CN104877756A - Rapeseed peeling method used for making oil through cold pressing - Google Patents

Rapeseed peeling method used for making oil through cold pressing Download PDF

Info

Publication number
CN104877756A
CN104877756A CN201510273235.2A CN201510273235A CN104877756A CN 104877756 A CN104877756 A CN 104877756A CN 201510273235 A CN201510273235 A CN 201510273235A CN 104877756 A CN104877756 A CN 104877756A
Authority
CN
China
Prior art keywords
rapeseed
peeling
hull
decorticate
brassicae campestris
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201510273235.2A
Other languages
Chinese (zh)
Other versions
CN104877756B (en
Inventor
吴学凤
姜绍通
罗水忠
潘丽军
郑志
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hefei University of Technology
Original Assignee
Hefei University of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hefei University of Technology filed Critical Hefei University of Technology
Priority to CN201510273235.2A priority Critical patent/CN104877756B/en
Publication of CN104877756A publication Critical patent/CN104877756A/en
Application granted granted Critical
Publication of CN104877756B publication Critical patent/CN104877756B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Fats And Perfumes (AREA)

Abstract

The invention provides a rapeseed peeling method for making oil through cold pressing and belongs to front-end procedures in a rapeseed oil making method. The rapeseed peeling method provided by the invention comprises the following steps: (1), rapeseed pre-processing, (2), microwave pre-processing, (3), crushing and peeling; (4) hull and kernel separating, (5), color sorting and peeling, and (6), oil making through cold pressing. The process is relatively simple, the investment is less, the microwave pre-processing is conducive to rapeseed crushing and peeling, hull and kernel adhesion is effectively reduced after crushing, moreover, a drying effect is played, the rapeseed peeling rate can reach 95 percent or above, and the shelling rate and the color sorting rate are both higher than 95 percent. Low temperature pressed crude oil obtained through low temperature pressing to the rapeseed kernel obtained after microwave treatment is light in color, more reasonable in nutrient substance composition, can be high-quality rapreseed oil without need of complex refining process, and meets the requirements of current consumers to green and healthy oil.

Description

A kind of rapeseed peeling method for cold pressing oil
Technical field
The invention belongs to food processing and production technical field, specifically a kind of method removing rapeseed hull.
Background technology
Rape is one of the most important oil crops of China and cash crop, and Annual planting area and ultimate production all occupy first place in the world.In domestic vegetables oil, about 50% derives from Semen Brassicae campestris.In study on rapeseed oil production, traditional oil-producing technique mainly contains once directly squeezing process, pre-squeezings-extract technology and direct leaching process, and modern oil-producing technique mainly refers to extract technology and low-temperature cold pressing technique etc. after employing expelling-expansion pretreatment.Wherein rapeseed peeling cold pressing oil is the New Processing that development in recent years is got up, and this technology can significantly improve the quality of grease and the utility value of grouts.Compared with hot moulding, although cold pressing oil oil yield is on the low side, cold press rapeseed oil has obvious Semen Lactucae sativae local flavor, but because Semen Brassicae campestris steams stir-fry process without high temperature before cold pressing oil, decrease the destruction to protein, Available Amino Acids, avoid high temperature process grease and produce the objectionable impurities such as trans fatty acid, oil polymers, remain the physiologically active substance in oil to greatest extent, as benefit materials such as vitamin-E, sterol, gamma-linolenic acid and functional foodstuff pigments.At present, along with people are to the attention of green health edible oil, increasing human consumer starts to favor in low-temperature cold pressing rapeseed oil.
Vegetable seed seed coat accounts for 12% ~ 19% of full seed, containing a small amount of grease and protein, mainly robust fibre in seed coat.In addition, the antinutritional factor such as most pigments, tannin, sinapic acid choline ester, phytic acid in Semen Brassicae campestris is also present in seed coat.Due to the existence of seed coat, the rapeseed oil color and luster of squeezing of not peeling is comparatively dark, mouthfeel is poor and containing some antinutritional factor, had a strong impact on the quality of rapeseed oil.After rapeseed peeling, not only material oleaginousness significantly rises, rapeseed oil quality also be improved significantly.More to rapeseed peeling low-temperature cold pressing technical study at present; (red legend is prosperous for grade as prosperous in red legend; Hu Qunliang; Xiang Hai; Jin Suying. the research and apply [J] of the direct cold pressing oil technique of Semen Brassicae campestris. Chinese oil, 2005,30 (3): 16-18.) the direct cold pressing oil technique of Semen Brassicae campestris carried out studying find that cold pressing oil can retain effective constituent in rapeseed oil effectively; decrease the discharge of refining sewage, be conducive to environment protection.Liu Changsheng (Liu Changsheng. cold press rapeseed oil low-temperature refining technology and quality characteristic research [D] thereof. Scientia Agricultura Sinica research institute, Xi'an, 2012) more detailed research has been carried out to the low temperature Scouring Technology of cold press rapeseed oil and quality characteristic thereof, have developed a kind of low temperature clean appropriateness refining techniques being suitable for low-temperature cold pressing rapeseed oil.(the Zhou Qi such as Zhou Qi, Yang Mei, Huang Fenghong, Zheng Chang, Liu Changsheng. microwave and decortication process vegetable seed are on the impact [J] of activeconstituents in oil. Chinese oil crops journal, 2011,33 (5): 507-512.) the cold pressing oil quality that high, medium and low erucic acid and sulfo-content vegetable seed are raw material is analyzed, to find after microwave that in oil, vitamin-E and content of phytosterol are the highest, and low erucic acid low-sulfur is for the vegetable seed quality being improved oil by microwave treatment preferably.Microwave may be used for processing Semen Brassicae campestris as can be seen here, but not yet finds with the method for microwave-assisted rapeseed peeling.Rapeseed peeling oil-producing technique has become a kind of new trend of rapeseed processing industry, and the research report for rapeseed peeling low temperature oil expression technology is a lot, but rarely seen specifically for the report improving rapeseed peeling rate; According to investigation, the rapeseed peeling rate of prior art is less than 80%.
Summary of the invention
In order to improve the quality of low-temperature cold pressing rapeseed oil, improving rapeseed peeling rate, the invention provides a kind of rapeseed peeling method for cold pressing oil.
A kind of rapeseed peeling method for cold pressing oil comprises following operation steps: the peeling rate of (1) Semen Brassicae campestris pre-treatment, (2) Microwave Pretreatment, (3) broken decortication, (4) separation of hull and kernel, (5) look choosing peeling Semen Brassicae campestris is greater than 95%.
Concrete operation step is as follows:
(1) Semen Brassicae campestris pre-treatment
Adopt angle shell, leaf, silt and flat seed in screening and selection by winnowing combined techniques removing raw material, obtain pre-treatment Semen Brassicae campestris;
(2) microwave treatment
By pre-treatment Semen Brassicae campestris microwave treatment, obtain microwave Semen Brassicae campestris;
(3) broken decortication
Microwave Semen Brassicae campestris joined in rape-seed hull removing machine and carry out the broken decortication of stone roller stranding, obtain broken rapeseed decorticate, peeling rate is 95% ~ 98%; Described peeling rate is the per-cent that the quality of separation of hull and kernel accounts for total vegetable seed quality;
(4) separation of hull and kernel
Successively being transferred in winnowing machine and sifting machine by broken rapeseed decorticate makes rapeseed hull be separated with rape seed, and obtain rapeseed decorticate benevolence, peeling rate is 90% ~ 95%; Described rapeseed decorticate benevolence comprises rape seed, rapeseed hull, non-rapeseed decorticate, broken rapeseed hull benevolence adhesion body; Described peeling rate is the per-cent that the quality isolating skin accounts for the total vegetable seed cortex amount of broken decortication;
(5) look choosing peeling
By described rapeseed decorticate benevolence further across color selector selected removal Semen Brassicae campestris scurf, obtain rape seed, look selects rate to be 95% ~ 98%; Described look select rate be obtain after look choosing skin, skin benevolence adhesion body, non-rapeseed decorticate quality sum to account for before look choosing the per-cent of the quality sum of skin, skin benevolence adhesion body, non-rapeseed decorticate in total rapeseed dehulled after separation of hull and kernel.
Microwave treatment conditions in described step (2): power 800 ~ 1000W, time 1 ~ 3min.
advantageous Effects of the present invention embodies in the following areas:
(1) the present invention first by microwave technique application in rapeseed peeling early stage pretreatment process, improve rapeseed peeling rate, improve microwave by for Semen Brassicae campestris structure deteriorate own on the one hand, especially the original structure of vegetable seed skin has been damaged, be beneficial to vegetable seed broken decortication in roller crusher, effectively improve peeling rate; Microwave makes some moisture in Semen Brassicae campestris cot capillary pipe structure flow out cell surface on the other hand, in fragmentation decortication, decrease the adhesion of skin benevolence, be beneficial to later stage separation of hull and kernel, microwave also has dry effect simultaneously, within a short period of time is dry by Semen Brassicae campestris, is beneficial to later stage rapeseed crushing decortication; In addition, the low temperature pressing crude oil lighter color that the rape seed that microwave treatment obtains obtains through low temperature pressing, composition of nutritive substance are more reasonable, do not need complicated refinery practice namely to can be high-quality rapeseed oil, meet the demand of current consumer to green health oil;
(2) processing condition of the present invention are gentle, drying process is replaced with Microwave Pretreatment by original Semen Brassicae campestris cold press milling process basis and operates, without the need to carrying out operation transformation on a large scale.
Embodiment
The invention belongs to the former process in Semen Brassicae campestris method of making oil.Below by embodiment, the present invention is described in further detail.
The explanation in the raw materials used source of following examples:
Blue or green excellent No. 10 Semen Brassicae campestris, are purchased from grease company limited of Shouxian County, Anhui Province Far Glory.
Embodiment 1:
Microwave-assisted rapeseed peeling operation steps for cold pressing oil is as follows:
(1) Semen Brassicae campestris pre-treatment
Adopt the large small impurities such as angle shell, leaf, silt and flat seed in screening and selection by winnowing combined techniques removing raw material, obtain pre-treatment Semen Brassicae campestris.
(2) microwave treatment
By pre-treatment Semen Brassicae campestris microwave treatment, microwave treatment conditions: power 1000W, time 1min, obtain microwave Semen Brassicae campestris.
(3) broken decortication
Microwave Semen Brassicae campestris joined in rape-seed hull removing machine and carry out the broken decortication of stone roller stranding, obtain broken rapeseed decorticate, peeling rate is 95%; Peeling rate is the per-cent that the quality of separation of hull and kernel accounts for total vegetable seed quality.
(4) separation of hull and kernel
Successively being transferred in winnowing machine and sifting machine by broken rapeseed decorticate makes rapeseed hull be separated with rape seed, and obtain rapeseed decorticate benevolence, peeling rate is 90%; Described rapeseed decorticate benevolence comprises rape seed, rapeseed hull, non-rapeseed decorticate, broken rapeseed hull benevolence adhesion body; Peeling rate is the per-cent that the quality isolating skin accounts for the total vegetable seed cortex amount of broken decortication.
(5) look choosing peeling
By rapeseed decorticate benevolence further across color selector selected removal Semen Brassicae campestris scurf etc., obtain rape seed, look selects rate to be 95%; Look select rate be obtain after look choosing skin, skin benevolence adhesion body, non-rapeseed decorticate quality sum to account for before look choosing the per-cent of the quality sum of skin, skin benevolence adhesion body, non-rapeseed decorticate in total rapeseed dehulled after separation of hull and kernel.
Embodiment 2:
Microwave-assisted rapeseed peeling operation steps for cold pressing oil is as follows:
(1) Semen Brassicae campestris pre-treatment
Adopt the large small impurities such as angle shell, leaf, silt and flat seed in screening and selection by winnowing combined techniques removing raw material, obtain pre-treatment Semen Brassicae campestris.
(2) microwave treatment
By pre-treatment Semen Brassicae campestris microwave treatment, microwave treatment conditions: power 900W, time 2min, obtain microwave Semen Brassicae campestris.
(3) broken decortication
Microwave Semen Brassicae campestris joined in rape-seed hull removing machine and carry out the broken decortication of stone roller stranding, obtain broken rapeseed decorticate, peeling rate is 97%.
(4) separation of hull and kernel
Successively being transferred in winnowing machine and sifting machine by broken rapeseed decorticate makes rapeseed hull be separated with rape seed, and obtain rapeseed decorticate benevolence, peeling rate is 93%.
(5) look choosing peeling
By the rapeseed decorticate benevolence that obtains after winnowing machine and sifting machine separation of hull and kernel further across color selector selected removal Semen Brassicae campestris scurf etc., obtain rape seed, look selects rate to be 96%.
Embodiment 3:
Microwave-assisted rapeseed peeling operation steps for cold pressing oil is as follows:
(1) Semen Brassicae campestris pre-treatment
Adopt the large small impurities such as angle shell, leaf, silt and flat seed in screening and selection by winnowing combined techniques removing raw material, obtain pre-treatment Semen Brassicae campestris.
(2) microwave treatment
By pre-treatment Semen Brassicae campestris microwave treatment, microwave treatment conditions: power 800W, time 3min, obtain microwave Semen Brassicae campestris.
(3) broken decortication
Microwave Semen Brassicae campestris joined in rape-seed hull removing machine and carry out the broken decortication of stone roller stranding, obtain broken rapeseed decorticate, peeling rate is 98%.
(4) separation of hull and kernel
Successively being transferred in winnowing machine and sifting machine by broken rapeseed decorticate makes rapeseed hull be separated with rape seed, and obtain rapeseed decorticate benevolence, peeling rate is 95%.
(5) look choosing peeling
By the rapeseed decorticate benevolence that obtains after winnowing machine and sifting machine separation of hull and kernel further across color selector selected removal Semen Brassicae campestris scurf etc., obtain rape seed, look selects rate to be 98%.

Claims (3)

1. for a rapeseed peeling method for cold pressing oil, it is characterized in that comprising following operation steps: the peeling rate of (1) Semen Brassicae campestris pre-treatment, (2) Microwave Pretreatment, (3) broken decortication, (4) separation of hull and kernel, (5) look choosing peeling Semen Brassicae campestris is greater than 95%.
2. a kind of rapeseed peeling method for cold pressing oil according to claim 1, is characterized in that concrete operation step is as follows:
(1) Semen Brassicae campestris pre-treatment
Adopt angle shell, leaf, silt and flat seed in screening and selection by winnowing combined techniques removing raw material, obtain pre-treatment Semen Brassicae campestris;
(2) microwave treatment
By pre-treatment Semen Brassicae campestris microwave treatment, obtain microwave Semen Brassicae campestris;
(3) broken decortication
Microwave Semen Brassicae campestris joined in rape-seed hull removing machine and carry out the broken decortication of stone roller stranding, obtain broken rapeseed decorticate, peeling rate is 95% ~ 98%; Described peeling rate is the per-cent that the quality of separation of hull and kernel accounts for total vegetable seed quality;
(4) separation of hull and kernel
Successively being transferred in winnowing machine and sifting machine by broken rapeseed decorticate makes rapeseed hull be separated with rape seed, and obtain rapeseed decorticate benevolence, peeling rate is 90% ~ 95%; Described rapeseed decorticate benevolence comprises rape seed, rapeseed hull, non-rapeseed decorticate, broken rapeseed hull benevolence adhesion body; Described peeling rate is the per-cent that the quality isolating skin accounts for the total vegetable seed cortex amount of broken decortication;
(5) look choosing peeling
By described rapeseed decorticate benevolence further across color selector selected removal Semen Brassicae campestris scurf, obtain rape seed, look selects rate to be 95% ~ 98%; Described look select rate be obtain after look choosing skin, skin benevolence adhesion body, non-rapeseed decorticate quality sum to account for before look choosing the per-cent of the quality sum of skin, skin benevolence adhesion body, non-rapeseed decorticate in total rapeseed dehulled after separation of hull and kernel.
3. a kind of rapeseed peeling method for cold pressing oil according to claim 2, is characterized in that: the microwave treatment conditions in described step (2): power 800 ~ 1000W, time 1 ~ 3min.
CN201510273235.2A 2015-05-26 2015-05-26 A kind of rapeseed peeling method for cold pressing oil Active CN104877756B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510273235.2A CN104877756B (en) 2015-05-26 2015-05-26 A kind of rapeseed peeling method for cold pressing oil

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510273235.2A CN104877756B (en) 2015-05-26 2015-05-26 A kind of rapeseed peeling method for cold pressing oil

Publications (2)

Publication Number Publication Date
CN104877756A true CN104877756A (en) 2015-09-02
CN104877756B CN104877756B (en) 2018-08-28

Family

ID=53945437

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510273235.2A Active CN104877756B (en) 2015-05-26 2015-05-26 A kind of rapeseed peeling method for cold pressing oil

Country Status (1)

Country Link
CN (1) CN104877756B (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107312623A (en) * 2017-07-19 2017-11-03 望谟县布依王油脂有限公司 A kind of processing method of the direct cold pressing oil of rapeseed
CN107557147A (en) * 2017-10-24 2018-01-09 中国农业科学院油料作物研究所 A kind of extracting method of fruit-like flavour rapeseed oil
CN108903005A (en) * 2018-05-31 2018-11-30 镇江虎瑞生物科技有限公司 A kind of technique that microwave method carries out soybean peeling and enzyme deactivation
CN109123690A (en) * 2018-06-26 2019-01-04 安徽山美生物科技有限公司 A method of tea shell is separated from tea seed
CN109652199A (en) * 2019-02-28 2019-04-19 湖南银华百隆现代农业发展有限公司 Processing method of aromatic rapeseed oil
CN110226729A (en) * 2019-07-19 2019-09-13 江西省农业科学院农产品质量安全与标准研究所 A kind of peeling sesame method
CN110628500A (en) * 2019-09-24 2019-12-31 湖南省义丰祥实业有限公司 Preparation method of high-oleic-acid nutritional health-care rapeseed oil
CN111019756A (en) * 2019-12-20 2020-04-17 仲恺农业工程学院 Industrial production and processing method of camellia seeds
CN111387301A (en) * 2020-04-21 2020-07-10 四川妈妈家农业开发有限公司 Preparation method of plateau rapeseed oil suitable for children to eat

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1597890A (en) * 2004-08-23 2005-03-23 隋利华 Process for extracting peanut oil and producing peanut protein and products thereof
CN101911983A (en) * 2010-07-13 2010-12-15 中国农业科学院油料作物研究所 Method for pre-treating oil crop seeds by using microwave
CN102942988A (en) * 2012-11-21 2013-02-27 安徽宏实光机电高科有限公司 Process for manufacturing oil by cold-squeezing of rape seeds
CN104293480A (en) * 2014-10-14 2015-01-21 合肥工业大学 Rapeseed peeling method suitable for cold pressing oil preparation

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1597890A (en) * 2004-08-23 2005-03-23 隋利华 Process for extracting peanut oil and producing peanut protein and products thereof
CN101911983A (en) * 2010-07-13 2010-12-15 中国农业科学院油料作物研究所 Method for pre-treating oil crop seeds by using microwave
CN102942988A (en) * 2012-11-21 2013-02-27 安徽宏实光机电高科有限公司 Process for manufacturing oil by cold-squeezing of rape seeds
CN104293480A (en) * 2014-10-14 2015-01-21 合肥工业大学 Rapeseed peeling method suitable for cold pressing oil preparation

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
倪培德主编: "《油脂加工技术》", 30 June 2007, 化学工业出版社 *
胡健华等: "油菜籽脱皮冷榨技术研究", 《中国油脂》 *
黄凤洪等: "油菜籽脱皮与加工利用", 《中国油脂》 *

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107312623A (en) * 2017-07-19 2017-11-03 望谟县布依王油脂有限公司 A kind of processing method of the direct cold pressing oil of rapeseed
CN107557147A (en) * 2017-10-24 2018-01-09 中国农业科学院油料作物研究所 A kind of extracting method of fruit-like flavour rapeseed oil
CN107557147B (en) * 2017-10-24 2021-04-02 中国农业科学院油料作物研究所 Extraction method of fruit-flavor rapeseed oil
CN108903005A (en) * 2018-05-31 2018-11-30 镇江虎瑞生物科技有限公司 A kind of technique that microwave method carries out soybean peeling and enzyme deactivation
CN109123690A (en) * 2018-06-26 2019-01-04 安徽山美生物科技有限公司 A method of tea shell is separated from tea seed
CN109652199A (en) * 2019-02-28 2019-04-19 湖南银华百隆现代农业发展有限公司 Processing method of aromatic rapeseed oil
CN109652199B (en) * 2019-02-28 2022-05-13 湖南银华百隆现代农业发展有限公司 Processing method of aromatic rapeseed oil
CN110226729A (en) * 2019-07-19 2019-09-13 江西省农业科学院农产品质量安全与标准研究所 A kind of peeling sesame method
CN110628500A (en) * 2019-09-24 2019-12-31 湖南省义丰祥实业有限公司 Preparation method of high-oleic-acid nutritional health-care rapeseed oil
CN111019756A (en) * 2019-12-20 2020-04-17 仲恺农业工程学院 Industrial production and processing method of camellia seeds
CN111387301A (en) * 2020-04-21 2020-07-10 四川妈妈家农业开发有限公司 Preparation method of plateau rapeseed oil suitable for children to eat

Also Published As

Publication number Publication date
CN104877756B (en) 2018-08-28

Similar Documents

Publication Publication Date Title
CN104877756A (en) Rapeseed peeling method used for making oil through cold pressing
CN104293480A (en) Rapeseed peeling method suitable for cold pressing oil preparation
CN105794995A (en) Technology for preparing Suanjiang tofu from LAB (lactic acid bacteria) fermented yellow serofluid
CN101851551A (en) Method for preparing cooking oil by taking tea seeds as raw material
CN107129859A (en) A kind of processing method for improving the fresh oil cut rate of squeezing out of olive
CN105602700A (en) Preparation method of cold-pressed peony seed oil with high oil yield
CN101297689A (en) Pure natural edible fresh chili oil and preparation thereof
CN107488499A (en) A kind of cold press tea-seed oil method
CN104473300B (en) A kind of Fructus anacardii shell breaking method
CN111548852A (en) Fresh-pressing manufacturing process of zanthoxylum oil
CN107043649B (en) Method for preparing camellia seed oil by near-solid enzymolysis combined with physical squeezing
CN104560370A (en) Preparation method of original ecological tea seed oil
CN103710138A (en) Decaisnea insignis seed oil extraction method
CN105132141A (en) Method for preparing prickly ash seed oil through mechanical compression
CN107904000B (en) Processing method of high-stability flavor type kenaf seed oil
CN105950281A (en) Extraction process of trichosanthes kirilowii seed oil
CN106833877A (en) A kind of colding pressing squeezes the method that combining ultrasonic ripple method extracts linseed oil
CN109593600A (en) A kind of cold press peanut oil process equipment and its method
CN102199487A (en) Method for producing virgin cold pressed Trichosanthes kirilowii Maxim seed oil
CN105802723B (en) A kind of preparation method of giving off a strong fragrance camellia seed oil
CN104194919A (en) Asparagus seed oil and preparation method thereof
CN105670767A (en) Method using camellia oleifera seed cake for oil expression
CN105542944A (en) Refining method of snakegourd seed oil
CN104745289A (en) Method and system for extracting part of crude oil from high-oil-content nut jam mud
CN110029012A (en) A kind of high-purity chufa root oil and its extracting method

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
EXSB Decision made by sipo to initiate substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant