CN1048147C - Insecticide with plant growth substances function - Google Patents

Insecticide with plant growth substances function Download PDF

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Publication number
CN1048147C
CN1048147C CN94118352A CN94118352A CN1048147C CN 1048147 C CN1048147 C CN 1048147C CN 94118352 A CN94118352 A CN 94118352A CN 94118352 A CN94118352 A CN 94118352A CN 1048147 C CN1048147 C CN 1048147C
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China
Prior art keywords
ammonia
corpse
animal
chinese herbal
present
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Expired - Fee Related
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CN94118352A
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Chinese (zh)
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CN1106212A (en
Inventor
赵信甥
李削克
王明泉
赵英男
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Zhao Xinyao
Zhao Yingnan
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赵信甥
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Abstract

The present invention relates to a high efficiency insecticidal agent with the function of growth promotion. The present invention is a Chinese herbal medicine preparation formed by preparing Chinese herbal medicines, such as pine needle branches, dog tail ferns, Huohuatiao, bitter apricot kernels, iron rod artemisia, flavescent sophora roots, drilgrass, wild chrysanthemum flowers, Beiwujia, Yincaohuo, southernwood, etc.; bone oil cadaverine, chicken feathers or animal cadaverine, naphthalene, phenol, sulfur, phosphorus and potassium oxide are added; after hybrid reaction, turkey red oil is added for emulsification, and thus, emulsion is made. The present invention has the advantages of easy obtainment of raw material, low production cost, no toxicity, no side effect and no damage to human beings or livestock, and is favorable to ecological balance; the present invention can influence the physiological metabolism of peeling aging pests and can kill out the peeling aging pests; besides, the present invention can promotion action to plant growth. Therefore, the present invention is an ideal new agricultural chemical.

Description

Insecticide with plant growth substances function
The present invention relates to a kind of agricultural insecticide, is a kind of crops growth encourage that makes, and makes the insecticide with plant growth substances function of insect extinction.
At present, the agricultural insecticide kind is a lot, and chrysanthemum lipid, organic phosphates, organochlorine class, carbamic acid lipid are arranged, it all is poisoning that these insecticides have individual general character, kill or tag and control worm by stomach, insect that is poisoned to death or the plant that is sprayed with agricultural chemicals are eaten up also and can be poisoned to death by animal, so because of spraying pesticide, people and animals usually suffer damage, natural enemy faces extinction, and the ecological balance is destroyed, but insect develops immunity to drugs, dosage is increasing, residual hazard is more and more produced pernicious follow bad.
The objective of the invention is to utilize Chinese herbal medicine to develop a kind of insecticide with plant growth substances function, to solve existing chemical pesticide insect is produced the hole property of medicine, people and animals are caused the prestige evil, natural enemy faces extinction, and the ecological balance is suffered the destruction problem.
The object of the present invention is achieved like this: according to the Chinese medicine theory, suppress and destruction with the physiological metabolism generation of plant secondary substance to the insect biology.This insecticide with plant growth substances function is to be Main Ingredients and Appearance with the Chinese herbal medicine, adds animal oil corpse ammonia, chicken feather or animal corpse ammonia, naphthalene, phenol, sulphur, phosphorus, potassium oxide and turkey red oil, makes emulsion, its raw material proportioning following (weight ratio)
Chinese herbal and crude drugs preparations 50--63% animal oil corpse ammonia 20--25%
Chicken feather or animal corpse ammonia 12--18% naphthalene 0.3--0.4%
Phenol 0.4--0.5% sulphur 0.7--0.9%
Phosphorus 0.4--0.5% potassium oxide 0.3--0.5%
Turkey red oil 1.8--2.0%
Chinese herbal and crude drugs preparations is to form (weight ratio) by following prepared from traditional Chinese medicines
Pine needle branch 1--3% favus of the scalp wooden dipper 2--5% king triurid 0--3%
HUOHUATIAO 4--6% GOUWEIJUE 3--5% henbane seed 0--3%
Leaf of Chinese ilex 3--5% folium isatidis 0--3% semen armeniacae amarae 2--5%
Drilgrass 2--5% gmelin worm wood 4--7% mother chrysanthemum 3--6%
Sweet wormwood 4--8% potentilla discolor 3--6% isatis root 2--4%
Stramonium 2--4% kuh-seng 5--8% Qiang spends 2--5%
The excessive grass of achene of Siberian cocklebur 3--6% is 3--6% subprostrate sophora 1--3% suddenly
Peach leaf 1--4% BEIWUJIA 3--7% vinegar stays sub-0--5%
Fly grass 0--3% ghost is seen fearness 2--3% GUIZHENZI 0--3%
Horse tooth 0--4%
Its production technology comprises: select materials, clean, pulverizing, fried, filter, concentrate, bone charing, reaction, filtration, chicken feather or spoil hydrolysis, filtration, concentrate, hybrid reaction, emulsification, packing operation, fried in heatable container, temperature is 75--90 ℃, hybrid reaction is in heatable pressure vessel, reaction temperature 40--80 ℃, pressure is 10132.5--202650pa.
This invention compared with prior art has the following advantages: 1) raw material is easy to get, and cost is low; 2) no side effects to the person poultry harmless, helps the ecological balance; 3) decortication is increased the insect radical cure of can becoming extinct in age; 4) contain amino acid and trace element, help plant growing; 5) contain alkaloid, bactericidal action is arranged.
Below in conjunction with embodiment production technology is described further:
Fig. 1 process chart.
Example 1 best proportioning (weight ratio)
Chinese herbal and crude drugs preparations 60.6% animal oil corpse ammonia 22% chicken feather or animal corpse ammonia 13%
Naphthalene 0.3% phenol 0.4% sulphur 0.8%
Phosphorus 0.5% potassium oxide 0.4% turkey red oil 2.0%
The best proportioning of Chinese herbal and crude drugs preparations: (weight ratio)
Pine needle branch 2.1% kuh-seng 8% king triurid 1%
Folium isatidis 0.5% GOUWEIJUE 5% Drilgrass 1.5%
Favus of the scalp wooden dipper 2.9% mother chrysanthemum 5.2% HUOHUATIAO 5%
Potentilla discolor 4.8% henbane seed 1.3% stramonium 3%
Leaf of Chinese ilex 6% Qiang spends 4.6% semen armeniacae amarae 2.7%
The achene of Siberian cocklebur 6% gmelin worm wood 6% subprostrate sophora 1.4%
Sweet wormwood 5.9% BEIWUJIA 5% isatis root 2.1%
Excessive grass 3.8% peach leaf, 3% vinegar suddenly stays son 3%
Fly grass 2.2% ghost is seen fearness 2.7% horse tooth 2%
GUIZHENZI 3.3%
Specification:
1, select materials: the Chinese herbal medicine of selecting for use Xia Qiu to gather is got herb or root, leaf, and bone, chicken feather or spoil are not limit;
2, clean: the Chinese herbal medicine water is peace and quiet, bone, chicken feather or spoil are cleaned, remove dust;
3, pulverize, with mower or manually be cut into 30--130mm, it is broken that bone is wanted with Chinese herbal medicine, and spoil is divided into the square of 60--150mm;
4, fried: Chinese herbal medicine is put into reactor, add water 1--3 doubly, temperature is controlled in the 75--90 ℃ of scope fried more than 12 hours, gets juice;
5, filter: operation (4) is fried in shallow oil juice filter, remove insoluble matter with filter or filter cloth;
6, concentrate: operation (5) filtrate is put into heatable container, boil, when concentration reaches 12 ° of Be, get Chinese herbal and crude drugs preparations and take out standby with 75--90 ℃ of stew fire;
7, bone charing: get os purum and put into the gas retort heating, treat that the complete charing of bone ends;
8, reaction: bone black is put into container add sulfuric acid reaction, get animal oil corpse ammonia liquid;
9, filter: operation (8) corpse ammonia liquid is filtered with filter or filter cloth, remove insoluble matter, get bone corpse ammonia and seal up for safekeeping standby;
10, chicken feather or spoil hydrolysis: with clean chicken feather or cut apart spoil and put into container, add water 2--3 doubly, add alkali 4--10%, stirring heats 40--70 ℃ treats that chicken feather or spoil dissolve the back fully and end, and promptly obtains compound amino acid;
11, filter: the compound amino acid that operation (10) is obtained filters with filter or filter cloth, removes insoluble matter;
12, concentrate: operation (11) filtrate is put into heatable container, boil, treat that concentration gets chicken feather when reaching 12 ° of Be or animal corpse ammonia is sealed up for safekeeping standby with 75--90 ℃ of scope stew fire;
13, hybrid reaction: operation (6) Chinese herbal and crude drugs preparations is put into heatable pressure vessel, add operation (9) animal oil corpse ammonia, (12) chicken feather or animal corpse ammonia, add naphthalene, phenol, phosphorus, sulphur and potassium oxide then, stir, be heated to 40--80 ℃, reacting more than 10 hours under the 10132.5--202650pa pressure;
14, emulsification: mixed reactant put into be finished product after mulser adds turkey red oil 1.8-2.0% emulsification;
15, packing: available liquid filling machine is packed into packaged in glass or the plastic bottle, the shake out warehouse-in.

Claims (3)

1, a kind of insecticide with plant growth substances function is to be Main Ingredients and Appearance with the Chinese herbal medicine, and interpolation animal oil corpse ammonia, chicken feather or animal corpse ammonia, naphthalene, phenol, sulphur, phosphorus, potassium oxide, turkey red oil are made emulsion, and its weight proportion is as follows:
Chinese herbal and crude drugs preparations 50--63% animal oil corpse ammonia 20-25%
Chicken feather or animal corpse ammonia 12--18% naphthalene 0.3-0.4%
Phenol 0.4--0.5% sulphur 0.7-0.9%
Phosphorus 0.4--0.5% potassium oxide 0.3-0.5%
Turkey red oil 1.8--2.0%.
Its weight proportion of Chinese herbal and crude drugs preparations is as follows:
Pine needle branch 1--3% favus of the scalp wooden dipper 2--5% king triurid 0--3%
Kuh-seng 5--8% GOUWEIJUE 3--5% folium isatidis 0--3%
Mother chrysanthemum 3--6% Drilgrass 2--5% HUOHUATIAO 4--6%
Leaf of Chinese ilex 3--5% henbane seed 0--3% potentilla discolor 3--6%
Qiang spends 2--5% stramonium 2--4% semen armeniacae amarae 2--5%
Sweet wormwood 4--8% gmelin worm wood 4--7% achene of Siberian cocklebur 3--6%
The excessive grass of BEIWUJIA 3--7% 3--6% ghost is suddenly seen fearness 2--3%
Peach leaf 1--4% GUIZHENZI 0--3% vinegar stays sub-0--5%
Horse tooth 0--4% fly grass 0--3% subprostrate sophora 1--3%
Isatis root 2--4%
Animal oil corpse ammonia is bone to be put into gas retort heat charing, puts into container then and adds sulfuric acid reaction, filtration, can obtain animal oil corpse ammonia.
Chicken feather or animal corpse ammonia are that chicken feather or spoil are put into container, add water 2---3 doubly, add alkali 4---10%, are stirred and heated to 40---70 ℃, treat to cross leaching liquid after chicken feather or spoil are dissolved fully, and heating concentrates and can get.
2, the described insecticide with plant growth substances function of claim 1, its production technology comprises: select materials, cleaning, herbal medicine are pulverized, fried, filter, concentrate, bone charing, reaction, filtration, chicken feather or spoil hydrolysis, filtration, concentrated, hybrid reaction, emulsification, packing operation, fried in heatable container, temperature is 75--90 ℃, hybrid reaction is with in the heatable pressure vessel, and reaction temperature is 40--80 ℃, and pressure is 10132.5--20265pa.
3, insecticide with plant growth substances function according to claim 1, its optimum weight proportioning is: Chinese herbal and crude drugs preparations 60.6% animal oil corpse ammonia 22% chicken feather or animal corpse ammonia 13% naphthalene 0.3% phenol 0.4% sulphur 0.8% phosphorus 0.5% potassium oxide 0.4% turkey red oil 2.0% Chinese herbal and crude drugs preparations % by weight proportioning: pine needle branch 2.1 king triurids 1 GOUWEIJUE 5 favus of the scalp wooden dippers 2.9 HUOHUATIAOs 5 henbane seeds 1.3 leaves of Chinese ilex 6 semen armeniacae amaraes 2.7 gmelin worm woods 6 sweet wormwoods 5.9 isatis roots 2.1 excessive grass suddenly 3.8 kuh-sengs, 8 folium isatidis, 0.5 Drilgrass, 1.5 mother chrysanthemums, 5.2 potentilla discolor, 4.8 stramoniums, 3 Qiang spend 4.6 achenes of Siberian cocklebur, 6 subprostrate sophoras, 1.4 BEIWUJIAs, 5 peach leafs, 3 flies grass, 2.2 horse teeth, 2 vinegar to stay sub 3 ghosts to see fearness 2.7 GUIZHENZIs 3.3
CN94118352A 1994-11-25 1994-11-25 Insecticide with plant growth substances function Expired - Fee Related CN1048147C (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
CN94118352A CN1048147C (en) 1994-11-25 1994-11-25 Insecticide with plant growth substances function

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CN1106212A CN1106212A (en) 1995-08-09
CN1048147C true CN1048147C (en) 2000-01-12

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Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103141523A (en) * 2013-02-06 2013-06-12 杨凌农科大无公害农药研究服务中心 Acanthopanax gracilistylus insecticide and its preparation method
CN106689229A (en) * 2016-12-20 2017-05-24 郭海桥 Botanical pesticide and preparation method thereof
CN110477033A (en) * 2019-08-20 2019-11-22 贵州省烟草公司铜仁市公司 A kind of tobacco insecticide and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN85100392A (en) * 1985-04-01 1986-08-27 广西壮族自治区天然药物研究中心 From the plant Radix Sophorae Tonkinensis, extract the method for treatment medicine for curing hepatitis
CN88100583A (en) * 1988-02-15 1988-10-26 陈能根 Speckle disappears and fills a prescription and method for making

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN85100392A (en) * 1985-04-01 1986-08-27 广西壮族自治区天然药物研究中心 From the plant Radix Sophorae Tonkinensis, extract the method for treatment medicine for curing hepatitis
CN88100583A (en) * 1988-02-15 1988-10-26 陈能根 Speckle disappears and fills a prescription and method for making

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Free format text: CORRECT: INVENTOR; FROM: ZHAO XINSHENG; LI XUEKE TO: ZHAO XINYAO; LI XUEKE

CP03 Change of name, title or address

Address after: The people of Handan city Congtai District Road No. 246 East

Inventor after: Zhao Xinyao

Patentee after: Zhao Yingnan

Inventor after: Li Xiaoke

Patentee after: Zhao Xinyao

Address before: Handan city Congtai Road No. 33

Inventor before: Zhao Xinsheng

Patentee before: Wang Mingquan

Inventor before: Li Xiaoke

Patentee before: Zhao Yingnan

Patentee before: Zhao Xinsheng

C19 Lapse of patent right due to non-payment of the annual fee
CF01 Termination of patent right due to non-payment of annual fee