CN104694178A - Method for preparing fuel oil - Google Patents
Method for preparing fuel oil Download PDFInfo
- Publication number
- CN104694178A CN104694178A CN201510050645.0A CN201510050645A CN104694178A CN 104694178 A CN104694178 A CN 104694178A CN 201510050645 A CN201510050645 A CN 201510050645A CN 104694178 A CN104694178 A CN 104694178A
- Authority
- CN
- China
- Prior art keywords
- parts
- raw material
- vegetable oil
- oil
- agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000295 fuel oil Substances 0.000 title claims abstract description 9
- 238000000034 method Methods 0.000 title claims description 5
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 33
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000002994 raw material Substances 0.000 claims abstract description 20
- 239000003921 oil Substances 0.000 claims abstract description 17
- 239000000654 additive Substances 0.000 claims abstract description 11
- 230000000996 additive effect Effects 0.000 claims abstract description 11
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 11
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 11
- 239000002002 slurry Substances 0.000 claims abstract description 9
- 239000000446 fuel Substances 0.000 claims description 20
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 20
- 239000008158 vegetable oil Substances 0.000 claims description 20
- 235000019198 oils Nutrition 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 16
- 102000004895 Lipoproteins Human genes 0.000 claims description 10
- 108090001030 Lipoproteins Proteins 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 10
- 239000013543 active substance Substances 0.000 claims description 10
- 239000003245 coal Substances 0.000 claims description 10
- 239000003350 kerosene Substances 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 8
- 239000000047 product Substances 0.000 claims description 8
- 150000001412 amines Chemical class 0.000 claims description 4
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 4
- 229930195729 fatty acid Natural products 0.000 claims description 4
- 239000000194 fatty acid Substances 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 229920001083 polybutene Polymers 0.000 claims description 4
- -1 sorbitan fatty acid ester Chemical class 0.000 claims description 4
- 239000006228 supernatant Substances 0.000 claims description 4
- 235000021355 Stearic acid Nutrition 0.000 claims description 3
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 3
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 3
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims description 3
- 239000008117 stearic acid Substances 0.000 claims description 3
- 229920002472 Starch Polymers 0.000 claims description 2
- 235000019698 starch Nutrition 0.000 claims description 2
- 239000008107 starch Substances 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 abstract description 10
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 230000000694 effects Effects 0.000 abstract description 2
- 239000010742 number 1 fuel oil Substances 0.000 abstract 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 abstract 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 abstract 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 abstract 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 abstract 1
- 239000005642 Oleic acid Substances 0.000 abstract 1
- 239000000853 adhesive Substances 0.000 abstract 1
- 230000001070 adhesive effect Effects 0.000 abstract 1
- 239000013064 chemical raw material Substances 0.000 abstract 1
- 238000004939 coking Methods 0.000 abstract 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 abstract 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
- 235000019871 vegetable fat Nutrition 0.000 abstract 1
- 235000013311 vegetables Nutrition 0.000 abstract 1
- 239000000470 constituent Substances 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- 239000002283 diesel fuel Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003209 petroleum derivative Substances 0.000 description 1
Landscapes
- Liquid Carbonaceous Fuels (AREA)
Abstract
The invention discloses a fuel oil and relates to the technical field of chemical raw material preparation. The fuel oil comprises the following raw materials in parts by weight: 6-14 parts of coal oil, 20-40 parts of vegetable fat, 3-7 parts of vegetable oleic acid, 10-16 parts of fine oil tar, 10-25 parts of methanol, 1-8 parts of surfactant, 5-15 parts of modified additive, 85-95 parts of coal oil slurry, 6-10 parts of low-level ether, 0.1-1.0 part of anti coking agent, and 0.5-1.5 parts of emulsifier. The fuel oil prepared by the invention has the beneficial effects of simple and convenient preparation process, high fuel oil quality, good energy-saving performance and environment protection without pollution, strong adhesive force and obvious using effect simultaneously in the application.
Description
Technical field
The present invention relates to industrial chemicals preparing technical field, be specifically related to a kind of preparation method of oil fuel.
Background technology
Major part petroleum products all can be used as fuel, but oil fuel has different explanations in different areas.Europe generally refers to the concept of oil fuel the dark viscous residue that crude oil stays through distillation, or it and compared with the admixture of light constituent, main be used as steam oven and various process furnace fuel or as big, slow diesel oil fuel and as various industrial fuel, oil fuel is in the processing of reality, due to the character of itself raw material, can there is pollution, and preparation is very difficult, the demand of producing fast can not be met.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of formula rationally, environment friendly and pollution-free, the preparation method of the oil fuel that preparation method is simple.
Technical problem to be solved by this invention realizes by the following technical solutions:
A kind of oil fuel, is characterized in that: the raw material composition comprising following weight part:
Kerosene 6-14 part; Vegetable oil lipoprotein 20-40 part, vegetable oil acid 3-7 part, smart tar 10-16 part, methyl alcohol 10-25 part, tensio-active agent 1-8 part, property-modifying additive 5-15 part, coal liquifaction slurry 85-95 part, rudimentary ether 6-10 part, anticoking agent 0.1-1.0 part, emulsifying agent 0.5-1.5 part.
Preferred weight part of each raw material is: kerosene 10 parts; Vegetable oil lipoprotein 30 parts, vegetable oil acid 5 parts, 14 parts, smart tar, methyl alcohol 20 parts, 4 parts, tensio-active agent, property-modifying additive 10 parts, coal liquifaction starch 90 parts, 8 parts, rudimentary ether, anticoking agent 0.5 part, emulsifying agent 1 part.
Described tensio-active agent is the one in stearic acid and Sodium dodecylbenzene sulfonate; Described property-modifying additive is polybutene amine; Described emulsifying agent is sorbitan fatty acid ester.
Another object of the present invention prepares the method for oil fuel in the present invention, it is characterized in that, comprise the following steps:
A, select one with the reactor of agitator, in reactor, then add important kerosene and Vegetable oil lipoprotein in formula open and stir, until mix completely;
B, the vegetable oil acid in raw material, smart tar and methyl alcohol all to be added in reactor, to stir and after being heated to 60-80 DEG C, isothermal reaction 2-4h;
C, after above-mentioned steps b reaction terminates, reactor is cooled to 20-25 DEG C, adds wherein, standing 5-10h after stirring by the coal liquifaction slurry in raw material and rudimentary ether;
Mixed aid is obtained for subsequent use after d, tensio-active agent, property-modifying additive, anticoking agent and emulsifying agent by raw material carry out pre-mixing;
E, until step c leave standstill terminate after, take out supernatant liquid, then by steps d mixed aid add wherein, after fully stirring, the product obtained is the present invention's fuel oil product to be prepared, packs and puts in storage.
The invention has the beneficial effects as follows: the oil fuel prepared in the present invention, it has preparation technology simple and convenient, and the quality of oil fuel is high, and good energy saving property is environment friendly and pollution-free, and in the application, strong adhesion, result of use is obvious simultaneously.
Embodiment
The technique means realized to make the present invention, creation characteristic, reaching object and effect is easy to understand, below in conjunction with specific embodiment, setting forth the present invention further.
Embodiment 1
A kind of oil fuel, comprises the raw material composition of following weight part:
Kerosene 6-14kg; Vegetable oil lipoprotein 20-40kg, vegetable oil acid 3-7kg, smart tar 10-16kg, methyl alcohol 10-25kg, Sodium dodecylbenzene sulfonate 1-8kg, polybutene amine 5-15kg, coal liquifaction slurry 85-95kg, rudimentary ether 6-10kg, anticoking agent 0.1-1.0kg, sorbitan fatty acid ester 0.5-1.5kg.
Its preparation method is:
A, select one with the reactor of agitator, in reactor, then add important kerosene and Vegetable oil lipoprotein in formula open and stir, until mix completely;
B, the vegetable oil acid in raw material, smart tar and methyl alcohol all to be added in reactor, to stir and after being heated to 60-80 DEG C, isothermal reaction 2-4h;
C, after above-mentioned steps b reaction terminates, reactor is cooled to 20-25 DEG C, adds wherein, standing 5-10h after stirring by the coal liquifaction slurry in raw material and rudimentary ether;
Mixed aid is obtained for subsequent use after d, tensio-active agent, property-modifying additive, anticoking agent and emulsifying agent by raw material carry out pre-mixing;
E, until step c leave standstill terminate after, take out supernatant liquid, then by steps d mixed aid add wherein, after fully stirring, the product obtained is the present invention's fuel oil product to be prepared, packs and puts in storage.
Embodiment 2
A kind of oil fuel, comprises the raw material composition of following weight part:
Kerosene 10kg; Vegetable oil lipoprotein 30kg, vegetable oil acid 5kg, smart tar 14kg, methyl alcohol 20kg, stearic acid 4kg, polybutene amine 10kg, coal liquifaction slurry 90kg, rudimentary ether 8kg, anticoking agent 0.5kg, sorbitan fatty acid ester 1kg.
Its preparation method is:
A, select one with the reactor of agitator, in reactor, then add important kerosene and Vegetable oil lipoprotein in formula open and stir, until mix completely;
B, the vegetable oil acid in raw material, smart tar and methyl alcohol all to be added in reactor, to stir and after being heated to 60-80 DEG C, isothermal reaction 2-4h;
C, after above-mentioned steps b reaction terminates, reactor is cooled to 20-25 DEG C, adds wherein, standing 5-10h after stirring by the coal liquifaction slurry in raw material and rudimentary ether;
Mixed aid is obtained for subsequent use after d, tensio-active agent, property-modifying additive, anticoking agent and emulsifying agent by raw material carry out pre-mixing;
E, until step c leave standstill terminate after, take out supernatant liquid, then by steps d mixed aid add wherein, after fully stirring, the product obtained is the present invention's fuel oil product to be prepared, packs and puts in storage.
More than show and describe ultimate principle of the present invention and principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (4)
1. an oil fuel, is characterized in that: the raw material composition comprising following weight part: kerosene 6-14 part; Vegetable oil lipoprotein 20-40 part, vegetable oil acid 3-7 part, smart tar 10-16 part, methyl alcohol 10-25 part, tensio-active agent 1-8 part, property-modifying additive 5-15 part, coal liquifaction slurry 85-95 part, rudimentary ether 6-10 part, anticoking agent 0.1-1.0 part, emulsifying agent 0.5-1.5 part.
2. a kind of oil fuel according to claim 1, is characterized in that: preferred weight part of each raw material is: kerosene 10 parts; Vegetable oil lipoprotein 30 parts, vegetable oil acid 5 parts, 14 parts, smart tar, methyl alcohol 20 parts, 4 parts, tensio-active agent, property-modifying additive 10 parts, coal liquifaction starch 90 parts, 8 parts, rudimentary ether, anticoking agent 0.5 part, emulsifying agent 1 part.
3. a kind of oil fuel according to claim 1, is characterized in that: described tensio-active agent is the one in stearic acid and Sodium dodecylbenzene sulfonate; Described property-modifying additive is polybutene amine; Described emulsifying agent is sorbitan fatty acid ester.
4. prepare a method for any one oil fuel in claim 1 and 2, it is characterized in that, comprise the following steps:
A, select one with the reactor of agitator, in reactor, then add important kerosene and Vegetable oil lipoprotein in formula open and stir, until mix completely;
B, the vegetable oil acid in raw material, smart tar and methyl alcohol all to be added in reactor, to stir and after being heated to 60-80 DEG C, isothermal reaction 2-4h;
C, after above-mentioned steps b reaction terminates, reactor is cooled to 20-25 DEG C, adds wherein, standing 5-10h after stirring by the coal liquifaction slurry in raw material and rudimentary ether;
Mixed aid is obtained for subsequent use after d, tensio-active agent, property-modifying additive, anticoking agent and emulsifying agent by raw material carry out pre-mixing;
E, until step c leave standstill terminate after, take out supernatant liquid, then by steps d mixed aid add wherein, after fully stirring, the product obtained is the present invention's fuel oil product to be prepared, packs and puts in storage.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510050645.0A CN104694178B (en) | 2015-01-30 | 2015-01-30 | A kind of preparation method of fuel oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510050645.0A CN104694178B (en) | 2015-01-30 | 2015-01-30 | A kind of preparation method of fuel oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104694178A true CN104694178A (en) | 2015-06-10 |
| CN104694178B CN104694178B (en) | 2016-08-24 |
Family
ID=53341741
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510050645.0A Active CN104694178B (en) | 2015-01-30 | 2015-01-30 | A kind of preparation method of fuel oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104694178B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105623752A (en) * | 2016-02-27 | 2016-06-01 | 安徽海德石油化工有限公司 | Soybean and plant mixed fuel oil and preparing method thereof |
| CN105623751A (en) * | 2016-02-27 | 2016-06-01 | 安徽海德石油化工有限公司 | Polyvinyl acetate-soybean mixed fuel oil and preparation method thereof |
| CN105713680A (en) * | 2016-02-27 | 2016-06-29 | 安徽海德石油化工有限公司 | Mixed plant fuel oil and preparation method thereof |
| CN105713681A (en) * | 2016-02-27 | 2016-06-29 | 安徽海德石油化工有限公司 | Low-temperature EVA hot melt adhesive-corn oil mixed fuel oil for paper and preparation method of mixed fuel oil |
| CN105733696A (en) * | 2016-02-27 | 2016-07-06 | 安徽海德石油化工有限公司 | Non-toxic epoxy resin-soybean protein plant fuel oil and preparation method thereof |
| CN105733697A (en) * | 2016-02-27 | 2016-07-06 | 安徽海德石油化工有限公司 | Environment-friendly graft chloroprene rubber and corn oil hybrid fuel oil and preparation method thereof |
| CN113583725A (en) * | 2021-08-26 | 2021-11-02 | 浙江百盟能源科技有限公司 | Production formula and preparation method of industrial oil for combustor |
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| WO2009038108A1 (en) * | 2007-09-21 | 2009-03-26 | Toshiharu Fukai | Emulsified petroleum product |
| WO2009135307A1 (en) * | 2008-05-06 | 2009-11-12 | Innovations Solutions Now Inc. | Biofuel or additive and method of manufacture and use |
| CN102382691A (en) * | 2010-08-30 | 2012-03-21 | 东莞市智造生物科技有限公司 | Highly clean biodiesel |
| CN102517100A (en) * | 2011-12-16 | 2012-06-27 | 深圳市盈懋科技有限公司 | Fuel oil from coal and preparation method thereof |
| CN104119963A (en) * | 2014-08-01 | 2014-10-29 | 东莞市向阳世纪能源有限公司 | Environment-friendly fuel oil and preparation method thereof |
-
2015
- 2015-01-30 CN CN201510050645.0A patent/CN104694178B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009038108A1 (en) * | 2007-09-21 | 2009-03-26 | Toshiharu Fukai | Emulsified petroleum product |
| WO2009135307A1 (en) * | 2008-05-06 | 2009-11-12 | Innovations Solutions Now Inc. | Biofuel or additive and method of manufacture and use |
| CN102382691A (en) * | 2010-08-30 | 2012-03-21 | 东莞市智造生物科技有限公司 | Highly clean biodiesel |
| CN102517100A (en) * | 2011-12-16 | 2012-06-27 | 深圳市盈懋科技有限公司 | Fuel oil from coal and preparation method thereof |
| CN104119963A (en) * | 2014-08-01 | 2014-10-29 | 东莞市向阳世纪能源有限公司 | Environment-friendly fuel oil and preparation method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105623752A (en) * | 2016-02-27 | 2016-06-01 | 安徽海德石油化工有限公司 | Soybean and plant mixed fuel oil and preparing method thereof |
| CN105623751A (en) * | 2016-02-27 | 2016-06-01 | 安徽海德石油化工有限公司 | Polyvinyl acetate-soybean mixed fuel oil and preparation method thereof |
| CN105713680A (en) * | 2016-02-27 | 2016-06-29 | 安徽海德石油化工有限公司 | Mixed plant fuel oil and preparation method thereof |
| CN105713681A (en) * | 2016-02-27 | 2016-06-29 | 安徽海德石油化工有限公司 | Low-temperature EVA hot melt adhesive-corn oil mixed fuel oil for paper and preparation method of mixed fuel oil |
| CN105733696A (en) * | 2016-02-27 | 2016-07-06 | 安徽海德石油化工有限公司 | Non-toxic epoxy resin-soybean protein plant fuel oil and preparation method thereof |
| CN105733697A (en) * | 2016-02-27 | 2016-07-06 | 安徽海德石油化工有限公司 | Environment-friendly graft chloroprene rubber and corn oil hybrid fuel oil and preparation method thereof |
| CN113583725A (en) * | 2021-08-26 | 2021-11-02 | 浙江百盟能源科技有限公司 | Production formula and preparation method of industrial oil for combustor |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104694178B (en) | 2016-08-24 |
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Address after: 238251 Ma'anshan province and Anhui City, Wujiang province fine chemical base Patentee after: ANHUI HAIDE CHEMICAL TECHNOLOGY Co.,Ltd. Address before: 238251 Ma'anshan province and Anhui City, Wujiang province fine chemical base Patentee before: ANHUI HAIDE PETROCHEMICAL Co.,Ltd. |
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Effective date of registration: 20240226 Address after: 243000 No.1 Chaosan Road, Provincial Fine Chemical Base, Hexian Economic Development Zone, Ma'anshan City, Anhui Province Patentee after: Anhui Jubaoshi Technology Co.,Ltd. Country or region after: China Address before: 238251 fine chemical base of Wujiang Town, Wujiang, Anhui Province Patentee before: ANHUI HAIDE CHEMICAL TECHNOLOGY Co.,Ltd. Country or region before: China |