and form plastic layer with obtained extrusion coating paper;Or
Person cuts the film, wire drawing and be woven into plastic layer, then sticks the plastic layer in the papery by the way that binding agent is viscous
With obtained extrusion coating paper on the surface of layer;
(3) extrusion coating paper is machined to antistatic paper and plastics compound bag.
The plastic layer of the antistatic paper and plastics compound bag provided by above-mentioned technical proposal, the present invention includes polyvinyl chloride, gathered
Ethene, alkyl quaternary ammonium salts, polyphenylene sulfide, sodium alkyl sulfonate, glycollic amide, cyclohexanone, tin indium oxide, glycerine, lactose, adjacent benzene two
Formic acid fourth diester and odium stearate, compared with the paper plastic bag of prior art, the plastic layer of the antistatic paper and plastics compound bag contains alkane
There is collaboration to make between based quaternary ammonium salt, polyphenylene sulfide, sodium alkyl sulfonate, glycollic amide, cyclohexanone and tin indium oxide, this six kinds of components
With, and can be had an effect between other components so that this paper and plastics compound bag has very excellent antistatic property, together
When the present invention fire-retardant paper and plastics compound bag for preparing that provides method is simple, reaction condition is gentle, suitable for mass production.
Other features and advantages of the present invention will be described in detail in subsequent embodiment part.
Embodiment
The embodiment to the present invention is described in detail below.It should be appreciated that described herein specific
Embodiment is merely to illustrate and explain the present invention, and is not intended to limit the invention.
The invention provides a kind of antistatic paper and plastics compound bag, the antistatic paper and plastics compound bag includes plastic layer and papery
Layer, the plastic layer is located on the surface of the paper layer;
Wherein, the plastic layer includes polyvinyl chloride, polyethylene, alkyl quaternary ammonium salts, polyphenylene sulfide, sodium alkyl sulfonate, second
Alkylolamides, cyclohexanone, tin indium oxide (containing 90% indium oxide, 10% tin oxide), glycerine, lactose, butylene phthalate
And odium stearate.
In the present invention, alkyl quaternary ammonium salts can be selected in wide scope, as long as with antistatic property, can be with
It is OTAC, Cetyltrimethylammonium bromide, octadecyldimethyl benzyl group ammonium chloride, octadecyl
One or more in dimethyl benzyl group ammonium bromide and cetyl dimethyl amine oxide, in order that obtained antistatic paper is multiple
The antistatic property for closing bag is more excellent, it is preferable that alkyl quaternary ammonium salts is selected from OTAC, hexadecyldimethylamine
One or more in base benzyl group ammonium chloride and cetyl dimethyl amine oxide.
In the present invention, the weight average molecular weight of polyvinyl chloride can be selected in wide scope, still, in order that obtained
The antistatic property of antistatic paper and plastics compound bag is more excellent, it is preferable that the weight average molecular weight of polyvinyl chloride is 50000-80000.
Certainly, the weight average molecular weight of polyethylene can also be selected in wide scope, in order that obtained antistatic paper
The antistatic property of complex pocket is more excellent, it is preferable that the weight average molecular weight of polyethylene is 14000-28000.
Similarly, the weight average molecular weight of polyphenylene sulfide can be selected in wide scope, obtained antistatic in order to improve
The antistatic property of paper and plastics compound bag, it is preferable that the weight average molecular weight of polyphenylene sulfide is 12000-18000.
Meanwhile, the content of each component can be selected in wide scope, in order to improve obtained antistatic paper and plastics compound bag
Antistatic property, it is preferable that relative to the polyvinyl chloride of 100 parts by weight, the content of polyethylene is 15-25 parts by weight, alkyl
The content of quaternary ammonium salt is 25-35 parts by weight, and the content of polyphenylene sulfide is 20-25 parts by weight, and the content of sodium alkyl sulfonate is 15-25
Parts by weight, the content of glycollic amide is 12-18 parts by weight, and the content of cyclohexanone is 6-9 parts by weight, and the content of tin indium oxide is
8-10 parts by weight, the content of glycerine is 2-6 parts by weight, and the content of lactose is 1-3 parts by weight, the content of butylene phthalate
For 1-5 parts by weight, the content of odium stearate is 2-4 parts by weight.
In the present invention, the material of the paper layer can be selected in wide scope, but be considered from antistatic property,
Preferably, the paper layer is brown paper or glassine paper.
Present invention also offers a kind of preparation method of antistatic paper and plastics compound bag, the preparation method includes:
(1) by polyvinyl chloride, polyethylene, alkyl quaternary ammonium salts, polyphenylene sulfide, sodium alkyl sulfonate, glycollic amide, cyclohexanone,
Film is made in extrusion molding after tin indium oxide, glycerine, lactose, butylene phthalate and odium stearate mixing;
(2) film is heated and is coated on the surface of paper layer and form plastic layer with obtained extrusion coating paper;Or
Person cuts the film, wire drawing and be woven into plastic layer, then sticks the plastic layer in the papery by the way that binding agent is viscous
With obtained extrusion coating paper on the surface of layer;
(3) extrusion coating paper is machined to antistatic paper and plastics compound bag.
In above-mentioned preparation method, alkyl quaternary ammonium salts can be selected in wide scope, as long as being with antistatic property
Can, can be OTAC, Cetyltrimethylammonium bromide, octadecyldimethyl benzyl group ammonium chloride,
One or more in octadecyldimethyl benzyl group ammonium bromide and cetyl dimethyl amine oxide, in order that obtained anti-quiet
The antistatic property of electric paper and plastics compound bag is more excellent, it is preferable that alkyl quaternary ammonium salts is selected from OTAC, 18
One or more in alkyl dimethyl benzyl group ammonium chloride and cetyl dimethyl amine oxide.
In above-mentioned preparation method, the weight average molecular weight of polyvinyl chloride can be selected in wide scope, still, in order that
The antistatic property of obtained antistatic paper and plastics compound bag is more excellent, it is preferable that the weight average molecular weight of polyvinyl chloride is 50000-
80000。
Certainly, the weight average molecular weight of polyethylene can also be selected in wide scope, in order that obtained antistatic paper
The antistatic property of complex pocket is more excellent, it is preferable that the weight average molecular weight of polyethylene is 14000-28000.
Similarly, the weight average molecular weight of polyphenylene sulfide can be selected in wide scope, obtained antistatic in order to improve
The antistatic property of paper and plastics compound bag, it is preferable that the weight average molecular weight of polyphenylene sulfide is 12000-18000.
Meanwhile, the content of each component can be selected in wide scope, in order to improve obtained antistatic paper and plastics compound bag
Antistatic property, it is preferable that relative to the polyvinyl chloride of 100 parts by weight, the content of polyethylene is 15-25 parts by weight, alkyl
The content of quaternary ammonium salt is 25-35 parts by weight, and the content of polyphenylene sulfide is 20-25 parts by weight, and the content of sodium alkyl sulfonate is 15-25
Parts by weight, the content of glycollic amide is that 12-18 parts by weight, the content of cyclohexanone are that 6-9 parts by weight, the content of tin indium oxide are
8-10 parts by weight, the content of glycerine are that 2-6 parts by weight, the content of lactose are 1-3 parts by weight, the content of butylene phthalate
For 1-5 parts by weight, the content of odium stearate is 2-4 parts by weight.
In above-mentioned preparation method, the material of the paper layer can be selected in wide scope, but from antistatic behaviour
It can consider, it is preferable that the paper layer is brown paper or glassine paper.
The present invention will be described in detail by way of examples below, in the present invention, and polyvinyl chloride and polyethylene are mountain
The commercially available product of eastern Linyi An Feng Chemical Co., Ltd.s, alkyl quaternary ammonium salts is purchased from Shandong Pai Ni Chemical Co., Ltd.s, and polyphenylene sulfide is
Shandong Sai Enji Chemical Co., Ltd.s commercially available product, sodium alkyl sulfonate is purchased from Yongtai Chemical Co., Ltd., and glycollic amide is wide outstanding personization
The commercially available product of work Co., Ltd, tin indium oxide is purchased from Wuhan Xing Zhongcheng Science and Technology Ltd.s, and cyclohexanone is purchased from positive chemical industry in Jinan
Co., Ltd.
Embodiment 1
(1) at 25 DEG C, by polyvinyl chloride (weight average molecular weight is 60000), polyethylene (weight average molecular weight is 20000),
OTAC, polyphenylene sulfide (weight average molecular weight is 15000), sodium alkyl sulfonate, glycollic amide, cyclohexanone,
(mass ratio of raw material is followed successively by 100 for tin indium oxide, glycerine, lactose, butylene phthalate and odium stearate:20:30:22:
20:14:7:9:4: 2:3:3) 2h is mixed, and film is made in extrusion molding at 210 DEG C;
(2) film is carried out being heated to 230 DEG C and be coated on the surface of paper layer to form plastic layer with obtained multiple
(paper layer and the thickness ratio of plastic layer are 1 to combined paper:1);
(3) above-mentioned extrusion coating paper is machined to antistatic paper and plastics compound bag A1.
Embodiment 2
(1) at 25 DEG C, by polyvinyl chloride (weight average molecular weight is 50000), polyethylene (weight average molecular weight is 14000),
Octadecyldimethyl benzyl group ammonium chloride, polyphenylene sulfide (weight average molecular weight is 12000), sodium alkyl sulfonate, glycollic amide, ring
(mass ratio of raw material is followed successively by 100 for hexanone, tin indium oxide, glycerine, lactose, butylene phthalate and odium stearate:15:
30:22:20:14:7: 9:2:1:1:2) 2h is mixed, and film is made in extrusion molding at 210 DEG C;
(2) film is carried out being heated to 230 DEG C and be coated on the surface of paper layer to form plastic layer with obtained multiple
(paper layer and the thickness ratio of plastic layer are 1 to combined paper:1.1);
(3) above-mentioned extrusion coating paper is machined to antistatic paper and plastics compound bag A2.
Embodiment 3
(1) at 25 DEG C, by polyvinyl chloride (weight average molecular weight is 80000), polyethylene (weight average molecular weight is 28000),
Cetyl dimethyl amine oxide, polyphenylene sulfide (weight average molecular weight is 18000), sodium alkyl sulfonate, glycollic amide, cyclohexanone,
(mass ratio of raw material is followed successively by 100 for tin indium oxide, glycerine, lactose, butylene phthalate and odium stearate:25:30:22:
20:14:7:9:6: 3:5:4) 2h is mixed, and film is made in extrusion molding at 210 DEG C;
(2) film is carried out being heated to 230 DEG C and be coated on the surface of paper layer to form plastic layer with obtained multiple
(paper layer and the thickness ratio of plastic layer are 1 to combined paper:1.2);
(3) above-mentioned extrusion coating paper is machined to antistatic paper and plastics compound bag A3.
Embodiment 4
Method according to embodiment 1 carries out obtained antistatic paper and plastics compound bag A4, unlike, change alkyl quaternary ammonium salts
Consumption cause polyvinyl chloride and alkyl quaternary ammonium salts mass ratio be 100:25.
Embodiment 5
Method according to embodiment 1 carries out obtained antistatic paper and plastics compound bag A5, unlike, change alkyl quaternary ammonium salts
Consumption cause polyvinyl chloride and alkyl quaternary ammonium salts mass ratio be 100:35.
Embodiment 6
Method according to embodiment 1 carries out obtained antistatic paper and plastics compound bag A6, unlike, change polyphenylene sulfide
Consumption causes the mass ratio of polyvinyl chloride and polyphenylene sulfide to be 100:20.
Embodiment 7
Method according to embodiment 1 carries out obtained antistatic paper and plastics compound bag A7, unlike, change polyphenylene sulfide
Consumption causes the mass ratio of polyvinyl chloride and polyphenylene sulfide to be 100:25.
Embodiment 8
Method according to embodiment 1 carries out obtained antistatic paper and plastics compound bag A8, unlike, change sodium alkyl sulfonate
Consumption cause polyvinyl chloride and sodium alkyl sulfonate mass ratio be 100:15.
Embodiment 9
Method according to embodiment 1 carries out obtained antistatic paper and plastics compound bag A9, unlike, change sodium alkyl sulfonate
Consumption cause polyvinyl chloride and sodium alkyl sulfonate mass ratio be 100:25.
Embodiment 10
Method according to embodiment 1 carries out obtained antistatic paper and plastics compound bag A10, unlike, change glycollic amide
Consumption cause polyvinyl chloride and glycollic amide mass ratio be 100:12.
Embodiment 11
Method according to embodiment 1 carries out obtained antistatic paper and plastics compound bag A11, unlike, change glycollic amide
Consumption cause polyvinyl chloride and glycollic amide mass ratio be 100:18.
Embodiment 12
Method according to embodiment 1 carries out obtained antistatic paper and plastics compound bag A12, unlike, change cyclohexanone
Consumption causes the mass ratio of polyvinyl chloride and cyclohexanone to be 100:6.
Embodiment 13
Method according to embodiment 1 carries out obtained antistatic paper and plastics compound bag A13, unlike, change cyclohexanone
Consumption causes the mass ratio of polyvinyl chloride and cyclohexanone to be 100:9.
Embodiment 14
Method according to embodiment 1 carries out obtained antistatic paper and plastics compound bag A14, unlike, change tin indium oxide
Consumption cause polyvinyl chloride and tin indium oxide mass ratio be 100:8.
Embodiment 15
Method according to embodiment 1 carries out obtained antistatic paper and plastics compound bag A15, unlike, change tin indium oxide
Consumption cause polyvinyl chloride and tin indium oxide mass ratio be 100:10.
Embodiment 16
(1) at 25 DEG C, by polyvinyl chloride (weight average molecular weight is 50000), polyethylene (weight average molecular weight is 14000),
It is alkyl quaternary ammonium salts, polyphenylene sulfide (weight average molecular weight is 12000), sodium alkyl sulfonate, glycollic amide, cyclohexanone, tin indium oxide, sweet
Oil, lactose, butylene phthalate and odium stearate.(mass ratio of raw material is followed successively by 100:15:30:22:20:14:7:9:
2:1:1:2) 2h is mixed, and film is made in extrusion molding at 210 DEG C;
(2) by the film cutting, wire drawing, be woven into plastic layer, then by the plastic layer by binding agent it is viscous stick in
So that extrusion coating paper is made, (paper layer and the thickness ratio of plastic layer is 1 on the surface of the paper layer:1);
(3) above-mentioned extrusion coating paper is machined to antistatic paper and plastics compound bag A16.
Comparative example 1
Carry out as described in Example 1, except that, alkyl quaternary ammonium salts is not contained in raw material, antistatic paper is made
Complex pocket B1.
Comparative example 2
Carry out as described in Example 1, except that, polyphenylene sulfide is not contained in raw material, antistatic paper is made and answers
Close bag B2.
Comparative example 3
Carry out as described in Example 1, except that, sodium alkyl sulfonate is not contained in raw material, antistatic paper is made
Complex pocket B3.
Comparative example 4
Carry out as described in Example 1, except that, glycollic amide is not contained in raw material, antistatic paper is made and answers
Close bag B4.
Comparative example 5
Carry out as described in Example 1, except that, cyclohexanone is not contained in raw material, antistatic paper-plastic stick is made
Bag B5.
Comparative example 6
Carry out as described in Example 1, except that, tin indium oxide is not contained in raw material, antistatic paper is made and answers
Close bag B6.
Detect example 1
The sheet resistance (R/ Ω) of the obtained antistatic paper and plastics compound bag is measured by sheet resistance tester.Detection knot
Fruit is as shown in table 1.
Table 1
A1 | A2 | A3 | A4 | A5 | A6 | A7 | A8 | A9 | A10 | A11 | |
R/109Ω | 8.2 | 7.8 | 7.9 | 7.7 | 6.9 | 7.5 | 7.4 | 7.7 | 7.8 | 8.1 | 8.0 |
Table 2
A12 | A13 | A14 | A15 | A16 | B1 | B2 | B3 | B4 | B5 | B6 | |
R/109Ω | 8.2 | 7.8 | 7.9 | 7.7 | 6.9 | 0.005 | 0.004 | 0.005 | 0.003 | 0.002 | 0.003 |
As shown in Table 1, the antistatic paper and plastics compound bag that the present invention is provided has excellent antistatic property, relative to A1-
A16, B1-B6 sheet resistance value are obviously reduced, and the smaller proof surface electrostatic dissipation of sheet resistance value is fewer, antistatic effect
Fruit it is poorer, it can thus be concluded that, alkyl quaternary ammonium salts, polyphenylene sulfide, sodium alkyl sulfonate, glycollic amide, cyclohexanone and tin indium oxide this six
There is synergy between kind component, and can be had an effect between other components so that this paper and plastics compound bag has very
Excellent antistatic property.
The preferred embodiment of the present invention described in detail above, still, the present invention are not limited in above-mentioned embodiment
Detail, in the range of the technology design of the present invention, a variety of simple variants can be carried out to technical scheme, this
A little simple variants belong to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned embodiment, in not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to it is various can
The combination of energy no longer separately illustrates.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally
The thought of invention, it should equally be considered as content disclosed in this invention.
Claims (6)
1. a kind of antistatic paper and plastics compound bag, it is characterised in that the paper and plastics compound bag includes plastic layer and paper layer, the modeling
The bed of material is located on the surface of the paper layer;
Wherein, the plastic layer includes polyvinyl chloride, polyethylene, alkyl quaternary ammonium salts, polyphenylene sulfide, sodium alkyl sulfonate, glycollyl
Amine, cyclohexanone, tin indium oxide, glycerine, lactose, butylene phthalate and odium stearate;Wherein, relative to 100 parts by weight
The polyvinyl chloride, the content of the polyethylene is 15-25 parts by weight, and the content of the alkyl quaternary ammonium salts is 25-35 weight
Part, the content of the polyphenylene sulfide is 20-25 parts by weight, and the content of the sodium alkyl sulfonate is 15-25 parts by weight, the ethanol
The content of acid amides is 12-18 parts by weight, and the content of the cyclohexanone is 6-9 parts by weight, and the content of the tin indium oxide is 8-10
Parts by weight, the content of the glycerine is 2-6 parts by weight, and the content of the lactose is 1-3 parts by weight, the phthalic acid fourth two
The content of ester is 1-5 parts by weight, and the content of the odium stearate is 2-4 parts by weight;Wherein, the Weight-average molecular of the polyvinyl chloride
Measure as 50000-80000, the weight average molecular weight of the polyethylene is 14000-28000, the weight average molecular weight of the polyphenylene sulfide
For 12000-18000.
2. antistatic paper and plastics compound bag according to claim 1, wherein, the alkyl quaternary ammonium salts is selected from octadecyl front three
One or more in ammonium chloride, octadecyldimethyl benzyl group ammonium chloride and cetyl dimethyl amine oxide.
3. the antistatic paper and plastics compound bag according to any one in claim 1-2, wherein, the paper layer is brown paper
Or glassine paper.
4. a kind of preparation method of antistatic paper and plastics compound bag, it is characterised in that the preparation method includes:
(1) by polyvinyl chloride, polyethylene, alkyl quaternary ammonium salts, polyphenylene sulfide, sodium alkyl sulfonate, glycollic amide, cyclohexanone, oxidation
Film is made in extrusion molding after indium tin, glycerine, lactose, butylene phthalate and odium stearate mixing;
(2) film is heated and is coated on the surface of paper layer and form plastic layer with obtained extrusion coating paper;Or will
Film cutting, wire drawing and plastic layer is woven into, then sticks the plastic layer in the paper layer by the way that binding agent is viscous
With obtained extrusion coating paper on surface;
(3) extrusion coating paper is machined to antistatic paper and plastics compound bag;
Wherein, relative to the polyvinyl chloride of 100 parts by weight, the consumption of the polyethylene is 15-25 parts by weight, the alkyl
The consumption of quaternary ammonium salt is 25-35 parts by weight, and the consumption of the polyphenylene sulfide is 20-25 parts by weight, the use of the sodium alkyl sulfonate
Measure as 15-25 parts by weight, the consumption of the glycollic amide be 12-18 parts by weight, the consumption of the cyclohexanone be 6-9 parts by weight,
The consumption of the tin indium oxide is that 8-10 parts by weight, the consumption of the glycerine are that 2-6 parts by weight, the consumption of the lactose are 1-3
Parts by weight, the consumption of the butylene phthalate are 1-5 parts by weight, and the consumption of odium stearate is 2-4 parts by weight;Wherein,
The weight average molecular weight of the polyvinyl chloride is 50000-80000, and the weight average molecular weight of the polyethylene is 14000-28000, institute
The weight average molecular weight for stating polyphenylene sulfide is 12000-18000.
5. preparation method according to claim 4, wherein, the alkyl quaternary ammonium salts is selected from octadecyl trimethyl chlorination
One or more in ammonium, octadecyldimethyl benzyl group ammonium chloride and cetyl dimethyl amine oxide.
6. preparation method according to claim 4, wherein, the paper layer is brown paper or glassine paper.
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CN2403720Y (en) * | 1999-12-30 | 2000-11-01 | 汕头市龙湖区灵野祥和有限公司 | Paper and plastic composite packing material |
CN202642331U (en) * | 2012-05-31 | 2013-01-02 | 马兆元 | Paper-plastic packing bag |
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