CN104758209A - Facial mask liquid improving wrinkle - Google Patents
Facial mask liquid improving wrinkle Download PDFInfo
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- CN104758209A CN104758209A CN201510119067.1A CN201510119067A CN104758209A CN 104758209 A CN104758209 A CN 104758209A CN 201510119067 A CN201510119067 A CN 201510119067A CN 104758209 A CN104758209 A CN 104758209A
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Abstract
The invention discloses a facial mask liquid improving wrinkle. By means of combination usage of hydrolysised corn protein peptide and mung bean protein hydrolysate with other various pure natural plant extraction liquids, a certain synergistic effect can be achieved, so that the facial mask liquid has a great anti-wrinkling effect and a function of promoting regeneration of skin. In addition, the facial mask liquid has a silk-like skin feeling so that the facial mask liquid is quite suitable for being used as a facial mask liquid. On the basis of the total mass of the facial mask liquid, the facial mask liquid comprises following components, by mass: 5-6% of the hydrolysised corn protein peptide, 3-5% of the mung bean protein hydrolysate, 1% of aloe extract, 1-2% of chrysanthemum indicum extract, 1-2% of sophora flavescens extract, 1-2% of angelica sinensis extract, 0.2-0.8% of atractylodes macrocephala extract and 0.2-0.3% of 1,2-hexylene glycol.
Description
Technical field
The present invention relates to a kind of facial mask liquid, particularly relate to that a kind of safety has no side effect, that there is good improvement wrinkle effect facial mask liquid, relate to the preparation method of above-mentioned facial mask liquid simultaneously.
Background technology
Everybody has a love of beauty.Along with growth in the living standard, the pursuit of people to U.S. is also more and more higher.Reduce wrinkle is the one of existing society beauty treatment.People, due to factors such as age growth, operating pressures, cause skin easily to occur fold, and in order to keep youth slow down aging here, just occurred the fashion beauty treatment maneuver removing wrinkle, this is one of high-end embodiment maneuver of one of existing fashionable element.
At cosmetic field, now comparatively effective wrinkle removing raw material or product price very high, as EGF epidermal growth factor etc., only have high-grade expensive product just can use.
Hydrolysed corn albumen oligopeptide (Hydyolyzed cornprotein), INCI title: hydrolysed corn albumen Hydyolyzed cornprotein, CAS:73049-73-7, price only about 70 yuan one kilogram, from wholefood---the protein extracted Semen Maydis, then through micromolecule polypeptide material that directed enzyme action and specific little peptide isolation technics obtain.Form from aminoacid, the aminoacid composition of corn peptide forms with the aminoacid of zein and has parallel relation, is rich in glutamic acid (Glu), alanine (Ala), leucine (Leu), proline (Pro).The same with other vegetable protein, the antioxidation of maize oligopeptide excellence, defying age and moisture-keeping functions.But when being used alone, its anti-wrinkle effect is very not obvious, does not almost observe.
Hydrolysis Semen phaseoli radiati albumen polypeptide, INCI title: hydrolysis Semen phaseoli radiati albumen HydrolyzedMungbeanProtein, CAS:100209-45-8, price is also only about 70 yuan one kilogram, be that raw material adopts advanced biological enzyme hydrolysis technique with Semen phaseoli radiati albumen, through enzymolysis, refining low molecular polypeptide, utilize HPLC Accurate Measurement sample protein molecular weight distribution, its molecular weight is mainly distributed between 408.41 ~ 1830.64.Semen phaseoli radiati peptide is rich in each seed amino acid, especially lysine content more very, research worker carries out the preliminary study of whitening and anti-oxidation efficacy to Semen phaseoli radiati polypeptide liquid, result shows, when sample concentration is 10%, tyrosinase inhibition rate is 49.98%, DPPH free radical scavenging activity be 69.14%, OH (hydroxyl Bai Youji) clearance rate is 58.62%.Equally, when being used alone, its anti-wrinkle effect is very not obvious, does not almost observe.
The present invention is in long-term practice, and find conbined usage Semen Maydis hydrolyzed protein and Semen phaseoli radiati polypeptide liquid, and during other multiple pure natural plant extracting solution, can reach certain synergism, it has the crease-resistant of highly significant, promotes the effect of promoting epidermization.In addition, skinfeel silk is sliding, is very suitable as facial mask liquid.Therefore, the present invention aims to provide a kind of raw material natural green, with low cost, and anti-wrinkle effect is good, can promote the facial mask liquid of skin regeneration.
Summary of the invention
The present invention is directed to the problem of current anti-wrinkle product high cost, provide a kind of facial mask liquid of improvement wrinkle newly.
Hydrolysed corn albumen oligopeptide (Hydyolyzed cornprotein) is from wholefood---the protein extracted Semen Maydis, then through micromolecule polypeptide material that directed enzyme action and specific little peptide isolation technics obtain.Form from aminoacid, the aminoacid composition of corn peptide forms with the aminoacid of zein and has parallel relation, is rich in glutamic acid (Glu), alanine (Ala), leucine (Leu), proline (Pro).The same with other vegetable protein, the antioxidation of maize oligopeptide excellence, defying age and moisture-keeping functions.
Hydrolysis Semen phaseoli radiati albumen polypeptide, be that raw material adopts advanced biological enzyme hydrolysis technique with Semen phaseoli radiati albumen, through enzymolysis, refining low molecular polypeptide, utilize HPLC Accurate Measurement sample protein molecular weight distribution, its molecular weight is mainly distributed between 408.41 ~ 1830.64.Semen phaseoli radiati peptide is rich in each seed amino acid, especially lysine content more very, research worker carries out the preliminary study of whitening and anti-oxidation efficacy to Semen phaseoli radiati polypeptide liquid, result shows, when sample concentration is 10%, tyrosinase inhibition rate is 49.98%, DPPH free radical scavenging activity be 69.14%, OH (hydroxyl Bai Youji) clearance rate is 58.62%.
Aloe is the one of Cycas revoluta, Aloe various in style, wherein fresh Aloe extraction solution is most good merchantable brand, it is a kind of wholefood, medicine, cosmetics additive of mystery, containing abundant skin-nourishing element, as various active compositions such as vitamin, aminoacid, glucoside, choline saccharide, compound mucopolysaccharide, protein, mineral, enzyme, aloin, aloe-emodins.
Flos Chrysanthemi Indici extracting solution is the head titbit of feverfew Herba Dendranthematis indici.Containing acacetin-7-rhamnose Fructus Vitis viniferae glycoside, Flos Chrysanthemi Indici lactone, Chrysanthemin, bitter principle, chrysol, chrysanthone, northern Camphora, another containing retinoid material and vitamin B1, there is balanced fat secretion, suppress anti-pox, prevent that powder is perverse, the effect of bactericidal antiphlogistic.
Radix Angelicae Sinensis, return, cloud is returned, and is the root of umbelliferae angelica by Thailand for another name.Be perennial herb, have strong fragrance, sweet in the mouth, pungent, micro-hardship.Medical science thinks that Radix Angelicae Sinensis includes multiple volatile oil, vitamin B complex, organic aliphatic acid, β-sitosterol, ligustilide, sesquiterpenoids.Having enriches blood adjusts effect of blood, menstruction regulating and pain relieving, loosening bowel to relieve constipation, for diseases such as blood deficiency and yellow complexion, dizzy cardiopalmus, menoxenias.It is the cosmetics additive of whitening and speckle dispelling ideal now
The Rhizoma Atractylodis Macrocephalae, Classification system Atractylodes macrocephala.Another name small wooden raft Ji, Rhizoma Atractylodis Macrocephalae, the winter Rhizoma Atractylodis Macrocephalae, wash rice art, poplar small wooden raft, Wu Shu, sheet art, Rhizoma Atractylodis etc., belong to catananche.The nice and cool weather of happiness, is used as medicine with rhizome, has multinomial medicinal function.Mainly be distributed in the mountain area wetlands such as Sichuan, Yunnan, Guizhou.Its Main Ingredients and Appearance containing volatile oil, atractylol, atractylone and vitamin A, the main diuresis of its pharmacology, reduces blood glucose, anticoagulant, strong human body and antibacterial action.
Technical scheme of the present invention is as follows:
Improve a facial mask liquid for wrinkle, relative to the gross mass of facial mask liquid, containing following component:
Hydrolysised corn protein peptide 5-6%; Hydrolysis Semen phaseoli radiati albumen liquid 3-5%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 1%-2%; Radix Sophorae Flavescentis extractive liquid 1%-2%; Radix Angelicae Sinensis extracting solution 1-2%; Rhizoma Atractylodis Macrocephalae extracting solution 0.2%-0.8%; 1,2-hexanediol 0.2%-0.3%.
Preferably, in described facial mask liquid, relative to the gross mass of facial mask liquid, also containing following component:
Transparent HANSHENGJIAO 0.05%-0.2%; Water-soluble azone 0.5%-2.0%; Glycyrrhizic acid dipotassium 0.3%-0.5%.
Preferably, in described facial mask liquid, relative to the gross mass of facial mask liquid, composed of the following components:
Hydrolysised corn protein peptide 5%; Hydrolysis Semen phaseoli radiati albumen liquid 3%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 1%; Radix Sophorae Flavescentis extractive liquid 2%; Radix Angelicae Sinensis extracting solution 1%; Rhizoma Atractylodis Macrocephalae extracting solution 0.8%; 1,2-hexanediol 0.3%; Water-soluble azone 0.8% and glycyrrhizic acid dipotassium 0.1%;
Improve a preparation method for the facial mask liquid of wrinkle, comprise the following steps:
(1) during heating water to 95 DEG C, vacuum suction, in emulsifying pot, adds transparent HANSHENGJIAO homogenizing process 4 minutes under processing condition;
(2) when temperature is reduced to below 40 DEG C, add in emulsifying pot and add hydrolysised corn protein peptide 5-6% with the gross mass of relative facial mask liquid; Hydrolysis Semen phaseoli radiati albumen liquid 3-5%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 1%-2%; Radix Sophorae Flavescentis extractive liquid 1%-2%; Radix Angelicae Sinensis extracting solution 1-2%; Rhizoma Atractylodis Macrocephalae extracting solution 0.2%-0.8%; 1,2-hexanediol 0.2%-0.3%; Water-soluble azone 0.8% and glycyrrhizic acid dipotassium 0.1%;
(3) be down to room temperature, complete the preparation to facial mask liquid.
Preferably, in the preparation method of the facial mask liquid of described improvement wrinkle, described hydrolysised corn protein peptide 5%; Hydrolysis Semen phaseoli radiati albumen liquid 3%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 1%; Radix Sophorae Flavescentis extractive liquid 2%; Radix Angelicae Sinensis extracting solution 1%; Rhizoma Atractylodis Macrocephalae extracting solution 0.8%; 1,2-hexanediol 0.3%, water-soluble azone 1% and glycyrrhizic acid dipotassium 0.2%.
Usefulness of the present invention is:
1, facial mask liquid of the present invention has outstanding improvement wrinkle, promotes effect of epidermal growth.
2, facial mask liquid processing technology of the present invention is simple, with low cost.
3, facial mask liquid of the present invention is not containing ethanol, and antiseptic, raw material natural green, without any side effects, facial mask liquid of the present invention is absorbed by mask carriers, and facial film applies comfortable ventilating on facial skin, and skinfeel is good.
Accompanying drawing explanation
Fig. 1 is the cell photo after facial mask liquid process NIH-3T3 mouse fibril cell of the present invention.
Detailed description of the invention
The all raw materials of the present invention can be obtained by conventional method, as " enzymatic hydrolysis of Semen phaseoli radiati albumen ", " food research and development " the 3rd phase in 2007, also can be buied by commercially available.And plant extraction liquid is as Flos Chrysanthemi Indici extracting solution, Radix Angelicae Sinensis extracting solution etc. also can extract by conventional method, also have the product that a large amount of company's supplies is relevant on the market.
The extracting solution that all embodiments of the present invention are used is purchased from Sheng Tong bio tech ltd, Guangzhou.
Embodiment 1:
Improve a preparation method for the facial mask liquid of wrinkle, comprise the following steps:
During heating water to 95, vacuum suction is in emulsifying pot, adds transparent HANSHENGJIAO homogenizing process 4 minutes under processing condition;
When temperature is reduced to below 40 DEG C, adds in emulsifying pot and add hydrolysised corn protein peptide 5% with the gross mass of relative facial mask liquid; Hydrolysis Semen phaseoli radiati albumen liquid 3%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 1%; Radix Sophorae Flavescentis extractive liquid 2%; Radix Angelicae Sinensis extracting solution 1%; Rhizoma Atractylodis Macrocephalae extracting solution 0.8%; 1,2-hexanediol 0.3%; Water-soluble azone 0.8% and glycyrrhizic acid dipotassium 0.1%;
Be down to room temperature, complete the preparation to facial mask liquid.
In described step one, relative to the gross mass of facial mask liquid, the additional proportion of transparent HANSHENGJIAO is 0.5%.
The all extracting solution of the present invention are purchased from Sheng Tong bio tech ltd, Guangzhou.
Embodiment 2:
Improve a preparation method for the facial mask liquid of wrinkle, comprise the following steps:
During heating water to 95, vacuum suction is in emulsifying pot, adds transparent HANSHENGJIAO homogenizing process 4 minutes under processing condition;
When temperature is reduced to below 40 DEG C, adds in emulsifying pot and add hydrolysised corn protein peptide 6% with the gross mass of relative facial mask liquid; Hydrolysis Semen phaseoli radiati albumen liquid 4%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 2%; Radix Sophorae Flavescentis extractive liquid 1%; Radix Angelicae Sinensis extracting solution 2%; Rhizoma Atractylodis Macrocephalae extracting solution 0.4%; 1,2-hexanediol 0.2%; Water-soluble azone 0.8% and glycyrrhizic acid dipotassium 0.1%;
Be down to room temperature, complete the preparation to facial mask liquid.
In described step one, relative to the gross mass of facial mask liquid, the additional proportion of transparent HANSHENGJIAO is 0.3%.
Embodiment 3:
Improve a preparation method for the facial mask liquid of wrinkle, comprise the following steps:
During heating water to 95, vacuum suction is in emulsifying pot, adds transparent HANSHENGJIAO homogenizing process 4 minutes under processing condition;
When temperature is reduced to below 40 DEG C, adds in emulsifying pot and add hydrolysised corn protein peptide 5% with the gross mass of relative facial mask liquid; Hydrolysis Semen phaseoli radiati albumen liquid 5%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 1%; Radix Sophorae Flavescentis extractive liquid 2%; Radix Angelicae Sinensis extracting solution 1%; Rhizoma Atractylodis Macrocephalae extracting solution 0.6%; 1,2-hexanediol 0.3%; Water-soluble azone 0.8% and glycyrrhizic acid dipotassium 0.1%;
Be down to room temperature, complete the preparation to facial mask liquid.
In described step one, relative to the gross mass of facial mask liquid, the additional proportion of transparent HANSHENGJIAO is 0.4%.
Embodiment 4:
Improve a preparation method for the facial mask liquid of wrinkle, comprise the following steps:
During heating water to 95, vacuum suction is in emulsifying pot, adds transparent HANSHENGJIAO homogenizing process 4 minutes under processing condition;
When temperature is reduced to below 40 DEG C, adds in emulsifying pot and add hydrolysised corn protein peptide 6% with the gross mass of relative facial mask liquid; Hydrolysis Semen phaseoli radiati albumen liquid 3%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 2%; Radix Sophorae Flavescentis extractive liquid 1%; Radix Angelicae Sinensis extracting solution 2%; Rhizoma Atractylodis Macrocephalae extracting solution 0.5%; 1,2-hexanediol 0.2%; Water-soluble azone 0.8% and glycyrrhizic acid dipotassium 0.1%;
Be down to room temperature, complete the preparation to facial mask liquid.
In described step one, relative to the gross mass of facial mask liquid, the additional proportion of transparent HANSHENGJIAO is 0.5%.
Embodiment 5:
Improve a preparation method for the facial mask liquid of wrinkle, comprise the following steps:
During heating water to 95, vacuum suction is in emulsifying pot, adds transparent HANSHENGJIAO homogenizing process 4 minutes under processing condition;
When temperature is reduced to below 40 DEG C, adds in emulsifying pot and add hydrolysised corn protein peptide 5% with the gross mass of relative facial mask liquid; Hydrolysis Semen phaseoli radiati albumen liquid 4%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 1%; Radix Sophorae Flavescentis extractive liquid 2%; Radix Angelicae Sinensis extracting solution 1%; Rhizoma Atractylodis Macrocephalae extracting solution 0.2%; 1,2-hexanediol 0.2%; Water-soluble azone 0.8% and glycyrrhizic acid dipotassium 0.1%;
Be down to room temperature, complete the preparation to facial mask liquid.
In described step one, relative to the gross mass of facial mask liquid, the additional proportion of transparent HANSHENGJIAO is 0.5%.
Embodiment 6:
(1) SRB test
SRB test is a cell proliferation colorimetric test.The NIH-3T3 mouse fibril cell proliferation quantity promoted by facial mask liquid of the present invention is measured by OD590nm.
In not containing the DMEM of serum, process 72 hours by the facial mask liquid of the present embodiment, matched group 1-3 carries out process 72 hours equally with the hydrolysed corn albumen oligopeptide of 10% and the hydrolysis Semen phaseoli radiati polypeptide of 10% respectively.
Found that, increase without obvious before the sample cell density of matched group and process, all obviously increase after the facial mask liquid process of the present embodiment 1-5, especially embodiment 1 can be observed increases very significantly.
As shown in Figure 1, the left side is the cell density of matched group, and the right is the cell density after the present embodiment 1 processes.
(2) skin micro-relief image analysis
20 volunteers, test in 30 days, the facial film application that forearm uses facial mask liquid of the present invention to make 15 minutes, first time uses latter 24 hours, use end after 12 hours with last, on skin pull (silica replica), measure wrinkle depth with image analytical method.
Result is as shown in table 1:
Table 1
Visible, facial mask liquid of the present invention has extraordinary improvement result to deep wrinkles, and instant effect, the especially formula of embodiment 1.
(3) toxicology test
Mice is selected to carry out toxicology test, result:
Acute oral toxicity: nontoxic
25% aqueous solution
Eye irritation: tolerate very much
25% aqueous solution
Sensitization test (STT): without sensitization
25% aqueous solution
Single epidermis patch test: fabulous toleration
25% aqueous solution
Result shows, and facial mask liquid of the present invention has very excellent skin-tolerant.
The above; be only the present invention's preferably detailed description of the invention; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (4)
1. improve a facial mask liquid for wrinkle, it is characterized in that: relative to the gross mass of facial mask liquid, containing following component:
Hydrolysised corn protein peptide 5-6%; Hydrolysis Semen phaseoli radiati albumen liquid 3-5%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 1%-2%; Radix Sophorae Flavescentis extractive liquid 1%-2%; Radix Angelicae Sinensis extracting solution 1-2%; Rhizoma Atractylodis Macrocephalae extracting solution 0.2%-0.8%; 1,2 hexanediol 0.2%-0.3%.
2. the facial mask liquid improving wrinkle according to claim 1, is characterized in that: relative to the gross mass of facial mask liquid, containing following component:
Hydrolysed corn protein liquid 5%; Hydrolysis Semen phaseoli radiati albumen liquid 3%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 1%; Radix Sophorae Flavescentis extractive liquid 2%; Radix Angelicae Sinensis extracting solution 1%; Rhizoma Atractylodis Macrocephalae extracting solution 0.8%; 1,2-hexanediol 0.3%, water-soluble azone 1% and glycyrrhizic acid dipotassium 0.2%.
3. improve a preparation method for the facial mask liquid of wrinkle, comprise the following steps:
(1) during heating water to 95 DEG C, vacuum suction, in emulsifying pot, adds transparent HANSHENGJIAO homogenizing process 4 minutes under processing condition;
(2) when temperature is reduced to below 40 DEG C, add in emulsifying pot and add hydrolysised corn protein peptide 5-6% with the gross mass of relative facial mask liquid; Hydrolysis Semen phaseoli radiati albumen liquid 3-5%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 1%-2%; Radix Sophorae Flavescentis extractive liquid 1%-2%; Radix Angelicae Sinensis extracting solution 1-2%; Rhizoma Atractylodis Macrocephalae extracting solution 0.2%-0.8%; 1,2-hexanediol 0.2%-0.3%;
(3) be down to room temperature, complete the preparation to facial mask liquid.
4. the preparation method improving the facial mask liquid of wrinkle according to claim 3, is characterized in that: according to the gross mass of relative facial mask liquid, described hydrolysised corn protein peptide 5%; Hydrolysis Semen phaseoli radiati albumen liquid 3%; Aloe extraction solution 1%; Flos Chrysanthemi Indici extracting solution 1%; Radix Sophorae Flavescentis extractive liquid 2%; Radix Angelicae Sinensis extracting solution 1%; Rhizoma Atractylodis Macrocephalae extracting solution 0.8%; 1,2-hexanediol 0.3%, water-soluble azone 1% and glycyrrhizic acid dipotassium 0.2%.
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| CN201510119067.1A CN104758209B (en) | 2015-03-18 | 2015-03-18 | A kind of facial mask liquid for improving wrinkle |
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| CN201510119067.1A CN104758209B (en) | 2015-03-18 | 2015-03-18 | A kind of facial mask liquid for improving wrinkle |
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| CN104758209B CN104758209B (en) | 2018-05-08 |
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| CN106860269A (en) * | 2017-01-19 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment anti-aging suncream |
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