CN104910841A - Anti-permeability hot-melt pressure-sensitive adhesive - Google Patents
Anti-permeability hot-melt pressure-sensitive adhesive Download PDFInfo
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- CN104910841A CN104910841A CN201510137013.8A CN201510137013A CN104910841A CN 104910841 A CN104910841 A CN 104910841A CN 201510137013 A CN201510137013 A CN 201510137013A CN 104910841 A CN104910841 A CN 104910841A
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Abstract
The invention discloses an anti-permeability hot-melt pressure-sensitive adhesive, which comprises the following components by weight ratio: 0-30% of SBS thermoplastic elastomer (styrene-butadiene-styrene segmented copolymer, short for SBS), 0-20% of SBS thermoplastic elastomer (styrene-isoprene-styrene segmented copolymer, short for SIS), 0-30% of alkene copolymer, 0-70% of No.1 tackifying resin, 1-70% of No.2 tackifying resin, 10-30% of mineral oil, 0-10% of wax, and 0.1-2% of anti-oxidant. Through reasonable formula design, on-line permeability of the hot-melt pressure-sensitive adhesive can be obviously improved, glue-leakage rate is reduced, shutdown frequency is reduced, base material waste is reduced, off-line permeability is obviously improved, mutual adhesion risk after finished product off-line package is controlled, the hot-melt pressure-sensitive adhesive can increase the anti-permeability performance, bonding intensity is not sacrificed, and initial and aging intensity of a structural adhesive are consistent with that of the common hot-melt pressure-sensitive adhesive.
Description
Technical field
The present invention relates to technical field of hot-melt pressure-sensitive adhesive, especially relate to a kind of disposable sanitary articles industry structure glue, ooze hot-fusible pressure-sensitive adhesive for on-line spray with the anti-reflective of bonding various material.
Background technology
Disposable sanitary articles industry is that the various materials such as various non-woven fabrics, Time of Fluff Slurry, macromolecule water uptake pearl, PE film and elastic are connected into a function entirety as sanitary napkin, protection pad, baby paper diaper, diaper, adult-incontinence urine pants etc. by melt viscosity.Hot-fusible pressure-sensitive adhesive is commonly used to bonding various material, its use procedure first in hot melt adhesive machine, is fused into liquid, squeezed to nozzle by glue pump, then be sprayed onto on base material by air, usual this hot melt adhesive requires to have certain open hour, initial bond strenght and aging bonding strength.When common hot-fusible pressure-sensitive adhesive meets above-mentioned basic demand simultaneously, permeate sometimes on a production line, the glue after infiltration can be deposited on the wheel shaft of production line, causes and shuts down frequently, affect production efficiency, waste other base material simultaneously; And finished product after off-line extrudes due to packed and transported, some glue can infiltrate, and causes adhesion between every sheet health product, and separately they, will tear health product.
Summary of the invention
In order to solve above-mentioned prior art problem; the invention provides and a kind of solve the online and off-line inverse-seepage problem of disposable sanitary articles hot-fusible pressure-sensitive adhesive; the power generating ratio time; finished product packing extrudes rear adhesion, does not destroy, and the anti-reflective simultaneously with suitable initial and aging bonding strength oozes hot-fusible pressure-sensitive adhesive.
Technical scheme of the present invention is: a kind of anti-reflective oozes hot-fusible pressure-sensitive adhesive, it is characterized in that: by following component by weight formulated: SBS thermoplastic elastomer (styrene-butadiene-styrene block copolymer, be called for short SBS) 0 ~ 30%, SIS thermoplastic elastomer (styrene isoprene styrene block copolymer (SIS), be called for short SIS) 0 ~ 20%, olefin copolymer 0 ~ 30%, a tackifying resin 0 ~ 70%, No. two tackifying resins 1 ~ 70%, mineral oil 10 ~ 30%, wax 0 ~ 10%, oxidation inhibitor 0.1 ~ 2%.
Described SBS thermoplastic elastic body styrene content is good 30 ~ 45%.
Described SIS thermoplastic elastic body styrene content is good 15 ~ 40%.
Described olefin copolymer adopt ethene and propylene copolymer or ethene and octene copolymer one or both, such olefin copolymer density range is 0.85 ~ 0.97g/cm з.Described ethene and propylene copolymer have that intensity is high, rigidity is large, good stability of the dimension, good processability, the features such as toughness is splendid, there is the advantage of polyethylene and polypropylene, the Performance Ratio high density polyethylene(HDPE) such as high temperature resistant, hardness is good, low temperature resistant, the Performance Ratio polypropylene such as shock resistance is good; Described ethene and octene have the advantages such as good dispersity, autohension and mutual viscosity are good, good weatherability, the molecular structure of the molecular structure class ceraceous of this kind of olefin copolymer, and solidification is very fast, can provide again good bonding strength simultaneously; Ooze hot melt adhesive integral formula for anti-reflective and play the effect improving curing speed, glue can be avoided to flow thus penetrating substrate, and the anti-reflective that improve hot-fusible pressure-sensitive adhesive oozes effect.
A described tackifying resin adopts natural tackifying resin, comprises rosin, rosin fat, terpenes, polymerization terpenes, styrenated terpene etc., specifically, adopt pentalyn or terpine resin one or both.
Described No. two tackifying resins adopt petroleum resin, comprise C5(carbon five) hydrogenation or non-hydrogenated petroleum resin, C9 (carbon nine) hydrogenation or non-hydrogenated petroleum resin, C 5 modified hydrogenation or non-hydrogenated petroleum resin, carbon nine modification hydrogenation or non-hydrotreated petroleum tree, hydrogenation dicyclopentadiene (DCPD) petroleum resin etc., specifically, adopt dicyclopentadiene (DCPD) petroleum resin of hydrogenation or full hydrogenation C9 petroleum resin one or both, such tackifying resin can improve increasing stickiness and the ageing resistance that anti-reflective oozes hot-fusible pressure-sensitive adhesive greatly.
Described mineral oil comprises naphthenic oil and paraffinic based oil, specifically, adopts naphthenic oil.
Described wax comprises paraffin, Microcrystalline Wax, various synthetic wax, specifically, adopt polyethylene wax or Microcrystalline Wax, described polyethylene wax (PE wax), polyethylene wax is called for short also known as macromolecule wax, be widely used because of its excellent winter hardiness, thermotolerance, chemical resistant properties and wear resistance, can improve the mobility of polyethylene, polypropylene, ABS, polyethylene wax has very strong internal lubrication effect; After the fusing point of Microcrystalline Wax, molecular weight and fusing, viscosity is all high than paraffin.
Described oxidation inhibitor adopts Hinered phenols antioxidant or ultraviolet absorbers.
Beneficial effect of the present invention is: the present invention is by rational formulating of recipe; significantly improve the online perviousness of hot-fusible pressure-sensitive adhesive; reduce strike-through rate; power generating ratio frequency, reduce base material waste, work improves off-line perviousness; the risk of mutual adhesion after controlling finished product off-line packaging; this patent, when promoting the anti-reflective of hot-fusible pressure-sensitive adhesive and oozing performance, does not sacrifice bonding strength, guarantees consistent with ordinary hot fusion pressure sensing structure glue of the initial of structure glue and aging intensity.
Embodiment
Be described principle of the present invention and feature below in conjunction with embodiment, example, only for explaining the present invention, is not intended to limit scope of the present invention.
A kind of anti-reflective oozes hot-fusible pressure-sensitive adhesive, it is characterized in that: by following component by weight formulated: SBS thermoplastic elastomer 0 ~ 30%, SIS thermoplastic elastomer 0 ~ 20%, olefin copolymer 0 ~ 30%, a tackifying resin 0 ~ 70%, No. two tackifying resins 1 ~ 70%, mineral oil 10 ~ 30%, wax 0 ~ 10%, oxidation inhibitor 0.1 ~ 2%.
The concrete material of the feed composition used in the following each embodiment of the present invention is as follows respectively:
Component A:SBS thermoplastic elastomer
A1:D1155J-Ke Teng limited-liability company produces, and linear SBS, wherein styrene content is 40%.
A2:Globalprene 3566-Lee Chang Yung Chemical Indust produces, linear SBS(styrene-butadiene-styrene block copolymer), wherein styrene content is 30%.
B component: SIS thermoplastic elastomer
B1:Vector4411-Tai Xiang Co., Ltd produces, linear SIS(styrene isoprene styrene block copolymer (SIS)), wherein styrene content is 40%.
The SIS that the auspicious father-in-law of B2:Quintac3433-produces, wherein styrene content is 16%.
Component C: olefin copolymer
C1:OBC9817-Tao Shi (DOW) produces, and ethene and octene segmented copolymer, MI is 15g/10min, and density is 0.877g/cm з.
C2:GA1900-Tao Shi (DOW) produces, and ethene and octene copolymer, density is 0.87g/cm з, MI is 1000g/10min.
Component D: number tackifying resin
D1:GA100SC-Huang Chuan chemical industry company limited produces, and pentalyn, softening temperature is about 100C.
D2:KT100-Ke Mao forest chemical limited-liability company produces, and terpine resin, softening temperature is about 100C.
Component E: No. two tackifying resins
E1:Escorez5300-EXXON CHEMICAL produces, and be dicyclopentadiene (DCPD) petroleum resin of hydrogenation, its ring and ball softening point is about 100 DEG C.
The full hydrogenation C9 petroleum resin of E2:FP-125-be Taiwan and benefit chemistry, its ring and ball softening point is about 125 DEG C.
Component F: mineral oil
The naphthenic oil that F1:KN4010-Kelamayi refinery is produced, its viscosity is 140mm2/s at 40 DEG C.
Component G: cerate
The polyethylene wax that G1:A-C 8-Honeywell produces, its melt drop temperature is 113 DEG C.
The Microcrystalline Wax that G2:PMW-ALPHAMIN produces, its melt drop temperature is 85 DEG C.
Component H: oxidation inhibitor
The Hinered phenols antioxidant that H1:Irganox 1010-CIBA produces.
The Hinered phenols antioxidant that H2:Irganox 1076-CIBA produces.The above-mentioned two kinds of oxidation inhibitor of normal conditions with the use of.
Embodiment 1
Take each component according to the weight ratio of correspondence, the aluminium pot that each component puts into temperature controllable is according to the order of sequence heated, is warming up to 170 DEG C, make raw material all melt and stir, pour into after vacuumizing in release silicon carton and cool.
Embodiment 2
Take each component according to the ratio of correspondence, all the other steps are with embodiment 1.
Embodiment 3
Take each component according to the ratio of correspondence, all the other steps are with embodiment 1.
Comparative example 1
For the anti-reflective first had oozes hot melt adhesive, for comparing with embodiment 1 ~ 3.
Comparative example 2
For the hot-fusible pressure-sensitive adhesive formula that tradition is conventional, for comparing with embodiment 1 ~ 3.
Claims (9)
1. an anti-reflective oozes hot-fusible pressure-sensitive adhesive, it is characterized in that: by following component by weight formulated: SBS thermoplastic elastomer (styrene-butadiene-styrene block copolymer, be called for short SBS) 0 ~ 30%, SIS thermoplastic elastomer (styrene isoprene styrene block copolymer (SIS) is called for short SIS) 0 ~ 20%, olefin copolymer 0 ~ 30%, a tackifying resin 0 ~ 70%, No. two tackifying resins 1 ~ 70%, mineral oil 10 ~ 30%, wax 0 ~ 10%, oxidation inhibitor 0.1 ~ 2%.
2. anti-reflective according to claim 1 oozes hot-fusible pressure-sensitive adhesive, it is characterized in that: in described SBS thermoplastic elastomer, styrene content is 30 ~ 45%.
3. anti-reflective according to claim 1 oozes hot-fusible pressure-sensitive adhesive, it is characterized in that: in described SIS thermoplastic elastomer, styrene content is 15 ~ 40%.
4. anti-reflective according to claim 1 oozes hot-fusible pressure-sensitive adhesive, it is characterized in that: described olefin copolymer adopt ethene and propylene copolymer or ethene and octene copolymer one or both, such olefin copolymer density range is 0.85 ~ 0.97g/cm з.
5. anti-reflective according to claim 1 oozes hot-fusible pressure-sensitive adhesive, it is characterized in that: described tackifying resin adopt in rosin, rosin fat, terpenes, polymerization terpenes, styrenated terpene one or both.
6. anti-reflective according to claim 1 oozes hot-fusible pressure-sensitive adhesive, it is characterized in that: described No. two tackifying resins adopt C5(carbon five) hydrogenation or non-hydrogenated petroleum resin, C9 (carbon nine) hydrogenation or non-hydrogenated petroleum resin, C 5 modified hydrogenation or non-hydrogenated petroleum resin, carbon nine modification hydrogenation or non-hydrogenated petroleum resin, hydrogenation dicyclopentadiene (DCPD) petroleum resin in one or more.
7. anti-reflective according to claim 1 oozes hot-fusible pressure-sensitive adhesive, it is characterized in that: described mineral oil adopts naphthenic oil or paraffinic based oil.
8. anti-reflective according to claim 1 oozes hot-fusible pressure-sensitive adhesive, it is characterized in that: described wax adopts polyethylene wax or Microcrystalline Wax.
9. anti-reflective according to claim 1 oozes hot-fusible pressure-sensitive adhesive, it is characterized in that: described oxidation inhibitor adopts Hinered phenols antioxidant or ultraviolet absorbers.
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Cited By (15)
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CN106047287A (en) * | 2016-05-30 | 2016-10-26 | 广东荣嘉新材料科技有限公司 | Low-temperature hot-melt pressure-sensitive adhesive for disposable hygienic product and preparation method thereof |
CN106047239A (en) * | 2016-05-30 | 2016-10-26 | 广东荣嘉新材料科技有限公司 | Wet-strength hot-melt adhesive for disposable hygienic product and preparation method thereof |
CN106085306A (en) * | 2016-08-24 | 2016-11-09 | 泉州市嘉华卫生用品有限公司 | A kind of diaper PUR and preparation method thereof |
CN107652928A (en) * | 2016-07-23 | 2018-02-02 | 广东聚胶粘合剂有限公司 | A kind of high viscous force hot-fusible pressure-sensitive adhesive gum of low spread |
CN108165217A (en) * | 2018-01-23 | 2018-06-15 | 浙江精华科技有限公司 | Paper diaper hot-fusible pressure-sensitive adhesive and its production method |
CN108531115A (en) * | 2018-04-21 | 2018-09-14 | 浙江精华科技有限公司 | A kind of amenities low temperature glue and preparation method thereof |
CN109536091A (en) * | 2018-11-20 | 2019-03-29 | 衢州市富星和宝黏胶工业有限公司 | A kind of urine present gum |
CN110205064A (en) * | 2019-06-06 | 2019-09-06 | 广东聚胶粘合剂有限公司 | A kind of disposable sanitary articles scrape gluing method with impervious hot melt adhesive and coating |
CN110616056A (en) * | 2019-10-16 | 2019-12-27 | 亿铖达(深圳)新材料有限公司 | Hot-melt peelable glue |
CN110699021A (en) * | 2019-10-24 | 2020-01-17 | 江苏嘉好热熔胶股份有限公司 | Special hot-melt pressure-sensitive adhesive for surgical hole towel and preparation method thereof |
CN110819274A (en) * | 2019-10-25 | 2020-02-21 | 上海嘉好胶粘制品有限公司 | Hot melt adhesive for pressure-free ointment and preparation method thereof |
EP3760684A1 (en) | 2019-07-05 | 2021-01-06 | Bostik Sa | Low tack hot-melt pressure sensitive adhesives |
CN115216258A (en) * | 2022-05-13 | 2022-10-21 | 嘉好(太仓)新材料股份有限公司 | Structural adhesive for producing low-temperature-resistant paper diapers and preparation method thereof |
CN115216260A (en) * | 2022-08-26 | 2022-10-21 | 江苏鸿泰锦新材料有限公司 | Environment-friendly strongly-adhesive hot melt adhesive for SPC floor mute mat and preparation method thereof |
CN115820174A (en) * | 2022-10-17 | 2023-03-21 | 嘉好(太仓)新材料股份有限公司 | Special hot-melt pressure-sensitive adhesive for destroying adhesive tape and application of adhesive tape |
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CN103562332A (en) * | 2011-04-08 | 2014-02-05 | 波士胶公司 | Polyolefin based hot melt adhesive containing a solid plasticizer |
CN103946332A (en) * | 2011-11-22 | 2014-07-23 | 汉高股份有限及两合公司 | Psa containing olefin block copolymers and styrene block copolymer |
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CN106047287A (en) * | 2016-05-30 | 2016-10-26 | 广东荣嘉新材料科技有限公司 | Low-temperature hot-melt pressure-sensitive adhesive for disposable hygienic product and preparation method thereof |
CN106047239A (en) * | 2016-05-30 | 2016-10-26 | 广东荣嘉新材料科技有限公司 | Wet-strength hot-melt adhesive for disposable hygienic product and preparation method thereof |
CN106047287B (en) * | 2016-05-30 | 2018-04-10 | 广东荣嘉新材料科技有限公司 | Disposable sanitary articles Low Temperature Hot-Melt Pressure Sensitive and preparation method thereof |
CN107652928A (en) * | 2016-07-23 | 2018-02-02 | 广东聚胶粘合剂有限公司 | A kind of high viscous force hot-fusible pressure-sensitive adhesive gum of low spread |
CN106085306A (en) * | 2016-08-24 | 2016-11-09 | 泉州市嘉华卫生用品有限公司 | A kind of diaper PUR and preparation method thereof |
CN108165217A (en) * | 2018-01-23 | 2018-06-15 | 浙江精华科技有限公司 | Paper diaper hot-fusible pressure-sensitive adhesive and its production method |
CN108531115A (en) * | 2018-04-21 | 2018-09-14 | 浙江精华科技有限公司 | A kind of amenities low temperature glue and preparation method thereof |
CN109536091A (en) * | 2018-11-20 | 2019-03-29 | 衢州市富星和宝黏胶工业有限公司 | A kind of urine present gum |
CN110205064B (en) * | 2019-06-06 | 2021-07-06 | 广东聚胶粘合剂有限公司 | Impervious hot melt adhesive for disposable hygienic product and coating and frictioning method |
CN110205064A (en) * | 2019-06-06 | 2019-09-06 | 广东聚胶粘合剂有限公司 | A kind of disposable sanitary articles scrape gluing method with impervious hot melt adhesive and coating |
EP3760684A1 (en) | 2019-07-05 | 2021-01-06 | Bostik Sa | Low tack hot-melt pressure sensitive adhesives |
WO2021004870A1 (en) | 2019-07-05 | 2021-01-14 | Bostik Sa | Low tack hot-melt pressure sensitive adhesives |
CN110616056A (en) * | 2019-10-16 | 2019-12-27 | 亿铖达(深圳)新材料有限公司 | Hot-melt peelable glue |
CN110616056B (en) * | 2019-10-16 | 2021-05-04 | 亿铖达(深圳)新材料有限公司 | Hot-melt peelable glue |
CN110699021A (en) * | 2019-10-24 | 2020-01-17 | 江苏嘉好热熔胶股份有限公司 | Special hot-melt pressure-sensitive adhesive for surgical hole towel and preparation method thereof |
CN110819274A (en) * | 2019-10-25 | 2020-02-21 | 上海嘉好胶粘制品有限公司 | Hot melt adhesive for pressure-free ointment and preparation method thereof |
CN110819274B (en) * | 2019-10-25 | 2021-07-16 | 上海嘉好胶粘制品有限公司 | Hot melt adhesive for pressure-free ointment and preparation method thereof |
CN115216258A (en) * | 2022-05-13 | 2022-10-21 | 嘉好(太仓)新材料股份有限公司 | Structural adhesive for producing low-temperature-resistant paper diapers and preparation method thereof |
CN115216258B (en) * | 2022-05-13 | 2023-06-20 | 嘉好(太仓)新材料股份有限公司 | Structural adhesive for producing low-temperature-resistant paper diapers and preparation method thereof |
CN115216260A (en) * | 2022-08-26 | 2022-10-21 | 江苏鸿泰锦新材料有限公司 | Environment-friendly strongly-adhesive hot melt adhesive for SPC floor mute mat and preparation method thereof |
CN115216260B (en) * | 2022-08-26 | 2024-03-19 | 江苏鸿泰锦新材料有限公司 | Environment-friendly strong-adhesion hot melt adhesive for SPC floor silence pad and preparation method thereof |
CN115820174A (en) * | 2022-10-17 | 2023-03-21 | 嘉好(太仓)新材料股份有限公司 | Special hot-melt pressure-sensitive adhesive for destroying adhesive tape and application of adhesive tape |
CN115820174B (en) * | 2022-10-17 | 2024-05-28 | 嘉好(太仓)新材料股份有限公司 | Hot-melt pressure-sensitive adhesive special for destroying adhesive tape and application of adhesive tape |
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