CN104800125A - Nail polish and preparation method thereof - Google Patents

Nail polish and preparation method thereof Download PDF

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Publication number
CN104800125A
CN104800125A CN201510221400.XA CN201510221400A CN104800125A CN 104800125 A CN104800125 A CN 104800125A CN 201510221400 A CN201510221400 A CN 201510221400A CN 104800125 A CN104800125 A CN 104800125A
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Prior art keywords
mixed material
nial polish
dispersion
film forming
forming matter
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CN201510221400.XA
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CN104800125B (en
Inventor
董月云
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Shanghai Wanhua Technology Co. Ltd.
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SHHANGHAI O'NINE TECHNOLOGIES Inc
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Abstract

The invention discloses nail polish and a preparation method thereof, and belongs to the technical field of cosmetics. The nail polish is prepared through the following steps: adding 15-30 parts by weight of a crushed natural film forming matter into 65-80 parts of a volatile solvent, and uniformly dispersing at the dispersing speed of 100-300 rpm, thereby obtaining a mixed material; leaving the mixed material to stand for 36-56 hours at the room temperature, finally adding 0.5-8 parts of a humectant into the mixed material, and dispersing for 3-5 minutes at the dispersion speed of 400-600rpm, wherein the natural film forming matter is at least one of mastic gum, sandarac gum, rosin, shell-lac and gum dammar. The nail polish is aqueous, is free of toxic effects on human bodies after being used for a long time, smooth in surface of a film and excellent in adhesion property to nail surfaces, the surface drying time is within 1 minute at the room temperature, the glossiness is greater than 80 degrees, and the effect of maintaining the nails can be achieved while the nails can be rapidly beautified.

Description

A kind of nial polish and preparation method thereof
Technical field
The invention belongs to cosmetic technical field, particularly relate to a kind of manufacture method of nial polish.
Background technology
Tradition is from drier oil nial polish, film forming matter is nitrocellulose, toluenesulfonamide/formaldehyde resin, phthalic anhydride/trimellitic anhydride/di-alcohols copolymer, tricresyl phosphate phenol ester, styrene/acrylic (ester) analog copolymers etc., such film forming matter is dissolved in ethyl acetate, butyl acetate, toluene, isopropyl alcohol equal solvent, is volatilized and in first face film forming by solvent.
Water-based nail polish, film forming matter aqueous acrylic emulsion or watersoluble polyurethane acrylic acid emulsion; Solvent is pure water; Cosolvent is alcohols or the alcohol ethers such as propylene glycol, glycerol, propylene glycol phenylate, butyl, dipropylene glycol methyl ether, dipropylene, makes emulsion film forming by the volatilization of moisture content and cosolvent.
Existingly lay claim to strong first, the product of supporting first is on the basis based on above-mentioned formula, add a small amount of functional component as hydrolyzed wheat protein, calcium pantothenate, hydrolysing oil Fructus Canarii albi (Olea europaea) leaf extract, Okoume resinae additive, thus reach the strong effect of fingernail.Owing to being the formula basis based on nial polish, a large amount of volatile solvents contained, as ethyl acetate, butyl acetate; Toluene etc., ethyl acetate, butyl acetate have obvious irritation abnormal smells from the patient in nial polish operating process, chafe and mucosa, and it is abnormal etc. that neurasthenic syndrome, hepatomegaly, feminine menstrual can occur Long Term Contact toluene, and xerosis cutis, chap, dermatitis.Film forming matter is containing phthalic ester plasticizer, and this constituents can disturbance endocrine, increases the probability of suffers from breast, harmful to human reproductive system.
Summary of the invention
For the problems referred to above, the invention provides a kind of film forming matter and support first nail polish based on the strong first that biotic component is harmless, and preparation method thereof, concrete scheme is as follows:
A kind of nial polish, is characterized in that, comprise following parts by weight ingredient:
Natural film forming matter 15-30 part, volatile solvent 65-80 part, wetting agent 0.5-8 part, quintessence oil 0.2-1 part;
Described natural film forming matter is agate base of a fruit natural gum, mountain reaches at least one in glue, Colophonium, Lac, gum dammar.
Preferably, any two kinds that described natural film forming matter is agate base of a fruit natural gum, mountain reaches in glue, Colophonium, Lac, gum dammar.
Preferably, described volatile solvent is at least one in ethanol, isopropyl alcohol, Oleum Terebinthinae.
Preferably, described wetting agent is at least one in propylene glycol, glycerol, butanediol, white mineral oil, carbamide, Aloe extract, Oleum Terebinthinae.
Preferably, described quintessence oil is at least one in angelica essential oil, Herba Pogostemonis essential oil, Olibanum quintessence oil, Myrrha quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil, Okoume tree resin extract.
The manufacture method of above-mentioned nial polish comprises the following steps:
S1: natural film forming matter is crushed to 100-300 order granularity;
S2: by weight, adds in volatile solvent by the natural film forming matter pulverized, is uniformly dispersed, obtains mixed material with the rate of dispersion of 100-300rpm;
S3: by mixed material left at room temperature 36-56 hour;
S4: by weight, adds wetting agent in mixed material, with the rate of dispersion of 400-600rpm dispersion 3-5min.
Further, in described step S4, before adding wetting agent in mixed material, mixed material need filter with 200 order nylon gauzes.
Further, also comprise step S5: add effect quintessence oil, with the rate of dispersion of 400-600rpm dispersion 3-5min, leave standstill to froth breaking complete.
Nial polish of the present invention, film forming matter is based on natural biological secretions as frankincense gum, agate base of a fruit natural gum, mountain reach glue, Colophonium, Lac, lacca etc., and life-time service to the toxic effect of human body, can not contain phthalic ester plasticizer.
The volatile solvent of film forming is dehydrated alcohol, isopropyl alcohol, Oleum Terebinthinae, and without any other solvent as ethyl acetate, butyl acetate, acetone, dimethylbenzene etc., zest is low, and safety is high.
Add natural 100% purity quintessence oil, as angelica essential oil, Herba Pogostemonis essential oil, Olibanum quintessence oil, Myrrha quintessence oil, blood circulation promoting, hyperplasia, metabolism, play the effect of bactericidal antiphlogistic, functions of detumescence, relieving inflammation, make Fingernail growth rate accelerate, the first face of nial polish film forming is more strong firm.
Nial polish of the present invention is water sample quality, brush on first face with hairbrush, under room temperature, surface drying time is within 1 minute, and film formation surface is smooth, and gloss is more than 80 °, more excellent adhesive force is had to first face, without obvious irritation abnormal smells from the patient in operating process, and with the fragrant of natural essential oil, film forming is quick, gloss is excellent, and being used alone can quick easily manicure maintenance simultaneously fingernail.
This nial polish is used alone, and can play the effect of strong first armor; Simultaneously film forming matter of the present invention is excellent with fingernail first face adhesive effect, can as end oil use.This nial polish, not containing any acidic additive, is directly brushed and can not have acid corrosion action to first face on first face; On its face, brush phototherapy glue as end oil, can carry out foster first while manicure, meanwhile, this nial polish is conducive to the removal of phototherapy glue product, and after removal, first face is smooth, not crude.
Strong first for nial polish of the present invention supports first effect, and be used alone (30 people) by experimenter to it, coordinate phototherapy glue to use (30 people), coordinate aqueous nail polish to use (20 people) to test respectively, experimental program is as follows:
1) be used alone
The present invention's nial polish of the present invention is brushed, surface drying under room temperature, the nial polish thickness 10-30 μm after surface drying in experimenter's first face.With every 1 week for one-period, again brush nial polish of the present invention after removal nial polish, 9 all after dates are observed, are added up and support first effect.
2) phototherapy glue is coordinated to use
The present invention's nial polish of the present invention is brushed in experimenter's first face, brush phototherapy glue (the phototherapy glue thickness 80-120 μm after surface drying) thereon after surface drying 5-10 second (the nial polish thickness 10-30 μm after surface drying) under room temperature, finally brush phototherapy sealing again.With every 3 for one-period, again brush after removal nial polish, 3 all after dates are observed, are added up and support first effect.
3) aqueous nail polish is coordinated to use
The present invention's nial polish of the present invention is brushed in experimenter's first face, brush aqueous nail polish (the aqueous nail polish thickness 50-80 μm after surface drying) thereon after surface drying 5-10 second (the nial polish thickness 10-30 μm after surface drying) under room temperature, finally brush aqueous gloss varnish again.With every 1 week for one-period, again brush after removal nial polish, 9 all after dates are observed, are added up and support first effect.
Observation, statistical result is as shown in table 1:
Form 1
The display of upper table result, its strong first is supported in first efficacy test, 80 experimenters, and fingernail is hardening, thickening, the speed of growth improves has 49, accounting 61.25%; What fingernail was hardening, thickening, brighter has 20 samples, accounting 25%; Accounting fingernail to maintenance effect adds up to 86.25%; As can be seen here, nial polish of the present invention has strong first significantly and supports first effect.
In addition, this nial polish coordinates phototherapy glue to use as primary coat, can play the effect to the attachment of first face, and itself and the ply adhesion of phototherapy glue are good.Implement according to above-mentioned test technology, 2 weeks to one month can be reached in the time of staying in first face.Significantly can reduce the removal time of phototherapy glue simultaneously, can the removal time of common for market phototherapy glue be reduced within 10 minutes from 15 minutes, reduce and unload the injury of first solvent to first face, after removal, the rough phenomenon of first face Glabrous, reaches the effect of maintenance fingernail simultaneously.
This nial polish coordinates aqueous nail polish to use as primary coat, plays the effect to the attachment of first face, good with the ply adhesion of aqueous nail polish.Implement according to above-mentioned test technology, the reservation complete cycle in first face can extend to 5-7 days from 1-3 days, reached maintenance fingernail simultaneously.
Detailed description of the invention
In order to more fully understand technology contents of the present invention, below in conjunction with specific embodiment technical scheme of the present invention being introduced further and illustrating.
Embodiment 1
20 parts of gum dammars are rejected impurity, is crushed to 100-300 order granularity with pulverizer.75 parts of dehydrated alcohol are dropped in dispersion machine, slowly adding gum dammar powder under the state keeping 100-300rpm rate of dispersion, obtain mixed material to being uniformly dispersed after, closing dispersion machine.By mixed material left at room temperature 48 hours, make gum dammar powder dissolution.Again the transparent homogeneous mixed material after standing dissolving is removed bottom insoluble residue thing and impurity, and filter with 200 order nylon gauze 3 layers.Then 4.5 parts of butanediols are dropped in mixed material after filtration, with high speed dispersor with the rate of dispersion of 400-600rpm dispersion 3-5min.Finally drop into 0.3 part of Olibanum quintessence oil and 0.2 part of angelica essential oil according to weight ratio, with 400-600rpm rotating speed dispersion 3-5min, leave standstill and within 1 hour, treat that its froth breaking is complete, obtains nial polish.
Embodiment 2
15 parts of agate base of a fruit resins are rejected impurity, is crushed to 100-300 order granularity with pulverizer.77 parts of dehydrated alcohol and 7.5 parts of Oleum Terebinthinaes are dropped in dispersion machine, keeps 100-300rpm rate of dispersion dispersion 2-3min, then under dispersity, slowly adding agate base of a fruit toner, obtain mixed material to being uniformly dispersed after, closing dispersion machine.By mixed material left at room temperature 48 hours, make gum dammar powder dissolution.Again the transparent homogeneous mixed material after standing dissolving is removed bottom insoluble residue thing and impurity, and filter with 200 order nylon gauze 3 layers.Finally drop into 0.3 part of Olibanum quintessence oil and 0.2 part of angelica essential oil according to weight ratio, with 400-600rpm rotating speed dispersion 3-5min, leave standstill and within 1 hour, treat that its froth breaking is complete, obtains nial polish.
Embodiment 3
16 parts of agate base of a fruit resins are rejected impurity, is crushed to 100-300 order granularity with pulverizer.76 parts of dehydrated alcohol and 7.5 parts of Oleum Terebinthinaes are dropped in dispersion machine, after keeping 100-300rpm rate of dispersion dispersion 2-3min, under stirring, slowly adding agate base of a fruit toner, obtain mixed material to being uniformly dispersed after, closing dispersion machine.By mixed material left at room temperature 48 hours, agate base of a fruit toner is dissolved.Again the transparent homogeneous mixed material after standing dissolving is removed bottom insoluble residue thing and impurity, and filter with 200 order nylon gauze 3 layers.Finally drop into 0.5 part of Myrrha quintessence oil according to weight ratio, with 400-600rpm rotating speed dispersion 3-5min, leave standstill and within 1 hour, treat that its froth breaking is complete, obtains nial polish.
Embodiment 4
25 parts of lac resins are rejected impurity, is crushed to 100-300 order granularity with pulverizer.48 parts of dehydrated alcohol and 23 parts of isopropyl alcohols are dropped in dispersion machine, after keeping 100-300rpm rate of dispersion dispersion 2-3min, under stirring, slowly adding lac resin powder, obtain mixed material to being uniformly dispersed after, closing dispersion machine.By mixed material left at room temperature 48 hours, make lac resin powder dissolution.Again the transparent homogeneous mixed material after standing dissolving is removed bottom insoluble residue thing and impurity, and filter with 200 order nylon gauze 3 layers.Then 3.5 parts of glycerol are dropped in mixed material after filtration, with high speed dispersor with the rate of dispersion of 400-600rpm dispersion 3-5min.Finally drop into 0.5 part of Myrrha quintessence oil according to weight ratio, with 400-600rpm rotating speed dispersion 3-5min, leave standstill and within 1 hour, treat that its froth breaking is complete, obtains nial polish.
Embodiment 5
10 parts of mountains are reached glue and 15 parts of lac resins rejecting impurity, be crushed to 100-300 order granularity with pulverizer.48 parts of dehydrated alcohol and 23 parts of isopropyl alcohols are dropped in dispersion machine, after keeping 100-300rpm rate of dispersion dispersion 2-3min, under stirring, slowly adds mountain reach glue, lac resin powder, be uniformly dispersed and obtain mixed material.By mixed material left at room temperature 56 hours, mountain is made to reach glue, lac resin powder dissolution.Again the transparent homogeneous mixed material after standing dissolving is removed bottom insoluble residue thing and impurity, and filter with 200 order nylon gauze 3 layers.Then 3.5 parts of butanediols are dropped in mixed material after filtration, with high speed dispersor with the rate of dispersion of 400-600rpm dispersion 3-5min.Finally drop into 0.5 part of Myrrha quintessence oil according to weight ratio, with 400-600rpm rotating speed dispersion 3-5min, leave standstill and within 1 hour, treat that its froth breaking is complete, obtains nial polish.
Embodiment 6
12 parts of Colophonium and 18 parts of agate base of a fruit natural gum are rejected impurity, is crushed to 100-300 order granularity with pulverizer.48 parts of dehydrated alcohol and 23 parts of Oleum Terebinthinaes are dropped in dispersion machine, after keeping 100-300rpm rate of dispersion dispersion 2-3min, under stirring, slowly adds Colophonium, agate base of a fruit gum powder, be uniformly dispersed and obtain mixed material.By mixed material left at room temperature 56 hours, Colophonium, agate base of a fruit gum powder are dissolved.Again the transparent homogeneous mixed material after standing dissolving is removed bottom insoluble residue thing and impurity, and filter with 200 order nylon gauze 3 layers.Then 3.5 parts of white mineral oils, 2.5 parts of Aloe extracts are dropped in mixed material after filtration, with high speed dispersor with the rate of dispersion of 400-600rpm dispersion 3-5min.Finally drop into 0.5 part of Herba Lysimachiae foenum-graeci quintessence oil according to weight ratio, with 400-600rpm rotating speed dispersion 3-5min, leave standstill and within 1 hour, treat that its froth breaking is complete, obtains nial polish.
Embodiment 7
10 parts of Lac and 14 parts of gum dammars are rejected impurity, is crushed to 100-300 order granularity with pulverizer.35 parts of isopropyl alcohols and 30 parts of Oleum Terebinthinaes are dropped in dispersion machine, after keeping 100-300rpm rate of dispersion dispersion 2-3min, under stirring, slowly adds Lac, gum dammar powder, be uniformly dispersed and obtain mixed material.By mixed material left at room temperature 56 hours, make Lac, gum dammar powder dissolution.Again the transparent homogeneous mixed material after standing dissolving is removed bottom insoluble residue thing and impurity, and filter with 200 order nylon gauze 3 layers.Then 3.5 parts of carbamide, 2.5 parts of glycerol are dropped in mixed material after filtration, with high speed dispersor with the rate of dispersion of 400-600rpm dispersion 3-5min.Finally drop into 0.2 part of Okoume tree resin extract, 0.2 part of Herba Lysimachiae foenum-graeci quintessence oil according to weight ratio, with 400-600rpm rotating speed dispersion 3-5min, leave standstill and within 1 hour, treat that its froth breaking is complete, obtains nial polish.
The above only further illustrates technology contents of the present invention with embodiment, so that reader is easier to understand, but does not represent embodiments of the present invention and is only limitted to this, and any technology done according to the present invention extends or recreation, all by protection of the present invention.

Claims (9)

1. a nial polish, is characterized in that, comprises following parts by weight ingredient:
Natural film forming matter 15-30 part, volatile solvent 65-80 part, wetting agent 0.5-8 part;
Described natural film forming matter is agate base of a fruit natural gum, mountain reaches at least one in glue, Colophonium, Lac, gum dammar.
2. nial polish according to claim 1, is characterized in that, any two kinds that described natural film forming matter is agate base of a fruit natural gum, mountain reaches in glue, Colophonium, Lac, gum dammar.
3. nial polish according to claim 1, is characterized in that, described volatile solvent is at least one in ethanol, isopropyl alcohol, Oleum Terebinthinae.
4. nial polish according to claim 1, is characterized in that, described wetting agent is at least one in propylene glycol, glycerol, butanediol, white mineral oil, carbamide, Aloe extract, Oleum Terebinthinae.
5. nial polish according to claim 1, is characterized in that, described nial polish also comprises quintessence oil 0.2-1 part.
6. nial polish according to claim 5, is characterized in that, described quintessence oil is at least one in angelica essential oil, Herba Pogostemonis essential oil, Olibanum quintessence oil, Myrrha quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil, Okoume tree resin extract.
7. a manufacture method for nial polish as claimed in claim 1, is characterized in that, comprise the following steps:
S1: natural film forming matter is crushed to 100-300 order granularity;
S2: by weight, adds in volatile solvent by the natural film forming matter pulverized, is uniformly dispersed, obtains mixed material with the rate of dispersion of 100-300rpm;
S3: by mixed material left at room temperature 36-56 hour;
S4: by weight, adds wetting agent in mixed material, with the rate of dispersion of 400-600rpm dispersion 3-5min.
8. the manufacture method of nial polish according to claim 7, it is characterized in that, in described step S4, before adding wetting agent in mixed material, mixed material need filter with 200 order nylon gauzes.
9. the manufacture method of nial polish according to claim 7, is characterized in that, after described step S4, also comprise step S5: add effect quintessence oil, with the rate of dispersion of 400-600rpm dispersion 3-5min, leaves standstill to froth breaking complete.
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Cited By (13)

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CN105213260A (en) * 2015-10-27 2016-01-06 桂林瑞丰环保微生物应用研究所 Low stimulation nial polish of a kind of environmental protection and preparation method thereof
CN105232383A (en) * 2015-10-27 2016-01-13 桂林瑞丰环保微生物应用研究所 Antibacterial caring nail polish and preparation method thereof
CN105232380A (en) * 2015-10-27 2016-01-13 桂林瑞丰环保微生物应用研究所 Nail polish with fragrance and preparation method thereof
CN105250174A (en) * 2015-10-27 2016-01-20 桂林瑞丰环保微生物应用研究所 Health care nursing type nail polish and preparation method thereof
CN105250155A (en) * 2015-11-16 2016-01-20 杭州莱凡网络科技有限公司 Calcium-added nail protecting liquid
CN105496814A (en) * 2015-12-02 2016-04-20 杭州莱凡网络科技有限公司 4D nail polish gel and application method thereof
CN105816353A (en) * 2015-08-03 2016-08-03 杭州莱凡网络科技有限公司 Microphototherapy nail polish
CN105816354A (en) * 2015-08-03 2016-08-03 杭州莱凡网络科技有限公司 Nail polish with sequins, laser powder and rhinestone powder
CN105816356A (en) * 2015-08-03 2016-08-03 杭州莱凡网络科技有限公司 Healthy nail polish
CN105816350A (en) * 2015-08-03 2016-08-03 杭州莱凡网络科技有限公司 Daily nail polish
CN106726714A (en) * 2016-12-23 2017-05-31 叶宗耀 A kind of nail polish and preparation method thereof
CN113861843A (en) * 2021-09-23 2021-12-31 南昌雨露实验器材有限公司 Neutral odorless gum and preparation method thereof
CN116254052A (en) * 2023-03-30 2023-06-13 胡大地 Dammar resin surface layer protective liquid

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CN105816350B (en) * 2015-08-03 2018-04-10 杭州莱凡网络科技有限公司 Daily disposable refers to coloured silk
CN105816354B (en) * 2015-08-03 2018-05-25 杭州莱凡网络科技有限公司 A kind of finger added with diamante, radium-shine powder, artificial diamond powder is color
CN105816353A (en) * 2015-08-03 2016-08-03 杭州莱凡网络科技有限公司 Microphototherapy nail polish
CN105816354A (en) * 2015-08-03 2016-08-03 杭州莱凡网络科技有限公司 Nail polish with sequins, laser powder and rhinestone powder
CN105816356A (en) * 2015-08-03 2016-08-03 杭州莱凡网络科技有限公司 Healthy nail polish
CN105816350A (en) * 2015-08-03 2016-08-03 杭州莱凡网络科技有限公司 Daily nail polish
CN105816356B (en) * 2015-08-03 2018-05-11 杭州莱凡网络科技有限公司 A kind of health refers to coloured silk
CN105816353B (en) * 2015-08-03 2018-04-24 杭州莱凡网络科技有限公司 Low-light, which is treated, refers to coloured silk
CN105232383A (en) * 2015-10-27 2016-01-13 桂林瑞丰环保微生物应用研究所 Antibacterial caring nail polish and preparation method thereof
CN105232380A (en) * 2015-10-27 2016-01-13 桂林瑞丰环保微生物应用研究所 Nail polish with fragrance and preparation method thereof
CN105250174A (en) * 2015-10-27 2016-01-20 桂林瑞丰环保微生物应用研究所 Health care nursing type nail polish and preparation method thereof
CN105213260A (en) * 2015-10-27 2016-01-06 桂林瑞丰环保微生物应用研究所 Low stimulation nial polish of a kind of environmental protection and preparation method thereof
CN105250155A (en) * 2015-11-16 2016-01-20 杭州莱凡网络科技有限公司 Calcium-added nail protecting liquid
CN105250155B (en) * 2015-11-16 2018-03-06 杭州莱凡网络科技有限公司 Add calcium armor water
CN105496814B (en) * 2015-12-02 2018-01-16 杭州莱凡网络科技有限公司 A kind of 4D nail polish glue and its application method
CN105496814A (en) * 2015-12-02 2016-04-20 杭州莱凡网络科技有限公司 4D nail polish gel and application method thereof
CN106726714A (en) * 2016-12-23 2017-05-31 叶宗耀 A kind of nail polish and preparation method thereof
CN113861843A (en) * 2021-09-23 2021-12-31 南昌雨露实验器材有限公司 Neutral odorless gum and preparation method thereof
CN116254052A (en) * 2023-03-30 2023-06-13 胡大地 Dammar resin surface layer protective liquid

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