CN104800137B - The applications of golden flower Flos Camelliae Japonicae extracts, preserving moisture and protecting skin composition and preparation method thereof - Google Patents
The applications of golden flower Flos Camelliae Japonicae extracts, preserving moisture and protecting skin composition and preparation method thereof Download PDFInfo
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- CN104800137B CN104800137B CN201510266465.6A CN201510266465A CN104800137B CN 104800137 B CN104800137 B CN 104800137B CN 201510266465 A CN201510266465 A CN 201510266465A CN 104800137 B CN104800137 B CN 104800137B
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Abstract
The invention discloses application of the golden flower Flos Camelliae Japonicae extracts in the cosmetics or health food with moisture-keeping efficacy, develop the new application of golden flower camellias, and preserving moisture and protecting skin composition is provided, mainly it is made of disodium ethylene diamine tetraacetate, Sodium Hyaluronate, pyrrolidone sodium carboxylate, trimethylglycine, Phenoxyethanol, methyl hydroxybenzoate, golden flower camellias water extract, grape seed oil, emulsifier.The present invention have many advantages, such as efficient moisture-retention, safety, mildly it is non-stimulated.
Description
Technical field
The invention belongs to cosmetic technical field, more particularly to the application of golden flower tea extractions, preserving moisture and protecting skin composition and
Its preparation method.
Background technology
Camellia nitidissima (Camellia nitidissima Chi) is known as " tea race queen " " plant kingdom giant panda " " " Dongfang " magic
Tea " etc. belongs to Theaceae Camellia Camellia Section Chrysantha, is high about 2~5 meters of evergreen shrubs or dungarunga.The great nature in China
Resources advantage, now Camellia Section Chrysantha has 34 kinds and 5 mutation in known global range, and NATURAL DISTRIBUTION removes 4 kinds of North Vietnam
And Yunnan Province of China, Guizhou, Sichuan are respectively produced outside a kind, remaining 27 kinds with 5 mutation in China's south Guangxi and the west and south.
Camellia nitidissima is Zhuang nationality in Guangxi traditional medication among the people,《Guangxi Chinese medicine standard》《Guangxi ethnic drug short course》《Extensively
Western medicinal garden medicinal plant register》《Modern Compendium of Materia Medica》《Medicinal Plants of Guangxi register》In it is on the books.Camellia nitidissima tea
Flower is for having blood in stool, irregular menstruation etc..The modern study of Camellia nitidissima medicinal material is started from the 1960s, being related to the life of Camellia nitidissima medicinal material
Pharmacy identification, the artificial culture of medicinal material, chemical composition, pharmacological activity etc..It has been investigated that total sugar content is up in golden flower camellias
39%, and additionally rich in polyphenol, flavones, saponin(e, content is respectively 4.42%, and 8.50%, 7.00% (woods Hua Juan, the Qin are small
Bright, Zeng Qiuwen waits the chemical composition of Camellia nitidissima camellias and physiologically active ingredient analysis food science and technologies [J] .2010, (10):88-
91.).The plant polyoses such as fucoidin, flammulina velutipes have moistening effect, thus it is speculated that golden flower camellias polysaccharide also has certain moisturizing
Effect.
In recent years, with the raising of people's living standard and aesthetical standard, more and more people pursue the tender careful flesh of water
Skin.And moisturizing is the most important link of skin care, is by preventing the loss of moisture in skin and absorbing in external environment
Moisture keeps moisture of skin that can improve the elastic and smooth of skin to achieve the purpose that keep to contain certain moisture in skin
Degree is to ensure skin health, the important measures of anti-aging.The prevalence of ideas such as " Chinese prescription " " advocating nature " " subtraction skin cares ",
Make the research and development of plant source skin-protecting factor there is great realistic meaning.And golden flower camellias are as a kind of new cosmetics moisturizing
Additive also has realistic meaning.
The content of the invention
The purpose of the present invention is intended to provide a kind of plant source raw material with moisture-keeping functions, is cosmetics and health products trade
Middle moisturizer provides new raw material and new selection, while expands the utilization scope of Camellia nitidissima.
To achieve the above object, the technical solution adopted by the present invention is as follows：
The present invention provides application of the golden flower Flos Camelliae Japonicae extracts in the cosmetics or health food with moisture-keeping efficacy.
Preferably, the golden flower Flos Camelliae Japonicae extracts are the water extract of golden flower camellias.
It is further preferred that the water extract of the golden flower camellias is to mix golden flower camellias with water, through boiling extraction, mistake
Filter, freeze-drying obtain.It is freeze-dried obtained powder and is easy to quantitative, storage；Freeze-drying can prevent active ingredient from being broken
Bad, main function is：Replenishing water and preserving moisture.
It is highly preferred that the boiling extraction carries out three times, first time, second, the golden flower camellias and water of third time extraction
Weight ratio be respectively 1:20、1:14、1:14.
The present invention also provides preserving moisture and protecting skin composition, containing above-mentioned golden flower Flos Camelliae Japonicae extracts, by weight percentage, by
Following raw material composition：
Golden flower Flos Camelliae Japonicae extracts containing abundant active skull cap components, can largely adsorb the moisture in air and firmly lock
Firmly moisture is not lost in, and has splendid moistening effect.
Pyrrolidone sodium carboxylate is natural moisture preserving ingredient and natural moisturizing factor (N M F) as obtained from glutamic acid
In important moisturizing ingredient, there is moisturizing moisture absorbing, effect feel be full of clearly it is pleasant, without glutinous greasy thick and heavy.
Trimethylglycine is a kind of natural, edible amino acid completely, and when physical condition changes, it is easy to handle
Hydrone discharges, and hydrone can be utilized by living cells.
Sodium Hyaluronate is a kind of preferable natural moisturizing factor, and major function is moisturizing.
Phenoxyethanol is preservative, and Phenoxyethanol biggest advantage is preferable to Pseudomonas aeruginosa effect；Property is mild, largely
For in baby products formula and mild formula, also there is relatively good effect to bacterium, but it is poor to the effect of fungi.Two
Person's collective effect is better.
Disodium ethylene diamine tetraacetate is ion chelating agent, and protection activity ingredient promotes product effect.
Emulsifier can emulsify oil phase at normal temperatures, obtain the lotion of fine and smooth temperature.
Oily based on grape seed oil, grape seed oil skin-friendly is strong, oil is oiliness, is easily absorbed by the skin, due to grape seed oil
With slight convergence, it can play the role of tightening skin quality, allergy will not be caused, acne will not be deteriorated.Not only safety
It is non-stimulated, and be easily absorbed by the skin, can pachylosis and angling be prevented with skin nutrition cell.
Preferably, the preserving moisture and protecting skin composition, by weight percentage, is made of following raw material：
Preferably, by weight percentage, it is made of following raw material：
Preferably, by weight percentage, it is made of following raw material：
The present invention also provides the preparation methods of the preserving moisture and protecting skin composition, comprise the following steps：
(1) water is mutually prepared：Deionized water is heated to 50-90 DEG C, adds in methyl hydroxybenzoate, is uniformly mixed；Add in ethylenediamine
Tetraacethyl disodium, Sodium Hyaluronate are uniformly mixed；It is cooled to room temperature；Pyrrolidone sodium carboxylate, trimethylglycine are added,
It is uniformly mixed；Phenoxyethanol is added, is uniformly mixed；It adds golden flower tea extractions, obtain aqueous phase liquid；
(2) prepared by oil phase：Grape seed oil is taken, adds emulsifier, is uniformly mixed, obtains oil phase feed liquid；
(3) water phase oil phase mixes：The obtained aqueous phase liquid of step (1) is slowly added into the oil phase feed liquid of step (2) preparation
In, it stirs evenly.
The primary efficacy of the golden flower Flos Camelliae Japonicae extracts of the offer of the present invention is moisturizing skin, and main moisturizing mechanism has：
(1) MMV methods (assay method referring to：The research Zhejiang University of the skin-protecting function factor in Gong Jin inflammation bamboo exocuticles
[D] .2010.) the water absorbing capacity experimental result that determines golden flower camellias see the table below, and experiment proves plus the base of golden flower Flos Camelliae Japonicae extracts
The water absorbing capacity of plinth formula (containing only deionized water, base oil, emulsifier) lotion is apparently higher than being not added with golden flower Flos Camelliae Japonicae extracts
Basic components lotion, and sustainable more than 4h；
| Skin moisture content (%) | 0 | 0.5 | 1 | 2 | 3 | 4 |
| Flos Camelliae Japonicae extract containing golden flower | 32.6±3.74 | 50.8±3.25 | 51.2±4.12 | 50.8±3.87 | 50.7±5.60 | 49.2±4.13 |
| Without golden flower Flos Camelliae Japonicae extracts | 30.2±2.16 | 41.2±2.67 | 35.3±3.28 | 34.1±2.20 | 32.8±1.24 | 30.7±3.40 |
(2) TEWL methods (assay method referring to：The research Zhejiang University of the skin-protecting function factor in Gong Jin inflammation bamboo exocuticles
[D] .2010.) the water lock capacity experimental result that determines golden flower camellias see the table below, and experiment proves plus the base of golden flower Flos Camelliae Japonicae extracts
The water lock ability of plinth formula lotion is apparently higher than the basic components lotion for being not added with golden flower Flos Camelliae Japonicae extracts, and sustainable more than 4h；
| Moisture of skin windage content (%) | 0 | 0.5 | 1 | 2 | 3 | 4 |
| Flos Camelliae Japonicae extract containing golden flower | 15±2.44 | 17.8±2.75 | 13.6±2.12 | 12.9±3.07 | 13.0±1.63 | 13.4±2.15 |
| Without golden flower Flos Camelliae Japonicae extracts | 18.4±2.56 | 28.5±3.60 | 20.3±2.27 | 18.9±2.10 | 16.8±3.04 | 18.2±2.84 |
(3) pyrrolidone sodium carboxylate in being formulated has moisturizing moisture absorbing；Sodium Hyaluronate has moisturizing；It absorbs
And keep moisture；
(4) trimethylglycine is when physical condition changes, it is easy to hydrone be discharged, allow hydrone can be by living thin
Born of the same parents utilize, and can effectively utilize the moisture of the absorptions such as golden flower Flos Camelliae Japonicae extracts, pyrrolidone sodium carboxylate, Sodium Hyaluronate.
The moisturizing factor collective effect of variety classes separate sources makes product effect more preferable.
Description of the drawings
1 width of attached drawing of the present invention, Fig. 1 are preparation technology flow chart of the present invention.
Specific embodiment
Following non-limiting examples can make those of ordinary skill in the art be more fully understood the present invention, but not with
Any mode limits the present invention.
Emulsifier selects the import 305 for originating in Guangzhou Yu Tai Chemical Industry Science Co., Ltd.
Aqueous Phase Raw Material：Deionized water, disodium ethylene diamine tetraacetate, Sodium Hyaluronate, pyrrolidone sodium carboxylate, trimethyl are sweet
Propylhomoserin, Phenoxyethanol, methyl hydroxybenzoate, golden flower camellia water extracts.
Oil phase raw material：Grape seed oil, emulsifier.
Embodiment 1
Preserving moisture and protecting skin composition by weight percentage, is made of following raw material：
1 preparation process flow of the present embodiment is as shown in Figure 1, concrete operation step is as follows：
(1) golden flower camellias are extracted：The water extract of the golden flower camellias is by golden flower camellias (preferably Camellia nitidissima dried leaf powder
End) mix with water, through boiling extraction three times, filtering, freeze-drying obtain, for the first time, second, the Camellia nitidissima extracted for the third time
The weight ratio of flower and water is respectively 1:20、1:14、1:14.
(1) water is mutually prepared：Deionized water is heated to 50-90 DEG C, adds in methyl hydroxybenzoate, is uniformly mixed；Add in ethylenediamine
Tetraacethyl disodium, Sodium Hyaluronate are uniformly mixed；It is cooled to room temperature；Pyrrolidone sodium carboxylate, trimethylglycine are added,
It is uniformly mixed；Phenoxyethanol is added, is uniformly mixed；It adds golden flower tea extractions, obtain aqueous phase liquid；
(2) prepared by oil phase：Grape seed oil is taken, adds emulsifier, is uniformly mixed, obtains oil phase feed liquid；
(3) water phase oil phase mixes：The obtained aqueous phase liquid of step (1) is slowly added into the oil phase feed liquid of step (2) preparation
In, until lotion uniform and smooth.
Embodiment 2
Preserving moisture and protecting skin composition by weight percentage, is made of following raw material：
Preparation process is the same as embodiment 1.
Embodiment 3
Preserving moisture and protecting skin composition by weight percentage, is made of following raw material：
Preparation process is the same as embodiment 1.
Claims (5)
1. preserving moisture and protecting skin composition, which is characterized in that containing golden flower Flos Camelliae Japonicae extracts, by weight percentage, by following raw material
Composition：
The golden flower Flos Camelliae Japonicae extracts are the water extract of golden flower camellias, and golden flower camellias are mixed with water, extract, filter through boiling,
Freeze-drying obtains.
2. preserving moisture and protecting skin composition according to claim 1, which is characterized in that by weight percentage, by following raw material
Composition：
3. preserving moisture and protecting skin composition according to claim 1, which is characterized in that by weight percentage, by following raw material group
Into：
4. preserving moisture and protecting skin composition according to claim 1, which is characterized in that by weight percentage, by following raw material group
Into：
5. the preparation method of preserving moisture and protecting skin composition, comprises the following steps described in claim 1-4 any one：
(1) water is mutually prepared：Deionized water is heated to 50-90 DEG C, adds in methyl hydroxybenzoate, is uniformly mixed；Add in ethylenediamine tetrem
Acid disodium, Sodium Hyaluronate are uniformly mixed；It is cooled to room temperature；Pyrrolidone sodium carboxylate, trimethylglycine are added, is mixed
Uniformly；Phenoxyethanol is added, is uniformly mixed；It adds golden flower Flos Camelliae Japonicae extracts, obtain aqueous phase liquid；
(2) prepared by oil phase：Grape seed oil is taken, adds emulsifier, is uniformly mixed, obtains oil phase feed liquid；
(3) water phase oil phase mixes：Step (1) is made aqueous phase liquid to be slowly added into the oil phase feed liquid of step (2) preparation, is stirred
It mixes uniformly.
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| CN107213057A (en) * | 2017-06-06 | 2017-09-29 | 安徽吉乃尔电器科技有限公司 | A kind of preparation method of Camellia nitidissima whitening emulsion |
| TWI747444B (en) * | 2019-08-14 | 2021-11-21 | 大江生醫股份有限公司 | Use of camellia chrysantha extract for improving anti-blue light damage effect |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1633982A (en) * | 2004-11-02 | 2005-07-06 | 黄扶民 | Nutritious face cream containing camellia chrysantha |
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2015
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1633982A (en) * | 2004-11-02 | 2005-07-06 | 黄扶民 | Nutritious face cream containing camellia chrysantha |
Non-Patent Citations (2)
| Title |
|---|
| "植物类黄酮作为护肤因子在化妆品领域的研究进展";焦晶晶，等;《精细化工》;20041031;第21卷;第98-102页 * |
| "金花茶茶花黄酮类化合物的分离纯化及抗氧化活性的初步研究";李石容;《中国优秀硕士学位论文全文数据库 农业科技辑》;20130315(第03期);摘要、第1、2、5页 * |
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