CN104777186A - Device for measuring rock hot line swelling coefficient by using pressure tester - Google Patents

Device for measuring rock hot line swelling coefficient by using pressure tester Download PDF

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CN104777186A
CN104777186A CN201510182750.XA CN201510182750A CN104777186A CN 104777186 A CN104777186 A CN 104777186A CN 201510182750 A CN201510182750 A CN 201510182750A CN 104777186 A CN104777186 A CN 104777186A
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silica gel
rock
gel heating
heating sheet
testing machine
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CN104777186B (en
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苏国韶
彭立锋
邹亚峰
秦子华
胡小川
鲁和
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Guangxi University
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Abstract

The invention provides a device for measuring a rock hot line swelling coefficient by using a pressure tester. The device comprises a rock test sample, a silica gel heating piece heating device, a single-shaft pressure tester, a heat-preservation and heat-insulation cushion, a heat-preservation and heat-insulation layer, a digital readout thermoelectric couple sensor and a digital readout thermoelectric couple reader, wherein a round hole is formed in the axis center of the top surface of the rock test sample; a line guide groove is formed in the top surface of the rock test sample; silica gel heating pieces are stuck at the periphery of the side face of the rock test sample; a temperature control thermoelectric couple sensor is fixed on the outer sides of the silica gel heating pieces; the heat-preservation and heat-insulation layer covers the outer parts of the silica gel heating pieces; the digital readout thermoelectric couple sensor is located in the round hole; and the rock test sample is arranged on the single-shaft pressure tester. According to the device, the pressure tester is used for measuring the rock hot line swelling coefficient; compared with existing other devices, the time needed by single time of determining can be shortened very well; and the problem of cooling heating equipment does not need to be considered, and the determination of the next test sample can be directly carried out, so that the efficient measurement of the rock hot line swelling coefficient in an engineering design is realized.

Description

A kind of device utilizing pressure testing machine to measure rock fever linear expansion coefficient
Technical field
The present invention relates to the hotline expansion coefficient field of measuring technique of rock mechanics experiment, more specifically relate to a kind of device utilizing pressure testing machine to measure rock fever linear expansion coefficient.
Background technology
The thermophysical property of rock, all has important theory and realistic meaning in the engineering construction in such as deep-lying tunnel, geothermal anomaly area, nuclear waste disposal, geothermal exploitation and deep coalmining and stone cultural artifact protection.And along with the development of underground works, the problem relating to rock fever mechanics relevant is also constantly being emerged in large numbers, such as temperature often changes the terrestrial stress change that 1 DEG C can produce 0.4 ~ 0.5MPa, temperature raises the terrestrial stress change produced will produce considerable influence to the mechanical property of rock mass, therefore, the research of the development law of rock material mechanical characteristic under the effect of temperature field just becomes of crucial importance.Wherein the hotline expansion coefficient of rock is as one of the important parameter of rock fever physical characteristics, is indispensable in rock fever mechanical characteristic analysis study and practice.
At present, for solid material, the measurement of hotline expansion coefficient has multiple method, has contactless and contact measurement method.Due to contactless measurement, it utilizes optical signalling to measure, and principle relative complex is often not suitable for the measurement of rock type materials.And contact measurement method uses most often by directly measuring the deflection of a free sample under temperature variation condition at present, again divided by temperature variation, realize the measurement of the hotline expansion coefficient of rock in this temperature range, the method principle is simple, but remains in some problems in application.The many employing oil of the method or water-bath are heated rock sample, measure rear firing equipment and water or oil by these heating means all to need to lower the temperature, the mensuration of next sample can be carried out afterwards, cause the general hotline expansion coefficient that can only measure a rock sample for a day, consuming time comparatively large, bring inconvenience to measurement.
Publication number is that the patent of invention of CN103235002A discloses a kind of rock thermal expansion coefficient testing device, the proving installation of this invention adopts connecting structure and built-in oil type of heating, strain bar is adopted to be equipped with high precision foil gauge, axial expansion strain after measurement rock sample is heated, realize the measurement of rock fever expansion coefficient, although this device inventive principle and the upper all fairly simple convenience of operation, but, a sample can only be measured at every turn, rear furnace chamber and deep fat cooling rate are measured comparatively slow, directly the measurement of the next sample of impact.In addition, publication number is measuring method and the measurement mechanism that the patent of invention of CN103868947A discloses a kind of 0 ~ 60 DEG C of rock thermal linear expansion coefficient, by arranging water bath with thermostatic control circulating control device, gradin alternating temperature water-bath circulating control device, be pasted with the aluminum alloy sample of conductor temperature self compensation resistance strain gage, temperature sensor, the devices such as precision data registering instrument and computing machine, with the aluminum alloy specimen of known hotline expansion coefficient, the thermal expansivity of foil gauge and the reliability of measuring method are verified, and by pasting the rock fever linear expansion coefficient value of the strain value acquisition degree of precision that foil gauge monitors to rock sample institute, although this invention can obtain the rock fever linear expansion coefficient of degree of precision, but the hotline expansion coefficient that this invention measures a rock sample generally needs 1 ~ 2 day time, exist equally with water-bath circulating-heating and measured the slower problem of rear firing equipment cooling rate, and the method measurement result rely on foil gauge in a way paste quality, if find that in mensuration process foil gauge is pasted to go wrong just to need to do over again, bring a lot of inconvenience so just to measurement rock fever linear expansion coefficient.
Summary of the invention
For above-mentioned existing problems, the object of the present invention is to provide a kind of device utilizing pressure testing machine to measure rock fever linear expansion coefficient, solve the problems referred to above and the deficiency of the existence of existing method, and meeting under the requirement of underground rock engineering design for rock fever linear expansion coefficient measuring accuracy, reduce the time cost that rock fever linear expansion coefficient is measured further.
In order to achieve the above object, the present invention is by the following technical solutions:
Utilize pressure testing machine to measure a device for rock fever linear expansion coefficient, comprise rock sample, silica gel heating sheet heating arrangement, uniaxial tension testing machine, insulation pad, heat insulation layer, digital display thermocouple sensor and digital display thermocouple readings device;
There is circular hole at the end face axle center place of described rock sample, and the end face of rock sample is provided with wire lead slot, and described wire lead slot is communicated with the edge of circular hole and rock sample;
Described silica gel heating sheet heating arrangement comprises silica gel heating sheet, silica gel heating sheet temperature controller and temperature-control heat couple sensor, described silica gel heating sheet is pasted on rock sample side surrounding, and be fastened by fiberglass adhesive tape, silica gel heating sheet is connected with silica gel heating sheet temperature controller by silica gel heating sheet wire; Described temperature-control heat couple sensor is fixed on outside silica gel heating sheet, and temperature-control heat couple sensor is connected with silica gel heating sheet temperature controller by temperature-control heat couple sensor conductor; Silica gel heating sheet outer wrap has heat insulation layer;
Described digital display thermocouple sensor is arranged in circular hole, and digital display thermocouple sensor is connected with digital display thermocouple readings device by digital display thermocouple wire, and digital display thermocouple sensor wire is embedded in wire lead slot; Described rock sample is positioned on uniaxial tension testing machine, is provided with insulation pad between rock sample end face and uniaxial tension testing machine and between rock sample bottom surface and uniaxial tension testing machine; Silica gel heating sheet wire, temperature-control heat couple sensor conductor and digital display thermocouple sensor wire are all drawn from the crack of heat insulation layer and insulation pad.
The degree of depth of described circular hole is 1/4 ~ 1/2 times of rock sample height; The size of the diameter of circular hole and digital display thermocouple sensor and digital display thermocouple sensor wire adapts.
The thickness of described heat insulation layer is 30 ~ 100mm.
The thickness of described insulation pad is 1 ~ 3mm.
The material of described heat insulation layer is insulating rubber plastic, and described insulation pad is silica gel rubber cushion.
After the sample that mensuration to be removed is good, the next sample assembled is positioned on uniaxial tension testing machine, directly can carries out the measurement of next sample hotline expansion coefficient.Described uniaxial tension testing machine is building laboratory conventional equipment, without the need to repacking, can directly use.
The principle of scheme of the present invention is as follows:
Along with temperature variation, for the thermal deformation that a free sample will produce, if will produce thermal stress when thermal deformation suffers restraints, hotline expansion coefficient conventional determining method measures heat distortion amount, then obtain the hotline expansion coefficient of sample divided by temperature variation.But for rock material, the thermal stress in measuring tempeature change procedure is feasible equally, and relatively simpler, because load has transferability, can not change because there is web member centre.Therefore, in elastic hot deformation process, directly do not measure deflection, but by measuring constraint thermal deformation and the resistibility that produces, then divided by the elastic modulus of material and resistibility active area, just can obtain heat distortion amount and the hotline expansion coefficient of material.Wherein, elastic modulus is material basic mechanical parameter, it is generally acknowledged known, also can be obtained by Rock Under Uniaxial Compression compression test in standard chamber.
When utilizing pressure testing machine to measure rock fever linear expansion coefficient, the shape and size choosing tested sample are required according to measurement elastic modulus of rock related specifications, can be right cylinder or square body, cylinder diameter or the square body length of side are preferably 48 ~ 54mm, and test specimen ratio of height to diameter should control 2.0 ~ 2.5.
The circular hole of certain depth and diameter is drilled through at sample end face axle center place, and a wire lead slot is gone out along end face axle center to fringe radiation, for putting thermocouple sensor monitoring sample axle center temperature, wrap heated for controlling temperature equipment at sample outside surface again and take effective Insulation, according to standard uniaxial compression experimental technique tested sample being placed on uniaxial tension testing machine and carrying out temperature control heating.Along with the rising of temperature, sample has the trend of expansion, but owing to cannot be expanded by testing machine constraint at two ends, cause sample inside to produce the power of opposing expansion, and react on testing machine, testing machine just can monitor the size of this resistibility by force snesor.To monitor temperature under sample original state for reference point, record and arrive preset temperature value and the change value of steady grab sample internal resistance bulging force, utilize formula below can the hotline expansion coefficient of Calculating material:
α = ΔF EAΔT
Wherein, α is hotline expansion coefficient, and unit is 10 -6/ DEG C; Δ T is the temperature difference of preset temperature value point and temperature reference point, and unit is DEG C; Δ F is that load corresponding to temperature variation is poor, and unit is kN; A is tested sample cross-sectional area, and unit is m 2; E is tested sample elastic modulus, and unit is GPa.
When carrying out hotline expansion coefficient based on uniaxial tension testing machine and measuring, it should be noted that, need to ensure that rock sample is in impaction state and the thermoelastic distortion stage of pressurized all the time within the scope of whole measuring tempeature, therefore, certain prestrain will be carried out before tested sample is heated, but the sample elasticity limit must be less than, generally be taken as about 5% of failing load, like this along with temperature constantly raises, pressure load can slowly increase, until reach stable, record corresponding temperature and loads change value, the hot line roc exhibition coefficient value of tested sample can be recorded according to formula above.
Owing to have employed technique scheme, tool following points beneficial effect of the present invention:
(1) the present invention is based on uniaxial tension testing machine, by changing according to standard uniaxial tension experimental technique monitoring rock interior thermal stress the rock sample assembled, realize the object measuring rock fever linear expansion coefficient, principle is simple, it is convenient to measure, and the present invention directly measures tested sample axle center internal temperature, ensure that thermometric precision, thus the accuracy of hotline expansion coefficient measurement result can be ensured.
(2) the present invention uses controllable temperature silica gel heating sheet to heat, and adopts rubber and plastic to carry out insulation, easy and simple to handle, safe and reliable, and can realize implementing to heat more quickly to rock sample, can measure a sample in the short period of time.
(3) equipment and instrument used in the present invention or material, all laboratory conventional equipment or material as uniaxial tension testing machine, silica gel heating sheet heating arrangement and rubber and plastic heat preserving and insulating material, can directly use in mensuration process, without the need to researching and developing new instrument and equipment or new material, this can make greatly to have saved financial cost when measuring sample hotline expansion coefficient.
(4) the present invention utilizes pressure testing machine to measure rock fever linear expansion coefficient, compared with other devices existing, the time required for unitary determination can be shortened preferably, and do not need the problem considering firing equipment cooling, directly can carry out the mensuration of next sample, realize the efficient measurement of rock fever linear expansion coefficient in engineering design.
(5) in addition, multiple sample can be prepared, after a Specimen Determination completes, without the need to carrying out radiating treatment in mensuration process, directly can carry out the measurement of the hotline expansion coefficient of next sample, this reduces the time cost that rock fever linear expansion coefficient is measured to a great extent.Although this device proposes for rock, in fact not by the restriction of material, can measure the hotline expansion coefficient of other compressible materials.Generally speaking, the present invention has simple, that measurement efficiency is high advantage.
Accompanying drawing explanation
Fig. 1 is the device schematic diagram utilizing pressure testing machine to measure rock fever linear expansion coefficient of the present invention;
Fig. 2 is the device sample manuscript utilizing pressure testing machine to measure rock fever linear expansion coefficient of the present invention;
Fig. 3 is the device tested sample wiring layout utilizing pressure testing machine to measure rock fever linear expansion coefficient of the present invention;
Fig. 4 is the device tested sample assembling plan view utilizing pressure testing machine to measure rock fever linear expansion coefficient of the present invention;
Fig. 5 is the device silica gel heating sheet heating arrangement schematic diagram utilizing pressure testing machine to measure rock fever linear expansion coefficient of the present invention.
Wherein: uniaxial tension testing machine 1, insulation pad 2, rock sample 3, silica gel heating sheet 4, heat insulation layer 5, temperature-control heat couple sensor 6, digital display thermocouple sensor 7, circular hole 8, wire lead slot 9, digital display thermocouple sensor wire 10, digital display thermocouple readings device 11, temperature-control heat couple sensor conductor 12, silica gel heating sheet wire 13, silica gel heating sheet temperature controller 14, AC power 15.
Embodiment
Below in conjunction with Figure of description, be measured as example with the hotline expansion coefficient measuring Wuzhou grouan rock sample, technical scheme of the present invention is described further.
Embodiment 1
Utilize pressure testing machine to measure a device for rock fever linear expansion coefficient, comprise rock sample 3, silica gel heating sheet heating arrangement, uniaxial tension testing machine 1, insulation pad 2, heat insulation layer 5, digital display thermocouple sensor 7 and digital display thermocouple readings device 11;
There is circular hole 8 at the end face axle center place of described rock sample 3, and the end face of rock sample 3 is provided with wire lead slot 9, and described wire lead slot 9 is communicated with the edge of circular hole 8 and rock sample 3;
Described silica gel heating sheet heating arrangement comprises silica gel heating sheet 4, silica gel heating sheet temperature controller 14 and temperature-control heat couple sensor 6, described silica gel heating sheet 4 is pasted on rock sample 3 side surrounding, and be fastened by fiberglass adhesive tape, silica gel heating sheet 4 is connected with silica gel heating sheet temperature controller 14 by silica gel heating sheet wire 13; Described temperature-control heat couple sensor 6 is fixed on outside silica gel heating sheet 4, and temperature-control heat couple sensor 6 is connected with silica gel heating sheet temperature controller 14 by temperature-control heat couple sensor conductor 12; Silica gel heating sheet 4 outer cover is equipped with heat insulation layer 5;
Described digital display thermocouple sensor 7 is arranged in circular hole 8, and digital display thermocouple sensor 7 is connected with digital display thermocouple readings device 11 by digital display thermocouple sensor wire 10, and digital display thermocouple sensor wire 10 is embedded in wire lead slot 9; Described rock sample 3 is positioned on uniaxial tension testing machine 1, is provided with insulation pad 2 between rock sample 3 end face and uniaxial tension testing machine and between rock sample 3 bottom surface and uniaxial tension testing machine 1; Silica gel heating sheet wire 13, temperature-control heat couple sensor conductor 12 and digital display thermocouple sensor wire 11 are all drawn from heat insulation layer 5 and the crack of insulation pad 2.
The degree of depth of described circular hole 8 is 1/4 ~ 1/2 times of rock sample 3 height; The size of the diameter of circular hole 8 and digital display thermocouple sensor 7 and digital display thermocouple sensor wire 10 adapts.
The thickness of described heat insulation layer 5 is 30 ~ 100mm.
The thickness of described insulation pad 2 is 1 ~ 3mm.
The material of described heat insulation layer is insulating rubber plastic, and described insulation pad is silica gel rubber cushion.
Embodiment 2
Utilize device of the present invention to carry out the method measured, according to sequencing, comprise the following steps:
1. rock sample processing: choose cylindrical grouan sample 3, diameter of section 50mm, high 100mm; Drill through the degree of depth at grouan sample 3 end face axle center place be 35mm and diameter is the circular hole 8 of 3mm, and go out along end face axle center to fringe radiation one wide and be deeply the wire lead slot 9 of 3mm;
2. silica gel heating sheet heating arrangement is installed: silica gel heating sheet 4 is pasted on grouan sample 3 side surrounding, and is fastened with fiberglass adhesive tape, silica gel heating sheet 4 is connected with silica gel heating sheet temperature controller 14 by silica gel heating sheet wire 13; Temperature-control heat couple sensor 6 fiberglass adhesive tape is fixed on test coupon bottom surface 65mm At The Height, temperature-control heat couple sensor 6 lower end is basic and circular hole 8 bosom is high together, and temperature-control heat couple sensor 6 is connected with silica gel heating sheet temperature controller 14 by temperature-control heat couple sensor conductor 12; Silica gel heating sheet heating arrangement as shown in Figure 5, can directly commercially or customization, and wherein heat length of a film 155mm, wide 98mm is slightly less than the height of sample 3;
3. wrap up heat insulation layer: determine that heating plate 4 is pasted smooth without after bulge projection, the heat insulation layer 5 of 80mm thickness in heating plate 4 outer wrap, heat insulation layer 5 is rubber-plastics material;
4. electroheat pair is installed: the circular hole 8 li digital display thermocouple sensor 7 being placed in grouan sample 3, digital display thermocouple sensor 7 is connected with digital display thermocouple readings device 11 by digital display thermocouple sensor wire 10, and digital display thermocouple sensor wire 10 is placed in wire lead slot 9;
5. install: the grouan sample 3 assembled as shown in Figure 4, is positioned on uniaxial tension testing machine 1, insulation pad 2 on grouan sample 3 end face and bottom surface pad; Silica gel heating sheet wire 13, temperature-control heat couple sensor conductor 12 and digital display thermocouple sensor wire 10 are all drawn from heat insulation layer 5 and the crack of insulation pad 2;
6. prestrain: start uniaxial tension testing machine 1 pair of rock sample 3 and apply initial load, and keep initial load size to stablize 15 ~ 30min, then record initial load value F 0with the axle center initial temperature T of rock sample 3 0;
7. add temperature measurement: the power supply 15 being communicated with silica gel heating sheet 4, needed the finishing temperature applied by the setting of silica gel heating sheet temperature controller 14, the present embodiment is set to 60 DEG C; After the stress and temperature stabilization of rock sample 3, record end of a period payload values F 1with the axle center finishing temperature T of rock sample 3 1;
8. calculate hotline expansion coefficient: the hotline expansion coefficient α value utilizing the tested rock of formulae discovery below,
α = F 1 - F 0 EA ( T 1 - T 0 )
In formula, A is the cross-sectional area of tested rock sample 3, and E is the elastic modulus of tested rock sample 3.
After taking off the grouan sample 3 measured, the next sample assembled is positioned on uniaxial tension testing machine, without the need to cooling down, directly can carry out the measurement of next sample hotline expansion coefficient, the measurement of the hotline expansion coefficient of 1 grouan sample 3 is consuming time is 125 minutes.
Test result is in table 1, and the measurement result of the PCY-C MEASURING THE THERMAL EXPANSION COEFFICIENT instrument produced with Xiang Tan Xiang Yi Instrument Ltd. is for benchmark, and the measurement relative error of device of the present invention is 2.8%.
In addition, the hotline expansion coefficient of other the 5 kinds of rocks utilizing the present invention to obtain is in table 1, and the measurement result of the PCY-C MEASURING THE THERMAL EXPANSION COEFFICIENT instrument produced with Xiang Tan Xiang Yi Instrument Ltd. is for benchmark, and maximum relative error of the present invention is 3.1%,
Meet the accuracy requirement needed for underground engineering design.
The measurement result of table 1 apparatus of the present invention and analyzer contrasts

Claims (6)

1. the device utilizing pressure testing machine to measure rock fever linear expansion coefficient, it is characterized in that, comprise rock sample, silica gel heating sheet heating arrangement, uniaxial tension testing machine, insulation pad, heat insulation layer, digital display thermocouple sensor and digital display thermocouple readings device;
There is circular hole at the end face axle center place of described rock sample, and the end face of rock sample is provided with wire lead slot, and described wire lead slot is communicated with the edge of circular hole and rock sample;
Described silica gel heating sheet heating arrangement comprises silica gel heating sheet, silica gel heating sheet temperature controller and temperature-control heat couple sensor, described silica gel heating sheet is pasted on rock sample side surrounding, and be fastened by fiberglass adhesive tape, silica gel heating sheet is connected with silica gel heating sheet temperature controller by silica gel heating sheet wire; Described temperature-control heat couple sensor is fixed on outside silica gel heating sheet, and temperature-control heat couple sensor is connected with silica gel heating sheet temperature controller by temperature-control heat couple sensor conductor; Silica gel heating sheet outer wrap has heat insulation layer;
Described digital display thermocouple sensor is arranged in circular hole, and digital display thermocouple sensor is connected with digital display thermocouple readings device by digital display thermocouple wire, and digital display thermocouple sensor wire is embedded in wire lead slot; Described rock sample is positioned on uniaxial tension testing machine, is provided with insulation pad between rock sample end face and uniaxial tension testing machine and between rock sample bottom surface and uniaxial tension testing machine; Silica gel heating sheet wire, temperature-control heat couple sensor conductor and digital display thermocouple sensor wire are all drawn from the crack of heat insulation layer and insulation pad.
2. the device utilizing pressure testing machine to measure rock fever linear expansion coefficient according to claim 1, is characterized in that: the degree of depth of described circular hole is 1/4 ~ 1/2 times of rock sample height; The size of the diameter of circular hole and digital display thermocouple sensor and digital display thermocouple sensor wire adapts.
3. the device utilizing pressure testing machine to measure rock fever linear expansion coefficient according to claim 1, is characterized in that: the thickness of described heat insulation layer is 30 ~ 100mm.
4. the device utilizing pressure testing machine to measure rock fever linear expansion coefficient according to claim 1, is characterized in that: the thickness of described insulation pad is 1 ~ 3mm.
5. the device utilizing pressure testing machine to measure rock fever linear expansion coefficient according to claim 1, is characterized in that: the material of described heat insulation layer is insulating rubber plastic.
6. the device utilizing pressure testing machine to measure rock fever linear expansion coefficient according to claim 1, is characterized in that: described insulation pad is silica gel rubber cushion.
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CN112903740A (en) * 2021-01-22 2021-06-04 中国石油大学(华东) Device and method for measuring thermal expansion coefficient of rock under confining pressure

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CN106885726A (en) * 2015-12-16 2017-06-23 鞍钢股份有限公司 Method for connecting multi-axis large-deformation sample with thermocouple
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CN107352054B (en) * 2017-06-19 2019-11-29 北京空间飞行器总体设计部 A kind of ground tooling of heat stabilization test deformation decoupling
CN111044556A (en) * 2019-12-18 2020-04-21 河海大学 Method and device for measuring load temperature strain coefficient of concrete sample at high temperature
CN112903740A (en) * 2021-01-22 2021-06-04 中国石油大学(华东) Device and method for measuring thermal expansion coefficient of rock under confining pressure

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