CN104722234B - Carbon nano tube dispersion device - Google Patents
Carbon nano tube dispersion device Download PDFInfo
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- CN104722234B CN104722234B CN201410772773.1A CN201410772773A CN104722234B CN 104722234 B CN104722234 B CN 104722234B CN 201410772773 A CN201410772773 A CN 201410772773A CN 104722234 B CN104722234 B CN 104722234B
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- ejector
- carbon nano
- nano tube
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Abstract
The invention discloses a carbon nano tube dispersion device belonging to the field of dispersion of nano materials. The device is mainly composed of a carbon nano tube spraying device, an airflow channel and a collection device. A liquefied gas working medium in the carbon nano tube spraying device enters the inner part of a carbon nano tube; in an application process, a nozzle switch is switched on so that the clustered carbon nano tube can be sufficiently dispersed by using the phase change of the working medium; a heating belt and a stirring paddle are used for realizing the aims of heating and sufficiently mixing, and the dispersion of the carbon nano tube is complete in the process and the pollution to the carbon nano tube is not caused; the dispersed carbon nano tube is driven by the flowing of the gas working medium to move to a bottom collection device of the device in the airflow channel; and the collection device is driven by a magnetic stirring device so that the carbon nano tube is uniformly dispersed in a collection process. The dispersion effect on the carbon nano tube is good and the efficiency is high, the device is simple and convenient to control and the use and maintenance costs are low.
Description
Technical field
The present invention relates to a kind of CNT dispersal device, especially relating to one kind makes the dispersed acquisition of CNT
The device of a large amount of single-root carbon nano-tubes, belongs to the field of dispersions of nano material.
Background technology
CNT, is nano level tube-like materials that graphite flake crimps according to certain helical angle, a diameter of.It has
Very big draw ratio, heat exchange performance alongst is preferable, and the heat exchange performance of its vertical direction is relatively low, utilizes
Its anisotropy passes through suitable orientation, it is possible to obtain have the composite of superior heat conductivility.But due between CNT
There is stronger Van der Waals force, along with its very big draw ratio, lead to it easily to reunite during production and application
Thus reducing its performance.And when using, often can be only achieved preferable use by fully dispersed for the aggregate of CNT
Effect.The dispersing apparatus of CNT mainly realize the dispersion of CNT using sonic oscillation, ball mill etc. at present.By making
With the said equipment dispersing Nano carbon tubes have dispersion not thoroughly, longevity of service, have necessarily destructive and dispersion to CNT
The low shortcoming of efficiency.
Chinese invention patent CN201310434933 provides a kind of CNT dispersal device based on draft flowing deformation, leads to
Cross cyclically-varying cavity volume volume, so that CNT and the mixture of epoxy resin is constantly compressed and loosen, obtain scattered
CNT.Though this kind of device can prepare the CNT of good dispersion, due to CNT and epoxy in work process
Mixed with resin, is unfavorable for application in other materials for the CNT.
Content of the invention
Deficiency that is uneven in the dispersion carrying out occurring during CNT dispersion for prior art, easily mixing with medium,
The invention provides a kind of efficient, device of free of contamination dispersing Nano carbon tubes, achievable CNT is dispersed, device letter
Single control is convenient, using and maintenance cost low.
To achieve these goals, the technical solution adopted for the present invention to solve the technical problems is：
A kind of CNT dispersal device is mainly made up of ejector, gas channel and collection device, wherein ejector
Specifically including charging plug, disk, stirring bracing strut, heating tape, heat-insulation layer, shaft, shell, stirring paddle, valve on ejector
Disk, valve, nozzle under control bar, stirring motor, working medium charge door, ejector；Gas channel and collection device specifically include
Pipe cap, ejector support, ejector, valve controling rod, nozzle, gas channel, sample presentation door, perforated trays, magnetic stirring apparatuses,
Air stream outlet passage, magnetic stirring apparatuses shell.Stirring motor is connected with ejector disk and is fixed on shell, shaft
It is connected with disk under stirring paddle and ejector, is fixed on shell by stirring bracing strut, cage connection has working medium charge door, adds
Material plug and valve, heating tape is wound in outer surface of outer cover, outer wrap heat-insulation layer, and valve passes through valve controling rod controlling switch shape
State, exit is connected to nozzle.Ejector is fixed in gas channel by ejector support, and gas channel upper end is sealed by pipe cap
Stifled, lower end is provided with feeding door, and magnetic stirring apparatuses are fixed on perforated trays lower end, perforated trays by magnetic stirring apparatuses shell
It is fixed in gas channel, valve controling rod one end is connected with valve, the other end is placed in outside gas channel convenient control, gas channel
Bottom is provided with air stream outlet passage.
The invention has the beneficial effects as follows, there is provided a kind of device of effective dispersing Nano carbon tubes.The present invention is to CNT
Dispersion effect is good and efficiency high, and device is simply easy to control, using and maintenance cost low.
Brief description
Fig. 1 is CNT dispersal device structure chart,
Fig. 2 is emitter construction figure,
In figure：1. pipe cap, 2. ejector support, 3. ejector, 4. valve controling rod, 5. nozzle, 6. gas channel, 7. send
Sample door, 8. perforated trays, 9. magnetic stirring apparatuses, 10. air stream outlet passage, 11. magnetic stirring apparatuses shells, 12. charging plugs,
Disk on 13. ejectors, 14. stirring bracing struts, 15. heating tapes, 16. heat-insulation layers, 17 shafts, 18. shells, 19. stirring paddles,
21. stirring motors, 22. working medium charge doors, disk under 23. ejectors, 24. valves.
Specific embodiment
Specific implementation that the present invention is further described below in conjunction with the accompanying drawings：
With reference to shown in Fig. 1, Fig. 2, a kind of CNT dispersal device is mainly by ejector 3, gas channel 6 and collection device
Composition it is characterised in that：Ejector specifically include charging plug 12, disk 13 on ejector, stirring bracing strut 14, heating tape 15,
Heat-insulation layer 16, shaft 17, shell 18, stirring paddle 19, valve controling rod 4, stirring motor 21, working medium charge door 22, ejector
Lower disk 23, valve 24, nozzle 5；Collection device specifically includes pipe cap 1, ejector support 2, sample presentation door 7, perforated trays 8, magnetic
Power agitating device 9, air stream outlet passage 10, magnetic stirring apparatuses shell 11；Stirring motor 21 is connected with disk 13 on ejector
And be fixed on shell 18, shaft 17 is connected with disk 23 under stirring paddle 19 and ejector, fixing by stirring bracing strut 14
On shell 18, shell 18 is connected with working medium charge door 22, charging plug 12 and valve 24, and heating tape 15 is wound in shell 18 appearance
Face, outer wrap heat-insulation layer 16, valve 24 passes through valve controling rod 4 controlling switch state, and exit is connected to nozzle 5；Ejector 3
It is fixed in gas channel 6 by ejector support 2, gas channel 6 upper end is blocked by pipe cap 1, and lower end is provided with sample presentation door 7,
Magnetic stirring apparatuses 9 are fixed on perforated trays 8 lower end by magnetic stirring apparatuses shell 11, and perforated trays 8 are fixed on air-flow and lead to
In road, valve controling rod 4 one end is connected with valve 24, and the other end is placed in the outer convenient control of gas channel 6, and gas channel 6 bottom sets
There is air stream outlet passage 10.
Operation principle of the present invention and work process are：
Open pipe cap 1, by plug 12, the working medium charge door 22 of feeding, add CNT and liquid refrigerant respectively, unlatching is stirred
Mixing motor 21 drives disk 13 on ejector to rotate, and makes disk 23 under ejector, shaft 17 and stirring paddle by magnetic force occlusion
19 synchronous axial system, stirring content prevents from being layered.Open sample presentation door 7, the open containers holding sample are placed in perforated trays 8
On, close sample presentation door 7 and pipe cap 1, electricity work, heated injectors 3 are given in heating tape 15, and magnetic stirring apparatuses are made to sample to electrician
Be stirred, open valve controling rod 4 make ejector 3 content be atomized spray, scattered CNT by sample reception and with
Uniform mixing.
Claims (1)
1. a kind of CNT dispersal device, is mainly made up of ejector (3), gas channel (6) and collection device, its feature exists
In：Ejector specifically includes charging plug (12), disk (13), stirring bracing strut (14), heating tape (15), heat-insulation layer on ejector
(16), shaft (17), shell (18), stirring paddle (19), valve controling rod (4), stirring motor (21), working medium charge door
(22), disk (23), valve (24), nozzle (5) under ejector；Collection device specifically include pipe cap (1), ejector support (2),
Sample presentation door (7), perforated trays (8), magnetic stirring apparatuses (9), air stream outlet passage (10), magnetic stirring apparatuses shell (11)；
Stirring motor (21) is connected with disk on ejector (13) and is fixed on shell (18), and shaft (17) is connected with stirring paddle
(19) disk (23) and under ejector, are fixed on shell (18) by stirring bracing strut (14), shell (18) is connected with working medium
Charge door (22), charging plug (12) and valve (24), heating tape (15) are wound in shell (18) outer surface, outer wrap heat-insulation layer
(16), valve (24) passes through valve controling rod (4) controlling switch state, and exit is connected to nozzle (5)；Ejector (3) passes through spray
Emitter support (2) is fixed in gas channel (6), and gas channel (6) upper end is passed through pipe cap (1) and blocked, and lower end is provided with sample presentation door
(7), magnetic stirring apparatuses (9) are fixed on perforated trays (8) lower end, perforated trays (8) by magnetic stirring apparatuses shell (11)
It is fixed in gas channel, valve controling rod (4) one end is connected with valve (24), the other end is placed in gas channel (6) and facilitates outward control
System, gas channel (6) bottom is provided with air stream outlet passage (10).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410772773.1A CN104722234B (en) | 2014-12-12 | 2014-12-12 | Carbon nano tube dispersion device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410772773.1A CN104722234B (en) | 2014-12-12 | 2014-12-12 | Carbon nano tube dispersion device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104722234A CN104722234A (en) | 2015-06-24 |
| CN104722234B true CN104722234B (en) | 2017-02-15 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410772773.1A Active CN104722234B (en) | 2014-12-12 | 2014-12-12 | Carbon nano tube dispersion device |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105057122A (en) * | 2015-07-19 | 2015-11-18 | 青岛科技大学 | Carbon nanotube dispersing equipment with cyclone separator |
| CN107297182A (en) * | 2015-09-10 | 2017-10-27 | 青岛科技大学 | A kind of CNT dispersing apparatus with electrostatic precipitator |
| KR102010459B1 (en) * | 2016-01-20 | 2019-08-13 | 주식회사 엘지화학 | Carbon nanotube pellet and method for manufacturing same |
| CN106040075A (en) * | 2016-06-20 | 2016-10-26 | 青岛科技大学 | Nanometer material scattering device |
| CN106955629B (en) * | 2017-03-28 | 2022-07-15 | 青岛科技大学 | Nano material dispersion devices |
| CN111686623B (en) * | 2020-06-17 | 2022-04-22 | 中铁二院重庆勘察设计研究院有限责任公司 | Carbon nanotube dispersion equipment for preparing concrete |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6921462B2 (en) * | 2001-12-17 | 2005-07-26 | Intel Corporation | Method and apparatus for producing aligned carbon nanotube thermal interface structure |
| JP2005334808A (en) * | 2004-05-28 | 2005-12-08 | Fuji Photo Film Co Ltd | Ultrasonic dispersing apparatus |
| CN100388967C (en) * | 2004-12-02 | 2008-05-21 | 鸿富锦精密工业（深圳）有限公司 | Particle dispersing method and its device |
| CN102225320B (en) * | 2011-03-25 | 2014-11-26 | 泉州师范学院 | Dispersing device for micron/nano-particle suspension |
| CN103521115B (en) * | 2012-07-04 | 2016-01-20 | 深圳市尚水智能设备有限公司 | A kind of dispersal device |
| CN204338085U (en) * | 2014-12-12 | 2015-05-20 | 青岛科技大学 | A kind of carbon nanotube dispersed device |
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| CN104722234A (en) | 2015-06-24 |
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