CN104664587A - Nebulized liquid containing American ginseng and preparing method thereof - Google Patents
Nebulized liquid containing American ginseng and preparing method thereof Download PDFInfo
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- CN104664587A CN104664587A CN201410855136.0A CN201410855136A CN104664587A CN 104664587 A CN104664587 A CN 104664587A CN 201410855136 A CN201410855136 A CN 201410855136A CN 104664587 A CN104664587 A CN 104664587A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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Abstract
The invention discloses nebulized liquid containing American ginseng and a preparing method thereof. The nebulized liquid comprises, by weight, 55% to 75% of propylene glycol, 10% to 20% of glycerol, 5% to 10% of American ginseng and 5% to 15% of distilled water. The nebulized liquid has the advantages that a formula of the nebulized liquid has no tobacco extract and nicotine but the herbal American ginseng; a ratio of the propylene glycol, the glycerol and water is appropriate, mist of the nebulized liquid is thick, and no stimulus is caused to the throat; no favors and fragrances but essential oil of the American ginseng is added, and no second-hand smoke damage is caused; American ginseng saponins, as main effective ingredient in the American ginseng, can be nebulized and inhaled to produce thick fragrance and drug effect, thus achieving the functions such as tonifying qi and nourishing yin, regenerating bodily fluids, nourishing heart, tonifying lung and kidney, and clearing heat to relive fidgetiness.
Description
Technical field
The invention belongs to electronic cigarette field, be specifically related to a kind of atomized liquid containing American Ginseng composition and preparation method thereof.
Background technology
Along with the understanding of people to cigarette harm is more and more deep, smokers urgently wish to occur that cigarette substitute is to save their health.Wherein, electronic cigarette as one of cigarette substitute, smoking cessation successful.Healthy electronic cigarette containing tar, without harmful substances such as carbon monoxide, nitrogen dioxide, arsenic, lead, mercury, can not avoid " second-hand-cigarette " to the harm of surrounding population.Through the development of several generations, current electronic cigarette atomizing liquid taste can realize variation, meets the demand that different smoker selects different taste.But electronic cigarette product on the market is mainly still given up material and is added in atomized liquid formula using tobacco extract, nicotine etc. as craving for tobacco, really cannot meet the demand of consumer health's smoking cessation, especially can not meet the treatment of smoking cessation demand of the smoker suffering from some special illness, limit to the envelop of function of electronic cigarette product.Electronic cigarette produce market has a high potential, electronics atomized liquid function singleness on market, especially rare with the product that traditional Chinese medicine ingredients is tasty.
American Ginseng is the dry root of Araliaceae American Ginseng, has boosting qi and nourishing yin, clearing heat and promoting fluid function.American ginseng total saponins is its primary medicinal component, and wherein the content of ginsenoside Rb1 and ginsenoside Re is the highest.American Ginseng has the effect of boosting qi and nourishing yin, born fluid, nourish heart beneficial lung nourshing kidney, clearing heat and relieving fidgetness, multiplexly clinically treats the various syndromes of deficiency of vital energy body fluid deficiency with yin asthenia generating intrinsic heat, and the chronic cough caused as lungs abnormal heat is losed heart; The lung pharynx mouth of suffering from a deficiency of the kidney caused by heat is made an uproar, cough breathe hard, dyspneal breath; The palpitation and amnesia that the heart-yin virtual loss causes, insomnia and dreamful sleep; The thirsty that taste body fluid deficiency causes, micro-knot of defecating, the red tongue of tongue lack.American Ginseng differs more than 2 times with the saponin(e total amount of ginseng, and Rbl contained by American Ginseng is far away higher than Rb contained by ginseng, this marked difference result in the medicinal difference that people participates in American Ginseng, contain grand alcohol type panicled fameflower root saponin(e 24 (the R)-F11 and ginsenoside RA0 of a certain amount of Losec ladder in addition in American Ginseng, not yet find in ginseng.
Summary of the invention
For solving the shortcoming and defect part of prior art, primary and foremost purpose of the present invention is to provide a kind of atomized liquid containing American Ginseng composition.This atomized liquid formula, by regulating the ratio of water and propane diols, can produce dense smog after making vaporization; In atomized liquid, add appropriate American Ginseng medicinal ingredient, smoker goes back Absorbable rod American Ginseng medicinal ingredient while enjoyment smog, plays the effect of boosting qi and nourishing yin, born fluid, nourish heart beneficial lung nourshing kidney, clearing heat and relieving fidgetness simultaneously.
Another object of the present invention is to the preparation method that the above-mentioned atomized liquid containing American Ginseng composition is provided.
For achieving the above object, the present invention adopts following technical scheme:
An atomized liquid containing American Ginseng composition, comprises the component of following percentage by weight: 55-75% propane diols, 10-20% glycerine, 5-10% American Ginseng composition and 5-15% distilled water; Described American Ginseng composition is American Ginseng volatile oil and American Ginseng medicinal extract, and above weight percentages of components sum is 100%.
Preferably, the described atomized liquid containing American Ginseng composition comprises the component of following percentage by weight: 72% propane diols, 15% glycerine, 5% American Ginseng composition and 8% distilled water.
Preferably, the described atomized liquid containing American Ginseng composition comprises the component of following percentage by weight: 65% propane diols, 12% glycerine, 8% American Ginseng composition and 15% distilled water.
Preferably, the described atomized liquid containing American Ginseng composition comprises the component of following percentage by weight: 63% propane diols, 20% glycerine, 10% American Ginseng composition and 7% distilled water.
The preparation method of the above-mentioned atomized liquid containing American Ginseng composition, comprises the following steps:
(1) pulverized by American Ginseng medicine materical crude slice and cross 80 mesh sieves, adding 70% ethanol of 12-14 times of American Ginseng quality, heating and refluxing extraction 3 times, each 2h, Extracting temperature 50-60 DEG C, obtain volatile oil compositions and extract; Volatile oil compositions obtains American Ginseng volatile oil through petroleum ether extraction and reduced pressure concentration, and extract obtains American Ginseng medicinal extract through reduced pressure concentration;
(2) American Ginseng volatile oil obtained in step (1) and American Ginseng medicinal extract weight sum are counted the weight of American Ginseng composition, take all the other component raw material according to the percentage by weight of each component; The American Ginseng medicinal extract distilled water that step (1) is obtained dissolves, and obtains By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the American Ginseng volatile oil that step (1) is obtained again, emulsifying 5-10min under the rotating speed of 3000-4000rpm, obtain the described atomized liquid containing American Ginseng composition.
Preferably, the temperature of the described extract reduced pressure concentration of step (1) is 60 DEG C.
Preferably, the emulsifying temperature described in step (2) is 25-30 DEG C.
Compared with prior art, the present invention has the following advantages and beneficial effect:
(1) traditional electronic cigarette atomizing liquid is the composition that skims the cream off milk from tobacco, is dissolved in the solvent of food-grade, adds a small amount of essence and flavoring agent simultaneously.The Essence of the multiple green plants of extracting, is inhaled in body the unique effects having and remove the cigarette poison rested in human body, remove craving for tobacco.But, still containing carcinogens such as nicotines in atomized liquid, the health of harmful to human.
Do not add tobacco extract in atomized liquid of the present invention, not containing nicotine, the substitute is and with the addition of Chinese herbal medicine American Ginseng medicinal ingredient.The present invention is by selecting the American Ginseng medicine materical crude slice of high-quality, adopt abstraction technique, from American Ginseng, extraction and isolation goes out main active ginsenoside and volatile oil, wherein volatile oil component smell is aromatic, have disperse induce sweat, the effect of resuscitation with aromatics, may be used for replacing tobacco essence, also there is health-care efficacy.
(2) atomized liquid formula of the present invention, the ratio of propane diols, G & W is suitable, atomized liquid smog is dense, to throat nonirritant; Do not add essence and flavoring agent, the substitute is the pure natural fragrance of American Ginseng volatile oil, endanger without second-hand-cigarette; The principle active component of American Ginseng is American ginseng saponin, can produce drug effect, reach boosting qi and nourishing yin, born fluid, beneficial lung nourshing kidney of nourishing heart by atomization while of being sucked and to be entered after in body not only strongly fragrant, the effect of clearing heat and relieving fidgetness.
Accompanying drawing explanation
Fig. 1 is the embodiment of the present invention 1 American Ginseng constituents extraction process chart;
Fig. 2 is the atomized liquid preparation technology flow chart of the embodiment of the present invention 1 containing American Ginseng composition.
Detailed description of the invention
Below in conjunction with embodiment and accompanying drawing, the present invention is described in further detail, but embodiments of the present invention are not limited thereto.
The invention discloses a kind of atomized liquid containing American Ginseng composition, it comprises the component of following percentage by weight: 55-75% propane diols, 10-20% glycerine, 5-10% American Ginseng composition and 5-15% distilled water.The preparation process that should contain the atomized liquid of American Ginseng composition is as follows:
(1) American Ginseng medicine materical crude slice was pulverized 80 mesh sieves, and added 70% ethanol of 12-14 times of American Ginseng quality, heating and refluxing extraction 3 times, each 2h, Extracting temperature 50-60 DEG C, obtain volatile oil compositions and extract; Volatile oil compositions obtains American Ginseng volatile oil through petroleum ether extraction and reduced pressure concentration, and extract obtains American Ginseng medicinal extract through reduced pressure concentration;
(2) American Ginseng volatile oil obtained in step (1) and American Ginseng medicinal extract weight sum are counted the weight of American Ginseng composition, take all the other component raw material according to the percentage by weight of each component; The American Ginseng medicinal extract distilled water that step (1) is obtained dissolves, and obtains By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the American Ginseng volatile oil that step (1) is obtained again, emulsifying 5-10min under the rotating speed of 3000-4000rpm, obtain the described atomized liquid containing American Ginseng composition.After the atomized liquid bottling capping obtained, through sterilizing, lamp inspection, finally packaging warehouse-in stores.
The preparation process of above-mentioned atomized liquid is after determining rational formula, realizes mainly through abstraction technique and emulsifying technology.Atomized liquid is made to play American Ginseng medicinal efficacy and reach best atomizing effect, the main active of American Ginseng must be gone out and prepares good properties and stable atomized liquid by extraction and isolation, its each composition especially American Ginseng volatile oil and aqueous phase can be uniformly distributed, without effects such as composition delays during atomization.Prepare good properties and stable atomized liquid, need to solve the difficult problem in stirring and emulsifying hybrid technology, design optimal parameter, wherein temperature, emulsification times, mixing speed all play vital effect.
Found by test, after using emulsifying to stir, obtained atomized liquid water-oil phase is uniformly dispersed, and can keep stable, and two-phase is not easy again to be separated.This system water oil is liquid, at room temperature can reach good emulsifying effectiveness, and higher than this temperature (40-70 DEG C) emulsifying effectiveness without work change, the energy that high temperature consumes is more, from cost-saving angle, emulsifying temperature is set to 25-30 DEG C.
Find in test that the water-oil phase dispersion effect of the obtained atomized liquid of high rotating speed (4000-6000rpm) is good, but the foam produced during emulsify at a high speed is more, the stirring at low speed of 3000rpm can cancellation bubble.Rotating speed too small (1000-2000rpm) shearing force is not enough to make the two-phase of atomized liquid to complete dispersion even, fine and smoothly.
Emulsification times also can impact the quality of atomized liquid, and because in atomized liquid formula of the present invention, the component content of volatile oil is less, viscosity is lower, can complete dispersion within a short period of time.5-10min, the few oil slick of atomized liquid foam is few, emulsion-stabilizing.Be less than 3min, because the time is too short, do not reach the effect of stable dispersion.
Embodiment 1
A preparation method for atomized liquid containing American Ginseng composition, as illustrated in fig. 1 and 2, comprises the following steps:
(1) American Ginseng medicine materical crude slice was pulverized 80 mesh sieves, and added 70% ethanol of 12 times of American Ginseng quality, heating and refluxing extraction 3 times (Extracting temperature 60 DEG C), each 2h, obtains volatile oil compositions and extract; Volatile oil compositions obtains American Ginseng volatile oil through petroleum ether extraction and reduced pressure concentration, and extract obtains American Ginseng medicinal extract through reduced pressure concentration;
(2) American Ginseng volatile oil obtained in step (1) and American Ginseng medicinal extract weight sum are counted the weight of American Ginseng composition, take all the other component raw material according to the percentage by weight of each component; The American Ginseng medicinal extract distilled water that step (1) is obtained dissolves, and obtains By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the American Ginseng volatile oil that step (1) is obtained again, with vacuum homogeneous emulsifying machine emulsifying 5min under the rotating speed of 3000rpm, emulsifying temperature is normal temperature (25-30 DEG C), obtains the described atomized liquid containing American Ginseng composition; After the atomized liquid bottling capping obtained, through sterilizing, lamp inspection; The above-mentioned atomized liquid containing American Ginseng composition comprises the component of following percentage by weight: 72% propane diols, 15% glycerine, 5% American Ginseng composition and 8% distilled water; Described American Ginseng composition is American Ginseng volatile oil obtained in step (1) and American Ginseng medicinal extract.
In this embodiment, American Ginseng medicinal ingredient ratio is less than normal, and smog is dense, is applicable to the crowd that just given up smoking.
Embodiment 2
A preparation method for atomized liquid containing American Ginseng composition, comprises the following steps:
(1) American Ginseng medicine materical crude slice was pulverized 80 mesh sieves, and added 70% ethanol of 14 times of American Ginseng quality, heating and refluxing extraction 3 times (Extracting temperature 50 DEG C), each 2h, obtains volatile oil compositions and extract; Volatile oil compositions obtains American Ginseng volatile oil through petroleum ether extraction and reduced pressure concentration, and extract obtains American Ginseng medicinal extract through reduced pressure concentration;
(2) American Ginseng volatile oil obtained in step (1) and American Ginseng medicinal extract weight sum are counted the weight of American Ginseng composition, take all the other component raw material according to the percentage by weight of each component; The American Ginseng medicinal extract distilled water that step (1) is obtained dissolves, and obtains By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the American Ginseng volatile oil that step (1) is obtained again, with vacuum homogeneous emulsifying machine emulsifying 5min under the rotating speed of 4000rpm, emulsifying temperature is normal temperature (25-30 DEG C), obtains the described atomized liquid containing American Ginseng composition; After the atomized liquid bottling capping obtained, through sterilizing, lamp inspection; The above-mentioned atomized liquid containing American Ginseng composition comprises the component of following percentage by weight: 65% propane diols, 12% glycerine, 8% American Ginseng composition and 15% distilled water; Described American Ginseng composition is American Ginseng volatile oil obtained in step (1) and American Ginseng medicinal extract.
In this embodiment, American Ginseng component ratio is moderate, can play a role in health care.
Embodiment 3
A preparation method for atomized liquid containing American Ginseng composition, comprises the following steps:
(1) American Ginseng medicine materical crude slice was pulverized 80 mesh sieves, and added 70% ethanol of 12 times of American Ginseng quality, heating and refluxing extraction 3 times (Extracting temperature 60 DEG C), each 2h, obtains volatile oil compositions and extract; Volatile oil compositions obtains American Ginseng volatile oil through petroleum ether extraction and reduced pressure concentration, and extract obtains American Ginseng medicinal extract through reduced pressure concentration;
(2) American Ginseng volatile oil obtained in step (1) and American Ginseng medicinal extract weight sum are counted the weight of American Ginseng composition, take all the other component raw material according to the percentage by weight of each component; The American Ginseng medicinal extract distilled water that step (1) is obtained dissolves, and obtains By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the American Ginseng volatile oil that step (1) is obtained again, with vacuum homogeneous emulsifying machine emulsifying 10min under the rotating speed of 3000rpm, emulsifying temperature is normal temperature (25-30 DEG C), obtain the described atomized liquid containing American Ginseng composition, after the atomized liquid bottling capping obtained, through sterilizing, lamp inspection; The above-mentioned atomized liquid containing American Ginseng composition comprises the component of following percentage by weight: 63% propane diols, 20% glycerine, 10% American Ginseng composition and 7% distilled water; Described American Ginseng composition is American Ginseng volatile oil obtained in step (1) and American Ginseng medicinal extract.
In this embodiment, American Ginseng medicinal ingredient ratio is higher, and atomizing effect is good, and health-care effect is obvious.
For verifying smoking cessation effect and the health-care effect of atomized liquid of the present invention, testing after adopting the atomized liquid formula in embodiment 3 to make electronic cigarette, randomly drawing 100 routine smokers, all have chronic cough to lose heart, swallow the ill symptomses such as mouth is made an uproar, palpitation and amnesia, insomnia and dreamful sleep.Put into electronic cigarette atomizing inhalator with atomized liquid 5ml of the present invention, suck 10 every day, within 2 months, draw 80ml altogether.Test effect 89% craving for tobacco significantly declines, and the symptoms such as 67% thirsty, chronic cough are losed heart, insomnia and dreamful sleep all make moderate progress, and illustrate that atomized liquid of the present invention has remarkable result to smoking cessation, have the health-care effect of nourish heart beneficial lung nourshing kidney, clearing heat and relieving fidgetness simultaneously.
Above-described embodiment is the present invention's preferably embodiment; but embodiments of the present invention are not restricted to the described embodiments; change, the modification done under other any does not deviate from Spirit Essence of the present invention and principle, substitute, combine, simplify; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (7)
1. the atomized liquid containing American Ginseng composition, is characterized in that, comprise the component of following percentage by weight: 55-75% propane diols, 10-20% glycerine, 5-10% American Ginseng composition and 5-15% distilled water; Described American Ginseng composition is American Ginseng volatile oil and American Ginseng medicinal extract, and above weight percentages of components sum is 100%.
2. the atomized liquid containing American Ginseng composition according to claim 1, it is characterized in that, this atomized liquid comprises the component of following percentage by weight: 72% propane diols, 15% glycerine, 5% American Ginseng composition and 8% distilled water.
3. the atomized liquid containing American Ginseng composition according to claim 1, it is characterized in that, this atomized liquid comprises the component of following percentage by weight: 65% propane diols, 12% glycerine, 8% American Ginseng composition and 15% distilled water.
4. the atomized liquid containing American Ginseng composition according to claim 1, it is characterized in that, this atomized liquid comprises the component of following percentage by weight: 63% propane diols, 20% glycerine, 10% American Ginseng composition and 7% distilled water.
5. the preparation method of the atomized liquid containing American Ginseng composition described in any one of Claims 1-4, is characterized in that, comprise the following steps:
(1) pulverized by American Ginseng medicine materical crude slice and cross 80 mesh sieves, adding 70% ethanol of 12-14 times of American Ginseng quality, heating and refluxing extraction 3 times, each 2h, Extracting temperature 50-60 DEG C, obtain volatile oil compositions and extract; Volatile oil compositions obtains American Ginseng volatile oil through petroleum ether extraction and reduced pressure concentration, and extract obtains American Ginseng medicinal extract through reduced pressure concentration;
(2) American Ginseng volatile oil obtained in step (1) and American Ginseng medicinal extract weight sum are counted the weight of American Ginseng composition, take all the other component raw material according to the percentage by weight of each component; The American Ginseng medicinal extract distilled water that step (1) is obtained dissolves, and obtains By Chinese Medicines; Then add propane diols and glycerine stirs and evenly mixs, obtain primary atomization liquid; Add the American Ginseng volatile oil that step (1) is obtained again, emulsifying 5-10min under the rotating speed of 3000-4000rpm, obtain the described atomized liquid containing American Ginseng composition.
6. preparation method according to claim 5, is characterized in that, the temperature of the described extract reduced pressure concentration of step (1) is 60 DEG C.
7. preparation method according to claim 5, is characterized in that, the emulsifying temperature described in step (2) is 25-30 DEG C.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410855136.0A CN104664587B (en) | 2014-12-31 | 2014-12-31 | Nebulized liquid containing American ginseng |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410855136.0A CN104664587B (en) | 2014-12-31 | 2014-12-31 | Nebulized liquid containing American ginseng |
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| CN104664587A true CN104664587A (en) | 2015-06-03 |
| CN104664587B CN104664587B (en) | 2017-01-11 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107090356A (en) * | 2017-04-27 | 2017-08-25 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl American Ginseng essence and its application in cigarette |
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|---|---|---|---|---|
| GB1255007A (en) * | 1968-04-10 | 1971-11-24 | Director General Office Of Mon | Manufacturing method for ginseng cigarettes or the like |
| CN1137363A (en) * | 1996-03-26 | 1996-12-11 | 高华选 | Chinese herbal medicine type tobacco liquor and its preparation method |
| CN1994159A (en) * | 2006-12-15 | 2007-07-11 | 姜志荣 | Kidney-strengthening mind-refreshing tobacco liquid for electronic atomized cigarette |
| CN103564647A (en) * | 2012-07-31 | 2014-02-12 | 马瑞 | Preparation method of traditional Chinese medicine spices for tobaccos |
| CN104026730A (en) * | 2014-07-01 | 2014-09-10 | 安徽中烟工业有限责任公司 | Scorch sweet aroma electronic cigarette juice |
-
2014
- 2014-12-31 CN CN201410855136.0A patent/CN104664587B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1255007A (en) * | 1968-04-10 | 1971-11-24 | Director General Office Of Mon | Manufacturing method for ginseng cigarettes or the like |
| CN1137363A (en) * | 1996-03-26 | 1996-12-11 | 高华选 | Chinese herbal medicine type tobacco liquor and its preparation method |
| CN1994159A (en) * | 2006-12-15 | 2007-07-11 | 姜志荣 | Kidney-strengthening mind-refreshing tobacco liquid for electronic atomized cigarette |
| CN103564647A (en) * | 2012-07-31 | 2014-02-12 | 马瑞 | Preparation method of traditional Chinese medicine spices for tobaccos |
| CN104026730A (en) * | 2014-07-01 | 2014-09-10 | 安徽中烟工业有限责任公司 | Scorch sweet aroma electronic cigarette juice |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107090356A (en) * | 2017-04-27 | 2017-08-25 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl American Ginseng essence and its application in cigarette |
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