CN104833765B - Pendency thin layer chromatograph - Google Patents
Pendency thin layer chromatograph Download PDFInfo
- Publication number
- CN104833765B CN104833765B CN201510255140.8A CN201510255140A CN104833765B CN 104833765 B CN104833765 B CN 104833765B CN 201510255140 A CN201510255140 A CN 201510255140A CN 104833765 B CN104833765 B CN 104833765B
- Authority
- CN
- China
- Prior art keywords
- control
- casing
- wet
- folder block
- grid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Investigating Or Analysing Materials By Optical Means (AREA)
Abstract
The invention discloses a kind of pendency thin layer chromatograph, a kind of can be to TLC separation, analysis, the device of imaging, the thin layer chromatograph that dangles includes: casing, cluster illumination lamps, camera head, the wet device of control and pendency constant-current device；Casing bottom is provided with several footing, casing front end is respectively equipped with several D/C power plug and three-position switch side by side, is provided with battery carrier in it, is equipped with battery in battery carrier, battery carrier front end is equipped with time panel, casing upper end is equipped with base plate, and base plate rear end bolt connects four groove columns, and front terminal bolt connects two cluster illumination lamps, it is provided with groove seat in the middle of four groove columns, it is equipped with control wet sump in groove seat, in control wet sump, is equipped with the wet grid of control, control upper end, wet grid side and be equipped with shifting grid rod；Terminal bolt cross structure press strip, N-shaped bridge and developing tank on described groove column, developing tank side bolt connects main folder block pin location, and chromatoplate is positioned on the inner side of N-shaped bridge, main folder block and sub-folder block and is clamped the nut fastening outside by sub-folder block.
Description
Technical field
The present invention relates to a kind of pendency thin layer chromatograph, a kind of can be to TLC separation, analysis, the device of imaging.
Background technology
Thin layer chromatography is conventional separating organic matters method, and developing solvent is flowed by vertical, moves on to outside chromatography cylinder by chromatoplate when developing solvent line reaches the top, under multi-wavelength excites, and the amount of the light speckle that detection is launched and chemical constitution.Chromatoplate can not chromatograph after moving on to outside chromatography cylinder the most in the same direction, because developing solvent is slow by the portable cord speed of this flowing phase of vertical upstream reason, when developing solvent line reaches the top, developer flow prompt drop is low, and Tomography Velocity is non-constant, separating degree reduces, it is impossible to continue to separate the component of long retention time.Continue the longer chromatography time and raising developing solvent flow velocity obtains the key problem that high separation is chromatography, in order to reach satisfied separating degree and meet the optimum flow rate of Fan Shi equation, it is necessary that design have the shooting thin layer chromatograph of pendency constant current function to monitor analysis layer state in real time.
Summary of the invention
In order to overcome above-mentioned deficiency, the present invention provide a kind of thin layer chromatography pendency can be separated, analyzes, pendency thin layer chromatograph that imaging is carried out simultaneously.
The technical solution adopted for the present invention to solve the technical problems is: pendency thin layer chromatograph includes: casing, cluster illumination lamps, camera head, control wet device and pendency constant-current device, its structure is: casing bottom is provided with several footing, casing front end is respectively equipped with several D/C power plug and three-position switch side by side, battery carrier it is provided with in it, battery it is equipped with in battery carrier, battery carrier front end is equipped with time panel, casing upper end is equipped with base plate, base plate rear end bolt connects four groove columns, front terminal bolt connects two cluster illumination lamps, it is provided with groove seat in the middle of four groove columns, control wet sump it is equipped with in groove seat, the wet grid of control it are equipped with in control wet sump, control upper end, wet grid side and be equipped with shifting grid rod；Terminal bolt cross structure press strip, N-shaped bridge and developing tank on described groove column, developing tank side bolt connects main folder block pin location, and chromatoplate is positioned on the inner side of N-shaped bridge, main folder block and sub-folder block and is clamped the nut fastening outside by sub-folder block；Being provided with ultraviolet lamp socket in described cluster illumination lamps, 254nm lamp, 365nm mercury lamp are separately fixed on ultraviolet lamp socket, and LED is located at the upper end of lamp bracket；Outer housing is cuboid, and its front end is provided with through hole, and through hole is equipped with quartz window, and quartz window is arranged on through hole by pressure ring；Described outer housing is that glass is made, and the wet grid of described control, N-shaped bridge are that 2000 mesh quartz screen plates are made, and described control wet sump, shifting grid rod, developing tank are that politef is made.
The invention has the beneficial effects as follows: pendency constant current assembly by developing solvent from developing tank siphon to N-shaped bridge, developing solvent from N-shaped bridge siphon to chromatoplate, it is achieved that the pendency constant current of developing solvent, the flow velocity of developing solvent is accelerated, is improve the development rate of component.Chromatoplate can be with Reusability, and simple in construction is easy to use.
Accompanying drawing explanation
The present invention is further described with detailed description of the invention below in conjunction with the accompanying drawings.
Fig. 1 is constant current thin layer chromatograph structural representation of the present invention.
Fig. 2 is constant current thin layer chromatograph exploded view of the present invention.
In figure 1, D/C power plug, 2, three-position switch, 3, casing, 4, quartz window, 5, cluster illumination lamps, 6, outer housing, 7, sub-folder block, 8, N-shaped bridge, 9, bridge press strip, 10, groove column, 11, control wet grid, 12, move grid rod, 13, control wet sump, 14, base plate, 15, battery carrier, 16, time panel, 17, footing, 18, groove seat, 19, chromatoplate, 20, main folder block, 21, developing tank.
Detailed description of the invention
As Figure 1-Figure 2, pendency thin layer chromatograph includes: casing, cluster illumination lamps, camera head, control wet device and pendency constant-current device, its structure is: casing 3 bottom is provided with several footing 17, casing 3 front end is respectively equipped with several D/C power plug 1 and three-position switch 2 side by side, battery carrier 15 it is provided with in it, it is equipped with battery in battery carrier 15, battery carrier 15 front end is equipped with time panel 16, casing 3 upper end is equipped with base plate 14, after base plate 14, terminal bolt connects four groove columns 10, front terminal bolt connects two cluster illumination lamps 5, it is provided with groove seat 18 in the middle of four groove columns 10, control wet sump 13 it is equipped with in groove seat 18, the wet grid 11 of control it are equipped with in control wet sump 13, control upper end, wet grid 11 side and be equipped with shifting grid rod 12；Terminal bolt cross structure press strip 9, N-shaped bridge 8 and developing tank 21 on described groove column, developing tank 21 side bolt connects main folder block 20 pin location, and chromatoplate 19 is positioned on the inner side of N-shaped bridge 8, main folder block 20 and sub-folder block 7 and is clamped the nut fastening outside by sub-folder block 7；Being provided with ultraviolet lamp socket in described cluster illumination lamps 5,254nm lamp, 365nm mercury lamp are separately fixed on ultraviolet lamp socket, and LED is located at the upper end of lamp bracket；Outer housing 6 is cuboid, and its front end is provided with through hole, and through hole is equipped with quartz window 4, and quartz window 4 is arranged on through hole by pressure ring；Described outer housing 6 is made for glass, and the wet grid of described control 11, N-shaped bridge 8 are that 2000 mesh quartz screen plates are made, and described control wet sump 13, shifting grid rod 12, developing tank 21 are made for politef.
Each lamp is controlled by time panel 16, images when lamp is bright；It is spaced at preset timed intervals and under the exciting of 254nm, 365nm and LED visible light, the Organic substance speckle separated is imaged respectively.No. 1 three-position switch controls 254nm illuminator, and No. 2 three-position switches control 365nm illuminator, and No. 3 three-position switches control LED light source lamp, and No. 4 three-position switches control the timing sequence luminescence of three kinds of lamps；For detecting the segregation phenomenon of lamellae under dynamically chromatography in real time, three-position switch connects utilizing camera interface, photographic head shooting obtain result and import computer monitor through data wire.The Organic substance speckle separated images, and can transmit and carry out chart adding analysis to the terminal such as microcomputer or mobile phone.After duration of run t1, the 1st speckle, close to solvent front, images picture 1；After duration of run t2, front 1 speckle disappears in constant current block, images picture 2；After duration of run t3, front 2 speckles disappear in constant current block, image picture 3；After duration of run tn, front n speckle disappears in constant current block, images picture n.The relation of picture 1 to picture n available chromatography spectrogram EXPANSION EQUATION FOR STEEL formula is overlapped, and obtains the spectrogram of whole speckle.
Claims (1)
- null1. a pendency thin layer chromatograph，Including: casing、Cluster illumination lamps、Camera head、Control wet device and pendency constant-current device，It is characterized in that: its structure is: casing (3) bottom is provided with several footing (17)，Casing (3) front end is respectively equipped with several D/C power plug (1) and three-position switch (2) side by side，Battery carrier (15) it is provided with in it，Battery carrier is equipped with battery in (15)，Battery carrier (15) front end is equipped with time panel (16)，Casing (3) upper end is equipped with base plate (14)，Base plate (14) terminal bolt afterwards connects four groove columns (10)，Front terminal bolt connects two cluster illumination lamps (5)，It is provided with groove seat (18) in the middle of four groove columns (10)，Control wet sump (13) it is equipped with in groove seat (18)，The wet grid of control (11) it is equipped with in control wet sump (13)，Control wet grid (11) upper end, side and be equipped with shifting grid rod (12)；Terminal bolt cross structure press strip (9), N-shaped bridge (8) and developing tank (21) on described groove column, developing tank (21) side bolt connects main folder block (20) pin location, chromatoplate (19) is positioned on the inner side of N-shaped bridge (8), main folder block (20) and sub-folder block (7) and is clamped by the nut fastening in sub-folder block (7) outside；Being provided with ultraviolet lamp socket in described cluster illumination lamps (5), 254nm lamp, 365nm mercury lamp are separately fixed on ultraviolet lamp socket, and LED is located at the upper end of lamp bracket；Outer housing (6) is cuboid, and its front end is provided with through hole, and through hole is equipped with quartz window (4), and quartz window (4) is arranged on through hole by pressure ring；Described outer housing (6) is that glass is made, and the wet grid of described control (11), N-shaped bridge (8) are that 2000 mesh quartz screen plates are made, and described control wet sump (13), shifting grid rod (12), developing tank (21) are that politef is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510255140.8A CN104833765B (en) | 2015-05-19 | 2015-05-19 | Pendency thin layer chromatograph |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510255140.8A CN104833765B (en) | 2015-05-19 | 2015-05-19 | Pendency thin layer chromatograph |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104833765A CN104833765A (en) | 2015-08-12 |
| CN104833765B true CN104833765B (en) | 2016-08-03 |
Family
ID=53811778
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510255140.8A Expired - Fee Related CN104833765B (en) | 2015-05-19 | 2015-05-19 | Pendency thin layer chromatograph |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104833765B (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1428545A (en) * | 1972-10-19 | 1976-03-17 | Takeshita Y | Apparatus for thin-layer or paper chromatography |
| CH615356A5 (en) * | 1976-04-07 | 1980-01-31 | Kreuzig Franz | Apparatus for uniform spraying of thin-layer plates with reagents for quantitative thin-layer chromatography |
| US4469601A (en) * | 1981-03-17 | 1984-09-04 | Varex Corporation | System and apparatus for multi-dimensional real-time chromatography |
| US4810471A (en) * | 1986-07-24 | 1989-03-07 | Rohm And Haas Co. | Vacuum manifold for extraction processing |
| DE10209159A1 (en) * | 2002-02-26 | 2003-09-11 | Thomas R Appel | Thin layer chromatography kit provides solvent conditioned atmosphere enclosure, sample loading, and plate handling facility |
| CN2924532Y (en) * | 2006-07-17 | 2007-07-18 | 长沙川戈科技发展有限公司 | Rod thin layer chromatograph |
-
2015
- 2015-05-19 CN CN201510255140.8A patent/CN104833765B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1428545A (en) * | 1972-10-19 | 1976-03-17 | Takeshita Y | Apparatus for thin-layer or paper chromatography |
| CH615356A5 (en) * | 1976-04-07 | 1980-01-31 | Kreuzig Franz | Apparatus for uniform spraying of thin-layer plates with reagents for quantitative thin-layer chromatography |
| US4469601A (en) * | 1981-03-17 | 1984-09-04 | Varex Corporation | System and apparatus for multi-dimensional real-time chromatography |
| US4810471A (en) * | 1986-07-24 | 1989-03-07 | Rohm And Haas Co. | Vacuum manifold for extraction processing |
| DE10209159A1 (en) * | 2002-02-26 | 2003-09-11 | Thomas R Appel | Thin layer chromatography kit provides solvent conditioned atmosphere enclosure, sample loading, and plate handling facility |
| CN2924532Y (en) * | 2006-07-17 | 2007-07-18 | 长沙川戈科技发展有限公司 | Rod thin layer chromatograph |
Non-Patent Citations (1)
| Title |
|---|
| TLC-IR法检测降糖中药及保健品中掺入2种双胍类药物;张宏莲 等;《药物分析杂志》;20131231;第33卷(第12期);2061-2064 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104833765A (en) | 2015-08-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US9568184B2 (en) | Lighting equipment and image projector | |
| JP2006251796A5 (en) | ||
| TW200607335A (en) | Flicker detection for image sensing devices | |
| CN102646373A (en) | LED display module with quick mounting-demounting structure | |
| TW200604675A (en) | Planer light source device and display device using it | |
| CN100545729C (en) | A kind of control method that is installed in the external camera flash-light on the portable terminal | |
| CN104833765B (en) | Pendency thin layer chromatograph | |
| CN203950105U (en) | Mobile phone LED light compensating lamp | |
| KR20110132084A (en) | Camera and method for displaying image thereof | |
| TW200642522A (en) | Full-color organic electro-luminescent display device and method for producing the same | |
| TW201736931A (en) | Extension photoflash light and camera system using the same | |
| CN205301789U (en) | Intelligent control advertisement projection lamp | |
| CN104792919B (en) | Constant current thin layer chromatograph | |
| CN107731072A (en) | Hand-held pinhole imaging system demonstrator | |
| CN108510877B (en) | Signboard convenient to installation and dismantlement | |
| CN209357232U (en) | Meter reading device with illumination function | |
| CN207179842U (en) | Air cleaning unit | |
| CN216057222U (en) | Light source assembly of integrated image sensor | |
| CN203204865U (en) | Sand painting equipment for creative teaching | |
| CN211203909U (en) | Constant-current frequency flashing light convenient to mount | |
| CN218788795U (en) | High waterproof nature camera device | |
| CN205987085U (en) | Camera infrared lamp device | |
| CN206021816U9 (en) | For the display floater and display of display | |
| CN105240757A (en) | Street lamp capable of turning on automatically | |
| KR101263723B1 (en) | Led lighting fitting equation |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| EXSB | Decision made by sipo to initiate substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160803 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |