CN104800100B - A kind of gentle disposable make-up remover and preparation method thereof - Google Patents
A kind of gentle disposable make-up remover and preparation method thereof Download PDFInfo
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- CN104800100B CN104800100B CN201510266286.2A CN201510266286A CN104800100B CN 104800100 B CN104800100 B CN 104800100B CN 201510266286 A CN201510266286 A CN 201510266286A CN 104800100 B CN104800100 B CN 104800100B
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Abstract
A kind of gentle disposable make-up remover, it is characterised in that consist of the following components in percentage by weight：Polyethylene 2%~10%, cetanol ethylhexoate 2%~20%, the isostearates 2%~20% of PEG 10, the glyceryl triisostearates 2%~20% of PEG 20, tocopherol acetate 0.2%~1%, phenyl trimethicone 2%~10%, dextrin palmitate 0.2%~3.0%, surplus is caprylic/capric triglyceride.The present invention make-up remover makeup removing ability it is good, property is gentle, it is safe, facilitate portable.
Description
Technical field
The invention belongs to cosmetic field, and in particular to a kind of make-up remover, and the make-up remover preparation method.
Background technology
Increasing ladies' selection does not take off adornment product, the anti-sweat eye-liner of such as waterproof, eyeliner etc. using lasting.For
Reach needs to add substantial amounts of film forming agent in the effect of the anti-sweat of more preferable waterproof, formula, and therefore, it is difficult to removal.The purpose of makeup removing
Not exclusively remove residual adornment, the also dirt in sweat, the air of sebum secretion thing and attachment on skin.Simply with washing
Face milk or make up remover etc. are difficult thorough removing, cause the nutritional ingredient in the skin care item subsequently used well to be inhaled by skin
Receive, or even produce acne, the problems such as triggering clogging of pores, acne.
Commercially available makeup remover is widely loved by consumers due to its salubrious skin sense, but most of color make-up products and persistence
Bottom adornment product is predominantly oil-soluble, thus aqua class or Hydrogels makeup removal products can not thoroughly removal it is clean, it is necessary to
By removing ornaments and formal dress, cotton rub is wiped, could the more effective facial dressing of removal；Other part product in order to reach preferable makeup removing effect,
The stronger surfactant of excitant is with the addition of, therefore should not be used in a lip.By contrast, although makeup remover has preferably
Molten adornment ability, but its greasy feeling is stronger, and flushing capacity is poor, and residual quantity is larger, and unsnatch needs to use mildy wash further clear after adornment
It is clean.In addition, makeup remover and makeup remover are liquid dosage form, there is long-distance travel inconvenient to carry, easy leakage and can not take winged
The shortcomings of machine.
The content of the invention
It is an object of the invention to the technical problem to be solved for more than, there is provided a kind of makeup removing ability is good, property
Gently, conveniently, safely portative disposable make-up remover.
It is a further object to provide the preparation method of above-mentioned make-up remover.
To achieve the above objectives, the invention provides following technical scheme：
A kind of gentle disposable make-up remover, it is characterised in that consist of the following components in percentage by weight：
Polyethylene 2%~10%, cetanol ethylhexoate 2%~20%, PEG-10 isostearates 2%~20%,
PEG-20 glyceryl triisostearates 2%~20%, tocopherol acetate 0.2%~1%, phenyl trimethicone 2%
~10%, dextrin palmitate 0.2%~3.0%, surplus is caprylic/capric triglyceride.
Preferably, make-up remover of the invention is consisted of the following components in percentage by weight：
Polyethylene 2%~6%, cetanol ethylhexoate 2%~8%, PEG-10 isostearates 2%~5%, PEG-
20 glyceryl triisostearates 10%~20%, tocopherol acetate 0.2%~0.5%, phenyl trimethicone 5%~
10%, dextrin palmitate 1%~3%, surplus is caprylic/capric triglyceride.
Preferably, make-up remover of the invention is consisted of the following components in percentage by weight：
Polyethylene 6%~10%, cetanol ethylhexoate 2%~20%, PEG-10 isostearates 2%~20%,
PEG-20 glyceryl triisostearates 2%~20%, tocopherol acetate 0.5%~1%, phenyl trimethicone 2%
~10%, dextrin palmitate 0.2%~1%, surplus is caprylic/capric triglyceride.
Present invention also offers the preparation method of the make-up remover, its step is as follows：
(1) it is polyethylene, dextrin palmitate, caprylic/capric triglyceride, PEG-10 isostearates, PEG-20 is sweet
Oily three isostearates, cetanol ethylhexoate are added, stirring；
(2) 84 DEG C~88 DEG C are warming up to, 10 minutes are incubated, mixing speed is maintained at 300 revs/min, vacuumizes, homogeneous 5
Minute；
(3) phenyl trimethicone, tocopherol acetate are sequentially added, opens stirring, be well mixed, cooling；
(4) when being down to 70 DEG C~75 DEG C, discharging.
The beneficial effects of the present invention are：
1st, with very high makeup removing ability, the salubrious grease of the not de- adornment composition of addition fully dissolving in formula, and compared with
The nonionic surface active agent of a high proportion of noble and unsullied resulting net force, more can comprehensively remove facial color make-up.
2nd, product property is especially gentle, and formula all components are especially gentle, it is adaptable to various skin types, especially select
With especially gentle PEG type nonionic surfactants, mucocutaneous or eye mucosa excitant, which is all showed, must compare yin, yang
Ionic surfactant it is low.
3rd, designed by optimization of C/C composites, make-up remover of the invention has good flushing capacity, water emulsification can be met, removed ornaments and formal dress
Afterwards need not be again with mildy wash or other face cleaning products with regard to very salubrious effect can be reached, with " disposable " performance.
4th, novel appearance, be translucent paste, being of tentacle, it is easy to sprawl, it is easy to carry, and the effect with Wet-dry
Really.
5th, the present invention have height security, can widely, safely be applied to eye and lip.
Compared with prior art, gentle disposable make-up remover of the invention overcomes the various shortcoming of traditional makeup removal products, adopts
With all oil system, the high nonionic surfactant of security has been selected as emulsifying agent, while from PEF and dextrin
Palmitate mixes and emulsified coefficient principle as thick stabilization system using similar, with efficient makeup removing, mildness
It is high, disposable, without excellent properties such as preservatives.
Brief description of the drawings
Fig. 1 is the cleaning capacity test result of the make-up remover of the present invention.
Embodiment
Technical scheme is described in further detail with reference to specific embodiment, but protection scope of the present invention
It is not limited in following examples.
Each component is weighed according to following mass percent, following each component can be bought by commercial channel and be obtained.
The preparation method of make-up remover described in embodiment 1~3, its step is as follows：
(1) by the polyethylene in said components, dextrin palmitate, caprylic/capric triglyceride, PEG-10 isostearic acids
Ester, PEG-20 glyceryl triisostearates, cetanol ethylhexoate are added in emulsification pot, open stirring；
(2) 84 DEG C~88 DEG C are warming up to, 10 minutes are incubated, mixing speed is maintained at 300 revs/min, vacuumizes, homogeneous 5
Minute；
(3) phenyl trimethicone, tocopherol acetate are sequentially added in emulsification pot, opens stirring, mixing is equal
It is even, cooling；
(4) when being down to 70 DEG C~75 DEG C, discharging；
(5) examine qualified, heat filling.
Makeup removing merit rating：
The make-up remover of embodiment 1~3 is determined respectively by following procedure to BB frosts, the cleaning capacity of eyeliner.
It is 7.2cm × 2.6cm models that 50mg BB frosts and 50mg eyeliners are equably applied into area on slide respectively
In enclosing, five groups are smeared altogether, respectively blank group, reference examples, the embodiment 2 of embodiment 1 and embodiment 3, every group by two pieces of difference
The slide of BB frosts and eyeliner, totally 10 pieces of slides were smeared, and weighs and records weight M1.10 pieces of slides are placed in
Taken out after being air-dried one day in 40 DEG C of biochemical cultivation cases.With the net beautiful clean skin liquid complete wetting makeup removing cottons of Bei Dema (Bioderma) (about
1g), apply respectively in the region that BB frosts and eyeliner are scribbled on slide, the make-up remover of additional embodiment 1~3 respectively takes about
0.5g in makeup removing cotton on, and uniform fold scribbling BB frost and eyeliner region in, wait 3 minutes after, with makeup removing cotton back and forth
Rinsed after rubbing 10 times with running water, all slides are placed in 40 DEG C of biochemical cultivation cases and air-dried 15 minutes by flushing after finishing,
Finally claim slide weight M once again2, and keep a record.Clean rate is calculated by below equation.
Fig. 1 shows and rubbed 10 times when with makeup removing cotton that the make-up remover of embodiment 1~3 is clear to two kinds of long wear cosmetics respectively
Clean rate all reaches more than 50%, and the especially makeup removing rate to eyeliner has reached 92%, and 66% is higher by than makeup remover clean rate.Because
Eyeliner contains the poly- trimethicone of film forming agent methyl or macromolecular colloid acrylic acid (ester) class/poly- diformazan of silicones class
Radical siloxane copolymer, the solvent of these products is typically ring five dimethyl silicone polymer, therefore the make-up remover of the present invention is because containing
The phenyl trimethicone composition good with its intermiscibility, which can be unloaded preferably, to be removed, and containing only common surfactant and many
The cleaning capacity of the relatively simple makeup remover of the compositions such as first alcohol is then poor.
In addition, the picture under microscope is shown, there is a wax crystallization than larger piece commercially available prod, and the embodiment of the present invention 1~3
Make-up remover without large stretch of wax crystallization, this phenomenon is solved well, makes the stability of product and to smear sense more excellent
It is different.
Product mildness and safety evaluation (human skin patch result)
Evaluation method：
1) tested material：The make-up remover of embodiment 1~3.
2) negative control：Blank control.
3) subject：Totally 40 people, male 15 people, the people of female 25,18~30 years old age, meet subject's aspiration inclusion criteria.
4) spot method for testing：Try device from qualified spot, in closed patch test method, by tested material about 0.02ml~
0.025ml is applied in spot examination device, and external application special adhesive tape is pasted on the bent side of subject's forearm, and tested material is removed after 24 hours, in going
Except 30min after tested material spot examination device, after observing dermoreaction after impression disappearance, press《Cosmetics health specification》(version in 2007)
Middle dermoreaction grade scale records its result.
5) evaluation of result：According to the form below (skin adverse reaction grade scale) records reaction result.
6) result of the test is as shown in the table：
Cosmetics human skin patch result
Table 2
Human skin patch result is shown：In the make-up remover of embodiment 1~3,40 subjects skins are all in the moon
Property reaction (grading system：0 grade).Foundation《Cosmetics health specification》(version in 2007) human body skin class patch experiment criterion,
Sample is to human body without skin adverse reaction.And in reference examples (commercially available internationally renowned brand make-up remover), there are 2 subjects to occur 1
Order reaction.It can be seen that, make-up remover mildness of the invention is high, and security is good.
Product stability is assessed
1. temperature stability test
(1) 48 DEG C of stability test：
Test sample：The make-up remover of embodiment 1~3
Testing time：4 weeks
Method of testing：Product (content) is fitted into 30mL PET bottle, it is labelled, indicate name of product, formula
Number, the information such as test condition, testDate, be placed in the heat-resistant stability of test product in 48 DEG C of biochemical cultivation case, exist respectively
The outward appearance of (recover to room temperature) observation product, smell, pH, the change of viscosity at 24 hours, 1 week, 2 weeks, 4 weeks, and by day part
Change, be recorded into report.
(2) 40 DEG C of stability tests：
Test sample：The make-up remover of embodiment 1~3
Testing time：12 weeks
Method of testing：Product (content) is fitted into 30mL PET bottle, it is labelled, indicate name of product, formula
Number, the information such as test condition, testDate, be placed in the heat-resistant stability of test product in 40 DEG C of biochemical cultivation case, exist respectively
The outward appearance of (recovery to room temperature) observation product, smell, pH, the change of viscosity at 24 hours, 1 week, 2 weeks, 4 weeks, 8 weeks and 12 weeks,
And the change of day part is recorded into report.
(3) room temperature (Ambient) stability test：
Test sample：The make-up remover of embodiment 1~3
Testing time：12 weeks
Method of testing：Product (content) is fitted into 30mL PET bottle, it is labelled, indicate name of product, formula
Number, the information such as test condition, testDate, be placed in sample cabinet, respectively 24 hours (surveying pH value, viscosimetric), 1 week, 2 weeks,
The outward appearance of observation product, smell, pH, the change of viscosity when 4 weeks, 8 weeks and 12 weeks (survey pH value), and by the change of day part, remember
In typing report.
(4) -18 DEG C of stability tests：
Test sample：The make-up remover of embodiment 1~3
Testing time：12 weeks
Method of testing：Product (content) is fitted into 30mL PET bottle, it is labelled, indicate name of product, formula
Number, the information such as test condition, testDate, be placed in the cold-resistant stability of test product in -18 DEG C of refrigerators, respectively 24 hours,
The outward appearance of (recovery to room temperature) observation product, smell, pH, the change of viscosity at 1 week, 2 weeks, 4 weeks, 8 weeks and 12 weeks, and when will be each
The change of section, is recorded into report.
(5) 48 DEG C and -18 DEG C of cyclical stability tests
Test sample：1 or more
Testing time：Continuous three loop tests (after first being placed 24 hours in 48 DEG C of biochemical cultivation cases, are put at room temperature
Put 24 hours, be then placed within -18 DEG C of refrigerators 24 hours, then recover to be one to room temperature again to circulate and observe result).
Method of testing：Product (content) is fitted into 30mL PET bottle, it is labelled, indicate name of product, formula
Number, the information such as test condition, testDate, be placed in 48 DEG C of biochemical cultivation case 24 hours, recover to room temperature to place 24 hours,
It is subsequently placed in -18 DEG C of refrigerators 24 hours, then recovers again to room temperature.Observe product when resisting cold heat-resisting alternate cycles product it is outer
The change of sight, smell, pH, viscosity etc., and be recorded into report.
2. sun light stability test
Test sample：The make-up remover of embodiment 1~3
Testing time：4 weeks
Sun optical tests, product (content) is fitted into 30mL PET bottle, labelled, indicates name of product, formula
Number, the information such as test condition, testDate, be placed on west place near the window (label facing away from sunshine), it is small 24 respectively
When, 1 week, 2 weeks, 4 weeks when the outward appearance of (recover to room temperature) observation product, the change of smell, and by the change of day part, be recorded into
In report.
As a result show, by the above stability test of 12 weeks, the stability of the make-up remover of embodiment 1~3 was preferable.
Claims (4)
1. a kind of gentle disposable make-up remover, it is characterised in that consist of the following components in percentage by weight：
Polyethylene 2%~10%, cetanol ethylhexoate 2%~20%, PEG-10 isostearates 2%~20%, PEG-
20 glyceryl triisostearates 2%~20%, tocopherol acetate 0.2%~1%, phenyl trimethicone 2%~
10%, dextrin palmitate 0.2%~3.0%, surplus is caprylic/capric triglyceride.
2. make-up remover according to claim 1, it is characterised in that consist of the following components in percentage by weight：
Polyethylene 2%~6%, cetanol ethylhexoate 2%~8%, PEG-10 isostearates 2%~5%, PEG-20 is sweet
Oily three isostearates 10%~20%, tocopherol acetate 0.2%~0.5%, phenyl trimethicone 5%~
10%, dextrin palmitate 1%~3%, surplus is caprylic/capric triglyceride.
3. make-up remover according to claim 1, it is characterised in that consist of the following components in percentage by weight：
Polyethylene 6%~10%, cetanol ethylhexoate 2%~20%, PEG-10 isostearates 2%~20%, PEG-
20 glyceryl triisostearates 2%~20%, tocopherol acetate 0.5%~1%, phenyl trimethicone 2%~
10%, dextrin palmitate 0.2%~1%, surplus is caprylic/capric triglyceride.
4. the preparation method of any one of claims 1 to 3 make-up remover, it is characterised in that its step is as follows：
(1) by polyethylene, dextrin palmitate, caprylic/capric triglyceride, PEG-10 isostearates, PEG-20 glycerine three
Isostearate, cetanol ethylhexoate are added, stirring；
(2) 84 DEG C~88 DEG C are warming up to, 10 minutes are incubated, mixing speed is maintained at 300 revs/min, vacuumizes, homogeneous 5 minutes；
(3) phenyl trimethicone, tocopherol acetate are sequentially added, opens stirring, be well mixed, cooling；
(4) when being down to 70 DEG C~75 DEG C, discharging.
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| CN105534755A (en) * | 2016-01-13 | 2016-05-04 | 广州丹奇日用化工厂有限公司 | Refreshing mild cleansing cream and preparation method thereof |
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